キラル分離の生産性と信頼性を高める

Agilent InfinityLab
Poroshell 120 キラルカラム

アプリケーション一覧

かつてないほど高速、高効率なキラル分離を実現
もうキラル分離の性能について妥協する必要はありません。

InfinityLab Poroshell 120 キラルカラムは、表面多孔質粒子を革新的なキラル結合相と組み合わせた初のカラムであり、次のような特長を実現しています。

– 全多孔質キラル結合相を上回る分離性能と分析スピード– 実績ある Agilent InfinityLab Poroshell 120 粒子技術による高い堅牢性と信頼性– あらゆるアプリケーションに適合するサイズ: 内径 2.1 mm と4.6 mm、長さ 50、100、150 mm の構成– 短い分析時間、卓越したピーク形状、高い分解能– 効率的なキラル分離により、スループットとラボの生産性を向上

既存の LC システムを用いて 5 分未満でキラル分離を実行

1

2

3

4

表面多孔質粒子が優れた効率とシャープなピーク形状を実現します。全多孔質カラムよりも短時間で分析できるため、スループットが飛躍的に向上します。

0

5

15

10

従来のキラル分離 -Agilent InfinityLab Poroshell 120 キラル分離 -他社全多孔性キラルカラム (250 x 4.6 mm、5 µm)

InfinityLab Poroshell 120 キラル -V (100 x 4.6 mm、2.7 µm)

全多孔質粒子表面多孔質粒子

1
1

0

5

2

10

min

3

23
4

15

min

0

アンフェタミンを

4

5 分未満で分離

510

1.D-(+)-アンフェタミン、2.L-(-)-アンフェタミン、3.D-(+)-メタンフェタミン、

1.D-(+)-アンフェタミン、2.L-(-)-アンフェタミン、3.D-(+)-メタンフェタミン、

流量 1.0 mL/min、室温、UV 220 nm

流量 1.0 mL/min、室温、UV 220 nm

4.L-(-)-メタンフェタミン、100:0.1:0.02 MeOH/HOAc/NH4OH、

min

15

4.L-(-)-メタンフェタミン、100:0.1:0.02 MeOH/HOAc/NH4OH、

1
23
4

0

5

10

15

min

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カラム選択ガイド

ほぼすべてのキラル化合物を分離:
4 種類の結合相が 4 つの LC モードで幅広い選択性を提供
カラム名

キラルセレクタ

InfinityLab Poroshell 120 キラル-CF

誘導体化シクロフルクタン (CF6)InfinityLab Poroshell 120 キラル-CD

ヒドロキシプロピル-β-シクロデキストリン

InfinityLab Poroshell 120 キラル-V

InfinityLab Poroshell 120 キラル-T

バンコマイシン (マクロライド抗生物質)

テイコプラニン (マクロライド抗生物質)

分離タイプ

主なアプリケーション

順相 (NP)

第一級アミン

逆相 (RP)

刺激剤、殺菌剤、t-Boc アミノ酸

極性有機 (PO)

複雑な分子

極性イオン性 (PI)

塩基性医薬品 (各種)

逆相 (RP)

アミン、
プロフェン

極性有機 (PO)

複雑な中性分子

極性イオン性 (PI)

ベータブロッカー、ヒドロキシ酸逆相 (RP)

アミノ酸、
ヒドロキシ酸、プロフェン

極性有機 (PO)

ヒダントイン、ベンゾジアゼピン

極性有機 (PO)第一級アミンRP = 逆相、PI = 極性イオン性、PO = 極性有機、NP = 順相

製品情報
部品番号

カラムの説明

部品番号

カラムの説明689775-604

InfinityLab Poroshell 120 キラル-V、2.1 x 50 mm、2.7 µm

InfinityLab Poroshell 120 キラル-CF、2.1 x 100 mm、2.7 µm

685775-604

InfinityLab Poroshell 120 キラル-V、2.1 x 100 mm、2.7 µm

683775-609

InfinityLab Poroshell 120 キラル-CF、2.1 x 150 mm、2.7 µm

683775-604

InfinityLab Poroshell 120 キラル-V、2.1 x 150 mm、2.7 µm

689975-609

InfinityLab Poroshell 120 キラル-CF、4.6 x 50 mm、2.7 µm

689975-604

InfinityLab Poroshell 120 キラル-V、4.6 x 50 mm、2.7 µm

685975-609

InfinityLab Poroshell 120 キラル-CF、4.6 x 100 mm、2.7 µm

685975-604

InfinityLab Poroshell 120 キラル-V、4.6 x 100 mm、2.7 µm

683975-609

InfinityLab Poroshell 120 キラル-CF、4.6 x 150 mm、2.7 µm

683975-604

InfinityLab Poroshell 120 キラル-V、4.6 x 150 mm、2.7 µm

689775-607

InfinityLab Poroshell 120 キラル-CD、2.1 x 50 mm、2.7 µm

689775-603

InfinityLab Poroshell 120 キラル-T、2.1 x 50 mm、2.7 µm

685775-607

InfinityLab Poroshell 120 キラル-CD、2.1 x 100 mm、2.7 µm

685775-603

InfinityLab Poroshell 120 キラル-T、2.1 x 100 mm、2.7 µm

683775-607

InfinityLab Poroshell 120 キラル-CD、2.1 x 150 mm、2.7 µm

683775-603

InfinityLab Poroshell 120 キラル-T、2.1 x 150 mm、2.7 µm

689975-607

InfinityLab Poroshell 120 キラル-CD、4.6 x 50 mm、2.7 µm

689975-603

InfinityLab Poroshell 120 キラル-T、4.6 x 50 mm、2.7 µm

685975-607

InfinityLab Poroshell 120 キラル-CD、4.6 x 100 mm、2.7 µm

685975-603

InfinityLab Poroshell 120 キラル-T、4.6 x 100 mm、2.7 µm

683975-607

InfinityLab Poroshell 120 キラル-CD、4.6 x 150 mm、2.7 µm

683975-603

InfinityLab Poroshell 120 キラル-T、4.6 x 150 mm、2.7 µm

689775-609

InfinityLab Poroshell 120 キラル-CF、2.1 x 50 mm、2.7 µm

685775-609

限られた時間でエナンチオマーをすばやく検出できます。

カラムの詳細は、次の Web ページをご覧ください。

www.agilent.com/chem/poroshell-120-chiral

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堅牢なキラルスクリーニングメソッド開発のための汎用プロトコル
キラルスクリーニングプロトコル
#
1

移動相

MeOH/20 mM ギ酸アンモニウム、pH 4.0

組成 (% v)

タイプ

90/10

RP

2

MeOH/20 mM ギ酸アンモニウム、pH 4.0

30/70

RP

3

ACN/20 mM ギ酸アンモニウム、pH 4.0

30/70

RP

4

ACN/20 mM ギ酸アンモニウム、pH 4.0

10/90

RP

5

MeOH/ギ酸アンモニウム

100/0.2 wt%

PI

6

ACN/MeOH/酢酸/TEA

60/40/0.3/0.2

PO

7

EtOH/ヘプタン/酢酸/TEA

20/80/0.3/0.2

NP

一般的な分析条件 (4.6 x 100 mm)

内径 2.1 mm (またはその他の寸法) のカラムには要調整
流量:

1 mL/min

検出器:

UV

平衡化:

カラム容量の 10 倍
カラム容量の 10 倍

分析時間:
温度:

室温

サンプル溶媒:MeOH または移動相

濃度:2 ～ 5 mg/mL

RP = 逆相、PI = 極性イオン性、PO = 極性有機、NP = 順相

スクリーニング用移動相の優先順位
カラム名

逆 相 モ ード (RP): ACN または MeOH と 水性

第 1 候補第 2 候補第 3 候補#5 (PI)#2 (RP)#1 (RP)

InfinityLab Poroshell キラル-V#5 (PI)#3 (RP)#1 (RP)

InfinityLab Poroshell キラル-CD#3 (RP)#6 (PO)#4 (RP)

InfinityLab Poroshell キラル-CF#6 (PO)#7 (NP)-

InfinityLab Poroshell キラル-T(塩緩衝液または添加剤) 移動相の組み合わせが一般的

極性有機モード (PO): 極性有機移動相溶媒 (アセトニトリル、メタノール)、添加剤あり/なし

極性イオン性モード (PI): イオン性化合物のイオン化またはリテンションを高めるために、極性有機移動相に塩緩衝液を追加

順相モード (NP): 非極性溶媒を 1 次溶媒とし、水性化合物を添加 せずに用いるのが一般的

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圧力、pH、および温度 パラメータ
カラム名

圧力上限 (bar)

pH 範囲

温度上限

InfinityLab Poroshell 120 キラル-CF

400 bar

3～7

45 °C

InfinityLab Poroshell 120 キラル-CD

400 bar

3～7

45 °C

InfinityLab Poroshell 120 キラル-V

400 bar

2.5～7

45 °C

InfinityLab Poroshell 120 キラル-T

400 bar

2.5～7

45 °C

移動相溶媒を切り替える場合は、圧力上限を超えないように注意すること

Agilent Poroshell 120 キラル結合相の構造
InfinityLab Poroshell 120 キラル -CF(シクロフルクタン CF-6)

InfinityLab Poroshell 120 キラル -CD(ヒドロキシプロピル β -シクロデキストリン)

InfinityLab Poroshell 120 キラル -V(バンコマイシン)

InfinityLab Poroshell 120 キラル -T(テイコプラニン)

