EN

E l ectro Syn nthesis
THE FULL POTENTIAL OF ELECTROSYNTHESIS | ElectraSyn 2.0

2 | ElectraSyn 2.0

The perfect workflow/// Electrosynthesis simplified and accelerated with ElectraSyn 2.0
ElectroSyn 2.0 is the smart solution for all oxidation / reduction reactions in the laboratory.
This compact and environmentally-friendly laboratory device is absolutely indispensable where
electrons need to flow, at the interface of electrochemistry and synthetic organic chemistry.
The ElectraSyn 2.0 has been developed in collaboration with Phil S. Baran, the renowned
professor at the Scripps Research Institute in La Jolla, California. It paves the way for massuse of sustainable, environmentally-friendly redox reactions.

Personalized application advice
You can get your own impression of the efficiency andeffectiveness of our ElectraSyn 2.0 electrosynthesis device
in the IKA Application Center. Our experts will show you
the application and will present the packages on offer
together with the extended range of accessories.

Worldwide service
To opt for ElectraSyn 2.0 is also to opt for the excellent
IKA technical service in your region. Our team is available
worldwide for your service and application needs. The
availability of replacement parts is guaranteed for 10 years.

Any questions?
Our service team is at your personal disposal:

00 8000 4524357 (00 8000 IKAHELP)
10 years
warranty**2+8 years after registering at
www.ika.com/register,
wearing parts excludedElectraSyn 2.0 | 3

3 devices in one/// Determine the voltammetry, apply the power, mix the substances
The variable all-in-one system ElectraSyn 2.0 allows you to develop
new electrochemical reactions and transformations on a laboratory
scale. ElectraSyn 2.0 permits sustainable, cost-effective synthesis as
it represents three devices in one:
Analytical device
ElectraSyn 2.0 gives an easy approach of cyclic voltammetry test forsynthetic chemists. The result will help customers understand theelectrochemical properties of the tested sample.
Potentiostat
ElectraSyn 2.0 provides constant voltage and constant current
reaction mode for electrolysis. The novel device also provides assist
mode, an unique reaction mode accessible to electrochemistry
beginners.
Magnetic stirrer
The tried and tested IKA stirring technology also forms part of theElectraSyn 2.0. In just a few seconds, a stirring attachment converts
the electrosynthesis device to a powerful magnetic stirrer for stirring
volumes up to 100 ml.

4

10/// FEATURES/// PACKAGES &TECHNICAL DATA

6/// BENEFITS

12/// ACCESSORIES

8/// POTENTIAL

16/// FAQS

4 | Features

The most important features
ElectraSyn 2.0 offers a wide variety of functions for the development of new electrochemical
reactions and transformations on a laboratory scale. Working with ElectraSyn 2.0 isconvenient and safe for both the experienced user and the novice.

IKA Menu Guide
The user-friendly, intuitive IKA Menu Guide directs the user
through the experiment. A single rotary knob suffices to findyour way easily through the settings.

Cyclic voltammetry (CV)Both analytical measurements and preparatory experiments
can be carried out using one and the same unit.

USB data transfer
USB flash drive exports CV result as CSV file which can be
opened in Excel.

Smart Assist
The Smart Assist mode provides support if the world of electrochemical reactions are uncharted territory for you. It provides ananalysis before execution and continues to provide communication during the reaction.

Alnico magnetic technology
Alnico magnetic technology ensures high levels of magnetic
coupling. This prevents sedimentation during the experiment.

USB port

Features | 5

ElectraSyn 2.0 app
The ElectraSyn 2.0 app allows users to connect their mobile devices (cell phone and tablet) to ElectraSyn 2.0 through WiFi. With
the help of the app, users can monitor their real time reaction
information within an effective range, send CV data and reaction
data through email, view and download further experimentsfrom the IKA Knowledge Base crowdsourcing platform, makeonline orders and watch tutorial videos of ElectraSyn 2.0. The
app is available in the Apple App Store and on Google Play.

