TEST REPORT
Erlr:r:Irr
nr:r:rrucr
Technical Report(ó817)268-0r38

October 19,2017

Date Received

September 24, 2017

. .Jagg I 9f leFactory Company Name:
Factory Address:
Project No.:
Client Reference No.:
Sample Type:i
I

I

Sample Pick Up Date:
Wastewater Discharge to:
On-Site Effluent Treatment Plant (ETP):
Discharge Type:
Test Period:

Factory l; BANLADESH
Dhaka Region, BANGLADESHI00l) Incoming water - Grab
1002) Raw Wastewater - 6 hours Time - weighted Composite1003) Discharged Wastewater - 6 hours Time - weighted Composite
September 24, 2017
Factory Owned ETP
Yes
Direct Discharge
September 25,2017 To October 19,2017

Sample Description:I00l) Incoming water
1002) Raw Wastewater
1003) Discharged Wastewater

REMARK
Ifthere are questions or concems on this report, please contact the following persons:General enquiry

Mr. Abu Hanif, Mail: abu.hanif@bd.bureauveritas.com

Invoicing

Mr. Mahabubur Rahman, Mail: mahabubur.rahman@bd.bureauveritas.com

Technical enquiry-Chemical

Mr. M. Nur Alam, Mail: nur.alam@bd.bureauveritas.com

This report shown the test result of the auxiliary chemical and/or raw material samples, which collected during particular factory
audit. The results of this report shall not be used for any regulatory compliance purposes.

* The sampling is agreed with client.

BUREAU VERITAS

coNsuMER PRODUCTS SERVTCES ( BANGLADESH ) LTD.

M.NIJRALAMSENIORMANAGER
ANALYTICAL LABORATORY

Prepared By:

Md. Mizan

Bure¿u Veritls

Consumer Products Sen ices (BD) Ltd,
Plot # ll0. DÍIPZ lrxtensio]r Area
Ganakbari. Savar. Dhaka. Bangladesh
Tel: 88-02-7701464-6. Fax: 88-02-7701463

Erlail: bvcps.bd(riTbd.Sureauveritas.cout
rvebsite: cps.burcauveri:as.corn
Thc conlcnt ofthis PDF filc is in accordance with lhe original issued repons for referetce only.
This Test Repoñ cannol be reproduced, excepl in full, wilhoul prior wrillen pemission ofthe company.

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Gl!trrln@reTechnical Report:(6817)268-0138
Octobsr I 9, 20 I 7
Page2 of 19

Photo of the Sample/ Samnlins LocationI00l) Incoming water

1002) Raw Wastewater

1003) Discharged WastewaterThc conlent ofthis PDF file is in accordancc with lhc original issued rcpofls for refercûce only.
This Test Repol cannot bc reproduced, except in full, w¡lhoüt priorwitten pemission ofthe company.

@Technical Report:(6817)268-0138
October 19,2017
Page 3 of 19

Executive Summarv
1A) Conventional Parameters

I001

I002

N/A

N/A

a

a

a

r003

Temperature
TSS

COD

Total-N
pH Value
Color [rnr] (436nm; 525nm; 620nm)
BOD5

Ammonium-N
Total-P

See result in page

05-08

AOX
Oil and Grease
PhenolColiform
Foam

ANIONS - Sulfide
ANIONS - Sulfite
I B) Conventional Parameters-METALSZDHC MRSL Substânces

r001

r002

I003

2A) APs and APEOs

NT

o

o

28) Chlorobenzenes and Chlorotoluenes

NT

o

o

2C) Chlorophenols

NT

o

o
o

2D) Azo Dyes

NTo2E) Carcinogenic Dyes

NT

o

o

2F) Disperse Dyes

NT

o

o

2G) Flame Retardants

NT

o

o

2H) Glycols

NT

o

o

2l) Halogenated Solvents

NT

o

o

2J) Organotin Compounds

o

a

o

2K) Perfluorinated and Polyfluorinated Chemicals

NT

o

o

2L) Phthalates

NT

o

o

2M) Poly Aromatic Hydrocarbons

NTo2N) Volatile Organic Compounds

NT

o

o

Note / Key. - Detectedo - Not Detected

NT - Not Tested

Thc @ntcnt ofthis PDF filc is in accordânce with thc original issucd repofs for refcrencc only.
This Test Rcpol cannot be reprcduccd, cxcept in full, withoul prior wittm pemission ofthe companl

Technical Report:(6817)268-0138
October 19,2017
Page 4 of 19

Obiective
The environment samples were tested for below parameters.
IA) Conventional ParameterslB) Conventional Parameters - METALS

2A) APs and APEOs
2B) Chlorobenzenes and Chlorotoluenes
2C) Chlorophenols
2D) Azo Dyes
2E) Carcinogenic Dyes
2F) Disperse Dyes

2G) Flame Retardants
2H) Glycols2l) Halogenated Solvents
2J) Organotin Compounds
2K) Perfluorinated and Polyfl uorinated Chemicals
2L) Phthalates
2M) Poly Aromatic Hydrocarbons
2N) Volatile Organic Compounds

Samplins Plan
Basically, three environment samples were sampled per factory including l) Incoming waler;2) Raw Wastewater and 3)
will be depended on the actual factory facilities andmanufacturing processes.

Discharged Wastewater. Total number of sample collected

Method of sampling used is time-weighted composite samples (agreed with client.). Composite sampling shall be performed
for no less than six hours, with no more than one hour between discrete samples. Each discrete sample shall be of equalvolume. Wastewater and freshwater samples should, as much as possible, be collected simultaneously, during the time that
PU is in normal operation. The sampling shall aim to analyse the snapshot ofwater quality characteristics ofthe operating
PU. Under no circumstance shall samples be taken during times when the production process is not running or thewastewater ìs diluted due to heavy rainfall, etc.

RemarkSampling procedure is with reference to below standards:l) South Australia EPA Guidelines (June 2007), Regulatory Monitoring and Testing Water and Wastewater
Sampling.
2) Australia EPA (Victoria) Guideline (June 2009), Sampling and Analysis of Waters, Wastewaters, Soils
and Wastes.

3) ISO 5667-3:2003, Water Quality - Sampling - Part 3: Guidance on the Preservation and Handling of
Water Samples.
4) ASTM D3976-92 (Reapproved 2010), Standard Practice for Preparation of Sediment Samples for
Chemical Analysis.
Field data records are attached in Appendix B.

The conlenl oflhis PDF fìle is in accordance wilh the original issued reporu for refcrence only.
This Tcsl Repol cannot be repmduced, except id full, wilhout priorMilto pemission ofthe comp¡ny.

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Technical Report:(6817)268-0r38
October 19,2017
Page 5 of 19

Test Result1A) Convention¡l Parameters
TemDerature

Test Method:

Measurement by thermometer

Tested ltemfs)

ResultUn¡tConclusion

I003

36.1 (Exceed Foundational Limit)

dee. C

DATA

Note:deg. C: degree Celsius ("C)

Foundational Limit: A 15 / max. 35"C; Progressive Limit: Â l0 / max. 30"C; Aspirational Limit: A5 I max.25"C

Total Susoended Solids (TSS)
Test Method:

Reference to APHA 22"d Edition-2540D & ALPA 2540D

Tested ltemls)

Result

Unit

Conclusionr003

22 (Foundational)

me/L

DATA

Note:
mg/L = milligram per liter
Foundational Limit: 50 mg/L; Progressive Limit: 15 mgll; Aspirational Limit: 5 mg/L

Chemical Oxygen Demand (COD)

TestMethod:

Referenceto ALPA5220B &EPA410.3

Tested ltem(s)Result

Unit

Conclusion

I003

60 (Progressive)

ms/L

DATA

Note:

mg/L: milligram per liter
Foundational Limit: 150 mg/L; Progressive Limit: 80 mg/L; Aspirational Limit: 40 mg/L

Total Nitroeen (Total-N)
Test Method:

Reference to APHA 22"d Edition2012,4500 N Org.B

Tested Item(s)Result

Unit

Conclusion

r003

6.7 (Progressive)

ms/L

DATA

Note:

mg/L: milligram per liter

BLq = g"¡o* Limit of Quantification LOQ: Limit of Quanti{ication
Foundational Limit:20 mg/L; Progressive Limit: l0 m{L; Aspirational Limit: 5 mg/L

The contcnt oflhis PDF file is in accordancc with thc original issucd rcporu for refcrence only.
This Test Rcpon cånnot bc reproduced, cxcept in full, withoul prior Mitten pcmission ofthe company.

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Technical Report:(6817)268-0138
October 19,2017
Page 6 of l9

pH Value:

Test Method

Reference to ALPA 4500-H+B & EPAI50.2

Unit

Result

Test ltem(s)r003Parameter
Temp. of sample

24des. CpH value ofsample

7.9

DATA

Conclusion
Note:deg. C = degree Celsius ('C)

Temp. = Temperature

Limit:6 - 9
Color [m-1] (436nm: 525nm: 620nm)
Test Method:

Tested ltemls)
I003

ISO 7887: 201l(E), B

Parameter
Trial (1,--436 nm)
Trial ()':525 nm)

pHResult

Unit

Conclusion

7.7

m-t

DATA

7.7

0.3 (Aspirational)
0.1 (Aspirational)m

Trial (),=620 nm)

7.7

0.1 (Aspirational)

m-l

DATA
DATA

Note:
Foundational Limit:7;5;3 m-r; Progressive Lirit:5;3;2 m-r; Aspirational Limit:2;l;l m-r

Biochemical Oxygen Demand (BODùTest Method:

Reference to APHA 22"d Edition-52108& ALPA 52108

Tested ltem(s)Result

Unit

Conclusion

I003

I 8 (Foundational)

ms/L

DATA

Note:

mg/L: milligram per liter
Foundational Limit: 30 mg/L; Progressive Limit: l5 mg/L; Aspirational Limit: 5 mgll.

Ammonia Nitrosen
Test Method

Reference to APHA 22'd Edition 2012,4500 NHr B.C

Tested ltem(s)Result

Unit

Conclusionr003

1.9 (Foundational)

ms/L

DATA

Note:

mg/L: milligram per liter
BLQ = g.¡o* Limit of Quantification LOQ: Limit of Quantification

Foundational Limit: l0 mg/L; Progressive Limit: I mg/L; Aspirational Limit: 0.5 mg/L

The contcni ofthis PDF file is in åccordance with the original issued repols for reference only.

ThisTesl Repon canrol be reprcduced, exccpt in full, withoul pr¡orwrilteil p€mission ofllìe compaûy.

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Technical Report:(68rÐ268-0138
October 19,2017
Page 7 of 19

Total Phosohorus lTotal-P)
Test Method:

Reference to APHA 22'd Edition -4500-P.E (2012)

Tested ltem(s)Result

Unit

Conclusion

I003

0.8239 (Foundational)

rng/L

DATA

Note:
mg/L = milligram per liter
Foundational Limit: 3 mg/L; Progressive Limit: 0.5 mg/L; Aspirational Limit: 0.1 mgll

Adsorbable Orsanic Halosen (AOX)
Test Method:

Reference to HJÆ 83

Tested ltem(s)Result

Unit

Conclusion

I003

0.600 (Progressive)

rîs/L

DATA

Nots:
mg/L = milligram per liter
Foundational Limit: 5 mg/L; Progressive Limit: I mg/L; Aspirational Limit: 0.1 mg/L

Oil and Grease
Test Method

Reference to APHA 22nd Edition -5520 B (2012)

Tested ltem(s)Result

Unit

Conclusionr003

9 (Foundational)

ms/L

DATA

Note:

mg/L: milligram per liter
Foundational Limit: l0 mg/L; Progressive Liñf:2mglL; Aspirational Limit:0.5 mg/L
PhenolTest Method

Reference to APHA 22"d Edifion2}l2, USEPA 420.1

Tested ltem(s)Result

I003

BLQ (LOQ. 0.0 ) (Progressive)
1

Unit
mglL

Conclusion

DATA

Note:

mgll- = milligram per liter
BLQ: Below Limit of Quantification LOQ: Limit of Quantification
Foundational Limit: 0.5 mg/L; Progressive Limit: 0.01 mg/L; Aspirational Limit; 0.001 mg/L

Thc contcnt oflhis PDF file ¡s in accordancc with lhc original issued ¡epons for refeence only.
This Tcst Repoñ cannol be reproduced, except in full, w¡lhout priorMiûcn pemission ollhe company.

@l!ÛI!Í:]tTm¡ñTechnical Report:(6817)268-0r38
October 19,2017
Page 8 of 19

Coliform
Test Method

Reference to APHA 22"d Edition 2012,9215 B

Tested ltem(s)ResultI003

32 (Progressive)

Unit
MPN/
100 mL

Conclusion

DATA

Note:
bacteria/lO0 mL: bacteria per 100 milliliters
Foundational Limit:400 / 100 ml; Progressive Limit: 100 / 100 ml; Aspirational Limit: 25 / 100 ml;

Foam

Test Method:

VisualTested ltem(s)Resultr003

No Foam

Unit

Conclusion

DATA

ANIONS - Sulfide
Test Method
Tested ltemfs)
I003

Reference to APHA22"d Edition 2012, lSl 3025 Part 29

ResultBLQ GOQ 1.0) (Exceed Foundational Limit)

Unit

Conclusion

mdL

DATA

Note:
mg/L = milligram per liter
BLQ: Below Limit of Quantification LOQ = ¡¡.¡t otQuantification
Foundational Limit: 0.5 mg/L; Progressive Limit: 0.05 mg/L; Aspirational Limit: 0.01 mg/L

ANIONS - Sulfite
Test Method
Tested ltemls)
I003

Reference to APHA 22nd Edition 2012,4500 SOj B

ResultBLQ GOQ 1.0) (Foundational)

Unit

Conclusion

ms/L

DATA

Note:
mg/L = milligram per liter
BLQ: Below Limit of Quantification LOQ = ¡¡-¡, otOuantification
Foundational Limit: 2 m{L; Progressive Limit: 0.5 m{L; Aspirational Limit: 0.2 m{LThe conlcnt oflhis PDF file is in accordancc w¡th the or¡ginal issued repons for reference

otly.

This Tesl Rcpon c¡nnot be ¡eproduced, excepl ¡n full, wilhout priorw¡lld pemission oflhe company.

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Technical Report:(6817)268-0138
October 19,2017
Page 9 of 1918) Conventional Parameters - METALSHeaw Metals
Antimony( Sb )Foundational Límit: 100 pg/L;
Progressive Limit: 50 pg/L;
Asoirational Limit: l0 us/L
Chromium( Cr ), total
Foundational Limit: 200 pg/L;
Progressive Limit: 100 pg/L;
Aspirational Limìt: 50 us/L
Cobalt( Co )Foundational Limit : 50 pg/L;
Progressive Limit: 20 pg/L;

l00l tus/L)

1002 tus/L)

1003 (us/L)

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

ND

t2

3

(Aspirationat)(Aspirational)(Aspirational)

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

Aspirational Limit: l0 uç/L
Copper( Cu )Foundalional Limit. 1000 pg/L;
Progressive Limit: 500 pg/L;
Aspirational Límit: 250 as/L

ND

38

35

(Aspirational)(Aspirational)(Aspirational)

Nickel (Ni)Foundat ional Limit :. 2 00 p g/L,
Progressive Limit: 100 pg/L;

Asoirational Límit: 50 us/L
Silver (Ag)Foundational Limit: 100 pg/L;
Progressíve Límit: 50 pg/L;Aspìrational Limit: 5 up/L

ND

l0

ll

(Aspirational)(Aspirational)(Aspirational)

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

Zinc(Zn)
Foundational Limit: 5000 pg/L;
Progressive Limit: 1000 pg/L:
Aspirational Limit: 500 us/L
Arsenic (As)Foundational Limil: 50 pg/L;
Progressive Limit: l0 pg/L;
Aspirational Limit: 5 us/L
Cadmium( Cd )Foundational Limit: 100 pg/L;
Progressive Limit: 50 pg/L;

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

Asoirational Limit: I0 us/L
Lead( Pb )Foundational Limit ; 1 00 p g/L,

ND

ND

ND

Progressive Limit: 50 pg/L;(Aspirational)(Aspirational)(Aspirational)

Asoirational Limit: l0 us/L
Mercury (Hg)
Foundational Limit: 10 pg/L;

ND

ND

ND

Progressive Limit: 5 pg/L;(Aspirational)(Aspirational)(Aspirationat)

Asoirational Limit : I us/L
Chromium VI( CrVI )Foundalional Limít: 50 pg/L;
Progressive Limit: 5 pg/L;

Aspirational Limit: I up/L
Cyanide( CN-)
Foundational Limit: 200 pg/L;
Progressive

Limit: 100 pg/L;

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

306

I 150

708

Aspirational Limit: 50 up/L
Manganese (Mn)

The conlcnt oflhis PDF lile is in accordancc wilh the original issued repods for referenc€ odly.
This Tel Repol cånnot be reproduccd, exc€pt ¡n fu¡|, wilhout priorwillcn pemission oflhe company.