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5

新薬製品化のスピードと信頼性を向上

成果を導き出すソリューション

低分子医薬品の創薬は、多くの手間とコストを伴う複雑な作業です。アジレントの総合的な医薬品ソリューションなら、効率と生産性が大幅に高まります。

初期段階での化合物の同定に役立つ自動化システムから、ADME/PK の研究において威力を発揮する高度な高感度 LC/MS システムまで、幅広い製品がお客様の分析をサポートします。これらのシステムで得られる再現性の高い正確な結果をもとに、創薬プロセス

全体にわたって的確な決定を下すことができます。

www.agilent.com/chem/biopharma_jp

Agilent InfinityLab:LC ワークフローの効率を最大化

InfinityLab の LC システム、カラム、および消耗品は、シームレスな連携により最大限の効率と性能を引き出すよう最適化されています。InfinityLab を使用すれば、ルーチン分
析や最先端研究などのあらゆる分野において、次のような利点があります。

– Agilent InfinityLab LC システムに最適な製品を簡単に特定– 最新の革新技術により LC ワークフローを最適化– 分析、機器、ラボの効率を向上

Agilent InfinityLab の製品と Agilent OpenLAB ソフトウェアおよび Agilent CrossLab

サービスを組み合わせ、エンドツーエンドのソリューションとサポートをご利用いただくことで、成果を最大限に高めることができます。

Agilent InfinityLab 消耗品:カラム接続に伴う時間とトラブルを最小化
InfinityLab クイックコネクトフィッティング

簡単操作のフィンガータイト接続で、誰でもリークのないカラム接続を確実に行えます。

200 回以上繰り返し使用しても、最大 1300 bar の安定性が維持されます。
InfinityLab クイックターンフィッティング

狭い空間での接続には、内蔵スプリング構造の Agilent InfinityLab クイックターンフィッ

ティングをご利用いただくことで、毎回確実なカラム接続を行えます。

www.agilent.com/chem/jp

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キラル分離の高速化と分離能向上を同時に実現
他 の InfinityLab Poroshell 120 カ ラ ム と 同 様 に、Poroshell 120 キラルカラムには、硬質シリカコアと多孔性外殻で構成される表面多孔質粒子が充填されています。

課題

キラルエナンチオマーの分離能

同じ、または同様の粒子径の従来型全多孔質粒子よりク

ロマトグラフィー効率に優れているため、高速での高分離

R 配置

能分離が可能です。

S 配置

R 配置

S 配置

従来

現在

革新技術

Agilent Poroshell 表面多孔性粒子技術

2.7 μm

分析スピード10～20 分

1 ～3 分

従来のキラル分離

2.7 μm 2.7 μm

2.7 μmPoroshell による
高速キラル分離生産性
従来のカラムAgilent InfinityLab
Poroshell 120 キラルカラム

により 10 倍のスループットを

2.7
2.7
μm
μm

実現

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成分別目次検索

リンクをクリックすると、該当ページに移動します。

アミン

鎮痛剤

抑制薬

1,1'-ビナフチル-2,2'-ジアミン ....................................... 10

プログルミド ................................................................... 24

オクトクロテピン............................................................ 41

1-ベンジル-2,2-ジフェニルエチルアミン .................... 10
1-(1-ナフチル)エチルアミン ...........................................11

1-(1,1-ビフェニル-4-イル)エタンアミン .......................11

1-(4-メトキシフェニル)エチルアミン.............................12

1-アミノテトラリン...........................................................126-メトキシ-1,2,3,4-テトラヒドロ-1ナフタレニルアミン .........................................................13

1-(2-メトキシフェニル)エタンアミン.............................13

1-(4-クロロフェニル)エチルアミン................................13
1,1-ジフェニル-1-フルオロ-2-アミノプロパン ............. 14

1,1-ジフェニル-2-アミノプロパン................................. 14

1,2,2-トリフェニルエチルアミン ................................... 14
2-アミノ-4-メチル-1,1-ジフェニルペンタン................. 14

2-クロロ-インダン-1-イルアミン ...................................15

4-メトキシ- α-メチルベンジルアミンビス(1-フェニルエチル)アミン................................................15ビス(α -メチルベンジル)アミン.......................................15

メキシレチン ....................................................................16

N-ベンジル- α-メチルベンジルアミン ...........................16N,α-ジメチルベンジルアミン .........................................16α-メチル-4-ニトロベンジルアミン .................................16α-メチルベンジルアミン ................................................ 17
アミノ酸および誘導体

2-アミノ-2-フェニル酪酸.................................................18

4-ニトロフェニルアラニン ..............................................18
AQC メチオニン...............................................................18

AQC フェニルアラニン ...................................................18

AQC セリン ......................................................................19
AQC チロシン ..................................................................19

Fmoc アラニン ................................................................19
Fmoc アスパラギン .......................................................19

Fmoc ロイシン ............................................................... 20

Fmoc フェニルアラニン ................................................ 20
Fmoc トリプトファン .................................................... 20

Fmoc バリン................................................................... 20

メチオニン ....................................................................... 21

p-クロロフェニルアラニン ............................................ 21
p-フルオロフェニルアラニン.......................................... 21
フェニルアラニン ............................................................ 21
トリプトファン ................................................................. 22

α-アミノ-2-チオフェン酢酸 ........................................... 22

3-アミノ-3-フェニルプロパン酸 .................................... 22
キヌレニン........................................................................ 22

トリプトファンアミド...................................................... 23

3,4-ジヒドロキシフェニルアラニン (DOPA) ............... 23

メサドン ........................................................................... 24
インドプロフェン............................................................ 25
ケトロラック ................................................................... 25

メトルファン..................................................................... 25
ネホパム .......................................................................... 25
トラマドール .................................................................... 26

麻酔薬

ヘキソバルビタール ........................................................ 27

メピバカイン ................................................................... 27
ブピバカイン ................................................................... 28

メホバルビタール ........................................................... 28
プリロカイン ................................................................... 28

抗凝血剤

クマクロル ....................................................................... 29
ワルファリン .................................................................... 29

抗けいれん薬フェンスクシミド ............................................................30α-メチル- α-フェニルスクシンイミド .............................30
抗うつ剤

ブプロピオン................................................................... 31
テマゼパム....................................................................... 31
ロラゼパム....................................................................... 31

ロルメタゼパム ............................................................... 31

ミアンセリン ................................................................... 32

オキサゼパム .................................................................. 32
フルオキセチン ............................................................... 32

ミアンセリン ................................................................... 32
トラニルシプロミン ........................................................ 33

トリミプラミン ................................................................ 33
ベンラファキシン............................................................ 33
ベータブロッカー

アセブトロール................................................................ 34
アルプレノロール ............................................................ 34
アテノロール .................................................................... 35
エスモロール ................................................................... 35

イソプロテレノール ....................................................... 36

バクロフェン ................................................................... 41
トルペリゾン ................................................................... 41

利尿薬

クロルタリドン................................................................ 42
ベンドロフルメサイアザイド ......................................... 42

殺菌剤

ベナラキシル ...................................................................43

エコナゾール ...................................................................43
フルトリアホル ................................................................43

ミコナゾール ...................................................................43
プラジカンテル ...............................................................44
プロチオコナゾール .......................................................44

ジクロルプロップ ............................................................44

フェノプロップ ................................................................44

ハロキシホップ................................................................ 45
マンジプロパミド ........................................................... 45

メコプロップメチルエステル ......................................... 45
メコプロップ ................................................................... 45

ナプロパミド ................................................................... 46
ブロマシル ....................................................................... 46
その他

2'-アミノ-1,1'-ビナフタレン-2-オール ............................ 47
ヒドロアトロパ酸 ........................................................... 47

トロパ酸 .......................................................................... 47

ヤコブセン触媒 .............................................................. 47

α-N,N-ジメチルアミノフェニルアセトニトリル ...........48

2-アミノ-1,2-ジフェニルエタノール ..............................48

フェニルアラニノール .............................................. 48, 49

4-クロロフェニルアラニノール ..................................... 49trans-1-アミノ-2-インダノール ..................................... 49

トリプトファノール ..........................................................50

チロシノール ....................................................................50α-(1-アミノエチル)-4-ヒドロキシベンジルアルコール .......................................................................50

2-(2-クロロフェノキシ)プロピオン酸 ..........................50
2-(3-クロロフェノキシ)プロピオン酸.......................... 51

2-(4-クロロフェノキシ)プロピオン酸.......................... 51

メタプロテレノール ........................................................ 36

2-フェノキシプロパン酸 ................................................ 51

ピンドロール ................................................................... 37

2-アミノ-1,1,13-トリフェニル-1-プロパノール ............. 52

メトプロロール ................................................................ 37
プロプラノロール............................................................ 38

サルブタモール ................................................................ 38

ソタロール ....................................................................... 39
テルブタリン .................................................................... 39

2-アミノ-1,1,-ジフェニル-1-プロパノール..................... 51

2-(カルボベンジルオキシアミノ)-3-フェニル-1プロパノール ................................................................... 52
cis-1-アミノ-2-インダノール .......................................... 52

ツロブテロール ...............................................................40
カルベジロール ...............................................................40

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神経伝達物質およびホルモン

オクトパミン .................................................................... 53
オキサゾリジノン

1,5-ジメチル-4-フェニル-2-イミダゾリジノン ............ 54

4-ベンジル-2-オキサゾリジノン ................................... 54

4-メチル-5-フェニル-2-オキサゾリジノン.................... 54
4-フェニル-2-オキサゾリジノン .................................... 54