Modularity
Apple App Store

Google Play Store

Several accessories are extending the functionality of ElectraSyn
2.0. The Carousel attachment transforms ElectraSyn 2.0 froma single reactor to a six-reactor screening system. It is perfectly
suitable to monitor, optimize, and scale up experiments. The
GOGO Module allows flexible vial placement, such as placing
the reaction vial in a cryo-bath. With Pro-Divide users can trigger
divided cell reactions whereas Pro-Seal vacuum allows the application of vacuum as low as 50 mbar to attain better reaction
system sealing. IKA e-Hive provides a platform for early stage
reaction discovery.

Single vial set up(vial holder)

6-reaction carousel

Stir plate

6 | Benefits

ElectraSyn 2.0 lifts the old tried and tested principleof electrochemistry to a completely new level:
Oxidation / reduction reactions can be carried out
simply, quickly, and safely in a single compact device.

FASTERThe ElectraSyn 2.0 works intelligently
and automatically and thus operates
considerably more quickly than conventional processes.

EASY TO OPERATEA new equipment concept, in combination with the tried and tested IKA
Menu Guide, also makes this complex
equipment simple to handle.

REPRODUCIBLE
The ElectraSyn 2.0 means that electrochemical reactions are finallycarried out in a standardized mannerand are thus reliably reproducible.
This finally facilitates mass productive
use of electrochemistry.

ENVIRONMENTALLY-FRIENDLY
The standard use of electricity tomove the electrons means thatlarge volumes of solvents, andthus chemical waste, can be saved.
This is both environmentally-friendly
and sustainable.

Benefits | 7

SIMPLER
Electrosynthesis with ElectraSyn 2.0 is
simple and tidy. It is no bigger than aconventional magnetic stirrer, and asmall space on the laboratory bench
is adequate for it.

RUGGEDNESSThe ElectraSyn 2.0 user interface isresistant to chemicals. The incorporated
glass is characterized by scratchresistance and extreme ruggedness.
FAST RESPONSE DISPLAY
The display is designed for perfectlegibility: It is large, well-lit andmounted in hardened glass.

IKA Knowledge BaseComprehensive fundamental expertise in electrochemistry,
lots of tips and a crowdsourcing platform are madeavailable by the IKA Knowledge Base for ElectraSyn 2.0.
Participate in the test rigs from other scientists and shareyour own experiences with your colleagues.
Acquire and share knowledge right now at:
www.ika.com/electrasyn

8 | POTENTIAL

Endless potential
ElectraSyn 2.0 brings two sections of chemistry together that so far have had
little to do with each other: electrochemistry and synthetic organic chemistry.
The ElectraSyn 2.0 is thus the perfect complement for a large number of users
between the analysis laboratory and large-scale chemistry. Whether it be processdevelopment, medical chemistry, radiochemistry, agrochemistry or substanceand material research – this miracle device offers enormous potential for simpler,
faster, environmentally-friendly working:[Natural products][Medicinal
chemistry][Analytical chemistry][Radiochemistry]

Mechanistic
studiesSensorDiagnostic

Quantitative
analysis[Agrochemicals]

Microarray
reactions

untapped
potential

POTENTIAL | 9

Electrochemical
applications[Early processdevelopment][Commodity chemicals]
H 2N[New materials][Specialty
chemicals]

Me
HO
Me

Me
OH
Me

NC

N

Al

OH
OH

OH

OH

Chemical space(molecular diversity)

Cl 2
NH 3

CN

NaOH

Scale

10 | Packages

ElectraSyn 2.0 Package

ElectraSyn 2.0 pro Package

Ident. No. 0020008980

Ident. No. 0040003261› ElectraSyn 2.0 base unit
+ vial holder+ single vial, 10 ml, complete+ 2 electrodes (graphite)+ stir plate (aluminum)+ stir bar

Ready-To-Go
package› ElectraSyn 2.0 base unit
+ vial holder+ single vial, 10 ml, complete+ 2 electrodes (graphite)+ stir plate (aluminum)+ stir bar+ set of CV electrodes:+ CV glassy carbon+ CV platinum+ reference electrode Ag | AgCl

Technical data | 11

Technical data
TECHNICAL DATA
Nominal voltage ( input)

48 VCD

Max. current (input)