@G¡IEETI@¡E

Technical Report:(6817)268-0138
October 19,2017
Page l0 of I 92J) Oreanotin Compounds

Organotin Comoounds
Monobutvltin (MBT)
Dibutylrin (DBT)
Tributyltin TBT)i

Tricyclohexyltin (TCyT)
Trioctyltin (TOT)
Monooctvltin IMOT)
Diphenyltin (DPhT)
Tetrabutyltin (TeBT)
vativesMono-, di- and tri-Dhenvltin derivatives
Mono-, di- and tri-octyltin derivatives

lOOl tus/L)

1002 tus/L)

1003 (us/L)

ND

0.'76

ND
ND
ND

ND
ND
ND

ND

Nt)

ND

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

ND
ND
ND
ND
ND
ND
ND
ND
ND

ND
ND
ND
ND

ND
ND
ND
ND
ND

Nf)
ND
ND
ND
ND
ND

Others Priorit]¡ Chemical Grouos

l00l (w/L)

lO{ì2 hø/L)

1003 (as/L)

NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT
NT

ND
ND
ND

ND
ND

ND

ND

2A) APs and APEOs
2B I Chlorobenzenes and Chlorotoluenes

2C ) Chlorophenols

Azo2E) Carcinogenic Dves
2F) Disperse Dyes
2C lFlame Retardants
2H) Glycols2l) Haloeenated Solvents
2K) Perfl uorinated and Polyfluorinated Chemicals

2L t Phthalates
Volatile

ND
ND
ND
ND
ND
ND
ND
ND
ND

ND
ND

ND
ND
ND
ND

ND
ND
ND
ND

Remark ¡Test method, repofing limit and list of chemical are summarized in tables of Appendix A.
ND = Not detected (Please refer to reporting limit shown in Appendix A.).

All results are in ppb as unit.

ppm: part(s) per million; ppb : part(s) per billion.
NT:Not Tested.

The conletrt oflhis PDF filc is in accordânce with the or¡g¡nal issued repots for refcrcncc only.
This T6l Repol caûnol bc reproduccd, cxccpt in full, wilhoul prior witts pemissior ofthc company.

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Technical Report:(6817)268-0138
October 19,2017
Page I I of 19

APPENDIX A
Parameters, limits and testing method aligned with the ZDHC Wastewater Guidelines(ìroupSLrbslance (analvtcs)(.AS \O

Octylphenol OP, mixed

Various (incl. 140-66-9,
1806-26-4, 27 r93 -28-8)

isomers

24. Alkylphenol (AP)and Alkylphenol
Ethoxylates (APEOs):
including all isomers

Nonylphenol NP[)ctectron Linlitt.)Testinq nìcfhùd

NP/OP: ISO 18857-2(modifieddichloromethane
exhaction) or ASTM
D7065 (GC/MS or

Various (incl. 104-40-5,
1 106649 -2, 25 154-52-3,
84852-15-3)

LCIMS(-MS)
5

Nonylphenol Ethoxylates
oPEO (2-16)

OPEO/NPEO (n>2):
rso 18254-l
OPEO/NPEO:

Various (incl. 9002-93-1,
9036-l 9-s, 68987-90-6)

ISOl8857-2 or ASTM
Nonylphenol Ethoxylates
NPEO (2-r8)
Chlorobenzene
1.2-Dichlorobenzene
1.3-Dichlorobenzene
1.4-Dichlorobenzene
1,2,3 -Trichlorobenzene

28. Chlorobenzenes
and Chlorotoluenes

2C. Chlorophenols

26027 -38-3, 37205-87 -t,

684t2-54-4, 127087 -87 -0)
t

08-90-7

95-50-1

541-73-l
to6-46-7
87-61-6

1.2-4-Trichlorobenzene

t20-82-l

1.3.5 -Trichlorobenzene

108-70-3

1.2.3.4-Tetrachlorobenzene
1.2.3.5 -Tetraclorobenzene
1.2.4,5 -Tetrachlorobenzene
Pentachlorobenzene
Hexachlorobenzene

634-66-2
634-90-2
95-94-3
608-93-5

2-Chlorotoluene
3-Chlorotoluene
4-Chlorotoluene
2.3-Dichlorotoluene
2"4-Dichlorotoluene
2,5-Dichlorotoluene
2,6-Dichlorotoluene
3.4-Dichlorotoluene
2.3.6-Trichlorotoluene
2.4.5-Trichlorotoluene
Aloha.2.4-Trichlorotoluene
Aloha.2.6-Trichlorotoluene
Alnha.3-4-Trichlorotol uene
Alpha, atpha,2,6tetrachlorotoluene
Alpha, alpha, alpha, 2-,6tetrachlorotoluene
Alpha, alpha,alpha,4tetrachlorotoluene

95-49-8

Pentachlorotoluene
Pentachloroþhenol (PCP)

2.3.4.5-Tetrachloronhenol
2.3.4.6-Tetrachloroohenol
2.3.5.6-Tetrachloroohenol
2,4,6-Trichloroohenol

D7065(LC,MS; GC/MSor LC/MSMS for n=1,2)

Various (inc. 9016-45-9,

I l8-74-t

108-41-8

106-43-4
32768-s4-0
95-73-8

0.2

GCA{S

19398-61-9
1

USEPA 82608,8270D.
Dichloromethane
extraction followed by

l8-ó9-4

9s-75-0207746-5
6639-30-l
94-99-5
2014-83-7

102-47-6
81-19-6
2136-89-2
5216-25-1

877-n-2
87-86-5
4901-51-3

s8-90-2
935-95-5
88-06-2

0.5

USEPA 8270 D
Solvent extraction,
derivatisation with
KOH, acetic anhydridefollowed by GC/MS

The content oflhis PDF fiìe is in accordancewilh lhe original issued repols for rcfcrence only.

ThisTest Repon cannot be reprcduced, exccpt in fùll, wilhout priorwillen pemission ofthc compåny.

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@Technical Report:(6817)268-0138
October 19,2017
Page 12 of 19(ìrou¡r

2D. Dyes - Azo(Forming Restricted
Amines)SLtbst¿nee (analvlcs)(. AS \O2.3.5-Trichloronhenol
2.4.5-Trichloroohenol
3.4.5-Trichloroohenol
2,3.4-Trichloroohenol
2.3.6-Trichloroohenol
2.3-Dichloroohenol
3,4-Dichlorophenol
2,4-Dichloroohenol
2.5-Dichloronhenol
2.6-Dichloroohenol
3.5-Dichloronhenol
2-Chlorophenol
3-Chloronhenol
4-Chloroohenol
4-Aminodiohenvl
Benzidine
4-Chloro-o+oluidine
2-Naohthvlamineo-Aminoazotoluene
5-nitro-o-toluidine
4-Chloroaniline
4-Methoxy-mphenylenediamine
4.4' -methvlenedianiline
3.3' -Dichlorobenzidine
3.3' -Dimethoxvbenzidine
3.3' -Dimethylbenzidine
4,4' -Methylene-di-o-toluidine
6-methoxy-m-toluidine (pCresidine)
4,4' -Methylene-bis-(2-chloroaniline)
4,4'-Oxydianiline

933-78-8

2E. DyesCarcionogenic or

Equivalent Concem

ISO 14154:2005

609-19-8
15950-66-0

973-75-5
576-24-9
95-77-2

t20-83-2
s83-78-8
87-65-0591-35-5
95-57-8
108-43-0
106-48-9

92-67-l
92-87-5
95-69-2
9 I -59-8

97-s6-3
99-55-8

106-47-8
615-05-4
10t-77 -9

9t-94-t
t19-90-4
rt9-93-7
838-88-0

EN 14362-l
EN 14362-3
0.1

120-'11-8

Reduction step with
Sodiumdithionite,solvent extraction,
GC/lvfS or LCIMS

10 I - l4-4

101-80-4
I 39-65- I

o-Toluidine

9s-s3-4
95-80-7

ohenvlenediamine
2.4.5-Trimethvlaniline
o-Anisidine
4-Aminoazobenzene
2-4-Xvlidine

9s-68-l

2.6-Xvlidine

87-62-7

C.I. Direct Black 38
C.I. Direct Blue 6
C.I. Acid Red 26
C.l. Basic Red 9
C.I. Direct Red 28
C.I. Basic Violet 14
C.l. Disperse Blue I
C.l. Disperse Blue 3
C.l. Basic Blue 26 (withMichler's Ketone > 0.1%)
C.l. Basic Green 4 (malachitesreen chloride)
C.l. Basic Green 4 (malachite
seen oxalate)
C.I. Basic Green 4lmalachitel cslrng nrcthod

95-95-44.4'-Thiodianiline
4-Methyl-m-[)etectiolr l.inlit

137-17-"1

90-04-0
60-09-3

t937-3'7 -7260246-2
3761-53-3

569-6t-9
573-58-0
632-99-5247545-8247546-9500

Liquid Extraction
LC/MS

2580-56-5
569-64-2
2437-29-8
10309-95-2
The contenl ofthis PDF file is in accordåncc with the original issued rcporo for reference only,This Test Repon cânnot be reproduced, except i¡ full, without prior willen pemissiotr ofthe company.

@

EEEN
gg¡E
Technical Report:(6817)268-0138
October 19,2017
Page l3 of 19(ìroupI)eter:tior¡ I ir¡til('AS \r¡Subslance (anälvlcs)'Ieslirtut_)rncrtlrotl

seen)

2F. Dyes-disperse(sensitizing)

Disperse Oranse I I
Disoerse Yellow I
Disoerse Blue 102
Disoerse Blue 106
Disperse Yellow 39
Disperse Ora¡se 37 I 59 /7 6
Disoerse Brown I
Disoerse Oranse I
Disperse Yellow 3
Disperse Red 1l
Disoerse Red I
Disperse Red l7
Disperse Blue 7
Disperse Blue 26
Disnerse Yellow 49
Disperse Blue 35
Disperse Blue 124
Disperse Yellow 9
Disnerse Oranse 3
Disoerse Blue 35

82-28-0
I l9-15-3
12222-97-8
12223-0t-7
t2236-29-2

1330l-6l-6
233ss-64-g
2581-69-3

283240-8287248-2
2872-s2-8
3179-89-3
3179-90-650

Liquid Extraction
LCIMS

3860-63-7
54824-3'.7-2

t2222-'75-2

6195t-5t-7
6373-73-5
730-40-556524-77-7

59536-65-l
Pentabromodiphenyl

ether(PentaBDE)
Octabromodiphenyl ether
lOctaBDE)
Decabromodiphenyl ether(DecaBDE)
Tris(2,3 -dibromopropyl)nhosohate ITRISÆDBPPI

Tetrabromobisphenol A

ITBBPA)
2G. Flame Retardants

Bis(2,3-dibromopropyl)
phosphate fBIS/BDBPP)
Hexabromocyclododecane

I 163-19-5

126-72-7
79-94-7(HBCDD)3296-90-0

ITCEP)
Tris( 1,3 -dichloro-isopropyl)
ohosohate ITDCP)
Short chain chlorinatedparaffins (SCCPs) (Cl0-Cl3)

Bis12-methoxvethvl)-ether
2-ethoxvethanol
2-ethoxyethyl acetate
Ethylene glycol dimethyl
ether

2-methoxvethanol
2-methoxyethylacetate
2-methoxvnronvlacetate
Triethylene glycol dimethyl
ether
1.2-Dichloroethane

USEPA 8270

tso 22032,usEPA 527
5412-25-9

2,2-Bis(bromomethyl)- 1,3prooanediol ßBMP)Tris(aziridinyl)-2I. Haloeenated32536-52-0

3t94-s5-6ohosohineoxide ITEPA)
Tris(2-chloroethyl) phosphate

2H. Glycols

32534-8t-9

5

and USEPA 8321B.

Dichloromethane
extraction GC/IVÍS or

LCl\4S(-MS)

545-55-l
I 1 5-96-8

13674-87-8
85535-84-8
I I I -96-6
I l0-80-5
I 1 l-15-9

US EPA 8270

t10-7 t-4

t09-86-4

50

110-49-670657-70-4

Liquid Extraction
LC/MS

GC-MS

n2-49-2
107-06-2

I

IJSEPA 82608

The contcntofthis PDF file ìs in accordance with the originål issued reporu for referenceoolÍThis Tcst RcFf, cannot be reproduce4 except in full, without prior miltm pemission ofthe company.

@

GTITHI

E¡E

Technical Report:(6817)268-0138
October 19,2017
Page 14 of 19(ìr'ou¡r

Subslancc (anâ ¡vtcs )l)etccrfion Linlit

C.\S \o.

1..

Solvents

2J. Organotin
Compounds

Methylene Chloride
Trichloroethvlene
Tetrachloroethvlene
Mono-, di- and tri-methyltin
derivatives
Mono-, di- and tri-butyltin
derivatives
Mono-, di- and tri-phenyltin
derivatives
Mono-, di- and tri-octyltin
derivatives
Perfl uoro-n-octanoic acid(PFOA)
Perfl uorobutanesulfonic acid

(PFBS)

2K. Perfluorinated andPolyfluorinated

Perfl uorooctanesulfonic acid

Chemicals (PFCs)

Perfl uoro-n-hexanoic acid

(PFOS)

75-09-2
79-01-6
127-18-4

I estìnu rncthorl

Headspace GC/MS or
Purge-and-Trap-GC/IVÍ S

Variousrso 17353

Various
0.01

Various

Derivatisation with

NaB(C2Hs)
GC/IVIS

VariousDIN 38407-42(modified)

335-67-l
29 420 - 49 -3. 29 420 - 43 -3

0.01

3s546-4 ,432-50-7(PFHXA)

307-24-4

8:2 FTOH

678-39-7

6:2 FTOH

64'7-42-7

Butvl benzvl ohthalate IBBP)

8s-68-7
84-74-2

Di-2-ethylhexyl phthalate(DEHP)
Di-n-octvl phthalate (DNOP
Di-iso-nonyl phthalate (DINP)
Di-iso-decvl ohthalate lDIf)P))

1

Ionic PFC:
Concentration or direct
injection, Lcllvf S(-MS);
Non-ionic PFC (FTOH):
derivatisation withacetic anhydride,
followed by GC/MS

n7-8t-7
I 17-84-028553-12-0

2676t-40-0
84-66-2

2L. Phthalates(including all otheresthers of phthalic acid)Di-n-oroovl phthalate IDPRP
Di-iso-butvl Dhthalate (DIBP
Di-cyclohexyl phthalate(DCHP)
Di-n-hexyl phthalate (DnHP)
Dinonvl nhthalate IDNPI
Dimethoxyethyl phthalate

IDMEP)
1,2-benzenedicarboxylic acid,di-C7-1 l-branched andlinearalkvl esters IDHNUP)
1,2-benzenedicarboxylic acid,

2M. Poly Aromatic
Hydrocarbons (PaHs)

13 l-16-8

84-69-5
84-61-7

84-75-3
84-76-427554-26-3

Anthracene
Pyrenet20-t2-7

Benzolghilperylene
Benzole]pyrene

t9l-24-2

50-32-8
129-00-0

Chrysene

192-97-2
I 93-39-s
20s-82-3
205-99-2
206-44-0
207-08-9
208-96-8
218-01-9

Dibenzla,hl anthracene

53-70-3

Benzolblfluoranthene
Benzolklfluoranthene

Dichloromethane
exhaction GC/MS

6851542-4

7 l 888-89-6

Fluoranthene

US EPA 8270D, ISOl 8856

tt7-82-8

di-C6-8-branched alkyl esters,
C7-rich IDIHP)
Benzolalovrene lBaPl

I

t0

I

US EPA 8270
DIN 38407-39
Solvent extraction
GC/T4Sthe contenl oflhis PDF fìle ¡s in accordance w¡lh lhe orig¡nål issued repotu for refsencconly.
This Tcst Repon cannot be reprcduced, excepl in fuu, wilhout prio¡wrillm pemission oflhe company.

ffià
ltuNi

\ö/
EIE

l:-Írir:uÍrTechnical Report:(6817)268-0138
October 19,2017
Page l5 of l9GroupSubs¡ancc (analvtes)

CAS No.