5,5-ジメチル-4-フェニル-2-オキサゾリジノン ............ 55

5,5-ジメチル-4-ベンジル-2-オキサゾリジノン ........... 55

5,5-ジメチル-4-メチル-2-オキサゾリジノン ................ 55(3a-cis)-3,3a,8,8a-テトラヒドロ-2H-インデノ[1,2-d]オキサゾール-2-オン........................................... 55

4-(1-H-インドール-3-イル-メチル)-2オキサゾリジノン ............................................................ 56
医薬品

1-インダノール ................................................................ 57

ベンゾイン ....................................................................... 57
クロフェジアノール ......................................................... 57
ホマトロピン ................................................................... 58
インダパミド.................................................................... 58
ロフェキシジン ............................................................... 58

p-クロロアンフェタミン ................................................ 59
フェニルこはく酸無水物 ............................................... 59

トリアジメノール ............................................................ 59

5-メチル-5-フェニルヒダントイン ................................ 59

アミノグルテチミド ........................................................60

バメタン ...........................................................................60
ジペロドン ................................................................ 60, 61

フルルビプロフェン........................................................ 61
マンデル酸 ...................................................................... 61

ナフトピジル .................................................................... 61

p-ヒドロキシマンデル酸................................................ 62

アムロジピン ................................................................... 62

ブロムフェニラミン ........................................................ 62
カルビノキサミン ............................................................ 62

検索

刺激薬

3,4-メチレンジオキシアンフェタミン (MDA) ............. 67

3,4-メチレンジオキシメタンフェタミン (MDMA)...... 67
3,4-ジメチルメトカチノン .............................................. 68

4-メチルエトカチノン ..................................................... 68

メトキサミン.................................................................... 68

ペンテドロン ................................................................... 69

シュードエフェドリ.................................................. 69, 70

α-ピロリジノペンチオフェノン ..................................... 70
ノルエフェドリン............................................................. 70
ノルメタネフリン............................................................. 70

ノルフェニレフリン ......................................................... 71

3,4-ジヒドロキシフェニルアラニン (DOPA) ............... 71
クレンブテロール ............................................................ 71
エチロン ........................................................................... 72

メチルフェニデート......................................................... 72

3-フルオロメトカチノン .................................................. 73
3,4-メチレンジオキシ-N-エチルアンフェタミン(MDEA) ........................................................................... 73

4-エチルメトカチノン ..................................................... 73
4-メチルエトカチノン ..................................................... 73
アミノレックス .................................................................74

アンフェタミン .................................................................74

ブチロン ...........................................................................74
カチノン ............................................................................74

フレフェドロン ................................................................ 75
メフェドロン .................................................................... 75
メタンフェタミン ............................................................ 75

メチルエフェドリン......................................................... 75
メチロン ........................................................................... 76

p-メトキシアンフェタミン ............................................. 76

ペンチロン....................................................................... 76
シネフリン........................................................................ 76

α-ピロリジノペンチオフェノン ..................................... 77

セチリジン ....................................................................... 63
クロルフェニラミン ........................................................ 63

シタロプラム ................................................................... 63

ジソピラミド.................................................................... 63

ケタミン ...........................................................................64
メトキシフェナミン ........................................................64

メトキシベラパミル ........................................................64

ニカルジピン ...................................................................64
オルフェナドリン............................................................. 65

ピペロキサン ................................................................... 65
プロメタジン ................................................................... 65

テトラヒドロゾリン......................................................... 65

サリドマイド .................................................................... 66
トリヘキシフェニジル .................................................... 66

トリメブチン .................................................................... 66

ベラパミル ....................................................................... 66

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9

アミン
1-ベンジル-2,2-ジフェニルエチルアミン

Retention (min):Resolution:

2.61/2.89 (Peak1/Peak 2)
3.51

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
30/70: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.98/3.15 (Peak1/Peak 2)
9.47

1-ベンジル-2,2-ジフェニルエチルアミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

3.44/3.77 (Peak1/Peak 2)
2.11

1,1'-ビナフチル-2,2'-ジアミン

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-CD (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
90/10/0.3/0.2: Acetonitrile/Methanol/Trifluoroacetate/TEA
Flow Rate:
1.0 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 254 nm

1,1'-ビナフチル-2,2'-ジアミン
Retention (min):Resolution:

2.64/2.79 (Peak1/Peak 2)
1.31

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2. 7μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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10

アミン
1-(1-ナフチル)エチルアミン
Retention (min):Resolution:

2.12/2.36 (Peak1/Peak 2)
2.29

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
Flow Rate:
1.0 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

1-(1-ナフチル)エチルアミン
Retention (min):Resolution:

2.64/2.95 (Peak1/Peak 2)
3.36

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-CF (4.6 x 100 mm, 2.7 μm)
Mobile phase:60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
Flow Rate:
1.0 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 280 nm

1-(1,1-ビフェニル-4-イル)エタンアミン

Retention (min):Resolution:

3.44/3.77 (Peak1/Peak 2)
2.11

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF (10 cm x 4.6 mm, 2.7 μm)
90/10/0.3/0.2: Acetonitrile/Methanol/Trifluoroacetate/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 254 nm

Retention (min):Resolution:

1.83/2.03 (Peak1/Peak 2)
2.59

1-(1,1-ビフェニル-4-イル)エタンアミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (4.6 x 100 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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11

アミン
1-(4-メトキシフェニル)エチルアミン
Retention (min):Resolution:

2.64/2.95 (Peak1/Peak 2)
3.36

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF (4.6 x 100 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 280 nm

Retention (min):Resolution:

2.43/2.65 (Peak1/Peak 2)
2.38

1-(4-メトキシフェニル)エチルアミン

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
Flow Rate:
1.0 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

1-アミノテトラリン
Retention (min):Resolution:

2.83/3.15 (Peak1/Peak 2)
2.81

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.78/2.18 (Peak1/Peak 2)
4.48

1-アミノテトラリン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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12

アミン
6-メトキシ-1,2,3,4-テトラヒドロ-1-ナフタレニルアミン
Retention (min):Resolution:

3.04/3.52 (Peak1/Peak 2)
4.42

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

0.72/0.91 (Peak1/Peak 2)
5.26

6-メトキシ-1,2,3,4-テトラヒドロ-1-ナフタレニルアミン

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
Flow Rate:
1.0 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

1-(2-メトキシフェニル)エタンアミン
Retention (min):Resolution:

2.64/2.95 (Peak1/Peak 2)
2.18

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

6.15/6.53 (Peak1/Peak 2)
1.31

1-(4-クロロフェニル)エチルアミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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13

アミン
1,1-ジフェニル-1-フルオロ-2-アミノプロパン
Retention (min):Resolution:

1.48/1.67 (Peak1/Peak 2)
3.20

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

1.87/2.13 (Peak1/Peak 2)
3.33

1,1-ジフェニル-2-アミノプロパン

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
Flow Rate:
1.0 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 230 nm

1,2,2-トリフェニルエチルアミン
Retention (min):Resolution:

1.64/1.93 (Peak1/Peak 2)
3.88

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

0.66/0.80 (Peak1/Peak 2)
4.49

2-アミノ-4-メチル-1,1-ジフェニルペンタン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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14

アミン
2-クロロ-インダン-1-イルアミン
Retention (min):Resolution:

2.97/3.25 (Peak1/Peak 2)
2.81

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.78/2.19 (Peak1/Peak 2)
5.58

4-メトキシ-α-メチルベンジルアミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

0.64/0.78 (Peak1/Peak 2)
5.04

ビス(1-フェニルエチル)アミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

0.92/1.29 (Peak1/Peak 2)
7.66

ビス(α-メチルベンジル)アミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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15

アミン
メキシレチン
Retention (min):Resolution:

8.38/8.81 (Peak1/Peak 2)
1.54

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
Flow Rate:
0.5 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

N-ベンジル-α-メチルベンジルアミン
Retention (min):Resolution:

0.99/1.32 (Peak1/Peak 2)
5.71

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
2.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

2.45/2.84 (Peak1/Peak 2)
3.47

N,α-ジメチルベンジルアミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 210 nm

Retention (min):Resolution:

16.25/17.10 (Peak1/Peak 2)
1.16α-メチル-4-ニトロベンジルアミン

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
Flow Rate:
0.3 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

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16

アミン
α-メチルベンジルアミン
Retention (min):Resolution:

3.67/3.92 (Peak1/Peak 2)
1.97

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 210 nm

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17

アミノ酸および誘導体
2-アミノ-2-フェニル酪酸
Retention (min):Resolution:

1.47/1.97 (Peak1/Peak 2)
5.16

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Ethanol/50 mM Ammonium Formate (pH 3.6)
1.0 mL/min
45 °C
1.0 μLUV 220 nm

Retention (min):Resolution:

4.69/5.20 (Peak1/Peak 2)
1.50

4-ニトロフェニルアラニン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 254 nm

Retention (min):Resolution:

1.55/2.25 (Peak1/Peak 2)
4.00

AQC メチオニン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
50/50: Acetonitrile/15 mM Ammonium Formate (pH 4.0)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.96/2.26 (Peak1/Peak 2)
2.32

AQC フェニルアラニン

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
50/50: Acetonitrile/15 mM Ammonium Formate (pH 4.0)
Flow Rate:
0.8 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

