RCarbon-13
Carbon-13benchtop
benchtop NMR
NMRFor organic chemists 13C NMR forms the backbone of routine molecular analysis. Spinsolve Carbon has
13C NMR forms the backbone of routine molecular analysis.
For organicchemists
outstanding
resolution
and uniquesensitivity that enables the power of proton-carbon NMR in a benchtop
Now you
have the powerof proton-carbon
NMR inbenchtop
instrument
instrument.
Thiscanbest-in-classspectrometeris the most flexible
anda costeffective
way to getthat
carbon-13
NMRyouin yourcanlaboratory.
use in your lab.

5 6
9 84 71415

10 16
11 17

1216,17
10,1114,15
12

6,7,8

HETCOR spectrum of lidocaine

HETCOR spectrum of lidocaine

WhoWho•Synthetic Chemists•Medicinal Chemists• Medicinaland Pharmaceutical• Organic Chemistry
Lecturers•Structure
Elucidation•Organic
ChemistryChemists			
Education• Small Molecule Research Scientists			 • Synthetic Chemists monitoring reactions		• Academics running practical laboratory classes 		• Post Graduate Chemistry StudentsWhy
Why$• No cryogens				• Low cost		
• Low maintenance•No cryogens •Low cost
•Low maintenance• Fast					• Accessible 			• Easy to operate•Fast•Easy
tooperate•Accessible• Convenient			
• Robust			• Exceptional performance•Convenient•Robust•Exceptional performanceExample
NMR
Spectra of Lidocaine using Spinsolve Carbon
13C NMR
Spectroscopy
13C13
Spectroscopy
13C NMR
C 13
NMR
Spectroscopy
CNMR
Spectroscopy
NMR
Spectroscopy
Example NMR Spectraof Lidocaine using Spinsolve Carbon.
Example NMR Spectra of Lidocaine using Spinsolve Carbon.
ExampleNMR
Spectraof Lidocaine
SpinsolveCarbon.
ExampleNMR
Spectraof Lidocaine
usingSpinsolveCarbon.
ExampleNMR
SpectraofLidocaine
usingusing
Spinsolve
Carbon.

210,1110,1110,1110,116786786

678783332CH3678161716
1714151212 1415141514151212141416
1015141115171215

10 10
16 16

10
11 16
17
11 17
11 17

1212CH3CH3CH2CH2CH2CH

3

10 16
11 17

1415

CH3CH316 12 16
16171417 CH2151217
14CH21512

3

210,115 65 6
9 8
5 65 69 8
7 64 52 9 89 84 79 8
27
4 7 4 4 7

CHCHCH

1D Proton with1Dpeak
assignments.
Carbon shows
peaks ofall carbons
Protonwith peak assignments. 1D CH
1D Carbon
shows
peaks of(top).
all carbons (top).
1DSpectral
Carbonshows
ofofall signals
carbons
usingpeaks
DEPT
selectsof (top).
Spectral editing
using editing
DEPT
selects
signalsCH,
CH
andCHgroups(rows2-4).
CH,
CH
andCHgroups(rows2-4).
1D Proton
withassignments.
peak assignments.
Carbonshows
peaksof DEPT
all carbons(top).signals
1D Protonwith peak
1Dshows
peaksofall carbons(top).
Spectraleditingusing
selects
3
2
3 Carbon
21DSpectral
editingusing
DEPT
selects
signalsofSpectraleditingusing
DEPT
selects
signalsofandCHgroups(rows2-4),CHofCH
10,1110,11
3
2
10,1110,1116
16
16
16
CH
,
CH
andCH
groups(rows2-4).
,
CHandCHgroups(rows2-4).
CH
14
14
3
2
3
2
1D Proton6,7,8
with peak assignments.
1D6,7,8
Carbon showsof all carbons(top).
6,7,8 peaks
14
6,7,8 1417
17

1D Proton with peak assignments.

12 15

16,17

6,7,8 16,17
6,7,8

10,11

10,11

16,17
14,15

14,15

6,7,8

12

14,15

14,15

1212

16,17
10,11

6,8

14,15
12

6,8

4

5,9

7
7
6,8
2 4 6,8
4
5,9
5,910,11 10,11
16
14
14
17
12 15 12 15

16
17

10,11
14
12 15

16
17

7

2

2D HMQC shows single-bond
22D HMQC
shows
single-bondcorrelations.
proton-carbon
proton-carbon correlations.

4

5,92D HMQC
shows shows
single-bond
2D HMQC
single-bond
2D HMQCcorrelations.
shows single-bondproton-carbon
proton-carbon correlations.
2

6,7,8
12
10,11

14,15

14,15

proton-carbon correlations.

14
12 15

16
17

12

10,11
7

6,845,914,15

15

10,1116,1714,15

12
10,116,815

10,11

16,17
14,15

5,92

6,816,1774

17 12 1512 15Spectral editing using DEPT
selects
signals of
10,1110,11
16
16
16,17
14
14
6,7,8 CH groups (rowsCH3, 6,7,8CH2 and2-4).
1717121216,17
12

75,912 15

10,1116,17

12
10,1110,11

17

7
4

7 12
7 2
6,86,82
4
4
5,95,92D HMBC shows long-range
222D HMBC
shows
long-range
proton-carbon
correlations.
7
proton-carbon
correlations.
6,845,92D HMBC shows long-range

2D HMBC shows long-range
2D HMBC
shows long-range
proton-carbon
correlations.
proton-carbon
correlations.
2proton-carbon correlations.

Software
The power of simplicity• Uncomplicated one-button operation		• Minimal user controlled parameters• Simple intuitive graphical interface			• Traditional NMR complexities are hidden• Automated and easy to use

DEPT-135 spectrum of 2 M lidocaine in d-chloroform. The inverted peaks are the CH2 carbons.

Features• 1D 1H, 19F and 13C experiments• Standard 5 mm NMR tubes• 2D COSY and homonuclear j-resolved
spectroscopy• T1 and T2 relaxation experiments• Spectral editing with DEPT
• Composite pulse decoupling• 2D heteronuclear correlation experiments
HETCOR, HMQC, HMBC

RSpecifications• Frequency: 42.5 MHz Proton, 10.8 MHz Carbon• Resolution: 50% linewidth < 0.7 Hz (16 ppb)
• Lineshape: 0.55% linewidth < 20 Hz• Dimensions: 58 x 43 x 40 cm• Weight: 55 kg• Magnet: Permanent and cryogen free
• Stray field: < 2 G all around system

Other Spinsolve products
Spinsolve

Spinsolve for education
RR• 1D Proton only system• 1H and 19F nuclei• Budget friendly price• Relaxation time experiments• Upgradeable• 2D COSY and JRES
• Reaction monitoring“Now the students are able to acquire their own NMR spectra as well as carry out the analysis of the compounds they
have made. This makes their undergraduate experiment more applicable to both research and industry settings andincreases their enthusiasm for Chemistry.”
Professor Frances Separovic, Head of Chemistry, University of Melbourne

Contact us now for a quote, or to arrange a demo or sample measurement.
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