Benzolalanthracene

56-55-3

Acenaphthene
Phenanthrene
Fluorene
Naphthalene
Benzene2N. Volatile Organic
Compound (VOCs)

Testing method

L)83-32-985-0 I -8
86-',73-7

9t-20-3
7 t-43-2

Xylenerso I 1423-l
Headspace- or Purge-

1330-20-7
95-48-7
106-44-5
108-39-4

o-cresolÞ-cresolm-cresolGroup

Detection Limit

Parameter substance

and-Trap-GC/MS
US EPA 8260
Limirs (mgil)or
otherwise specifìed

CAS No.

APF'
L5/

al0/

Lt5t

Temperature

max.
25"C

max_

max.

30'c

35.C

TSS

5

l5

50

COD
Total-N

40

80

150

5

l0

20

2tl;l

5;3i2

7;5t3

30

pH

6-9

Color [m- l] (436nm; 526nm;
62Onm)

14. Conventional
Parameters (sumparameters)

Testing nrethod

BOD5Ammonium-N
Total-PAoX
Oil and Grease

5

l5

0.5

I

l0

0.1

0-5
I

3

5

0.5
0.001

2

10

0.01
0.2

0.0s
0.5

0.1

Phenol0.01
0.500/l 00 r00/100|5/100nl
nl
nl
No foam/ Dissipating/
Persistent

Coliform(bacteria/ I 00ml)
Persistent Foam

Apply the standard
methods that best apply
to the region (ISO, EU,
US, China), please refer
toZDHC Wastewater
Guidelines for moredetails on the testing
methodANIONS
SulfideSulfiteDeteotion

Group

Para¡reter/subslanceLi¡nit(pgi L)'

2

Linrils (pgrl)

Testing rnethod

AP}-744043-9
7439-92-l

0.1
I

IO

50
50

100

l0

7439-97-6

I

5

l0

7440-224

0.0s
I

5

Cobalt( Co )7440484

I

t0

50
20

50

Nickel (Ni)
Antimony( Sb )7440-02-0
7440-36-0
7440-18-2
7440-s0-8
7440-66-6

I
I

50

100

200

10

50

100

5

l0

50

250

500
I 000

1000

5000

100

200

I

5

50

50

100

200

Cadmium( Cd )Leadl Pb )Mercurv lHs)

lB. Conventional
Parameters - METALSCAS No.

0.5

Arsenic lAsl
Coooer( Cu
Zinc( Zn\
Chromium( Cr ). total
Manganese( Mn )Chromium VII CrVI )Cyanide( CN-)

I

500
50

744047-3
7439-96-s
t8540-29-9
Various (incl.
57 -t2-5)

20

100
100

Apply the standard
methods that best apply
to the region (lSO, EU,
US, China), please refer
toZDHC Wastewater
Guidelines for moredetails on the testing
methodF:

Note / KeyT¡e content ofthis PDF file is in accordånce w¡lh lhe originål issued rcpons for rcfercncc only.

IhisTcst Rcpon cannot be reproduced, cxcept in fu¡¡, wilhout prior willen pemission oflhc company.

@

GIIEEIII
EIETechnical Report:(68r7)268-0138
October 19,2017
Page l6 of 19

ppm: part(s) per million; ppb = part(s) per billion
U. S. EPA = United States Environmental Protection Agency
APHA = American Public Health Association

Comment 1: The report [(6817)268-0138] is sub-contracted to BVCPS (Shanghai, China) For Perfluorinated Chemicals,
Flame Retardants, Halogenated Solvents, Glycols, VOC & AOX Test.
Comment 2: The report [(6817)268-0138] is sub-contracted to BVCPS (Chennai, India) For Phenol, Ammonium-N, TotalN, ANIONS - Sulfide, ANIONS - Sulfite & Coliform Test.

The conte¡t oflhis PDF filo is in åccordance with the original issued repods fo¡ refrence only.
This Tef Repof cåûot be ßproduccd, except in full, wilhout p¡iorwittfl pemisßion ofthe company.

Report No.: 1720001388
Date of Reeort:3Tl 0/13¿J

TEST REPORTCLIENT DETAILSLABORATORY DETAILSClient Name:SGS Atfiliate and Laboratory

Client Contact

SGS Contact:

Rafiqul lslam, Chemical Lab Manager

Telephone:

Telephone:+88029676500 Ext-220

Factory ll; BANLADESH
Dhaka Region, BANGLADESH

Email:

Address:I

SGS Bangladesh Lim¡ted

Email:

raf iqu l. islam@sqs.com

Address:

Noor Tower, 1 10 Bir Uttam C.R Datta
Road, Dhaka-1205, Bangladesh

I

I

FACTORY DET
Factory Name:
Factory Contact:

Factory ll; BANLADESH
Dhaka Region, BANGLADESH

Telephone:Ema¡l:

Address:
Discharge Dest¡nation
SAMPLE AND TESTING DETAILSSampling Affiliate:

SGS Bangladesh Limited

Sampling Engineer:

Mr. Md. Manir Hossain

Date of Sample Collection

12/10t2017

No. of Samples:

Water (1); Sludge (l)Sample Description:1) Discharge Wastewater(6- hour composite)2) Sludge(Grab)
Sampling Method:

1) 6-hour Composite
2) GrabSample Volume

26L water in total; 3 kg sludge in total

Testing Aff¡liate:

SGS Bangladesh Limited

Sample Received Date:

12/10/2017

Test Performing Period:

121 1012017 - 31 t1 0t2017

REMARKS1.This test document cannot be reproduced in any way, except ¡n full content, without prior approval in writing by the laboratory
2.The results shown in this test report refer only to the sampling and the sample(s) tested unless otherwise stated.

3. AOX test has been subcontracted from SGS INSTITUT FRESENIUS, sample no 171143243 clate- 30.10.201 7.
Sign forand on behalf of
SGS Ëangladesh Lld

tl
RAFIQUL ISLAM
Chemical Lab Manager

Feport No.: 17200013E6
Date of Repo¡t:31/t0/20i2
Page 2 ot 23

POSITIVE SUMMARY
Factory ll; BANLADESH
Dhaka Region, BANGLADESH

Silplô lO

1720001388

Smpþ lD

1720001S8

Dabol smpüng

12110t2017

Dale olsffiplng

12t10P017

ZDHC L¡mits

Smpling Location

Silpling sbnüne

ÑAFaclory Performance

12:00 PM

Smpling €nd dme

06:00 PMDat€of ffipb rcæiv€d

12110t201?

fi|ETHODS

Repon¡ng
L¡mit

UNIT

USÊPA170.1 orGBÆ 131Ss

lncom¡n0
Water

R¡w

Wastew¿ter(Direct

Lhtt

Lhn

USEPA 405.1, APHA 521 08, ISO 5815-1 or HJ SO5

34

coD

USEPA 410.4, APHA 5220D, tSO 6060 or GB/T 1 tgi4

mg/L

Raw

Wætewatea

Water

Wßtewåter

(Oirætng/LF0lf¡ll
F@ndational

mg/L

mg/L

410 or 30

Ä5 or 25

30

10

5

150

80

40

50

15

6-9

6-9

/ max.35^15

Fulfiìl
22

Foundatoml
Llmit

mg/L

100

FulfillFoundationâl

Lioit
TSS

USÊPA 160.2, APHA 2540D. ISO 1 1923 or GBfr
1 1901

5

mga

21

Fulfill
F@ndational

Lr¡it
pH Value

USEPA 150.1, APHA 4500-H+, ISO 10523 or cBÆ
6920

Fu,lil¡8,9Aspiatþôal

ffi
ffi

6-9

Limlt

Colour (436nm; 525nm; 620nm)

Coliform

SulfileISO 7887 (Method B)m¡

USEPA 9132, ISO 9308 or GB/T 5750.12

25

JSEPA 377.1, lSOl 0304-3 or HJ 84

0.2

9,5;6.7;4.9

2:1;1

Fulf¡ll

Bacteria/

Progressive
Limit

100ñl

mg/L

Dal€ofsdpþ ræeid

6.0

12110po17
Sludg6

Dr$haag6
hcom¡ñg

L¡mit

';,

07:00 PM

Sdpl6 D6cñprbn

ursnaigeo
CÁS No.

Sbdg€

Silpling sh(th€Sæd¡ng end tm6
A€pkatlonal

Un¡t

Silple Descriptbn
TEilS

Smp¡ing Localjon

400

100

2

0.5

0.2

Repoili.g
Limit

UNIT

Sludgæ

ReÞorl t¡o.r 1 72ü)01 3EE

Daþ ol Report:3l/10/2017
Page 3 of 23

ORGANIC & INORGANIC ANALYSIS
Factory ll; BANLADESH
Dhaka Region, BANGLADESH

Sampb lDNA

Dal€ ol smpliñO

M

M

Sanplng hcatbn

NA

NA

Samp¡ng sld tims

NÂNÂ

Sampl¡¡g end timeNANA

06:00 PM

Dale ol sdgþ re#

NA

NA

1210t2017

Sampla D4cdplbn

lrElrsCAS No.

Såmplê Colour Dê¡cr¡Þt¡on

I¡IETHODS

RepoÉlng
Ltmtt

UNIT

Visuâl Obs¿ryation

1720001388

SmplêlD

1720001388

121012017

Dalô of sampÍng

1/1012017

ZDHC L¡mits
12:00 PM

Factory PerformanceRåw

ußchargdWâsþwåbr
(Dl.êclL¡m¡t

34

405.1, APHA 52108, ISO 5815-1 or HJ 505

mdL

22

bplbbml
Lhil

Raw

Wâ¡têwrbr

Wa6tèw¡br(Olrccl

mS/L

mS/L

mS/L

10

FullilFdnddionâi

415 / md35

FuffillFounddionâl

0r 30

^10

or 25

^5

30

10

r50

80

50

15

6-9

6-9

6-9

7;5i3

5;3;2

2;1',1

10

2

0.5

0.01

FulfllmS/L

100

Foundatbñal
Lhnit

mS/L

21

Fou¡dational

40

Fulfll160.2, APHA 2540D, ISO 1 19æ or cB/T
1S01

Lh¡!
Fulfill

150.1, APHA 4500-H+, EO 10523 or eB/T

s.9

Asp¡rat¡onâl

Limit
7887 {Method B)

and Geæe

1664, ISO 9377-2, HJ 637

9J;6.7;4,9

0.5

mg/L

Fu¡lill
ñ.d.

Aspirat¡onalLìñit
pheñolics

5530 B, C & D, SO 1402 or HJ 503

1550, tSO 9562, HJ/T 83

0.001

m9/L

n.d.

Full¡llAgpiâtiona¡
Limit

0.1

mS/L

ñ.d.

Aspirat¡oñâl

0.00r

Fulfill
0.1

Limit
Nitrogen (l'oÞLN)351,2, APHA 4500P-J, ÂpHA 4500N-C, ßOmdL

lso 29441, HJ 636

n.d.

FultillAsp¡Éüoôal

20

i0

L¡mit

NitrogenPhosphorus (Toþl"P)

350.1, APHA 4500NH3-N, FO 7150, ISO
11732, HJ 535 or HJ 536

365.4, APHA 4500pJ, SO 6878, tSO 1 188s
GB/T 1 1 893

9132, SO 9308 or GB/T 5750.12

FullillÂspiralioôal
Lm¡t

0.5

m0/L

ñ.d.

0.1

møL

nd,

Asp¡rational
L¡mit

33

Progrgssive

25Bâcþda /100m1Dæof Edpb ræôivd

1210t2017

Sfrpb Oesdp¡ion

SLdge

Reponing
L¡mil

UN'T

Sludgoo

DK GreY

fknn
APHA5220D, ISO 6060 or GB/T 1

07:00 PMuEcnâtg4
hcomlng
Watsr

Limil

(5day)

Umir

Rcddi.h170,1 orGB/T 13195

Sludgô

Silphg str timeSañpÍ4 end ùmeFouúüoDl

NA

hcomlng
Waba

Sffp¡ng Locabñ

10

0.5

Fullill
3

0,5

400

100

FulÍillLimil0.1Rêpoll l¡o,:17ãXt01388
Dôte of Refþrt3l/10/æ17Påse 4 of 23

ORGANIC & INORGANIC ANALYSIS
Factory ll; BANLADESH
Dhaka Region, BANGLADESH

Sampls lD

NA

NA

1720001388

Sffpb lO

1720001388

Dala ol mplng

NANA

1410n017

D& ofsmpÌng

M012017Samphg Locabn

NANASæptng dd tìmeM

NA

1200 PM

Oals otwpbræ6dNANA

1ù10Þ017

Sample Dsciphn

NA

ZDHC L¡mits

Factory Pelormance

CAS No.

I¡ÊTHODS

L¡m¡l

UtrT

07:00 PM

Sanp¡q end liæLiñ¡rursnargco
Repoñlñg

Sludsostr time

Sañg¡ng066ô PM

TEItrI

Sañplñg Locatbn

L¡mil

kplnbmlL¡nl

Dab ol sffipþ rdd141012017SÐpb Dædpbn

Sbdge

DEChâageo

hcohlngRåw

Wstôralêr

hcom¡ngWaÞrWæþwater(DlrætWâtÞrRauWastêwatâr

Wastdalèr
(Olæd

mdL

mdL

mg/L

Nol vis¡blê

Nol *ible

Nol visible

0.1

0-05

0.o5

0.01

0.5

0.2

0.1

0.05

0.01

0.05

0,01

0.1

Reporüng

UNT

Sludgêo

mdks

n.d.

0.005

mS/kg

n.d.

0.05

0.01

mg/kS

n.d.

0.2

0.1

0.05

0.05

0.005

0,001

ñS/kS

n-d.

0.05

o.o2

0.0r

0.5

0.25

0.05

0.01

mg/kg

n.d.

L¡mil

Fulill-oam

Nol vi!¡ble

Notvbibtè

Aspi€líoñal
L¡mitl, A¡bN

FulfllUSEPA 3352, APHA4sOO.CN, HJ 484,
HJ 745 (for sludqe)

lyañile

0.05

mS/L

n-d-

Aspiralionâl
Limit

0.5

Fu[Il

ìulfiie

APHA 4500-S2-D, ISO 10530 or GBI/T 16489

0.01

mg/L

n.d.

ìuffreUSEPA 3?7.1. lSO1030+3 or HJ 84

o-2

mg/L

6.0

0.01

mdL

n.d.

Aspirâfþnal
Limit

0.5

l. l¡.t¡16{sb)FuÍil!