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18

アミノ酸および誘導体
AQC セリン
Retention (min):Resolution:

1.38/1.60 (Peak1/Peak 2)
2.14

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
50/50: Acetonitrile/15 mM Ammonium Formate (pH 4.0)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

3.11/3.46 (Peak1/Peak 2)
1.77

AQC チロシン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
50/50: Acetonitrile/15 mM Ammonium Formate (pH 4.0)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

2.63/3.16 (Peak1/Peak 2)
3.68

Fmoc アラニン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
60/40: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

2.62/2.89 (Peak1/Peak 2)
1.51

Fmoc アスパラギン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
60/40: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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19

アミノ酸および誘導体
Fmoc ロイシン
Retention (min):Resolution:

2.70/3.14 (Peak1/Peak 2)
3.20

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
60/40: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

2.81/3.55 (Peak1/Peak 2)
3.71

Fmoc フェニルアラニン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
60/40: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

3.04/3.46 (Peak1/Peak 2)
2.20

Fmoc トリプトファン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
60/40: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

2.63/2.89 (Peak1/Peak 2)
1.55

Fmoc バリン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
60/40: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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20

アミノ酸および誘導体
メチオニン
Retention (min):Resolution:

1.85/2.59 (Peak1/Peak 2)
6.76

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
60/40: Methanol/Water
0.8 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

3.31/3.73 (Peak1/Peak 2)
2.81

p-クロロフェニルアラニン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Ethanol/50 mM Ammonium Formate (pH 3.6)
0.5 mL/min
45 °C
1.0 μLUV 220 nm

Retention (min):Resolution:

3.37/3.70 (Peak1/Peak 2)
1.90

p-フルオロフェニルアラニン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/50 mM Ammonium Trifluoroacetate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 254 nm

Retention (min):Resolution:

2.92/3.29 (Peak1/Peak 2)
2.75

フェニルアラニン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Ethanol/50 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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21

アミノ酸および誘導体
トリプトファン
Retention (min):Resolution:

3.17/3.66 (Peak1/Peak 2)
3.04

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
30/70: Ethanol/50 mM Ammonium Formate (pH 3.6)
Flow Rate:
0.5 mL/min
Temperature:
45 °C
Injection Volume:
1.0 μL
Detection:
UV 254 nm

α-アミノ-2-チオフェン酢酸
Retention (min):Resolution:

1.33/1.86 (Peak1/Peak 2)
7.35

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/50 mM Ammonium Formate (pH 3.6)
1.0 mL/min
45 °C
1.0 μLUV 254 nm

Retention (min):Resolution:

2.90/3.16 (Peak1/Peak 2)
2.25

3-アミノ-3-フェニルプロパン酸

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/50 mM Ammonium Formate (pH 3.6)
0.5 mL/min
35 °C
1.0 μLUV 210 nm

Retention (min):Resolution:

2.21/2.54 (Peak1/Peak 2)
3.61

キヌレニン

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-V (15 cm x 4.6 mm, 2.7 μm)
Mobile phase:
30/70: Methanol/50 mM Ammonium Formate (pH 3.6)
Flow Rate:
1.0 mL/min
Temperature:
45 °C
Injection Volume:
1.0 μL
Detection:
UV 230 nm

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22

アミノ酸および誘導体
トリプトファンアミド
Retention (min):Resolution:

2.23/2.50 (Peak1/Peak 2)
2.75

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
Flow Rate:
1.0 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

3,4-ジヒドロキシフェニルアラニン (DOPA)
Retention (min):Resolution:

1.30/1.48 (Peak1/Peak 2)
2.95

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/50 mM Ammonium Formate (pH 3.6)
1.0 mL/min
45 °C
1.0 μLUV 230 nm

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23

鎮痛剤
メサドン
Retention (min):Resolution:

4.00/4.27 (Peak1/Peak 2)
2.21

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
Mobile phase:
20/80: Acetonitrile/50 mM Ammonium Formate (pH 3.6)
Flow Rate:
0.7 mL/min
Temperature:
45 °C
Injection Volume:
1.0 μL
Detection:
UV 230 nm

メサドン
Retention (min):Resolution:

6.88/7.49 (Peak1/Peak 2)
2.09

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
90/10: Ethanol/15 mM Ammonium Formate (pH 3.6)
Flow Rate:
0.5 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 254 nm

プログルミドRetention (min):Resolution:

8.90/9.65 (Peak1/Peak 2)
2.18

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
30/70: Methanol/50 mM Ammonium Trifluoroacetate (pH 3.6)
Flow Rate:
0.3 mL/min
Temperature:
45 °C
Injection Volume:
1.0 μL
Detection:
UV 220 nm

プログルミドRetention (min):Resolution:

2.42/2.66 (Peak1/Peak 2)
1.77

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
Flow Rate:
0.5 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

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24

鎮痛剤
インドプロフェン
Retention (min):Resolution:

8.22/9.13 (Peak1/Peak 2)
2.10

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
15 °C
1.0 μLUV 254 nm

Retention (min):Resolution:

1.25/1.35 (Peak1/Peak 2)
2.68

ケトロラック

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.3 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
45 °C
1.0 μLUV 220 nm

Retention (min):Resolution:

2.19/2.51 (Peak1/Peak 2)
3.34

メトルファン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
80/20: Methanol/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

3.66/3.93 (Peak1/Peak 2)
2.10

ネホパム

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
0.7 mL/min
45 °C
1.0 μLUV 220 nm

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25

鎮痛剤
トラマドールRetention (min):Resolution:

7.44/7.95 (Peak1/Peak 2)
1.90

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-V (15 cm x 4.6 mm, 2.7 μm)
Mobile phase:
30/70: Methanol/50 mM Ammonium Formate (pH 3.6)
Flow Rate:
0.3 mL/min
Temperature:
45 °C
Injection Volume:
1.0 μL
Detection:
UV 230 nm

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26

麻酔薬
ヘキソバルビタール
Retention (min):Resolution:

4.63/4.99 (Peak1/Peak 2)
1.54

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
30/70: Methanol/15 mM Ammonium Formate (pH 3.6)
Flow Rate:
0.5 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

ヘキソバルビタール
Retention (min):Resolution:

4.70/5.29 (Peak1/Peak 2)
2.92

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
30/70: Methanol/15 mM Ammonium Formate (pH 3.6)
Flow Rate:
0.5 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

メピバカイン
Retention (min):Resolution:

4.01/4.36 (Peak1/Peak 2)
1.42

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

4.75/5.14 (Peak1/Peak 2)
2.25

メピバカイン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
30 °C
1.0 μLUV 220 nm

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27

麻酔薬
ブピバカイン
Retention (min):Resolution:

1.58/1.85 (Peak1/Peak 2)
3.76

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

2.60/2.87 (Peak1/Peak 2)
2.63

メホバルビタール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
45 °C
1.0 μLUV 220 nm

Retention (min):Resolution:

4.78/5.18 (Peak1/Peak 2)
2.31

プリロカイン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.1: Methanol/Acetic Acid/Triethylamine
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

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28

抗凝血剤
クマクロル
Retention (min):Resolution:

1.96/2.20 (Peak1/Peak 2)
3.06

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
30/70: Acetonitrile/15 mM Ammonium Acetate (pH 3.6)
Flow Rate:
1.0 mL/min
Temperature:
45 °C
Injection Volume:
1.0 μL
Detection:
UV 220 nm

ワルファリン
Retention (min):Resolution:

3.75/4.45 (Peak1/Peak 2)
3.38

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/50 mM Ammonium Formate (pH 3.6)
1.0 mL/min
45 °C
1.0 μLUV 230 nm

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29

抗けいれん薬
フェンスクシミド
Retention (min):Resolution:

4.50/4.91 (Peak1/Peak 2)
2.37

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
30/70: Methanol/15 mM Ammonium Formate (pH 3.6)
Flow Rate:
0.5 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
0.5 μL
Detection:
UV 220 nm

フェンスクシミド
Retention (min):Resolution:

7.83/8.43 (Peak1/Peak 2)
2.04

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/15 mM Ammonium Formate (pH 3.6)
0.3 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

7.73/8.32 (Peak1/Peak 2)
1.92

α-メチル-α-フェニルスクシンイミド

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/50 mM Ammonium Formate (pH 3.6)
0.3 mL/min
25 °C
1.0 μLUV 230 nm

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30

抗うつ剤
ブプロピオン
Retention (min):Resolution:

4.63/4.99 (Peak1/Peak 2)
1.54

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

2.92/3.38 (Peak1/Peak 2)
4.63

テマゼパム

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
20/80: Acetonitrile/50 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

0.69/1.22 (Peak1/Peak 2)
8.65

ロラゼパム

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100: Methanol
2.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.40/1.55 (Peak1/Peak 2)
2.71

ロルメタゼパム

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100: Methanol
1.0 mL/min
10 °C
1.0 μLUV 220 nm

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31

抗うつ剤
ミアンセリン
Retention (min):Resolution:

6.41/7.06 (Peak1/Peak 2)
1.50

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
Flow Rate:
1.0 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 254 nm

ミアンセリン
Retention (min):Resolution:

1.24/2.08 (Peak1/Peak 2)
9.77

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
2.0 mL/min
45 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

0.72/1.33 (Peak1/Peak 2)
9.49

オキサゼパム

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100: Methanol
2.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.76/2.02 (Peak1/Peak 2)
3.46

フルオキセチン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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32

抗うつ剤
トラニルシプロミン
Retention (min):Resolution:

5.04/5.48 (Peak1/Peak 2)
2.53

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
30 °C
1.0 μLUV 220 nm

Retention (min):Resolution:

1.95/2.27 (Peak1/Peak 2)
3.37

トリミプラミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

5.67/6.13 (Peak1/Peak 2)
2.12

ベンラファキシン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.1: Methanol/Acetic Acid/Triethylamine
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

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33

ベータブロッカー
アセブトロール
Retention (min):Resolution:

7.08/7.63 (Peak1/Peak 2)
1.76

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
Flow Rate:
1.0 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

アセブトロール
Retention (min):Resolution:

7.01/7.56 (Peak1/Peak 2)
2.12

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (15 cm x 4.6 mm, 2.7 μm)
100/0.2/0.1: Methanol/Acetic Acid/Triethylamine
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

3.40/3.73 (Peak1/Peak 2)
2.78

アルプレノロール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

2.84/3.08 (Peak1/Peak 2)
2.31

アルプレノロール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.8 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

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34

ベータブロッカー
アテノロールRetention (min):Resolution:

6.56/7.31 (Peak1/Peak 2)
2.46

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.1: Methanol/Acetic Acid/Triethylamine
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

7.91/8.49 (Peak1/Peak 2)
1.76

アテノロール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

エスモロールRetention (min):Resolution:

11.55 /12.66 (Peak1/Peak 2)
2.70

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Formate
0.3 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

エスモロールRetention (min):Resolution:

3.48/3.73 (Peak1/Peak 2)
2.02

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.7 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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35

ベータブロッカー
イソプロテレノール
Retention (min):Resolution:

7.76/8.56 (Peak1/Peak 2)
2.70

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
100/0.2/0.1: Methanol/Trifluoroacetate/Ammonium Hydroxide
Flow Rate:
0.7 mL/min
Temperature:
45 °C
Injection Volume:
1.0 μL
Detection:
UV 230 nm

イソプロテレノール
Retention (min):Resolution:

4.60/4.96 (Peak1/Peak 2)
1.0

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.62/1.89 (Peak1/Peak 2)
3.01

メタプロテレノール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
3.5 mL/min
45 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

4.63/4.98 (Peak1/Peak 2)
1.89

メタプロテレノール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

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36

ベータブロッカー
メトプロロール
Retention (min):Resolution:

1.62/1.89 (Peak1/Peak 2)
3.01

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
3.5 mL/min
45 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

4.80/5.13 (Peak1/Peak 2)
1.99

メトプロロール

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
Flow Rate:
0.3 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

ピンドロールRetention (min):Resolution:

4.25/4.66 (Peak1/Peak 2)
2.56

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

3.76/4.01 (Peak1/Peak 2)
2.33

ピンドロール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.7 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

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37

ベータブロッカー
プロプラノロール
Retention (min):Resolution:

4.09/4.56 (Peak1/Peak 2)
3.11

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
Flow Rate:
1.0 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 230 nm

プロプラノロール
Retention (min):Resolution:

2.85/3.14 (Peak1/Peak 2)
2.45

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

5.69/6.34 (Peak1/Peak 2)
2.66

サルブタモール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
45 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

3.89/4.30 (Peak1/Peak 2)
2.90

サルブタモール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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38

ベータブロッカー
ソタロール
Retention (min):Resolution:

5.97/6.73 (Peak1/Peak 2)
2.77

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

2.93/3.38 (Peak1/Peak 2)
3.28

ソタロール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

2.92/3.74 (Peak1/Peak 2)
6.48

テルブタリン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.1: Methanol/Acetic Acid/Triethylamine
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.99/2.18 (Peak1/Peak 2)
2.34

テルブタリン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

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39

ベータブロッカー
ツロブテロール
Retention (min):Resolution:

2.50/2.82 (Peak1/Peak 2)
3.51

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
100/0.2/0.1: Methanol/Acetic Acid/Triethylamine
Flow Rate:
1.0 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

ツロブテロール
Retention (min):Resolution:

1.65/1.82 (Peak1/Peak 2)
2.94

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

7.76/8.37 (Peak1/Peak 2)
1.50

カルベジロール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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40

抑制薬
バクロフェン
Retention (min):Resolution:

2.11/2.50 (Peak1/Peak 2)
2.87

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
100/ 0.1 wt %: Methanol/Ammonium Trifluoroacetate
Flow Rate:
1.5 mL/min
Temperature:
45 °C
Injection Volume:
1.0 μL
Detection:
UV 220 nm

バクロフェン
Retention (min):Resolution:

2.05/2.29 (Peak1/Peak 2)
1.83

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

3.94/4.24 (Peak1/Peak 2)
2.23

オクトクロテピン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (15 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/50 mM Ammonium Formate (pH 3.6)
0.7 mL/min
45 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

1.69/1.93 (Peak1/Peak 2)
3.05

トルペリゾン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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41

利尿薬
クロルタリドンRetention (min):Resolution:

4.60/4.94 (Peak1/Peak 2)
2.45

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
10/90: Acetonitrile/50 mM Ammonium Formate (pH 3.6)
0.7 mL/min
40 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

5.26/6.24 (Peak1/Peak 2)
2.54

クロルタリドン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/16 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

5.91/6.64 (Peak1/Peak 2)
2.79

ベンドロフルメチアジド

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/50 mM Ammonium Trifluoroacetate (pH 3.6)
0.5 mL/min
45 °C
1.0 μLUV 220 nm

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42

殺菌剤
ベナラキシルRetention (min):Resolution:

1.64/1.87 (Peak1/Peak 2)
3.13

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (10 cm x 4.6 mm, 2.7 μm)
30/70: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

3.17/3.43 (Peak1/Peak 2)
2.15

エコナゾール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (10 cm x 4.6 mm, 2.7 μm)
30/70: Acetonitrile/15 mM Ammonium Trifluoroacetate (pH 3.6)
0.7 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

2.89 /3.14 (Peak1/Peak 2)
2.54

フルトリアホルMethod Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
30/70: Acetonitrile/50 mM Ammonium Formate (pH 3.6)
1.0 mL/min
15 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

4.17/4.42 (Peak1/Peak 2)
2.18

ミコナゾール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
30/70: Acetonitrile/50 mM Ammonium Formate (pH 3.6)
0.7 mL/min
40 °C
1.0 μLUV 230 nm

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43

殺菌剤
プラジカンテル
Retention (min):Resolution:

7.04/7.58 (Peak1/Peak 2)
1.85

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
20/80: Acetonitrile/50 mM Ammonium Formate (pH 3.6)
0.7 mL/min
45 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

2.86/3.16 (Peak1/Peak 2)
2.59

プロチオコナゾール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (10 cm x 4.6 mm, 2.7 μm)
30/70: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.22/1.54 (Peak1/Peak 2)
4.91

ジクロルプロップ

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.3 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

4.10/4.71 (Peak1/Peak 2)
3.00

フェノプロップ

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/50 mM Ammonium Trifluoroacetate (pH 3.6)
0.5 mL/min
45 °C
1.0 μLUV 220 nm

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44

殺菌剤
ハロキシホップ
Retention (min):Resolution:

1.12/1.37 (Peak1/Peak 2)
4.48

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.3 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

7.65/8.22 (Peak1/Peak 2)
1.87

マンジプロパミド

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
45 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

12.73/13.39 (Peak1/Peak 2)
1.74

メコプロップメチルエステル

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (15 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/50 mM Ammonium Formate (pH 3.6)
0.5 mL/min
45 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

1.14/1.31 (Peak1/Peak 2)
3.59

メコプロップ

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
100/0.3 wt %: Methanol/Ammonium Trifluoroacetate
Flow Rate:
1.0 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

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45

殺菌剤
ナプロパミドRetention (min):Resolution:

3.40/3.74 (Peak1/Peak 2)
2.26

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/50 mM Ammonium Formate (pH 3.6)
1.0 mL/min
45 °C
1.0 μLUV 220 nm

Retention (min):Resolution:

3.57/3.78 (Peak1/Peak 2)
1.76

ナプロパミド

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
0.3 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

7.54/8.34 (Peak1/Peak 2)
2.10

ブロマシル

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

4.67/5.05 (Peak1/Peak 2)
2.33

ブロマシル

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/50 mM Ammonium Trifluoroacetate (pH 3.6)
0.5 mL/min
45 °C
1.0 μLUV 220 nm

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46

その他
2'-アミノ-1,1'-ビナフタレン-2-オール
Retention (min):Resolution:

2.16/2.28 (Peak1/Peak 2)
1.45

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
30/70: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

1.23/1.44 (Peak1/Peak 2)
3.36

ヒドロアトロパ酸

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (10 cm x 4.6 mm, 2.7 μm)
100/0.3 wt %: Methanol/Ammonium Trifluoroacetic Acid
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

2.31/2.45 (Peak1/Peak 2)
1.98

トロパ酸

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
30/70: Acetonitrile/50 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

2.92/3.28 (Peak1/Peak 2)
3.23

ヤコブセン触媒

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (10 cm x 4.6 mm, 2.7 μm)
90/10/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 254 nm

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47

その他
α-N,N-ジメチルアミノフェニルアセトニトリル
Retention (min):Resolution:

1.14/1.31 (Peak1/Peak 2)
3.59

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (10 cm x 4.6 mm, 2.7 μm)
100/0.3 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