1,500 mA

Max. input power

40 W

Voltage output

30 / 10 V

Current output

100 mA

EC-Motor rating output

9W

Speed range

50 – 400 – 1,500 rpm

Setting accuracy speed

10 rpmStirring quantity max. per stirring
position (H2O)

100 mlStirring bar length

10 mmOperation elements

Capacitive touch / Turning knob

Speed control

Turning knob

Display

TFT

Analog output

noRS 232 interfacenoUSB interface

yes

IP rating

IP 40

Permissible ambient temperature+5 °C – +40 °C

Permissible relative humidity

80 %Dimensions incl. single-vial Adapter(W × H × D)

130 × 150 × 250 mm

Weight

1.4 kgPOWER SUPPLY
Input

100 – 240 VAC
1.5 A
50 – 60 Hz

Output48 VCD
39,84 W LPS(limited power source)

Protection classII (double insulated)

12 | Accessories

ACCESSORIESCarousel, e-Hive, GOGO Module, Pro-Divide or Calibrationcap – all these attachments and a great variety of different
electrodes pave the way for standardization and reproducibilityof electrochemical experiments in your lab.

Carousel complete
Product

Description

Ident. No.

Carousel

Attachment for multi measurements

0020017512

Carousel complete

Attachment for multi measurements,
incl. glass vials

0040005427

e-HiveScreening platform with a maximum of
24 reactions

0040004945

GOGO Module

Universal extension for ElectraSyn 2.00040006052

Pro-Seal

Vial cap for gas exchange

0040007151

Pro-Divide

Reaction cell for divided electrochemistry

0040006482

Calibration cap

Calibration cap for ElectraSyn 2.00040007388

Copper electrode inner

Anode copper (24 pcs.)

0040007427

Graphite electrode inner

Anode graphite (24 pcs.)

0040007430

Stainless electrode inner

Anode stainless steel (24 pcs.)

0040007429

Copper electrode outer

Cathode copper (24 pcs.)

0040007436

Graphite electrode outer

Cathode graphite (24 pcs.)

0040007438

Stainless electrode outer

Cathode stainless steel (24 pcs.)

0040007443

ATTACHMENTS

GOGO Module

ELECTRODES FOR E-HIVE

e-HiveGraphite electrode
inner

Copper electrodeouterAccessories | 13

Product

Description

Ident. No.

Glass vial complete 5 ml

Glass vial 5 ml incl. lid,
glass and magnetic bar

0040003171

Glass vial complete 10 ml

Glass vial 10 ml incl. lid,
glass and magnetic bar

0040003170

Glass vial complete 20 ml

Glass vial 20 ml incl. lid,
glass and magnetic bar

0040003168

Glass vials 5 ml

Glass vial 5 ml, set of 10

0040003327

Glass vials 10 ml

Glass vial 10 ml, set of 10

0040003325

Glass vials 20 ml

Glass vial 20 ml, set of 10

0040003324

ElectraSyn 2.0
Electrode Starter Kit

Kit of 9 electrodes, set of 12(glassy carbon, set of 2 only)

0020017204

ElectraSyn 2.0
Complete Vial Kit

Kit of 5 ml, 10 ml and 20 ml vials complete,
10 spare vials of each volume0010003810

ElectraSyn 2.0
vials only

Kit of 10 x 5 ml, 10 x 10 ml,
10 x 20 ml vials

0010003811

ElectraSyn 2.0
Complete Starter Kit

Kit of 5 ml, 10 ml, 20 ml vials complete;
10 spare vials of each volume; 9 electrodes,
set of 12 (glassy carbon, set of 2 only)

0040004013

Electrode
CV Package

Kit of electrodes (CV glassy carbon,
CV platinum, reference electrode)

0040002864

VIALS / ELECTRODESGlass vial 5 ml

Glass vial
complete 10 ml

ElectraSyn 2.0 Complete Starter Kit

MICROVIALS / MICROELECTRODES

Microvial 1 ml

ElectraSyn 2.0 Micro Starter Kit complete

Microvial 1 ml

Glass vial 1 ml incl. lid, glass and magnetic bar

0040003294

Microvial 2 ml

Glass vial 2 ml incl. lid, glass and magnetic bar

0040003295

Micro glass vials 1 ml

Glass vial 1 ml, set of 100020017207

Micro glass vials 2 ml

Glass vial 2 ml, set of 100020017206

ElectraSyn 2.0
Micro electrode Starter Kit

Kit of 8 electrodes, set of 12(glassy carbon, set of 2 only)