7440-36{700
Dig8sÌioñ lollowêd by þP or PP/MS analys¡6

Limitrefereñce to USEPA 200.7, UsEpa 200.8,
Arsenic (As)Cadmium (Cd)(c0Hsþvâlent Chromium (CrCobalt(Co)Copper (Cu)

Leâd (Pb)74404A-2

740-43-9

0C, USEPA 6020Á, ISO 11885, HJ 700 orD¡goslion tollowêd by þP or ICP/MS ânalysis
refårencê b USEPA 200.7, USÊPA 200.8,
0C, USEPA6020A, ISO 11885, HJ 700 orDigêstion followsd by þP or EP/MS anâlysis

Fulfll
0.005

mg/L

n.d.

0.01

mg/L

nd,

Fullill
AspiÉIrcnal
Limit

0.05

mg/L

n.d.

AspiÞfoñalrêlererceb USEPA200.7, USÊPA 200.8,
740-47-3

744047-3,
185{-29-9

7440-484

0C, USEPA 60204, ¡SO 1 1885, HJ 700 or
Digestion lollowêd by ICP or þP/MS analysis
r6terencs b IJSEPA 218.6, ISO 18412, cB 7467
eûact¡on ild derivãlisl¡on lollowed byanalysisrelers¡æ to USEPA 30604&71964 for studq€
relerence to L,SEPA 200.7, USEPA 200.8,
USÊPA60204, ISO 11885, HJ700or
Digesüon followêd by þP or EP/MS analysit

tupiøüoñal

Asp¡ratbnal
Umtr

FutfÌll
Limit
0,001

mg/L

n.d,

Full¡llAspiÞliona¡

Liñ¡t
0.01

mg/L

n.d.

Fulfill
Aspiralbnal

Unit740-50-8

rete.ence to USEPA200.7, USEPA 200.8,
6010c, usEPA6020A, tso 11885, HJ 700 or
Dbestbn lollNd by þP or ICP/MS ana¡ysis

0.25

7439-92-1

relerence b USEPA200.7, USEPA 200.8,
6010c, usEPA6020A, ßO 1 1885, HJ 700 0r
Digestion followed by PP or þP/MS ana¡Æis

0.01

mg/L

n.d.

Fullill
Asp¡Etional
L¡mit

mg/L

n.d.

FullillAsp¡Þt¡onal
Limit

0.1

4

Repon l¡o.:172q)01384
Date of Report:31/10/20f 7
Page 5 of 23

ORGANIC & INORGAN¡C ANALYSIS
Factory ll; BANLADESH
Dhaka Region, BANGLADESH

Sample lD

1720001388

sffiplâ lot7200013aa

Dale ofsamplng

12t1012017

Dateolsampling1ù1U2017

Samplins Localbn
SamÞlino stdÌineZDHC Limils

NA
NA

Factory Pelorñance

12:00 PM

Sâmpli¡g end tiñeNA

06{0 PM

Daleofsampþ ræôid

ÑA

1210Þ017

Foundabnål
LimatPrcgÞssfoê
L¡miltuÞlhlon6l
L¡mil

Sample Desciplion

CAS No.

Iolal Mercury (Hg)

Iolâl Nickel (Ni)Iotal Sllver (Ag)

Iotal Zinc (zn)7439-97-6

7440-O2-O

METHODS
rercrence þ usÈPAzuo./, UsEPA ?00.s,
JSEpA 6010C, USEPA 6020A, USEPA 7473, tSO
18412, HJ 597 or Acid Dìgestion followed by þP or
CP/MS analreis¡/ith reference b LJSEPA 200.7, USEPA 200.8,
JSEPA 6010C, USEPA 60204, tSO 1 1885, HJ 700 0r\cid Digestion lollowed by PP or rcÈMS analysis

Reponlng

Llhlt

0.001

UilT

mg/L

hcomlngWaþrWaaþwater(Dlrætn.d.

lncoßlng
Water

Raw

u6cñafgeo
Wastawalêr
(OlæctFultillAspkal¡onal

mg/L

mg/L

mdL

0.01

0.005

0.001

0.2

0.1

0.05

0.1

0.05

0.005

Samp¡ñs Locatbn

SludgeSañplng sdrimê

07:00 PMDaþ ol sæ9b rd6d

1A1012017

Smple Desipbn

SludgeRepod¡ng

Liñf

UNfT

Sludgeo

0.1

mlkg

nd,

Lìñit
0.05

mg/L

n.d.

Êulfìll
Aspirat¡onal
Lrmit

740-22-4

trilh reference b TJSEPA 200.7, USEPA 200.8,
JSEPA 6010C. USEPA 60204, ISO 1 1885, HJ 700 or\cid Digestion lollowd by ICP or þPtuS analysß

0.005

7440-66-6

trilh reference b IJSEPA 200.7, USEPA 200.8,
JSEPA 6010C, USEPA 60204, tSO 1 1885, HJ 700 0r\cid Digestion lollowed by ICP or þP/MS analysÉ

0.5

mg/L

ñ.d.

5

lls/L

n.d.

o-2

mdks

nd.

5

!s/L

n.d.

0.2

mdks

n.d.

5

pg/L

n.d.

0.2

mS/kS

n.d.

udL

nd,

mg/kg

n.d.

røL

n.d.

0.1

mS/kS

n.d.

!s/L

n.d.

0.1

mg/kg

n.d.

24. AkylÞhenob (APs) and AkylÞhenol Ethoxylåtes

ñdL

Fullill
ñ.d.

Aspirat¡onal

Limil
FuliillAspkalional
Limit

0.5

(ÆEOs)

Multiple, including

f,cMphenol (OP), mì¡ed ¡somere

Wilh relerence lo ISO 18857-2 or ASTlt4 07065
1 40-66-9, 1806-26
followed by GC/MS or LC/MS analys¡s4, 27193-28-8
Muhiple, including\,lonylphenol(NP), mi¡6d

104-40-5,11066wirh relofênce to lso 19857,2 or AsfM 07065
49-2,25154-52-3.
followed by GC/MS or LC/MS analys¡s84852-15-3. 90481
Multiple, iñcluding
9002-93-1,9036Wilh rôleråñce to ISO 1€254-1, ISO 18857-2 or ASTM
f, ctylphenol ethoxylâles (OPEO)
07065 tollowed byGC/MS or LC/MS analysis
689S7-90-6
Multiplo, including,'lonylphenol ôtholates (NPEO) 9016-45-9,26027- Wilh referencå ro SO 18254-1, tSO 18857-2 or ASTM
38-3, 37205-87-1, D7065 tollowed by GC/MS or LC/MS analysi6
ì9412-54-4,
28, ChloroboMeæs ånd chlorolotueæs (COCa),2-Dichlorobenzene

108-90-7

rôteronce 1o USEPA 82608. USEPA 82700 or
enraclion rollowed by GC/MS analysis

95-50nreference ro USEPA 82608, USEPA 82700 orènractjon lollowed by GC/MS anâ¡ysis541-73-1

reference þ IJSEPA 82608. USEPA 82700 or
etracl¡oñ lollowed by GC/MS ânalysis

0.2

Bs/L

n-d.

0.1

mS/kS

n.d.

106-46-7

relerenêe b USEPÂ 82608, USËPA 82700 or
by GC/MS analysis

o.2

Bs/L

n.d.

0.1

mdks

n.d.

o.2

Repon No.:172(x)O13EE
Dâte of ReÞort:31/10/20f 7
Page 6 of 23

ORGANIC & INORGANIC ANALYSIS
Factory ll; BANLADESH
Dhaka Region, BANGLADESH

Sample lODaþolsamplingNA

1720001388

Sample lD

1720001388

12102017

Dal6 ol samp¡ng

1il101n17

ZDHC L¡m¡ts

Samplñg Locabn
Samplng sø rim€

NA

Factory Performance

12:00 PMSãmpl¡g end timeNA

06:00 PMDåleo,silple @odNA

12t1012017

CAS No.

uñil

L¡ml

(Dl.ecl

Water

Raw

uÉcnargêo
Wastêwabr(Ol@ct

mS/L

mg/L

mS/L

Sbdge

Ropoling
Limit

UNF

Sludgêo

ñ.d.

0.1

mg/kg

nd,

felerence to USEPA 82608, USEPA 8270D or
6nraction followed by GC/MS analysis

0.2

tsL

n.d.

0.1

mS/kS

n.d.

rofâronc€ to USEPA 82609, UsEpA e270D or€nrâcl¡on lollowed by GC/MS analysis

0.2

¡g/L

n.d.

0.1

mg/kg

n.d.

rof€ronc€ b IJSEPA 82608. USEPA 8270D oreÍracl¡on lollow€d by GC/MS ånalysis

0.2

pAIL

n.d.

0.1

ñg/kq

n.d.

relerence þ IJSEPA 82608. LJSEPA 8270D or€nracl¡on followed by GC/MS analysis

o.2

us/L

ô.d.

0.1

mg/kg

n¡.

relerence to LlsEPA 82608, UsEpA a270D oreÍradion lollowed by GC/MS analysis

0.2

us/L

n.d.

0.1

mdks

n.d.

relerence þ LJSEPA 82608, USEPA 82700 or
by GC/MS analysiE

o-2

ps/L

î.d.

0.1

mg/kg

n.d.

relerence to IJSEPA 82608, USEPA 8270D or
followed by GC/MS añalysis

0.2

¡s/L

n.d.

0.1

mg/kg

n.d.

95<9€

referenceto USEPA 82608. USEPA 8270D or
enraction followed by GC/MS analysis

0.2

usll

n.d.

0.1

mg/kq

n.d.

108-41€

relereñce to USEPA 82608, USEPA 8270D oreÍraclion followed by GC/MS ânalysis

0.2

uøL

n.d.

0.1

mg/kg

n.d.

106-434

reference to USEPA 82608, USEPA 8270D or
elraction followed by GC/MS analysis

0.2

tslL

n.d.

0.1

mg/kg

n.d.

32768-54-0

felerèñæ lo IJSEPA 82608, USEPA 8270Ð orenracl¡on lollowed by GC/MS ânallsis

o.2

BdL

n.d.

0.1

ñdks

n.d.

95-73€

refer€nce to USEPA 82608, UsEpA 9270D orÞfaction followed by GC/MS ana¡ysis

0.2

!s/L

n.d.

0.1

mg¡(g

ñ.d,

19398-61-9

relerence to USEPA 82608, usEpA 82700 or
enractioñ followed by GC/MS analysis

o.2

ps/L

n.d-

0.1

mdks

n.d.

120-82-1

Telrachlorobeñzene

hcomlng

1/10t2017

Smpb Descripüon

vslL,2,4-Trichlorobenzene,2,3,s-letachlorobenzene

uNlf

Râw

Daþ of sæph ræôtud

o.2

a7-61 -6

,2,3,4-TêÍachlo.obenzenê

Llhlt

hcohlng

07:00 PMrelerence to USEPA 82608. UsEpA a270D or
enracl¡on lollowèd by GC/MS analysis,2,S"lrichlorobenzene,3,5-Tr¡chlorobenzene!¿IETHODS

RepoitlrE

SludgeSampling sø liñe

Samp[4 end ùmeL¡h¡tSåñplo D6ciplion

ITEMS

Sampfi¡g Locatbn

108-70-3

634{6-2

634-90-2

95-94-3

608-93-5

114-74-1

Reporl No.:172q)01388
Date of Report:3'l /1 0/20 17
Page 7 ol 23

ORGANIC & INORGANIC ANALYSIS
Factory ll; BANLADESH
Dhaka Region, BANGLADESH

sampþ lÐDatsolsmpling

NA

Sampling Locatbñ

NA

1720001388

Smp¡elD

1720001388

1ù1012017

D& otsamp¡ng

M012017ZDHC Lim¡tsSampÍng sldrimeNANA

12:00 PM

Sañpling eñd time

06:00 PM

Dale ol snpb @etuÞd

12/10Þ017

Factory Performance

L¡mil

L¡nit

L¡mil

Samp[ng Locúñ

St¡dgê

Samp¡ing sÞn ùme

07:00 PM

Dale of smpb ræofud

1210t2017Såñpb Dscdplbn

Sþdgeußcnargæ
Repodlng

lñcom¡ng
Water

naw

Waslewatel(Dircctlncohlhg

Raw

Wâstewaþr
(Dlrcct

Repofring
Limit

uNn

SludgeO

n.d.

0.1

mg/kg

n.d.

!øL

n.d.

0.1

mg/kg

n.d.

0.2

us/L

n.d.

0.1

mS/kS

n.d.

Wilh r€fer€nce b USEPA 82608, USEPA 82700 orSolvÞnt enraction follored by co/lr4s analysis

0-2

Bs/L

nd.

0.1

mg/kg

n.d.

2077-46-5

With relerence b IJSEPA 826q8, USÊPA 82700 or
Solvenl enrâclioñ lollowed by GC/MS &alysis

0.2

øL

n.d.

0.1

møkg

nd,

2,4,5-Tdchlorotoluene6639-30-1

With relerence to IJSEPA 82608, USEPA 8270D or
Solvent efracfon lollowsd by GC/MS ânâlysis

0.2

udL

n.d.

0.1

mdkg

n.d.

¿,4,6-Trbhlo¡otoluene

23749-65-7

Wilh relereñce to USEPA 82608, l.lsEPA 8270D or
Solvent efraclion followed by GC/MS analysis

0.2

us/L

n.d.

0.1

mg/kg

n.d.

],4,s-Trbhlorotoluene

21472-86-6

Wilh reference þ USEPA 82608, USEPA 8270D or
Solvenl efraclion followed by GC/MS analysis

0.2

¡rS/L

n.d.

0.1

mg/kg

nd.

¿,3,4,5-Tetachloroioluene

76057-12-0

Wilh reference io USEPA 82608, USEPA 8270D or
Solvenl eftâction followed by GC/MS analysis

0.2

ps/L

n.d.

0.1

ñdks

nd.

2,3,4,6-letachlorololuene875-401

With rêference io USÊPA 82608, LJSEPA 82700 or
Solveil enÊclion lollored by GC/MS analysß

0.2

ugÂ

n.d.

0.1

mdkg

n.d.

29733-70-A

With reterence to IJSEPA 82608, L.lsEPA 8270D or
Solventexyaclion followed by GC/MS ânalysis

us/L

n.d.

0.1

mg/kg

n.d.

rEMS

CAS No.

2,6-Dichlorololueñe

1

18'69-4

wirh relerence to USEPA 82608, USEPA 8270D or
Solvenlenraolion followed by GC/MS analysis

o.2

¡g/L

3,4-Dichlorololuene

95-75-0

wirh relerence to USEPA 82608, USEPA8270D or
Solvenl efraclion followed by GC/MS analysiso.2

1,5-Dichlorotoluene

251A647-4

Wilh referenc6 b USEPA82608, USEPA 8270D orSolvêil onraction followed by GC/MS anâlysis

2,3,4-Trichlorotoluene7359-72-0

u,3,6-Trichlorotoluene¿,3,5,6-Tetachlorotolue¡e)entachlorotoluene877-11-2

MtrHODS

Llh¡t

UNT

mS/L

mg/L

mg/L

û/ilh reference b USEPA 92608, LJSEPA 8270D or
Solvenl exlractioñ followed byGC/MS analysis

0.2

sdL

n.d.

0.1

mg/kg

n.d.

relereñce to USEPA 82700, ISO 1 4154 or
and dertualisation wilh KOH, acel¡cf ollo@d by cCÂ\4S analysis.

0.5

udL

ñ.d.

0.0Æ

mdks

n.d.

¿C. Chlo.ophonob

95-57-8

Repol No.:172qt013EE
Date of nepqrt:31/10/2017
Page I of 23

Factory ll; BANLADESH
Dhaka Region, BANGLADESH

ORGANIC & INORGANIC ANALYSIS
Sañpb lÐ1Datêofsamplirg

NA

720001388

Silpbl0r720001388

121012017

Dal€ of sampÍng

141U2017

ZDHC Lim¡tsSanpÌng Locatbñ
Sanplng sE tim6

12t00 PMNA

1211012017

Ràw

ußcnargd
Wastetaler

lncomlng(Dlrect

Water

Samplng end time
Da19 ol sffpb ræsfued

Factory PerformanceNASåmp[ng Locarbn

SLdge

Sampling sÞnüñe

07:00 PM

Dala of smpbræeivd

1410P017

06:00 PMNA

&prôüoml
L¡m¡t

Um¡t

L¡mil

Sample Descdplbn

irÊMsTdchlorophenol

CAS No.