3.81/4.03 (Peak1/Peak 2)
1.30

2-アミノ-1,2-ジフェニルエタノール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF (10 cm x 4.6 mm, 2.7 μm)
30/70: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

4.56/4.89 (Peak1/Peak 2)
1.58

2-アミノ-1,2-ジフェニルエタノール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

3.29/3.58 (Peak1/Peak 2)
2.35

フェニルアラニノール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF(10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 210 nm

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48

その他
フェニルアラニノール
Retention (min):Resolution:

2.33/2.52 (Peak1/Peak 2)
1.96

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

3.27/3.53 (Peak1/Peak 2)
2.34

4-クロロフェニルアラニノール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

2.93/3.47 (Peak1/Peak 2)
4.38

trans-1-アミノ-2-インダノール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 210 nm

Retention (min):Resolution:

1.79/2.06 (Peak1/Peak 2)
3.67

trans-1-アミノ-2-インダノール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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49

その他
トリプトファノール
Retention (min):Resolution:

3.39/3.74 (Peak1/Peak 2)
2.88

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 280 nm

Retention (min):Resolution:

3.39/3.74 (Peak1/Peak 2)
2.88

チロシノール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 280 nm

Retention (min):Resolution:

6.84/7.29 (Peak1/Peak 2)
1.91

α-(1-アミノエチル)-4-ヒドロキシベンジル-アルコール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

3.31/3.79 (Peak1/Peak 2)
2.95

2-(2-クロロフェノキシ)プロピオン酸

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
100/0.3 wt %: Methanol/Ammonium Trifluoroacetate
Flow Rate:
1.0 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 230 nm

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50

その他
2-(3-クロロフェノキシ)プロピオン酸 (メタクロルフェンプロップ )Retention (min):Resolution:

1.24/1.38 (Peak1/Peak 2)
2.51

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.3 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

1.24/1.54 (Peak1/Peak 2)
4.92

2-(4-クロロフェノキシ)プロピオン酸

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.3 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.23/1.44 (Peak1/Peak 2)
3.36

2-フェノキシプロパン酸

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.3 wt %: Methanol/Ammonium Trifluoroacetic Acid
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.81/1.99 (Peak1/Peak 2)
2.66

2-アミノ-1,1,-ジフェニル-1-プロパノール

Method Conditions
Column: 	InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
Mobile phase:
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
Flow Rate:
1.0 mL/min
Temperature:
Ambient (23 °C)
Injection Volume:
1.0 μL
Detection:
UV 220 nm

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51

その他
2-アミノ-1,1,13-トリフェニル-1-プロパノール
Retention (min):Resolution:

1.28/1.54 (Peak1/Peak 2)
4.66

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

2-(カルボベンジルオキシアミノ)-3-フェニル-1-プロパノール
Retention (min):Resolution:

13.85/14.94 (Peak1/Peak 2)
1.50

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.64/1.82 (Peak1/Peak 2)
2.80

cis-1-アミノ-2-インダノール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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52

神経伝達物質およびホルモン
オクトパミン
Retention (min):Resolution:

4.22/4.62 (Peak1/Peak 2)
2.08

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

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53

オキサゾリジノン
1,5-ジメチル-4-フェニル-2-イミダゾリジノン
Retention (min):Resolution:

1.81/1.99 (Peak1/Peak 2)
2.66

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

5.60/6.08 (Peak1/Peak 2)
1.92

4-ベンジル-2-オキサゾリジノン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
80/20: Methanol/50 mM Ammonium Formate (pH 3.6)
0.3 mL/min
Ambient (23 °C)
1.0 μLUV 254 nm

Retention (min):Resolution:

0.51/0.72 (Peak1/Peak 2)6.51

4-メチル-5-フェニル-2-オキサゾリジノン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100: Methanol
2.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.63/1.86 (Peak1/Peak 2)
2.79

4-フェニル-2-オキサゾリジノン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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54

オキサゾリジノン
5,5-ジメチル-4-フェニル-2-オキサゾリジノン
Retention (min):Resolution:

2.58/2.78 (Peak1/Peak 2)
1.96

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
0.5 mL/min
35 °C
1.0 μLUV 220 nm

Retention (min):Resolution:

0.55/0.71 (Peak1/Peak 2)
3.32

5,5-ジメチル-4-ベンジル-2-オキサゾリジノン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100: Methanol
2.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

0.53/0.70 (Peak1/Peak 2)
4.84

5,5-ジメチル-4-メチル-2-オキサゾリジノン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100: Methanol
2.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm(3a-cis)-3,3a,8,8a-テトラヒドロ-2H-インデノ[1,2-d]オキサゾール-2-オン
Retention (min):Resolution:

3.80/4.03 (Peak1/Peak 2)
1.91

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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55

オキサゾリジノン
4-(1-H-インドール-3-イル-メチル)-2-オキサゾリジノン
Retention (min):Resolution:

2.59/2.76 (Peak1/Peak 2)
1.98

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100: Methanol
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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56

医薬品
1-インダノール
Retention (min):Resolution:

7.62/8.06 (Peak1/Peak 2)
2.26

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
20/80: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

5.31/5.63 (Peak1/Peak 2)
2.11

ベンゾイン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
20/80: Acetonitrile/50 mM Ammonium Formate (pH 3.6)
0.7 mL/min
40 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

3.63/3.99 (Peak1/Peak 2)
2.53

クロフェジアノール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
0.6 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

3.63/3.99 (Peak1/Peak 2)
2.53

クロフェジアノール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
0.6 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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57

医薬品
ホマトロピン
Retention (min):Resolution:

3.37/3.77 (Peak1/Peak 2)
2.25

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
10/90: Acetonitrile/50 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

13.65/14.48 (Peak1/Peak 2)
1.12

インダパミド

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
15/85: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
0.3 mL/min
10 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

7.82/8.29 (Peak1/Peak 2)
1.97

ロフェキシジン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (10 cm x 4.6 mm, 2.7 μm)
10/90: Acetonitrile/50 mM Ammonium Formate (pH 3.6)
0.5 mL/min
45 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

9.16/9.53 (Peak1/Peak 2)
1.15

ロフェキシジン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm) x2
100/0.2/0.05: Methanol/ Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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58

医薬品
p-クロロアンフェタミン
Retention (min):Resolution:

9.76/10.15 (Peak1/Peak 2)
1.54

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
15/85: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.47/1.66 (Peak1/Peak 2)
2.83

フェニルこはく酸無水物

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (10 cm x 4.6 mm, 2.7 μm)
30/70: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

7.42/9.38 (Peak 1/Peak 2), 9.97/10.42 (Peak 3/Peak 4)
7.49 (Peak 1/Peak 2), 1.63 (Peak 3/Peak 4)

トリアジメノール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
25/75: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
35 °C
1.0 μLUV 220 nm

Retention (min):Resolution:

1.26/1.59 (Peak1/Peak 2)
5.83

5-メチル-5-フェニルヒダントイン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100: Methanol
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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59

医薬品
アミノグルテチミド
Retention (min):Resolution:

4.28/4.63 (Peak1/Peak 2)
2.50

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (15 cm x 4.6 mm, 2.7 μm)
100/0.5 wt %: Methanol/Ammonium Trifluoroacetate
0.5 mL/min
10 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

8.74/9.30 (Peak1/Peak 2)
1.52

バメタン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

5.19/5.69 (Peak1/Peak 2)
2.24

バメタン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
0.8 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

8.80/9.87 (Peak1/Peak 2)
2.44

ジペロドン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.7 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

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60

医薬品
ジペロドン
Retention (min):Resolution:

8.19/8.86 (Peak1/Peak 2)
1.40

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

8.59/9.37 (Peak1/Peak 2)
1.50

フルルビプロフェン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

0.91/1.11 (Peak1/Peak 2)
3.56

マンデル酸

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/80 mM Ammonium Acetate (pH 5.0)
0.5 mL/min
45 °C
1.0 μLUV 220 nm

Retention (min):Resolution:

3.80/4.03 (Peak1/Peak 2)
1.91

ナフトピジル

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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61

医薬品
p-ヒドロキシマンデル酸
Retention (min):Resolution:

1.09/1.24 (Peak1/Peak 2)
2.87

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/50 mM Ammonium Formate (pH 3.6)
1.0 mL/min
45 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

9.58/10.39 (Peak1/Peak 2)
2.06

アムロジピン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

4.91/5.37 (Peak1/Peak 2)
2.05

ブロムフェニラミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
0.7 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

8.61/9.30 (Peak1/Peak 2)
1.92

カルビノキサミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

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62

医薬品
セチリジン
Retention (min):Resolution:

15.48/16.14 (Peak1/Peak 2)
1.12

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm) x2
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
0.3 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

4.74/5.14 (Peak1/Peak 2)
1.95

クロルフェニラミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
0.7 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

7.38/8.14 (Peak1/Peak 2)
2.15

シタロプラム

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.7 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

ジソピラミドRetention (min):Resolution:

4.88/5.26 (Peak1/Peak 2)
2.12

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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63

医薬品
ケタミン
Retention (min):Resolution:

9.72/10.31 (Peak1/Peak 2)
1.22

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (15 cm x 4.6 mm, 2.7 μm)
90/10: Ethanol/15 mM Ammonium Formate (pH 3.6)
0.3 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.67/1.82 (Peak1/Peak 2)
2.54

メトキシフェナミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

16.03/17.26 (Peak1/Peak 2)
1.17

メトキシベラパミル

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm) x2
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