0040004016

ElectraSyn 2.0
microvials only

Kit 10 x 1 ml, 10 x 2 ml vials

0040004103

ElectraSyn 2.0
Microvial Kit
complete

Kit of 1 ml and 2 ml vials complete,
10 spare vials of each volume0040004014

ElectraSyn 2.0
Micro S­ tarter Kit complete

Kit of 1 ml and 2 ml vials complete;
10 spare vials of each volume;
8 electrodes, set of 12(glassy carbon, set of 2 only)

0040004015

14 | Accessories

Product

Ident. No.

ELECTRODES

1

2

3

1

Electrode graphite (12 pcs.)

0040002858

2

Electrode glassy carbon (2 pcs.)

0040002842

Electrode lead bronze (2 pcs.)

0020016076

Electrode lead (12 pcs.)

0040002843

Electrode tungsten (2 pcs.)

0040002845

3

Electrode niobium (2 pcs.)

0040002846

4Electrode copper (12 pcs.)

0040002847

Electrode magnesium (12 pcs.)

0040002848

Electrode titanium (12 pcs.)

0040002849

Electrode zinc (12 pcs.)

0040002850

Electrode stainless steel (12 pcs.)

0040002851

Electrode platinum plated (2 pcs.)

0040002852

Electrode platinum foil (2 pcs.)

0040005015

Electrode platinum on ceramics (2 pcs.)

0040006753

Electrode gold plated (2 pcs.)

0040002853

Electrode silver plated (2 pcs.)

0040002854

Electrode aluminum (12 pcs.)

0040003174

Electrode boron doped diamond (2 pcs.)

0040002856

Electrode tin (12 pcs.)

0040002857

7

Electrode nickel (12 pcs.)

0040002859

8

Electrode RVC foam (12 pcs.)

0040002860

Electrode nickel foam (12 pcs.)

0040002861

Electrode cobalt (2 pcs.)

0040003385

Electrode reference (1 pc.)

0040002865

Electrode CV glassy carbon (1 pc.)

0040002863

5

4

5

6

6

7

8

9

9

Accessories | 15

Product

Ident. No.

MICROELECTRODES
Microelectrode aluminum (12 pcs.)

0040004029

Microelectrode boron-doped diamond (2 pcs.)

0040004036

2

Microelectrode cobalt (2 pcs.)

0040004039

3

Microelectrode copper (12 pcs.)

0040004027

4

Microelectrode glassy carbon (2 pcs.)

0040004022

5

Microelectrode gold (2 pcs.)

0040004034

Microelectrode graphite SK-50 (12 pcs.)

0040004021

Microelectrode lead (12 pcs.)

0040004028

Microelectrode lead bronze (12 pcs.)

0040004030

Microelectrode magnesium (12 pcs.)

0040004025

Microelectrode nickel (12 pcs.)

0040004023

7

Microelectrode nickel foam (12 pcs.)

0040004101

8

Microelectrode niobium (2 pcs.)

0040004032

Microelectrode platinum (2 pcs.)

0040004038

Microelectrode silver (2 pcs.)

0040004035

Microelectrode stainless steel (12 pcs.)

0040004024

Microelectrode tin (12 pcs.)

0040004037

Microelectrode titanium (12 pcs.)

0040004033

Microelectrode tungsten (2 pcs.)

0040004031

Microelectrode zinc (12 pcs.)

0040004026

Microelectrode graphite V2100 (2 pcs.)

0040004040

1

1

2

3

6

4

5

6

9

7

8

9

16 | Screening System

Screening System Package(8 cells)

Screening System Package(6 cells)

Ident. No. 0040003642

Ident. No. 0040003631

Screening System

TECHNICAL DATAThe Screening System is perfectly suited for constant current
electrosynthesis in “multibatch” mode. The combination ofboth divided and undivided batch cells enables you to quickly
carry out research on multiple electroconversions at the sametime. In addition, you can combine the system with otherequipment in the laboratory.