MÉIHODS

Repofrlhg

Llmit

UNIT

sþdge

hcohlhg
Waiôr

Raw

We6têwaler(Olæct

mg/L

mg/L

mg/L

Repoding

Liñit

UNtT

Sludgêo

108-43-0

reference b USEPA 8270D, ISO 14'15¿
and deriEtisation wilh KOH, acetic
f ollowed by GC/MS analysis.

0.5

ps/L

n.d.

0.025

møkg

nd,

106-48-9reference to IJSEPA 82700, ISOand derivatisation wilh KOH, acet¡cf ollowed by GC/MS analysis.

0.5

tlglL

ñ.d.

0.025

mg/kg

n.d.

576-24-9

relerence to IISEPA 8270Ð, ISO 14154 or
and dertualisation with KOH, acet¡clollo@d by GC/MS ânalys¡s.

0.5

!g/L

n.d.

0.025

mg/l(gñ.d.

120'43-2

relerence to USEPA 8270D, lso i4154 or
and der¡valisaloñ with KOH, acetb
lollowed by GC/MS ânâllsis.

0.5

ps/L

n.d.

0.025

mg/kg

n.d.

583-78-8

relerence to USEPA 8270D, lso 14154 or
and derivatisation with KOH, acetic
by GC/MS analysis.

0.5

PS/L

n.d.

0.025

mlkg

nd,

87-65-0reference to L,SEPA 82700, ISO 14154 or
and derivatisation wilh KOH, acelic
followed by GC/[4S añalysis.

0.5

rdL

n.d.

0.025

mdks

n.d.

95-77-2¡eiereñce to USEPA 8270D, tSO 14154 or
and derivalisation with KOH, acel¡c,ollowed by GC/MS analys6.

0.5

¡s/L

n.d.

0.025

mg/kg

ñ.d.

reference þ USEPA 82700, ISO 14154 or
and dertuatisalion dth KOH, acetb
followed by GC/MS analysis.

0.5

gg/L

n.d.

0.025

mg/kS

n.d,

15950-66-0

reference Ìo LJSEPA 8270D, ISO 14154 or
and deriEtisation wilh KOH, acelic
followed by GC/MS analysis.

0.5

vdL

n.d.

0.025

mdkg

n.d.

933-78-8

reierence to USEPA 8270D. ISO 14154 or
and derivatisation with KOH, acelac
f ollowed by GC/MS analys6.

0.5

uøL

ñ.d.

0.025

mg/kg

n.d.

933-75-5rele¡ence to USEPA 82700. ISO 14154 or
and detualisation with KOH, acetb
lollowed by GC/MS analysis.

0.5

!s/L

n.d.

0.025

mg/kg

n.d.

95-954

reler€nc€ to USEPA 8270D. ßo 14154
ånd de¡iEl¡sation wilh KOH, acetic
tollored by GC/MS añalysis.

0.5

vgtL

n.d.

0.025

mSlkS

n.d-

88-06-2

relerence to USEPA 82700. ISO 1 4154
and derivalisalion with KOH, acel¡cfollowsd by GC/MS analysis.

0.5

!s/L

n.d.

0.025

mg/kg

ñ.d.

609-ls-greference to USEPA 8270D, ISO 14154
and deilvati6atbn wilh KOH, acelic
lollowed by cÕ/MS analysis.

0.5

pg/L

n.d.

0.025

mg/kS

Repon tlo.:1720ü)1388
Date of Beport:3l/10/æ17
Page I of 23

ORGANIC & INORGANIC ANALYSIS
Factory ll; BANLADESH
Dhaka Region, BANGLADESH

Såñple lD

1Dale otsñplingNA

720001388

SmpblD

1720001388

1211012017

Daþotsamping

141U2017

ZDHC L¡mits

Sanpling Locdbn
Samplng sldrimeNANA

12:00 PMNA

1410t2017

Sampling end time

Factory Performance

Samp¡¡s Locabn

Sbdge

Samplinosøüne

07:00 PM

Dâb ol sæpb rðcôfod

121012017

0Ê:00 PM

Oaleof smpb ræetud

Liñ¡t

Lim¡t

L¡ml

SLdge

TEI¡ts2,3,4,5-Tef achlorophenol

CAS No-4901-51 -3

Repod¡ng

ilElHODS

Llmlt

trìth relereñce to USEPA 8270D, ISO i4154 or solrenr{radion ând derivalisâtion with KOH, acet¡cànhydride followed by GC/MS anâtysis.

UilIT

Faw

Wætawâter
(Dlrect

hcomlng
Waler

Raw

Wâstewabr(Dlrcct

hS/L

hg/L

mg/L

Reporting
Limit

UNTT

Sl!dgeo

0.025

mg/kg

n.d.

0.025

mg/kg

n.d.

n.d.

0.5

F9/L

n.d.

0.5

ps/L

n.d.

0.5

Fg/L

ñ.d.

0.025

mg/kg

reference to USEPA 82700, ISO 14154 or solwn^/ith:frâcl¡onand dodvatisâtion with KOH, acetic¡nhydride lo¡lowed by GC/MS analysis.

0.5

tslL

n.d.

0,025

mg/kg

92-67"1relerenco to USEPA 82700, EN 14362-1, EN
or Solvonl snrâction with sodiuñ dithontg
lollowod by GC/MS and HPLC añâtysis.

0.1

Fs/L

n.d.

0.1

nstko

n.d,

92-87-5roference to USEPA 82700, EN 14362-1, EN
1{362-3 or Solvent èfrælioñ with sdium dithonite
by GC/MS and HPLC analysis.

0.1

tslL

n.d.

0,1

møkg

nd.

95-69-2

reloreñce b IJSEPA 8270D, EN 14362-1, EN
14362-3 or Solvent e*raction with sodium d¡thoñite
followed by GC/MS and HPLC analysis.

0.1

FslL

n.d.

0.1

ûSlkg

ñ.d.

91-59-8

relerence b USEPA 82700, EN 14362-1, EN,lí162-3 or Solvent etÞctìoñ with sdium dithonte
lollowed by GC/MS and HPLC analysis.

0,1

p9/L

nd,

0.t

mdks

n.d,

97-56-3

refereñce to USEPA 8270D, EN 14362-1, EN
4362-3 or Solwnl e(raction with sodium dithonite
followed by GC/MS and HPLC analysis.

0.1

rdL

n.d.

0.1

mS/kS

n.d.

99-55€

relerence to USEPA 82700, EN i4362-1, EN,1362-3 or Solvent eÍraction with sodium dithonite
tollowed by GC/MS and HPLC analFis.

0.1

ps/L

n.d.

0.1

møks

n.d.

06-47-8

reterence to USEPA 8270D, EN 14362-1, EN
or Sd@d enrâctioñ with sdium dithonitê
lollowed by GC/MS and HPLC analysis.

0.1

!siL

n.d.

0.1

msag

n.d.

615-05-4

reference ro USEPA 8270D, EN 14362-1, EN
or Solvent eirætion wilh sodiuñ dithonite
followed by GC/MS and HPLC analysis,

0.1

ps/L

n.d.

0.1

mdkg

n.d,

101-77-9

relerence to USEPA 92700, EN 14362{, ENor Solvenl eÍractioñ with sod¡um dithonite
followed by GC/MS and HPLC añâlysis.

0.1

0.1

mg/kS

n.d.

ililh reference þ USEPA 8270D, ßO 14154 orsolwn

2,3,4,6-lef achlorophenol

58-90-2¡{raci¡on and derivâtisation with KOH, acetic¡nhydride followed by GC/MS añalysis.
/Vith relerence to USEPA 8270D, ISO 14154or

2,3,5,6-lelrachlorophonol

lncohlng

935-95-sPenÞchloropheñols

87-86-5elwn

tnraction ând dertuatisation with KOH, acet¡c¡nhydrde follored byGC/MS añalysh.

20. Azo dyos

1

!siL

n.d.

Repon l¡o.: 1 720ü) ! 3aa
Date of Repoñ:3f /10/20f 7
Page 10 of 23

ORGANIC & INORGANIC ANALYSIS
Factory ll; BANLADESH
Dhaka Region, BANGLADESH

Sample l0NADatê of sampling

1720001388

Dd6 olsamplng

12101417

NA

M

NA

12:00 PMNA

NA

14102017

Sampling eñd limeDaþ olsfrpl€ ræôild

Sañple lD

12102017

ZDHC L¡mits

Sampling kcatbn
Sampling 6ldtine

1720001388

Factory Pelormance

06100 PM

Sañplng Locarbû

SludgeSamptrng sÞn üm€

07:00 PM

Samp¡iq end limo&plÞdomlFoúnùtonÂl
Limil

L¡mil

L¡ñ¡T

Sample DGcription

Daþ ol sÐpþ ræoid

1210t2017sæpb Desdplbn

Studseuacnargæ
ITEilSCAS No,

MflHODS

Reponlng
Llmlt

UNIT

0.1

Fg/L

0.1

lhcoh¡ngRåwWætewatêa

hcomlngRâwWabÌ

Wæ1ilãter

(thect

Wator

Waslewaþr

Wâ5towâþr
(Dlrcct

Repofring
Limit

UNTT

Sludgeo

n.d.

0.1

mg/kg

n.d.

ps.tr

n.d.

0.1

mg/kg

n.d.

mdL

mdL

mlL

relereñceb USEPA8270D, EN 14362-1, EN
91-94-1

followed by GC/MS and HPLC analysis.

119-904

refereñce b IJSEPA 8270D, EN 14362-1, EN
or Solvent eñrâction wilh sdium dilhoñitelo¡lowed by GC/MS and HPLC âñalysis.

119-93-7

relerence Ìo USEPA 82700, EN 14362-1, EN
or Solvont eÍrætion with sdium dithoñite
followed by GC/MS añd HPLC ânalysis.

0.1

ps/L

n.d.

0.1

mdkg

nd.

838-A8-0

reterence io USEPA 8270D, EN 14362-1, EN
or Solvenl e{raction wilh sodium dilhoniterol¡owd by GC/MS and HPLC analysis,

0.1

fs/L

ñ.d.

0.1

mdks

n.d.

0.1

ps/L

n.d.

0.1

mdks

ñd.

101-144

reference lo USEPA 82700, EN 14362-1, EN
or Solvent enraction wilh sodiuû d¡lhonite
followed by GC/MS and HPLC analysis.

0.1

rdL

ñ.d.

0-1

mdks

n.d.

101-804

relerence to USEPA 82700, EN 14362-1, EN
or Solvent eRraclion wilh sodium dilhonite
followed by GC/MS añd HPLC analysis.

0.1

tslL

ñ.d.

0.1

mg/kg

ñ.d.

0.1

!s/L

n.d.

0.1

mdks

n.d.

95-53-4

reference to USEPA 82700, EN 14362-1, EN
or Solvenl elraction wilh sodium dithonite
followed by GC/MS and HPLC analysis.

0.1

Fs/L

n.d.

0.1

mg/kg

n.d.

95-80-7

reterence to USEPA 8270D, ÉN 14362-1, EN
14362-3 or Solvônl eÍraction with sod¡um dithonfre
lollowed by GC/MS and HPLC analysis.

0.1

!siL

n.d.

0.1

mgag

n.d.

137-17-7

relerence to USEPA 82700, EN 14362-1, EN
1 {162-3 o¡ Solveil enrâction with sod¡um dithonile
by GC/MS and HPLC analys¡s.

0.1

,\g L

nd.

0.1

mg/kg

ñ.d.

0.1

!s/L

n.d.

0.1

mlks

n.d.

0.1

trdL

n.d.

0.1

mg/kg

n.d.

0.1

ps/L

n.d.

0.1

møks

n.d.

relereñce to USEPA 82700, EN 14362-1, EN
120-71-A

lollowed by GC/¡jS and HPLC ana¡ysis.

reforeñce to USEPA 8270D, EN 14362-f, EN
133-65-1

followed by GC/lt¡S and HPLC añalysis,

Tilmethy¡añiliñerefêr€nc€to USEPA82700, ÊN 14362-1, EN
90-04-0
by GC/MS and HPLC analysir.

60-09-3

relerenceb |SEPA8270D, ËN 14362-1, EN
14362-3 or Solv€nt êtraction wilh sdium dithoñite
by GC/MS and HPLC analysis.

95-6S-1

relerenceþ LJSEPA8270D, EN 14362-1, EN
1€62-3 or Solvent etraclion with sdiùm dfrhontre
by GC/MS and HPLC anålysis.

10ReÞon ilo.r 1720001388
Date ot Report:31/10/2017
Page 11 ol 23

ORGANIC & INORGANIC ANALYSE
Factory ll; BANLADESH
Dhaka Region, BANGLADESH

Sampþ lD1

Dd€olsmpliñO

720001388

smpblDi7200013sa

12h0t2017DaÞolsampÍng

1210A017

ZDHC L¡mits

Sâmp¡ing Locdbn

Samplingsrdfne

NA1200 PMNÄ

12t1DpO17

Sâñpliñg eñd limeÐaþ ol sõpl€ ræôiv6d

Factory Pelormance

06100 PMNA

Samp¡ng Locatbñ

SludgeSamÞ¡ng sdrime

07:00 PM

Sffiplnq end lime&plÞdoùl
L¡mil

Lim¡t

L¡mii

Sample D6cñplbn

Dale of silpb ræ6ivd

1ù10t2017Sañpþ Ðescñplbn

Sludgeußcnåfg@
TEMS

CAS No.

1,6-Xylhinê

a7-62-7

METHODS'virh

Fepoñlhg
Llmh

UNfT

hcohlhgW¡lar

Râw

Wast4ãbr
(Dlrêctlhcohlng
Waler

Raw

Wætåwaþr

Waslewa!ôr
(Dlrect

mg/L

mg/L

mg/L

Roponing
Limit

UNIT

Sludgeo

0,1

mg/kg

ñ.d.

relerence to USEPA 8270D, EN 14362-1, EN
0.1

cs/L

n.d.

'edudion lollowod by GC/MS and HPLC ânalysis.

lE. Carclnogehlc dyes
Red 263761-53-3

eÍraction lollored by LC/MS anâlysis.

500

ps/L

ñd,

mS/kg

n.d.

Bluê 26

2580-56-5

eÍraclion tollo@d by LC/MS analysb.

500

pdL

ñ.d.

mdks

ñ.d.

Green 4 (malachite green)

10309"95-2

ertraclion followed by LC/MS analysis.

500

FS/L

n.d.

ñg/kg

ñ.d.

5694+2enrâctiôn followed by LC/MS analysis.

500

¡rs/L

n.d.

mg/kS

ñ.d.

2437-29-A

e{raction followed by LC/MS analys¡s.

s00

!s/L

nd.

mS/kS

n.d.

569'61-9e{râction follored by LC/MS analys¡s.

500

tslL

n.d.

mg/kg

n.d.

632-99-5

elraclion follored by LC/MS analysis.

500

FIL

n.d.

mdkg

n.d.

1937-37-7

etiraction followed by LC/MS analysis.

500

udL

n.d.

mS/kS

n.d.

2602-46"2e{raction followed by LC/MS analysig.

500

PS/L

n.d.

mg/kg

n.d.

573"58-0

exraction fo¡lowêd by LC/MS añalysb.

500

trslL

n.d.

ñg/kg

n.d.

2475-45-8

followed by LC/MS anÊlysis.

500

rdL

n.d.

mS/kS

n.d.

lollowed by LC/MS analys¡s.

500

tslL

n.d.

mg/kg

n.d.

