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first and second enantiomers to the R-PVPP molecule. A.Preparation of First and Second Enantiomers 1) Preparation of2-[(2-Amino-1-phenyl-ethyl)amino]-1-phenyl-ethan-1-ol (substrate) and Preparation of Benzimidazole (product) The first stepis the preparation of the S-enantiomer of the (R-1-phenylethyl)amino derivative. The racemic starting material
1-[(2-amino-1-phenyl-ethyl)amino]-2-phenyl-ethanol is reacted with an enantiomerically pure secondary amine to give the Senantiomer and the racemic product. The racemic product is subjected to enantiomer resolution and isolated by means of achiral HPLC column. In this isolation procedure, the racemic product is converted into the first enantiomer and the second
enantiomer by enantiomeric exchange of a sodium salt as a base. The sodium salt is isolated by means of a chiral HPLC column
and crystallized. The second step is the preparation of the corresponding benzimidazole (product). For this reaction, the firstenantiomer is isolated by means of an enantiomeric separation and crystallized. To this end, the compounds
2-[(2-amino-1-phenyl-ethyl)amino]-1-phenyl-ethan-1-ol and 5-bromo-1-phenyl-2-benzimidazole are subjected to coupling
reactions. B) Preparation of the Third Enantiomer As the first step, the third enantiomer is isolated by means of an enantiomericseparation and crystallized from the racemic mixture using the enantiomeric separation, by means of an enantiomeric separation
or by means of a chiral HPLC column. As the second step, the third enantiomer is prepared from the firstpatch for Dmifit Tool And Hpbq138 Exe Zip. - Download - Download-File.com. Where can I get free ibm rtfm tutorials.
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