0.68/0.77 (Peak1/Peak 2)
2.78

ニカルジピン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
2.0 mL/min
45 °C
1.0 μLUV 230 nm

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64

医薬品
オルフェナドリン
Retention (min):Resolution:

2.06/2.31 (Peak1/Peak 2)
2.92

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

4.72/5.12 (Peak1/Peak 2)
2.18

ピペロキサン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.1: Methanol/Acetic Acid/Triethylamine
0.7 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.95/3.00 (Peak1/Peak 2)
7.52

プロメタジン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
2.0 mL/min
Ambient (23 °C)
1.0 μLUV 254 nm

Retention (min):Resolution:

1.79/1.95 (Peak1/Peak 2)
2.49

テトラヒドロゾリン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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65

医薬品
サリドマイドRetention (min):Resolution:

0.66/1.02 (Peak1/Peak 2)
8.50

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100: Methanole
2.0 mL/min
45 °C
1.0 μLUV 220 nm

Retention (min):Resolution:

1.74/1.96 (Peak1/Peak 2)
2.66

トリヘキシフェニジル

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.53/1.71 (Peak1/Peak 2)
2.98

トリメブチン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

19.35/20.44 (Peak1/Peak 2)
1.13

ベラパミル

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm) x2
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
0.3 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

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66

刺激薬
3,4-メチレンジオキシアンフェタミン (MDA)
Retention (min):Resolution:

9.61/10.06 (Peak1/Peak 2)
1.71

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
10/90: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

30.31/32.27 (Peak1/Peak 2)
1.16

3,4-メチレンジオキシアンフェタミン (MDA)

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm) x2
95/5: Ethanol/15 mM Ammonium Formate (pH 3.6)
0.4 mL/min
Ambient (23 °C)
1.0 μLUV 263 nm

Retention (min):Resolution:

6.95/7.33 (Peak1/Peak 2)
1.54

3,4-メチレンジオキシメタンフェタミン (MDMA)

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
15/85: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
0.7 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

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67

刺激薬
3,4-ジメチルメトカチノン
Retention (min):Resolution:

19.35/20.44 (Peak1/Peak 2)
1.13

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (10 cm x 4.6 mm, 2.7 μm) x2
90/10: Methanol/15 mM Ammonium Formate (pH 3.6)
0.3 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

22.98/24.98 (Peak1/Peak 2)
1.52

3,4-ジメチルメトカチノン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
95/5: Ethanol/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 254 nm

Retention (min):Resolution:

1.87/2.23 (Peak1/Peak 2)
3.62

メトキサミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (10 cm x 4.6 mm, 2.7 μm)
10/90: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

8.32/8.93 (Peak1/Peak 2)
1.24

メトキサミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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68

刺激薬
ペンテドロン
Retention (min):Resolution:

3.54/3.87 (Peak1/Peak 2)
2.68

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
10/90: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 254 nm

Retention (min):Resolution:

7.95/8.53 (Peak1/Peak 2)
1.80

ペンテドロン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Ethanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 254 nm

Retention (min):Resolution:

3.08/4.01 (Peak1/Peak 2)
8.98

シュードエフェドリン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
10/90: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

7.70/8.27 (Peak1/Peak 2)
2.04

シュードエフェドリン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
0.7 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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69

刺激薬
シュードエフェドリン
Retention (min):Resolution:

8.34/8.84 (Peak1/Peak 2)
1.40

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 254 nm

Retention (min):Resolution:

14.24/15.21 (Peak1/Peak 2)
1.34

α-ピロリジノペンチオフェノン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CD (15 cm x 4.6 mm, 2.7 μm)
15/85: Acetonitrile/15 mM Ammonium Formate (pH 3.6)
0.3 mL/min
10 °C
1.0 μLUV 254 nm

Retention (min):Resolution:

4.26/4.57 (Peak1/Peak 2)
1.96

ノルエフェドリン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
0.8 mL/min
Ambient (23 °C)
1.0 μLUV 210 nm

Retention (min):Resolution:

4.46/4.96 (Peak1/Peak 2)
2.88

ノルメタネフリン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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70

刺激薬
ノルフェニレフリン
Retention (min):Resolution:

4.30/4.77 (Peak1/Peak 2)
2.84

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-CF (10 cm x 4.6 mm, 2.7 μm)
60/40/0.3/0.2: Acetonitrile/Methanol/Acetic Acid/TEA
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

1.30/1.48 (Peak1/Peak 2)
2.95

3,4-ジヒドロキシフェニルアラニン (DOPA)

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/50 mM Ammonium Formate (pH 3.6)
1.0 mL/min
45 °C
1.0 μLUV 230 nm

Retention (min):Resolution:

2.28/2.72 (Peak1/Peak 2)
3.70

クレンブテロール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
2.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

2.48/2.75 (Peak1/Peak 2)
2.66

クレンブテロール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1/0.02: Methanol/Acetic Acid/Ammonium Hydroxide
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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71

刺激薬
クレンブテロール
Retention (min):Resolution:

13.38/14.18 (Peak1/Peak 2)
1.50

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

3.75/4.13 (Peak1/Peak 2)
2.61

クレンブテロール

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.1: Methanol/Acetic Acid/Triethylamine
0.7 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

4.68/5.04 (Peak1/Peak 2)
1.58

メチルフェニデート

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-T (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

0.68/0.90 (Peak1/Peak 2)
5.18

メチルフェニデート

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Formate (pH 3.6)
2.75 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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72

刺激薬
3-フルオロメトカチノン
Retention (min):Resolution:

6.15/6.57 (Peak1/Peak 2)
1.50

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
30/70: Methanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 254 nm

Retention (min):Resolution:

5.67/5.96 (Peak1/Peak 2)
1.58

3,4-メチレンジオキシ-N-エチルアンフェタミン (MDEA)

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

7.85/8.38 (Peak1/Peak 2)
1.74

4-エチルメトカチノン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Ethanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 254 nm

Retention (min):Resolution:

6.73/7.33 (Peak1/Peak 2)
2.23

4-エチルメトカチノン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Ethanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 254 nm

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73

刺激薬
アミノレックス
Retention (min):Resolution:

5.17/5.53 (Peak1/Peak 2)
1.98

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.05: Methanol/Acetic Acid/Ammonium Hydroxide
0.7 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

2.08/2.28 (Peak1/Peak 2)
2.48

アンフェタミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

5.71/6.10 (Peak1/Peak 2)
1.97

ブチロン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.1: Methanol/Acetic Acid/Triethylamine
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

2.01/2.23 (Peak1/Peak 2)
2.65

カチノン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
15 °C
1.0 μLUV 220 nm

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74

刺激薬
フレフェドロン
Retention (min):Resolution:

5.68/6.10 (Peak1/Peak 2)
1.85

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.1: Methanol/Acetic Acid/Triethylamine
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

8.56/9.19 (Peak1/Peak 2)
1.84

メフェドロン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Ethanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 254 nm

Retention (min):Resolution:

4.25/4.71 (Peak1/Peak 2)
2.73

メタンフェタミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1/0.05: Methanol/Acetic Acid/Triethylamine
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

3.69/3.95 (Peak1/Peak 2)
1.92

メチルエフェドリン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1/0.05: Methanol/Acetic Acid/Triethylamine
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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刺激薬
メチロン
Retention (min):Resolution:

6.52/7.03 (Peak1/Peak 2)
2.08

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.2/0.1: Methanol/Acetic Acid/Triethylamine
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

3.35/3.63 (Peak1/Peak 2)
2.47

p-メトキシアンフェタミン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
0.6 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

Retention (min):Resolution:

8.88/9.55 (Peak1/Peak 2)
1.72

ペンチロン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Ethanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 230 nm

Retention (min):Resolution:

10.67/11.62 (Peak1/Peak 2)
1.92

ペンチロン

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
90/10: Ethanol/15 mM Ammonium Formate (pH 3.6)
0.5 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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刺激薬
α-ピロリジノペンチオフェノン
Retention (min):Resolution:

1.64/1.92 (Peak1/Peak 2)
4.33

Method Conditions
Column:Mobile phase:
Flow Rate:
Temperature:
Injection Volume:
Detection:

InfinityLab Poroshell 120 Chiral-V (10 cm x 4.6 mm, 2.7 μm)
100/0.1 wt %: Methanol/Ammonium Trifluoroacetate
1.0 mL/min
Ambient (23 °C)
1.0 μLUV 220 nm

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カラム別目次

検索

リンクをクリックすると、該当ページに移動します。

InfinityLab Poroshell 120 Chiral-CD
1-benzyl-2,2-diphenylethylamine................... 10
1,1'-binaphthyl-2,2'-diamine............................. 10
Methadone........................................................... 24
Bupropion............................................................. 31
Temazepam......................................................... 31
Chlorthalidone..................................................... 42
Benalaxyl...............................................................43
Econazole.............................................................43
Flutriafol................................................................43
Miconazole...........................................................43
Praziquantel.........................................................44
Prothioconazole..................................................442'-amino-1,1'-binaphthalen-2-ol...................... 47
Hydratropic acid.................................................. 47
Jacobsen's catalyst........................................... 47
Tropic acid............................................................ 47
α-N,N-dimethylaminophenyl acetonitrile....48
1,5-dimethyl-4-phenyl-2-imidazolidinone....54
1-indanol................................................................57
Benzoin..................................................................57
Chlophedianol......................................................57
Homatropine........................................................58
Indapamide..........................................................58
Lofexidine..............................................................58
p-chloramphetamine........................................59
Phenylsuccinic anhydride................................59
Triadimenol...........................................................59
3,4-methylenedioxyamphetamine (MDA)... 67
3,4-methylenedioxymethamphetamine(MDMA).................................................................67
3,4-dimethylmethcathinone............................67
4-methylethcathinone.......................................68
Methoxamine.......................................................68
Pentedrone...........................................................69
Pseudoephedrine...............................................69
α-pyrrolidinopentiophenone............................70
InfinityLab Poroshell 120 Chiral-CF
1-(1-naphthyl)ethylamine................................. 11
1-(1,1-biphenyl-4-yl)ethanamine..................... 11
1-(4-methoxyphenyl)ethylamine.................... 12
1-aminotetralin.................................................... 12
6-methoxy-1,2,3,4-tetrahydro-1naphthalenylamine............................................ 13
2-amino-1,2-diphenylethanol..........................48
phenylalaninol......................................................48
4-chlorophenylalaninol..................................... 49trans-1-amino-2-indanol................................... 49