Græn 4 (malachile green

Green 4 (malachlegreen

Red 9

Vio¡et 14

Black 38

Blue 6

Red 28

Blue 1

Blue 32475-46-91lRopo]l tlo.:172q)01388
D¿te of Repod:31/10/ã)17
Page 12 or 25

ORGANIC & INORGANIC ANALYSIS
Factory ll; BANLADESH
Dhaka Region, BANGLADESH

samplê lD

1720001388

Dalâ oI sañplng

NASampþ lD

12t10p017

Oate oltrpÍng172000138S
1ù1012017

ZDHC Lim¡ts

Sanp¡ng Locabñ
Samplng sH tim€

NA

12:00 PMNA

12t10t2017

Sampllng end tiñe

Factory Performance

06:00 PM

Daleolsffpb ræsfud

Samplng Locdbn

SLdge

Samplng stdtiñe

07:00 PM

Sâmplng eñd linetuptåüonål
L¡ñ¡T

Um¡t

L¡m¡l

Sample DescñplionÐataof smpb ræetud

1/10t2017Sûple Desc.iplion

sbdge

DECh¿fged
TEMS

CAS No.

)isperse Orange 11

HflHODS

Reponlng
Llmll

uNr

hcomlngW6ter

Râw

lncohlng(Dlrect

Watea

Wa6tewaler(Olrcct

mS/L

mg/L

mg/L

Repodjng

Uñl

UNfI

Sludgoo

I

mg/kg

n.d.

a2-24-O

Sol€nl enrâction lollowed by LC/MS analys¡s.

500

t¡g/L

n-d.

Brown 123355-64-8

enraction followed by LC/MS analysis,

50

FdL

ñ.d.

mg/kg

n.d.

Blue 73179-90-6

effâclioñ followed by LC/MS analys¡s.

50

fg/L

n.d.

mg/kg

n.d.

26

3860"63'7

etract¡on fo¡lowed by LC/MS analysis,

50

tstL

n.d.

mg/kg

ñ.d.

oxtraction followed by LC/MS âñalysis.

50

udL

n.d.

mS/kS

nd.

lF. Dlsperso dyg6

Blue 35

5652+77-7

Eluo 10212222-97-A

etaclion followed by LC/MS analysis.

50

!s/t

n.d.

mS/kg

Blue 10612223-01-7

eiraclion followed by LC/MS anâ¡ys¡s.

50

!s/L

n.d.

mg/kg

n.d.

Blue 124

61 951 -51 -7

efraction fol¡owod by LC/MS analysis,

50

FS/L

n.d.

mlks

nd,

Orange 1

2581-69-3

enraclion lollowed by LC/MS analysis.

50

Æ/L

n.d.

møk9

n.d.

Orange 3

730"40-5

enraction fo¡lo@d by LC/MS analysis.

50

us/L

ñ.d.

mg/kg

ñ.d.

Orang6 37l59,ry6

r3301-6r-6

ef¡aclion followed by LC/MS analysìs.

50

!s/L

n.d.

msÂs

n.d.

Red 1

2872-52-A

enracüon follored by LC/MS analysis.

50

Bg/L

nd,

mg/kg

n.d.

2872-48-2

enraction followed by LC/MS analys¡s.

50

udL

n-d-

møks

n¡.

Red 11

Repon No.:17200O138E
Date of Roport:3f /f 0/20f 7
Page l3 of z¡

ORGANIC & INORGANIC ANALYSIS
Sample lD

Factory ll; BANLADESH
Dhaka Region, BANGLADESH

1

Dal6 olsmplingNA

720001388

SmplslD

1720001388

12t1012017

Daleofsamp[ng141ù2017

ZDHC L¡mils

Sampling Localbn
Sampling s6üñe

12:00 PM

Sampling end l¡me
Dal6 of sdph ræetud

NA

Faclory Pertormance

Sañplñg Locahn

SludgoSaßplnq sþdtim6

07:00 PM

06:00 PMSilpÍng end timeNA

1/10Þ017

DaÞ o, silple ræddR¿w

uFcnafgeoWælewater(Dlrect

L¡mil

L¡m¡t

L¡nil

Sample Oðcdptio.

iTEMS

MfHODSCAS No.

Reponhg
Llm¡t

uf,lT

1ù10t2017
Sludgelncomlng

bcohlng

Râw

Wâôtewâbr(Dlrccl

mg/L

mg/L

mg/L

Reponi¡g
Limtr

UNTT

Sludqeolisperse Red 173179€9-3

Solvente{raclion tollowd by LC/MS âñalysb.

50

us/L

n.d.

mgkg

n.d.

lisperse Yellow 1

1

19-15-3

Solvent

efraclion followed by LC/MS añalysis.

50

us/L

n.d.

mg/kg

n.d.

)isperse Yellow 32832-40-8

Solvent e*aclion followed by LC/MS anâlysis.

50

Pg/L

n.d.

mS/kg

n.d.

)ispeße Yellow I

6373-73-s

Solvènle{ractjon followed by LC/MS analysis.

50

pg/L

nd.

mg/kg

n.d-

)isperse Yellow 3912236-29-2

Solvenl exfâction

follored by LC/MS analys¡s.

50

!s/L

n.d.

mS/kS

n.d.

)ispeße Yellow 49

54824"37-2

Solvent eftaclio¡ to¡lowed by LC/MS analysis.

50

ug/L

ñ.d.

mdks

n¡.

lG. Flaæ Ghldànls

59536-65r.elereñce to USEPA 527, USEPA 8270, USEPA
B, ISO 22032 orelvent efracton lollowed by
or LC/MS analysìs

Ës/L

n.d.

mS/kS

n.d.

Penìabromodiphenyl ethers(PenÞ80Ë)

32534-81 -9

reference lo USEPA 527, USEPA 8270, USEPA
B, ISO 22032 or solvent enraction followed by
or LC/MS analysis

vglL

nd,

mg/kg

n.d.

OcÞbromod¡phenyl ethers(OdaaDE)

32536-52-0

relerencE to USEPA 527, USEPA 8270, USEPA
B, BO 22032 or solvenl etaction followed by
or LC/MS añalysß

!s/L

¡.d.

mdks

n.d.

163-1 9-5

relerence to USEPA 527, USÊPA 8270, USEPA
B, ISO 22032 orso¡€nl efraclion lollowed by
or LC/MS úalysis

tglL

n.d.

mg/kg

n.d.

15-96-8

reference to USEPA 527, USEpA 8270, USEPA
B, ISO 22032 or glvent enraction lollowed by
or LC/MS analys¡s

5

ulL

n.d.

møks

n.d.

545-55-1

reference lo USEPA 527, USËPA 8270, USEPA
B, SO 2032 or sol€nt eûâction followed by
LC/MS analysis

5

!s/L

nd.

ñdks

nd.

79-94-7

relerence to USEPA 527, USEPA 8270, USEPA
B, ISO 22032 orsolvent enradioñ lollowed by
LC/MS analysis

ps/L

n.d.

mS/kS

n.d.

Polybrominat€d b¡ph€nyls(PBBs)

Dæabromodiphenyl elhers
lDecaBDE)

1

Iris(2rhloroelhyl) phosphâle
ITcEP)

1

13

Reporl t¡o.: 1 72(þ01 388
Date of Beport:31/10/201?
Pãge 14 of 23

T
I

ORGANIC & INORGANIC ANALYSIS
Sañple lD

Factory ll; BANLADESH
Dhaka Region, BANGLADESH

1

NA

NA

720001388

Smplel01720001388

12h012017Daþofsmplng

1/1ù2017

ZDHC L¡m¡ts

Sampli¡g Localbn
Sampli¡g sldümeÑANA

12:00 PM

Factory Performance

Sañp¡ng Locatbn

SludssSamplng sÞdtiñ€

07:00 PMDaþ ol silpþ rdd

12t10t2017

06:00 PM
Oal€ ol ffplôræêild

Asplbbnål

1ù10P017

NA

L¡mil

L¡m¡t

L¡mil

SludgeCß Nô.

TEMS

MflHODS

134237-50-6,
Hexabrcmoryclododecane(HBCD0)Bis(2,3dib¡omopropyl)phosphate (BlS),5412-25-9

UNIT

hcohlngRaw

u6cnafgeoWætewâter
(Dlrect

hcomlngRawWå5tewaûer

(Dlrccl

mS/L

mg/L

mg/L

Reporting

Liñfr

UNtr

Sl!dgeoú/ith relerence to USEPÂ 527, USEPA 8270, USEPA
3321 B, ISO 22032 orsol@ñl è{radion lollowed by
SC/MS or LC/MS andysis

!s/L

n.d.

mdkg

n.d.

ùvih reference to USEPA 527, usÉPA 8270, USEPA
3321 B, ISO 22032 orsolvent è(radìon lollowed by
3C/MS or LC/MS analysis

t¡g/L

n.d.

møkg

n.d.

tg/L

n.d.

mg/kg

n.d.

pdL

n.d.

mg/kg

ñ.d.

És/L

nd.

mS/kS

n.d.

sg/L

n.d.

mg/kg

n.d.

y'v¡th relerence to USEPA 527, USEPA

Tils(2,3dibromopropyl)
phospharo (TRIS)

2,2-Bis(brom omethyl)-134237-51-7

134237-52-A.
25637-99-4.31%-

Repodlhg
Llmit

126-72-7

1,3-

propamdþl (BgMP)
Trß(l,3lichloro-2-propyl)
phosphare (T0ÕPP)

Shoil Chain Chlorinal€dParall¡ns (SCCP), C,o{1.

3296-90-0

8270, USEPA
33218, ISO 22032 orsolvent e{racl¡on lollowed by
3C/MS or LC/MS analysis

5

ililh reference b USEPA 527, USEPA 8270, USEPA
13218, ISO 22032 orslvent e{ractbn fo¡lowed by
3C/MS or LC/MS ânâlysis¡/ilh reference to USEPA 527, USEPA 8270, UsEpA
13674-47-885535"84-8¡3218, ISO 22032 orsolvent enrætion followed by
3C/MS or LC/MS úalysis¡/ilh reference to USEPA 527, USEPA 8270, USEPA
33218, ISO 22032 or slvent eiraction lollowed by¡C/MS or LC/MS anâlysìs

lH. Glycol¡

11 1"96-6

rôt€renc€ þ USEPA 82700 or solvênl êfrâclion
by GC/MS or LC/MS analys¡s

50

pglL

n.d.

mg/kg

n.d.

10-80-5

relerence lo USEPA 8270D or 60lvent enracuon
by GC/MS or LC/MS analys¡s

50

FøL

n.d.

mg/kg

n.d.

t-15-9reference to USEPA 8270D or solvent eÍraction
by GC/MS or LC/MS a¡alysis

50

fdL

n.d.

mS/kS

n.d.

110-71-4

relerence b USEPA 82700 or solvent eÍraction
byGC/MS or LC/MS analysis

50

!g/L

ñ-d,

mdks

n.d.

109-86-4

relerence ro USEPA 82700 or solvent enracrion
by GC/MS or LC/MS anålys¡s

50

vglL

n.d.

mdks

n-d-

0-49-6

reterence to usÊPA 82700 or solvent etÞctbn
by GC/MS or LC/MS analys¡s

50

tdL

n.d.

mg/kg

o.d.

70657-70-4

reference to USEPA 82700 0f solvent etrætbn
by GC/MS or LC/MS analysis

50

¡s/L

ñ.d.

mdks

ñ.d.

1

acelaleglycol dimelhyl ether

1 1

1 1

14

Repoñ t¡o,:17200013EE
Dete of Repoil:31/10/æ17
Page lS ol 23

ORGANIC & INORGANIC ANALYSIS
Factory ll; BANLADESH
Dhaka Region, BANGLADESH

sample lD

1720001388

Såñpb lD

1720001388

Dal6 oJsanpling

1211012017

Dareofsampling1ù1012017

Sampli¡g Localbn

NA

Sañpling Êrdfm€

NA

ZOHC L¡mits
1230 PM

Sanp¡ñg eñd lime

06:00 PMDaþ ol sampþ @td

1211012017

Factory Performance

Samp¡ng Locatbn

SludgeSampbo sa üm€

07:00 PM

Sampliq end ùñe
L¡ñ¡t

L¡mit

L¡mil

Date o[smpbræeildSample D6cñplbn

sbQe
Dlschargd

TEßuflHoDs

CAS No.

lriethylene glycol d¡methyl elher

112-49-2

ililh referenæ to USEPA 82700 or solvent e*ractioñ
ollowd by GC/MS or LC/MS analys¡s

Repoñl¡lg
Llm¡l

UNIT

1ù102017

lìcom¡ng

RôwWasþwalet(Dlrccl

50

FdL

n.d.

1

tslL

n.d.

pg/L

n.d.

udL

ñ.d.

!dL

n.d.

uEcnârgd
lhcom¡ng
Wâter

Raw

Wastêwaler(Olrect

mg/L

mg/L

mg/L

Rêponjng
L¡mil

UNIT

Sludgeo

mS/kS

n.d.

ll. Halogenâbal soþents

1.2-Dichlo roethâne

107-06-2

Wilh re{erence to USEPA 82608, Purge&Trâp, Headspace or Solvent enraclion follored byGC/MS
analysis75-09-2

With reference lo IJSEPA 82608, Purge&Trap, Headspace or Solvent eÍracl¡on to¡¡owed byGC/MS
anâlysis79-01-6

With relerenæ b IJSEPA 82608, Purgê&T¡ap, Headspæe or SolventeÍraction lollowed by GC/MS
analysis\¡ethylene chloride

IrichloroelhenefeÍâchloroethenê

127-1A-4

Wilh reierence to USEPA 82608, Purge&Trâp, Headspâce or Solvent enÉction follo@d by GC/MS

1

1

I

ânalysis

1

mdkg

1

mdks

n.d.

1

mg/kS

n.d-

1

nS/kg

n.d.

¡J. OEanotlh Compounds

d! and ti-melhyltin

{MMT)

(oMT)

(rMr)

dÈ and lri-butyltin

(MBT)

(DBT)

Multiple

reference to 1SO17353 and dortuatisalion wilh
dielhyl dithiocaòamâb followed by GC/MS

0.01

FdL

n.d.

0.1

mg/kg

n.d-

Multiplerelerencê to 15017353 and dertuatisaìion withd¡ethyl dithiocarbâmâte follored by GC/MS

0.01

!s/L

nd.

0.1

myks

n.d.

Multiple

reference to 1SO17353 and derivatisation with
dielhyl dilhiocarbañate followed by GC/MS

0.01

pdL

ñd,

0.i

møkg

ñ.d.

Mulliplerelerence to lSOl 7353 and derivelisatÞn with
diethyl dithiocaòamate tollo@d by GC/MS

0.01

¡jdL

n.d.

0.1

ñs/ks

n.d.

Multiplerelerence to 1SO17353 and derivâtisation with
dielhyl dlhiocarbamate followed by GC/MS

0.01

pdL

n.d.

0.1

ñdks

n3.

1846-3,78763-54-9

relerence to lSOl 7353 and derivatisllon with
diethyl d¡lhiocarbamale followed by GC/MS

0.01

!s/L

0.1

mS/kS

ñ.d.

1002-53-5

relereñce b lso17353 and derMtisetion wilh
dierhyl dlhiocarbamate ioltowed by GC/MS

0.01

BS/L

0.1

hg/kg

1 1

n.d.

Repo¡l Ì,1o.; l 7200013E8
Date of Report:31/10/2017
Page'15 of æ

Factory ll; BANLADESH
Dhaka Region, BANGLADESH

ORGANIC & INORGANIC ANALYSIS
Sample lD

NA

NADale olsmplinoNASañÞli¡s localbn

NA

Sampling sr4tim6

NA

Sanplng eñd limeDatê of sañpb

rdd

NA

NA

1

720001388

Sdplel01720001388

1U10t2017

Dale ofsâñplng

1/1ù2017

ZDHC L¡m¡ts

Factory Performance

12:00 PMNA

06:00 PMNA

1214t201?

CAS No.