SCREENING SYSTEMPACKAGE (6 | 8 CELLS)CONTINUOUSLY ADJUSTABLE POWER SUPPLY
Voltage output

0 – 32 V (± 1 mV)

Supply voltage

115 or 230 V(50 Hz / 60 Hz)

MAGNETIC STIRRER
Speed range

0 – 1500 rpm

REACTION CELLS

Scope of delivery> Reaction block> Electrolysis cells> Power supply>	IKA Plate (RCT digital) including
PT 1000 temperature sensor> Cable set> Screw drive>	Electrode graphite (16 pcs.)

Number of cells

6 or 8Usable volume of undivided cell

8 ml

Usable volume of divided cell(per chamber)

8 ml

Material

PTFE

Divided cells

Yes (reaction block with
6 cells)

Temperature control

Yes (RT to 100 °C)

Scale Up | 17

Scale up with ElectraSyn flow
ElectraSyn flow basic is a system for continuous flow electrosynthesis. The heart of this system is the electrosynthesis flow
cell – in short, ElectraSyn flow. It consists of two half cells, eachequipped with an electrode. By combining similar and dissimilar
half cells / electrodes, ElectraSyn flow provides maximum flexibility for research in the field of electrosynthesis. It also enables
the laboratory scale production of a variety of products using
electrosynthesis.

6ElectraSyn flow basic
Ident No.: 0020014266
1

ElectraSyn flow eco
Ident No.: 0020014267

4

5

Scope of delivery
1
2
3
4
5
6

Nine half cells with accessories
One nafion-membrane for cell splitting
R 104 stand with cell holder and H 44 boss head clamp
Power supply adapter with cords
Peristaltic pump with tubing
Practical carrying / storage case for small components

3

2

CONTINUOUSLY ADJUSTABLE POWER SUPPLY
Voltage0 – 35 V (± 6 mV)Current

0 – 1 A (± 50 μA)

Mains voltage

100, 115 or 230 V(50 Hz / 60Hz)

PERISTALTIC PUMP
Flow rate per tube

0.01 – 0.61 ml / min

Overall flow rate

0.02 – 1.22 ml / min

Inner tubing diameter

0.25 mm

Mains voltage

100 – 230 V(50 Hz / 60 Hz)

18 | FAQ

FAQ
Why electrochemistry?
Electrochemistry can trigger reactivity that will be inaccessible
otherwise; electrochemistry is sustainable and environmental
friendly by allowing less expensive and less toxic reagents;
electrochemistry contributes to safety by avoiding dangerous
operating procedures.

Why ElectraSyn 2.0?
ElectraSyn 2.0 is a three-in-one device with a featured Smart
Assist mode for beginners. Compared to traditional equipment
setup, ElectraSyn 2.0 is cheaper and takes up smaller space –the device is as big as a stir plate. Experiments on ElectraSyn 2.0
are very simple, in comparison with traditional setup which
requires time consuming connections and wirings. ElectraSyn 2.0
also provides standardized reaction vials and electrode dimension, which guarantees reaction reproducibility. In general,
ElectraSyn 2.0 offers great accessibility for both experienced
users and beginners.

Which is the right electrode for me?
For undivided cell, if the desired reaction is oxidation, use the
combination of non-sacrificial anode and cathode on whose
surface it is easier to observe hydrogen revolution than organic
compound reduction; if the desired reaction is reduction, use the
combination of sacrificial anode and cathode on whose surface it
is easier to observe organic compound reduction than hydrogen
revolution.