Tryptophanol........................................................50
Tyrosinol................................................................50α-(1-aminoethyl)-4-hydroxybenzylalcohol...................................................................50
Octopamine..........................................................53
Norephedrine.......................................................70
Normetanephrine...............................................70
Norphenylephrine...............................................71
InfinityLab Poroshell 120 Chiral-T
2-amino-2-pheylbutyric acid........................... 18
4-nitrophenylalanine.......................................... 18
AQC Methionine.................................................. 18
AQC Phenylalanine............................................. 18
AQC Serine............................................................ 19
AQC Tyrosine....................................................... 19
Fmoc Alanine....................................................... 19
Fmoc Asparagine............................................... 19
Fmoc Leucine......................................................20
Fmoc Phenylalanine..........................................20
Fmoc Tryptophan...............................................20
Fmoc Valine..........................................................20
Methionine............................................................ 21
p-chlorophenylalanine ..................................... 21
p-fluorophenylalanine....................................... 21
Phenylalanine...................................................... 21
Tryptophan...........................................................22
α-amino-2-thiophenacetic acid......................22
3,4-dihydroxyphenylalanine (DOPA) ............ 23
Proglumide........................................................... 24
Indoprofen............................................................ 25
Ketorolac............................................................... 25
Hexobarbital.........................................................27
Mepivacaine.........................................................27
Coumachlor..........................................................29
Warfarin.................................................................29
Phensuximide......................................................30
α-methyl-α-phenylsuccinimide......................30
Lorazepam............................................................ 31
Lormetazepam.................................................... 31
Mianserin..............................................................32
Oxazepam.............................................................32
Acebutolol.............................................................34
Alprenolol..............................................................34
Atenolol..................................................................35
Esmolol..................................................................35
Isoproterenol .......................................................36
Metaproterenol....................................................36
Metoprolol.............................................................37

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Pindolol..................................................................37
Propanolol............................................................38
Salbutamol...........................................................38
Sotalol....................................................................39
Terbutaline............................................................39
Tulobuterol............................................................40
Baclofen................................................................ 41
Bendroflumethiazide......................................... 42
Chlorthalidone..................................................... 42
Dichloroprop........................................................44
Fenoprop...............................................................44
Haloxyfop..............................................................45
Mecoprop methyl ester....................................45
Mecoprop ...........................................................45
Bromacil................................................................46
Napropamid.........................................................46
2-(2-chlorophenoxy)propionic acid...............50
2-(3-chlorophenoxy)propionic acid............... 51
2-(4-chlorphenoxy)propionic acid................. 51
2-phenoxypropanoic acid................................ 51
4-benzyl-2-oxazolidinone.................................54
4-methyl-5-phenyl-2-oxazolidinone..............54
4-phenyl-2-oxazolidinone.................................54
5,5-dimethyl-4-phenyl-2-oxazolidinone....... 55
5,5-dimethyl-4-benzyl-2-oxazolidinone....... 55
5,5-dimethyl-4-methyl-2-oxazolidinone....... 55
5-methyl-5-phenylhydantoin...........................59
Aminoglutethimide............................................60
Bamethan.............................................................60
Diperodon.............................................................60
Flurbiprofen.......................................................... 61
Mandelic acid....................................................... 61
Naftopidil............................................................... 61
p-hydroxymandelic acid................................... 62
Pseudoephedrine ..............................................69
3,4-dihydroxyphenylalanine (DOPA)............. 71
Clenbuterol...........................................................71
Ethylone.................................................................72
Methylphenidate.................................................72
4-methylethcathinone.......................................73
InfinityLab Poroshell 120 Chiral-V
1-benzyl-2,2-diphenylethylamine................... 10
1,1'-binaphthyl-2,2'-diamine............................. 10
1-(1,1-biphenyl-4-yl)ethanamine..................... 11
1-(1-naphthyl)ethylamine ................................ 11
1-(4-methoxyphenyl)ethylamine.................... 12
1-aminotetralin.................................................... 12
1-(2-methoxyphenyl)ethanamine.................. 13

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1-(4-chlorophenyl)ethylamine......................... 13
6-methoxy-1,2,3,4-tetrahydro-1naphthalenylamine............................................ 13
1,1-diphenyl-1-fluoro-2-aminopropane......... 14
1,1-diphenyl-2-aminopropane......................... 14
1,2,2-triphenylethylamine................................. 14
2-amino-4-methyl-1,1-diphenylpentane
propane................................................................. 14
2-chloro-indan-1-ylamine................................. 15
4-methoxy-α-methylbenzylamine................. 15bis(1-phenylethyl)amine .................................. 15bis(α-methylbenzyl)amine............................... 15
Mexiletine.............................................................. 16
N-benzyl-α-methylbenzylamine.................... 16
N,α-dimethylbenzylamine................................ 16
α-methyl-4-nitrobenzylamine......................... 16
α-methylbenzylamine....................................... 17
3-amino-3-phenylpropanoic acid..................22
Kynurenine............................................................22
Tryptophanamide...............................................23
Methadone........................................................... 24
Proglumide........................................................... 24
Methorphan......................................................... 25
Nefopam............................................................... 25
Tramadol...............................................................26
Hexobarbital.........................................................27
Mepivacaine.........................................................27
Bupivacaine..........................................................28
Mephobarbital.....................................................28
Prilocaine..............................................................28
Phensuximide......................................................30
Fluoxetine.............................................................32
Mianserin..............................................................32
Tranylcypromine.................................................33
Trimipramine........................................................33
Venlafaxine...........................................................33
Acebutolol.............................................................34
Alprenolol..............................................................34
Atenolol..................................................................35
Esmolol..................................................................35
Isoproterenol .......................................................36
Metaproterenol....................................................36
Metoprolol.............................................................37
Pindolol..................................................................37
Propanolol............................................................38
Salbutamol...........................................................38
Sotalol....................................................................39
Terbutaline............................................................39
Carvedilol..............................................................40
Tulobuterol............................................................40
Baclofen................................................................ 41
Octoclothepin...................................................... 41
Tolperisone........................................................... 41

Mandipropamid...................................................45
Bromacil................................................................46
Napropamid.........................................................46
2-amino-1,2-diphenylethanol..........................48
phenylalaninol...................................................... 49trans-1-amino-2-indanol................................... 49
2-amino-1,1,-diphenyl-1-propanol................... 51
2-amino-1,1,13-triphenyl-1-propanol.............. 52
2-(carbobenzyloxyamino)-3-phenyl-1propanol................................................................ 52
cis-1-amino-2-indanol........................................ 52(3a-cis)-3,3a,8,8a-tetrahydro-2Hindeno[1,2]doxazol2-one...................................55
4-(1-H-indol-3-yl-methyl)-2-oxazolidinone....56
Chlophedianol......................................................57
Lofexidine..............................................................58
Bamethan.............................................................60
Diperodon............................................................. 61
Amlodipine............................................................ 62
Brompheniramine.............................................. 62
Carbinoxamine.................................................... 62
Cetirizine................................................................63
Chlorpheniramine...............................................63
Citalopram ...........................................................63
Disopyramide.......................................................63
Ketamine...............................................................64
Methoxyphenamine...........................................64
Methoxyverapamil.............................................64
Nicardipine............................................................64
Orphenadrine.......................................................65
Piperoxan..............................................................65
Promethazine......................................................65
Tetrahydrozoline.................................................65
Thalidomide.........................................................66
Trihexylphenidyl..................................................66
Trimebutine..........................................................66
Verapamil..............................................................66
3,4-methylenedioxyamphetamine (MDA)....68
Methoxamine.......................................................68
Pentedrone...........................................................69
Pseudoephedrine...............................................70
Clenbuterol...........................................................71
Ethylone.................................................................72
Methylphenidate.................................................72
3-fluoromethcathinone..................................... 73
3,4-methylenedioxy-N-ethylamphetamine(MDEA)..................................................................73
4-ethylmethcathinone.......................................73
4-methylethcathinone.......................................73
Aminorex............................................................... 74
Amphetamine...................................................... 74
Butylone ............................................................... 74
Cathinone.............................................................. 74
Flephedrone......................................................... 75

Qクイックリンク:検索

Mephedrone......................................................... 75
Methamphetamine............................................ 75
Methylephedrine................................................. 75
Methylone............................................................. 76
p-methoxyamphetamine................................. 76
Pentylone.............................................................. 76
Synephrine........................................................... 76
α-pyrrolidinopentiophenone............................77

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