Tr¡buvrin (TBT){MOT)

Dioclyllin (DOT)

Ir¡ocMlin (TOl)

Vlono-, di- and ti-phenyltin
Jorivatives

U0nophenyltin {MPhT)

liphenyltin (DPhT)rrþhenylln (TPhT)

Llñlt

UNIT

hcomlngWaþrRåw

WasLwatêr
(Dlrect

07:00 PM

Unil

L¡m¡l

Deolsmpb r6cåivd

141U2017

Smpb Descnptu.

Sþdse

D6Cnarged

lñcomlng
Wåter

Bat

Wastewaþr
(Dl@ct

mg/L

møL

mdL

Reportjng

Liml

UNfI

SludseO

56573'85-4

Wilh relerence b 1SO17353 anddèrtuatìsation wilh
sodium diethyl dilhiocarbañate iollowd by GC/ttSanålysis.

0.01

uøL

n.d.

0.1

mdkg

n.d.

Multiple

With relerence to 1SO17353 ând derivalisatioñ withsodium dielhyl dithiocarbmate toilowed by GC/MS
analysb.

0.01

us/L

ñ.d.

0.1

mS/kg

ñ.d.

5231-57-9

With reference to tSOl7353 and derivatisal¡on withsodium diethyl df hiocarbamale followed by GC/MS
analysis.

0.01

Fg/L

n.d.

0.1

mS/kS

n.d.

94410-05-6,
1253144.4

Wilh relerence b SO17353 añd dorivatisation wilh
sodium diêlhyl d¡lhiocaóamate followed by GC/MS
anâlysis.

0.01

vglL

n.d.

0.1

mdkg

ñd.

MultiplèWith reference to (SO17353 and dsrivatisation wilh
sodium diethyl dilhiocarbamaþ followsd by GC/I/ISä¡alysis.

0.01

lrglL

n.d.

0.1

mS/ks

n.d,

Mulliple

Wilh reieroncê to 1S017353 and d6rûaliül¡oñ withsodium di€lhyl dilhiocarbâmato follored by GC/MS
analysis.

0.01

so/L

n.d.

0,1

mS/kg

n.d.

lvlultiplê

With ret€rênce þ 1SO17353 and dgrivatisation wilh
sodium dielhyl dithiocarbamate tollowed by GC/ù]Sanalysis.

0.01

ug/L

ñ.d.

0.1

ñg/kg

n.d.

Multiple

With relerence to 15017353 añd derivatisalioñ wilh
sodium di€lhyl dlhiocaÉâñale followed by GC/MS
analysb,

0.01

¡dL

n.d.

0.1

mg/kg

n.d,

With relerence to 6017353 and derivatist¡on úth
sodium diethyl d¡lhiocarbamale lollored by GC/MS
anâlysis.

0.01

Fs/L

nd.

0.1

mdko

n.d,

0.05

mg/kg

n.d.

0.05

mdks

n.d.

0.05

mS/kS

n.d.

0.05

møkg

n.d.

Mono-, d¡- and ai'ocfyltin
derivativês

Monooctyltin

MEIHODSRêpofrlhg

Sþdge

Sâmpliôg sÞn ÍmeSamp¡q end lño

L¡ñ¡t

Dlschatgd
TEre

Sanplng Lo¿abñ

1892"20{,668-34-8¿K. Pelluorin¡þd / PolyfluoÍnatêd Chêm¡oats (pFCs)

1763-23-1

relerence þ D1N38407-42 orôEN/TS 15968 and
by LCMS o¡ LC/MVMS analysis

0.01

!s/L

n.d,

335-67r

relerence þ 01N38407-42 or CENÆS r5968 and
by LCMS or LC/MS/MS analys¡s

0.01

us/L

n.d.

reterence to 01N38407-42 orCEN/TS 15968 and
by LCMS or LC/MS,/MS analysb

0.01

!s/L

n.d.

relerence to 01N38407-42 0r cEN/Ts 15968 and
by LCMS or LC/MS/MS analysis

0.01

uglL

n.d.

375-73-5,5993366-3,29420-49-3,

2942043-3
307-24-4

15

Repon ilo.:172q)013aE
Date of Report:3f /f 0/201?
Page 17 ol æ

Factory ll; BANLADESH
Dhaka Region, BANGLADESH

ORGANIC & INORGANIC ANALYSIS
Smplel0NA1720001388

Dal€ of samplng

NA

1Z1DÞ017

Sampþ lD
Dat€ olNA

Factory Perlormance

12:00 PMSåmpling Ênd l¡meDaþ of smpbræetud

CAS No.

MFHODS

Roponlhg
Llm¡l

UMT

1ù1012017

0600 PMNA

NA

Sañplng Locabñ

SludgeSamp¡ng s6 rim€

07:00 PM

Samplng and tim€

ßpi6bÞl

12102017

L¡ñil

L¡m¡t

L¡mil

Dâþ ol sdpþ ræidSanpb Ðêscdplion

ITEHS

1720001388

ZDHC Lim¡ts

Samplng Loeb¡

Sffipfiñq 66 time

ffpling

121012017S¡udgelhcohlng

Raw

Water

Wastowater

u6cnafgeoWælewater(Dlrcctl¡cohlng

Râw

Wastew¡¡êrWalêrWætewaþr

(DlÞct

mg/L

mg/L

mg/L

Repoding
Limit

UNfl

Sludgeoililh reference to D1N38407-42 orCÊN/TS i5968 and

3r2 FIOH

647-42-7

3:2 FTOH

lerivâl¡satioñ w¡th acelic anhydride lollowèd by GC/MS
rñalysis.

!s/L

n.d.

0.5

mg/kg

n.d.

678-39-7

relerence b 01N38407-42 or CEN/TS 15968 and^/ilhleriw¿iisatlon with acetic anhyd.ide tollowed by GC/MS¡nalysis.

ps/L

n.d-

0.5

mdks

n.d.

117-81-7

retereñce to USEPA €2700, lso 18s56, oreirætion lollowed by GC/MS añalysis

10

us/L

n.d.

mS/kS

n.d.

r 1 7-82-8

reference to USEPA8270D, ISO 18856, o.
eÍråct¡on lol¡owed by GC/MS analysis

t0

!g/L

n.d.

mg/kS

n.d.

117-A4-O

reterenæ lo USÊPA 8270D, ISO 18856, oreffacl¡on tollowod by GC/MS analysis

10

vs/L

ñ.d.

mg/kS

n.d.

referenco to USEpA 8270D, ISO 18956, or
onraction lollowod by GC/MS analysis

10

Fg/L

n.d.

mg/kg

n.d.

6851548-0USÊPA 82700, ¡SO 18856, or
efracl¡on followsd by GC/MS analysis

10

!s/L

n.d.

mg/kg

n.d.

8+75-3

reterence ro USEPA €270D, ISO 19956, or
by GC/MS analysiE

10

us/L

ñ.d.

mg/kg

ñ.d.

a4-74-2

rele¡encê b USEPA 82700, ISO 18856, orf ollowed by GC/MS ânâ¡ysjs

t0

uslL

n.d.

mg/kg

n.d.

85€8-7

relerence b USEPA 8270D, ISO 18856, or
lollowed by GC/MS analysis

10

vslL

n.d.

mdkg

n.d.

84-76-4

reference b USEPA 8270D, ISO 18856, or
followed by GC/MS analysjs

10

telL

n.d.

ms/ks

n.d.

reference b USEPA 8270D, ISO 18856, or€fracl¡on followêd by GC/MS analysis

10

Bs/L

n.d,

mg/kS

n.d,

relerence þ USEPA 8270D, ISO 18856, or
etraction followed by GC/MS añalysis

10

ÉdL

n.d.

mg/kg

n.d.

2L. Phthalales
Hexyl) Phlhalale

Phthalare (DNoP)

Phthalâte (DIDP)

Phthalare (DINP)

Phthalate (DNHP)

Phlhalate (DBP)

Butyl Phthâlate (BBP)

phthalate (DNP)

Phlhalaie (DÊP)

Pht|alale (DPRP)

2676140-0,
6851 5-43-1

28553-12-0,

8+66-2

131-16-8

17

Reporl No.: l72q)01388
Date of RepoÌt:3i/10/2017
Page 18 ot æFactory ll; BANLADESH
Dhaka Region, BANGLADESH

ORGANIC & INORGANIC ANALYSIS
SâmplelD
Dale ofsañplng

NA

str tiñ€r**6d

Sañpb lD

1720001388

1ù108017

Dd€ ol silp[ng1Ù101n17

NA
NA

Samplìng end timeDatê ol smpb

1720001388

ZDHC Lim¡ts

Sanp¡ng Locabñ
Samptrng

NA

NA
NA

NA

12:00 PM

Factory Performance

06:00 PM

Sâmpli¡s Locdbn

StJdgeSamplngs6üña

07100 PM

Sañpfq end ùme&pbrüoml

1211012017

L¡ñ¡t

Limal

Limil

Daþ ot strpb ræoivd

1ù10t2017

Sanpb Oescnphn

Sludgeu6chafgñ
TEMS

CAS No.

)ibo-Buryl Phthalâre (DEP)

84-69-5)icyclohexyl Phlhalate (DCHP)

84-61 -7)i-bo-octyl Phthalate (DÐP)

27554-26-3,2-Beñzenedicâborylic acid, Di"
l7-11 Brânched and Linear\lkyl Eslers (DHNUP)

6851542-4,2-Benzenedicaborylic acìd, 0i,'6-8 Branched Alkyl Eslers, C7ch (DIHP)

71888-89-6

50-32-8

120-12-7,2,3-cdlpyreñe

METHODSilith relerence to USEPA 82700, ISO 19856. oriolwnl enracfion followed byGC/MS analysis
Â/ilh reference to USEPA 82700, tso 18856, orìolvenl enraclloh lollowed byGC/MS ânalysìs
il/ith þÍerence to IJSEPA 8270D, ISO 19956, orÐfuônl onraction followed by GC/MS analysisr'Vith r€fÞrenceb USEPA 82700, ISO 18856, orrolw¡l eñract¡on followâd byGC/MS analysis
82700, lso 18856, or
iolvent efracl¡on followed byGC/MS analysi6,1/irh reterence to usÊPA

referenco lo USEPA 8270, DIN 38407-39 or
lollowed by GC/MS analysis

rÉfarence

Repo¡tlng

Llhll

UNIT

10

Fg/L

10

Råw

Waalilâter

lncomlng
Waler

Raw

Wasleú¡ter(Dlroct

Sludg.o

n.d.

mg/kg

n.d.

udL

n.d.

mg/kg

n.d.

10

!s/L

n.d.

mg/kg

n.d.

10

BdL

n.d.

mS/kS

n.d.

f0

us/L

nd.

mg/kg

n.d.

!g/L

n.d.

mslkg

n.d.

Èg/L

n.d.

mg/kg

n.d.

Wâlor

(DlGctWa6tâwaþr

mg/L

hg/L

Reporting
Limit

UNT

b USEPA 8270, DIN 38407-39 or
lollowed by GC/MS analysis[ìcohlng

mg/L

129-00-0

relerence to IJSÊPA 8270, 0lN 38407-39 or
lollowed by GC/MS a¡alysis

Fs/L

n.d.

mg/kg

n.d.

191 -24-2

relerence to USEPA 8270, 0lN 38407-39 orf ollowed by GC,À¡S analysi6

udL

n.d.

ñdks

n.d.

152-97-2

reference to USEPA 8270, DtN 38407-39 or
lollowed by GC/MS analys¡s

!s/L

n.d.

mg/kg

ñ.d.

193-39-5

reference þ USÊPA 8270, DIN 38407-39 oretâclion lollowed by GC/MS analysis

ps/L

n.d.

mS/kS

n.d.

205-82"3refêrence b USEPA 8270, DIN 38407-39 or
efraclion followed by GC/MS ânalysis

Bg/L

nd,

mg/kg

n.d.

205"9S-2

felereñce to USEPA 8270. DIN 38407-39 0r
efraci¡on lollowèd by GC/MS analysis

tglL

n.d.

mdks

n.d.

18

Rêpon t¡o.:'l 720001348
DåtE of Reporl:3Í/10/2017

Paga t9 ot 23

Factory ll; BANLADESH
Dhaka Region, BANGLADESH

ORGANIC & INORGANIC ANALYSIS
sample lo

1720001388

Sample lD

1720001388

Datê ol sañpling

12108017D¿l€ olsamplng

1410Þ017

ZDHC L¡m¡ts

Sanplng Locatbn
Samp¡ng s6 tim6

NA

Samplng end tiheNA

Dab ol sæpb ræild

12r00 PM

Factory Pelormance

CAS No.

206-4-O

lenzofkìfluoÉnthene

207-08-9

iltrHODS

06:00 PMtuÞlr!üoml

12t1At2ô17

L¡mil

Limil

L¡ñ¡i

>henanthrene{aphlhalene85-01-8R¿w

DECñargd
Weôlewaþr
(Direct

mg/L

mg/L

mg/L

SludgeReponing
Limil

UNTI

Sludgeo

mg/kg

n.d.

Wilh reference to USEPA 9270, DIN 38407-39 or
solwnl eÍrâcl¡on followôd byGC/MS analysis

1

!s/L

n.d.

1

mS/kS

ñ.d.

1

Fg/L

n.d.

I

mS/kg

n.d.

Æ/L

n.d.

1

mg/kg

nd.

tsJL

n.d.

1

mdkg

nd,

udL

ñ.d.

1

mg/kg

n.d.

udL

n.d.

1

mg/kg

n.d.

tgtL

n.d.

mg/kg

n.d.

!s/L

n.d.

hS/kS

nd.

hg/kg

n.d.

Wilh r€ference b IJSEPA 8270, olN 38407-39 or
solwnl efiact¡oñ lollowsd by GC/MS analysis

83-32-9(OlÞcllncomlng
Waler

1

21 8-01-9\cenaphthene

Wâ¡lewâter

1/10t2017

Sañpb Oescdplionn.d.

:hrysene

56-55-3Råw

Dalo of smpþræeild

!s/LWith retôronce to USÊPA 8270, DtN 38407-39 or
solvenl extraclion lollowod by GC/MS analysis

lenzolalañlhraceneUNtrhcohlñg

07100 PM1solvenl elraclon followed byGC/MS analysis

208-96-8

53-70-3

Llmlt

With relerence to USEPA 8270. DtN 38407-39 or{cenaphthylene)ibenz[a,h]anthracenê

Repoilhg

S!dgesÞnilmeSampliDg

Smple D6€nplìon

lrEMS

Sampli¡g Localbn

With relereoce 1o IJSEPA 8270. DIN 38407-39 or

solwntenraction tollowed by GC/MS añalysis

1with relefence to USEPA 8270, DIN 38407-39 0r
solventexraction lollowed by GC/MS analysis
With retereñce to USEPA 8270. DIN 38407-39 or

solwnt enraction followed by GC/MS analy6is
With referênce b USÊPA 8270. DIN 38407"39 orìolwnl eirâclion followed byGC/MS analys¡686-73-7

With relerence b USEPA 8270. DIN 38407-39 or
Ðl@nte{racl¡on lollowed by GC/MS ânalysis

91-20-3ffith relerence to USEPA 8270, DIN 38407-39 or
Ðl@nteiraction followed by GC/MS analyôis

us/L

n.d.

71-43-2

reference lo USEPA 82608, tSO 1 1423-1,
Head-space or So¡€nt efractioñ
by GÕ/MS analysis

ps/L

n.d.

0,1

mg/kg

n.d.

1330-20-7

relereñce to USEPA 82608, ISO 1 1423-1
Head-space or Solvenl eiÉction
byGC/MS analysis

¡siL

n.d.

0.1

ñdks

n.d.

95-48-7

reference to USEPA 92608, USEPA8270D, FO
1423i, Pu¡ge&Trap, Head-space or Solvonl
by GC/MS analys¡s

gs/L

n.d.

0.1

mg/kg

n.d.