The Beginnings: Apparatus for electrolysis with stirring
standmotors and regulating starters for the rotating
electrodes (electrochemical method)

Basics | 19

BasicsElectrochemistry deals with both chemical transformations
that generate electricity, and chemical transformations thatare induced by electricity. In the span of two hundred years, itevolved from a few obscure and eccentric laboratory phenomena
into a highly sophisticated and comprehensive scientificdiscipline, with applications that permeate all corners of society.
Today, batteries of all sizes – from the delicate hand watch tothe powerful Tesla automobile – stem from electrochemistry.
Corrosion prevention of metal objects, from a tiny galvanizednail to thousands of miles of underground gas pipelines, isbased on fundamental principles of electrochemistry. Powerful
sensors such as the glucose meter used by tens of millions
everyday are developed from the basic understanding of thecorrelation between glucose oxidation and the magnitude of its
corresponding electrical signal. Scores of commodity chemicals,
including aluminum and PVC, are manufactured at an industrial
scale every year using electrochemical processes. Beyond
practical applications, electrochemistry plays a pivotal role in the
search for new materials, more sustainable energy sources, andnovel strategies for environment cleanup

Divided vs. Undivided Cells
In an undivided electrochemical cell, the cathode and anodeare housed in the same chamber. This setup is easy to carry out,
as no elaborate glassware / reactor is needed. In addition, thedistance between the two electrodes can be easily adjusted,
and ionic species can move freely between the electrodes. An
example of an electrochemical reaction in a simple undivided
cell is water electrolysis in a regular cup with two pencil leads
as electrodes. This is something that can be done outside
the confines of a laboratory environment. IKA’s supply ofstandardized vials, electrodes, and their easy assembly makes it
extremely convenient for a chemist to quickly evaluate effect ofdifferent electrodes on a specific reaction.
In a divided electrochemical cell, the cathode and anode are kept
in different chambers, separated by an ion-permeable membraneor salt bridge. This, of course, requires that special membrane orsalt bridge and a reaction vessel of complicated design. Anotherconsideration when using a divided cell is that the resistanceis typically high due to the separation of electrodes, which
may lead to a slower reaction. However, a divided cell allows
the possibility of maintaining different chemical environments
around the two electrodes, thereby bringing out fine-tuned
reactivity inaccessible via an undivided cell. In the case of waterelectrolysis, the divided cell furnishes hydrogen and oxygen gasesin the cathode and anode chambers, respectively. This makes it
possible to deliver hydrogen and oxygen as pure products in thedivided cell, as opposed to a mixture of hydrogen and oxygen in
an undivided cell.

Constant Current vs. Constant Voltage
An electrochemical reaction can be executed at a constant cell
current (galvanostatic) or a constant voltage (potentiostatic).
In a constant current reaction, it is easy to calculate the total
charge consumption. The disadvantage of the constant current
reaction is that the voltage profile of the reaction is often
overlooked. The potential that the reaction starts at and the way
it changes throughout the course of the reaction are factors
critical to the outcome of the reaction. As the redox active
species deplete in the course of a constant current reaction, thepotential increases. If unattended, this can lead to undesired
redox processes and become detrimental to the reaction. If
the reaction is executed with the total amount of charge (e.g.,
2 Faradays per mole), it is possible for the potential profile tostay within an acceptable range in the course of the reaction.
However, if a reaction is run continuously (e.g., for 16 hours), it isespecially important in this case to pay attention to the potential
and make sure it stays within an acceptable range.
In a constant voltage reaction, the reaction is typically executedwith a constant cell voltage which is set by the redox potentialof the intended transformation. If there is no prior knowledge
about the redox system, cyclic voltammetry studies are often
required to set a potential value for the reaction. Constantvoltage reactions are less prone to runaway side reactions. The
magnitude of the current flow depends on the overall resistanceof an electrochemical cell – a high resistance cell will lead tolow current and a slow reaction. Ensuring the current and thereaction rate stay within an acceptable range becomes a point ofinterest for constant voltage reactions.
Overall, the potential range of a constant current reaction must
be carefully monitored and controlled to avoid unintended redox
processes that may be detrimental to the reaction. Similarly, thecurrent of a constant voltage reaction must remain at a sufficientlevel to achieve an acceptable rate of reaction. In both cases,
the cell resistance can be adjusted, via electrolyte concentration,
solvent, cell configuration, electrode surface area, etc., to achieve
the control of voltage or current respectively.
Find more information on: www.ika.com/electrasyn

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Subject to technical changes
Information regarding delivery is not binding.

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202010_ElectraSyn 2.0_Brochure_IWS_EN/// WORLDWIDE