1

ll,l. Volât¡le OÌgan¡c Compounds (VOCS)'19

Repoñ l¡o.: 172o(xlt36E
Date ot RepodSl/10/æ17
Page æ ol æ

ORGANIC & INORGANIC ANALYSIS
Factory ll; BANLADESH
Dhaka Region, BANGLADESH

Sâmple lD

NA

Dalô ol sâñp¡ng

NA

Sanplñg Lo€bn

NA

NASamÞ¡ns 6d tìm€

NA

NA

NA

1720001388

Sampb lD

1720m1388

12t108017

De ol smpüng

1210tæ17

ZDHC L¡m¡ts
12r00 PM

Samp¡ng end lim€

NANA

06:00 PMDåþ ol sdpl€ ræefued

NANA

1210n017

Silpl€ D*cdption

NA

Factory Peform¡ñce

Sâmptng Locdbn

Sbdee

sH tiñ6

07:00 PM

SamphgSamp¡q end üñê&plñüoml
L¡m¡r

Llm[

L¡m¡l

D&olsmpb@ôd

1210t2017

Sdpb Desñphn

Studgeoßcnaæo
TETtr¡[flHODSCAS No.

Jvilh relerence b USEPA 8260S, USEPA

105-4-5

Roporth{

I 1423-1, Purge&Trap,

Llmit

ultfT

¡rcohlhg
WaþrR¡wWæHatêa

(Þhecthcomlng
Watsr

Baw

Wâ¡ter¡brl,llaslew¡br

(DlÞd

ñdL

mdL

hdL

Repoding
Limil

UNlr

Sludgeo

8270D, 60

Head-space or Sol€nl

BSÀ

n.d.

0.1

mqks

n.d.

ps/L

n,cl,

0.1

hdks

n.d.

ttraclioñ tollowed by GC/MS analys¡sn-crcsl

1

08-394lvilh rel€rênce þ USEPA 82604, USEPA 8270D, ßOI 1423-1, Purge&Trâp, Head-spæe or Solwnt:taclion followêd by GC/MS anâlys¡sÊo@lks:n.d. = Nol oetoctôd
N.A. = NotâpplicableÔ Sludge ìs reported base on dry ñæs, % moblure = 95.4%

Roporl tlo,: l720lxl1 388
Dat6 ol Roport:31 /l 0/20f 7
Pago 2l ot 23

PIPING PLAN""The piping plan was not provided by the factory**

ü8.

¡grb@Éd,ffisc621

Repon No.: 1720001388
Date of Report:s1/10/2017
Page 22 ol 23

SAMPLING PHOTOSGPS Data: 24"t 7.816' N, 09023.1 88' ESAÍTIPLING LOCATION, CLOSE.UP vlEw

SAÍIIPLING LOCATION, CLOSE.UP VIEWSAÍTIPLING LOCATION, FAR VIEW

SAilPLING I-OCATION, FAR VIEW

22

Report No.: 1720001388
Date ol Reporl:3'1/10/2017
Page 23 of 23

SAMPLING PHOTOSGPS Data:

GPS Data: 24"1 7.046' N, 09023.098' E

SAMPLING LOCATION, CLOSE-UP VIEWSAMPLING LOCATION, CLOSE-UP VIEW

SAIIIPLING LOCATION, FAN VIEW

SaMPL|NG LOCAT|ON, FAR V|EW--. END OF REPORT ""'23

TEST REPORT
fjrl|:t:uÍr

nr:llr¡ilGr
Technical Report(6817)289-0102

October 3 l, 2017

Date Received

October 15,2017

Page I of 17

Factory Company Name:
Factory Address:
Project No.:
Client Reference No.:
Sample Type:

Factory lll, Devision l; BANLADESH
Dhaka Region, BANGLADESH
I00 l) Incoming water - Grab Samples*1002) Discharged Wastewater - Time-Weighted Composite Grab Samples*1003) Sludge - Grab Samples*

Sample Pick Up Date:
Discharge Type:
Wastewater Discharge to:
On-Site Effluent Treatment Plant (ETP)
Test Period:

October 15,2017
Direct Discharge
Factory Owned ETP
Yes

October 16,2017 To October 31,2017

Sample Description:I00l) Incoming water
1002) Discharged Waste \¡r'ater
1003) Sludge

REMARK
Ifthere are questions or concerns on this report, please contact the following persons:General enquiry

Mr. Abu Hanif. Mail: abu.hanif@bd.bureauveritas.com

Invoicing

Mr. Mahabubur Rahman, Mail: mahabubur.rahman@bd.bureauveritas.com

Technical enquiry-Chemical

Mr. M. Nur Alam, Mail: nur.alam@bd.bureauveritas.com

This report shown the test result of the auxiliary chemical and/or raw material samples, which collected during particular factory
audit. The results ofthis report shall not be used for any regulatory compliance purposes.

* The sampling is agreed with client.

BIJREAUVERJTASCONSUMER PRODUCTS SERVICES ( BANGLADESH ) LTD.

M.NURALAMSENIORMANAGER
AÀ{ALYTICAL LABORATORY

Prepared By:

Md. Abu Taher

Bureau Veritas
Consumer Products Services {BD) Ltd.
Plot # 130, DEPZ Extcnsion Area
Ganakbari. Savar. Dhaka. Bangladesh'l'el : 88-02-770 I 4 64 -{>. F ax:

88-02-7 7 0 I 463

Etail: bvcps.bd(@bd.bu¡eauveritas.cour
website: cps.burcauveritas.corn
The content ofthis PDF ñle is in accordåûce wilh lhe original ßsued repols for rcfsencc only.
This Tcsl Repon cannot be reproduced, except in fu¡1, withoüt p¡iorwillen pemission oflhe company.

@

EI!trEIT@IE

Technical Report:(6817)289-0102
October 3 1, 20 l 7
Page2 of 17

Photo of the Samnle/ Sampling LocationI00l) Incoming water

1002) Discharged WastewaterI003) Sludge

The conlent oflhis PDF filc ¡s in accorda¡cc wilh the original issued repofs for refercnce only.
This Test Repon cannot be reproduced, exccpl in full, without prior w¡tten petrission ofthe company.

ffià

w

EüEL
@¡ñ

Technical Report:(6817)289-0r02
October 3 l, 20l 7
Page 3 of 17

Executive Summarv
I A) Conventional Parameters

r001

I002

I003

Temperature
TSS

coD
pH Value
Color [m-rl

NA

BODs

See result in page
5-7

NA

Total-PAOX
Oil and Grease
FoamlB) Conventional Parameters -METALS

a

o

o

ZDHC MRSL Substances

I001

r002

r003

2A) APs and APEOs

NT

o

o

2B) Chlorobenzenes and Chlorotoluenes

NT

o

o

2C) Chlorophenols

NT

o

o

2D) Azo Dyes

o

o

a

2E) Carcinogenic Dyes

NT

o

o

2F) Disperse Dyes

NT

o

o

2G) Flame Retardants

NT

o

o

2H) Glycols

NT

o

o

2I) Halogenated Solvents

NT

o

o

2J) Organotin Compounds

NT

o

o

2K) Perfluorinated and Polyfluorinated Chemicals

NT

o

o

2L) Phthalates
2M) Poly Aromatic Hydrocarbons

NT

o

o

NT

o

o

2N) Volatile Organic Compounds

NT

ô

o

Note / Key¡ - Detectedo - Not Detected

NT - Not Tested

NA- Not Applicable

The conlent oflhis PDF file is in accordance with thc original issued repols for refscncc only.
This Tcst Repol cannot be reprcduccd, cxcept in full, withoul priorwittcn pemission oflhc compãny.

ffià

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Technical Report:(6817)289-0102
October 3 1, 20 I 7
Page 4 of 17

Obiective
The environment samples were tested for below parameters.

lA) Conventional ParameterslB) Conventional Parameters - METALS

2A) APs and APEOs

28) Chlorobenzenes and Chlorotoluenes
2C) Chlorophenols
2D) Azo Dyes
2E) Carcinogenic Dyes
2F) Disperse Dyes
2G) Flame Retardants
2H) Glycols
2I) Halogenated Solvents
2J) Organotin Compounds
2K) Perfluorinated and Polyfluorinated Chemicals
2L) Phthalates
2M) Poly Aromatic Hydrocarbons
2N) Volatile Organic Compounds

Samnlins Plan
Basically, three environment samples were sampled per factory, including l) Incoming water; 2) Discharged Wastewater and3) Sludge. Total number ofsample collected will be depended on the actual factory facilities and manufacturing processes.

Msthod of sampling used is time-weighted composite grab samples (agreed with client.). Composite sampling shall be
performed for no less than six hours, with no more than one hour between discrete samples. Each discrete sample shall be ofequal volume. Wastewater and freshwater samples should, as much as possible, be collected simultaneously, during the timethat PU is in normal operation. The sampling shall aim to analyse the snapshot of water quality characteristics of theoperating PU. Under no circumstance shall samples be taken during times when the production process is not running or thewastewater is diluted due to heavy rainfall, etc.

RemarkSampling procedure is with reference to below standards:
1) South Australia EPA Guidelines (June 2007), Regulatory Monitoring and Testing Water and Wastewater
Sampling.
2) Australia EPA (Victoria) Guideline (June 2009), Sampling and Analysis of Waters, Wastewaters, Soils
and Wastes.

3) ISO 5667-3:2003, Water Quality - Sampling - Part 3: Guidance on the Preservation and Handling of
Water Samples.
4) ASTM D3976-92 (Reapproved 2010), Standard Practice for Preparation of Sediment Samples for
Chemical Analysis.
Field data records are attached in Appendix B.

The contenl ofthis PDF file is iû âccordance with lhe originrl issued repols for refs€nce only.
This Test Repon camot be reprcduced, excepl in full, without priorwritlcn pemissior oflhe compåny.

@¡if]liÌtltr
gÐg

Technical Report:(6817)28e-0102
October 31, 2017
Page 5 of 17

Test ResultlA) Conventional Parameters
Temperature

Test Method:

Measurement by thermometer

Tested ltem(s)Result

Unit

Conclusion

t002

31.5 (Foundational)

deg. C

DATA

Note:deg. C: degree Celsius ('C)

FoundationalLimit: Al5 /max.3í"C;ProgressiveLimit: 410/max.30oC; AspirationalLimit: A5 lmax.25"C

Total Susoended Solids (TSS)
Test Method:

Reference to APHA 22nd Edition-2540D & ALPA 2540D

Tested Item(s)Result

Unit

Conclusiont002

2l lFoundational)

ms/L

DATA

Note:
mg/L : milligram per liter
Foundational Limit: 50 mg/L; Progressive Limit: 15 mg/L; Aspirational Limit: 5 mg/L

Chemical Ox]¡gen Demand (COD)
Test Method:

Reference to ALPA 52208 & EPA 410.3

Tested Item(s)Result

Unit

Conclusion

1002

96 ßoundational)

ms/L

DATA

Note:
mg/L = milligram per liter
Foundational Limit: 150 mg/L; Progressive Limit: 80 mg/L; Aspirational Limit:40 mg/L

Thc contentofthis PDF file is in accordancc with thc original issued rcpots forrefqence only.

ThisTest Repot cannot beæprcduced, cxcept in full, without prior Mittcn pemission oflhe company.

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Technical Repof:(6817)28e-0102
October 3 l, 2017
Page 6 of 17

oH Value:

Test Method

Reference to ALPA 4500-H+B & EPAI50.2

Unit

Result

Test ltemls)

1002

Parameter
Temp. of sample

25

des. CpH value ofsample

6.9

DATA

Conclusion
Note:

Temp.: Temperaturedeg. C: degree Celsius ("C)

Limit: 6 - 9

Color [m-t] (436nm: 525:620nm)
Test

Method: ISO 7887: 2011(E), B

Tested Item(s)Parameter
Trial (À:436 nm)
Trial (1"=525 nm)
Trial (I:620 nm)

1002

DH

Result

Unit

Conclusion

6.8

1.5 (Asoirational)

m-r

6.8

0.7 (Aspirational)

m-l

6.8

0.2 (Aspirational)

m-l

DATA
DATA
DATA

Note:
Foundational Limit: 7;5;3 m-r; Progressive Limit: 5;3;2 m-r; Aspirational Limit: 2;1;l m-t

Biochemical Oxygen Demand (BODs)
Test Method:

Reference to APHA 22nd Edition-52108 & ALPA 52108

Tested ltem(s)Result

Unit

Conclusion

r002

14 (Progressive)

rns/L

DATA

Note:

mg/L: milligram per liter
Foundational Limit: 30 mg/L; Progressive Limit: l5 mg/L; Aspirational Limit: 5 mg/L

Thc content ofthis PDF file is in accordsnce wilh th€ original isßued repofls for rcferencc only.

ThisTesl RepoÍ cannot be rcprcducc4 except in full, wilhout prior wilten pemission oflhc company.

ffià

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l:Ífìr:üÍr
gf,¡E
Technical Report:(68rÐ289-0r02
October 3 l, 2017
Page 7 of 17

Total Phosphorus lTotal-P)
Test Method:

Reference to APHA 22"d Edition -4500-P.E (2012)

Tested ltemfs)

Result

Unit

Conclusion

t002

0.2677 (Progressive)

fJ:lP/L

DATA

Note:

mg/L = milligram per liter
Foundational Limit: 3 mg/L; Progressive Limit: 0.5 mg/L; Aspirational Limit: 0.1 mlL

Adsorbable Oreanic Haloeen (AOX)
Test Method:

Reference to HJÆ 83

Tested ltem(s)Result

Unit

Conclusiont002

L60 (Foundational)

rnq/L

DATA

Note:

mg/L: milligram per liter
Foundational Limit: 5 mg/L; Progressive Limit: I mg/L; Aspirational Limit: 0.1 mg/L

Oil and Grease
Reference to APHA 22nd Edition -55208 Q0I2)

Test Method
Tested Item(s)Result

Unit

Conclusion

t002

5 ßoundational)

ms/L

DATA

Note:

mg/L: milligram per liter
Foundational Limit: 10 mg/L; Progressive Limit 2 mglL; Aspirational Limit: 0.5 mg/L

Foam

Test Method:

VisualTested Item(s)Resultr002

No Foam

Unit

Conclusion

DATA

The conlenl oflhis PDF file is in åccordance wilh th€ origiúål issued repols for rcferc¡cconly.
ThisTesl Repol cannol be reprcduced, cxccpt in full, wilhoul priorwitten pemission oflhc compåny.

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l:rlrir:ilr¡@¡E
Technical Report:(6817)289-0102
October 3 l, 201 7
Page 8 of 17

I B) Conventional

Parameters - METALSHeaw Metals
Antimony( Sb )Foundalional Limit: 0.1 mg/L;
Progressive Limit: 0.05 ng/L;
Aspirational Límit : 0.0 I ms/L

Chromium( Cr ), total
Foundalional Limít: 0.2 mg/L;
Progressive Limit: 0.1 mg/L;
Asoírational Limit: 0.05 mø/L
Cobalt( Co )Foundalional Limit: 0.05 mg/L,
Progressive Limit: 0.02 ng/L;
Aspirational Límit: 0.01 ms/L
Copper( Cu )Foundational Limit: I mg/L;
Progressive Limit: 0.5 mg/L;
Aspiralional Límit: 0.25 ms/L

l00l (ms/L)

1002 (ms/L)

ND

ND(Aspirational)(Aspirational)

0.00s(Aspirational)

0.007(Aspirational)

ND

ND(Aspirational)(Aspirational)

0.030

0.045

(Aspirational)(Aspirational)

ND

0.002
(Aspirational)

lOO3 (mo/ks)

N/A

Nickel (Ni)Foundalíonal Limit: 0.2 mg/L;
Progressive Limit: 0.1 mg/L;
Aspirational Limit: 0.05 ms/L
Silver (Ag)Foundational Limit: 0.1 mg/L;
Progressive

Limit: 0.05 ng/L;(Aspirational)

ND

ND(Aspirational)(Aspirational)

Nf)

0.213
(Aspirational)

Asoirationql Limit: 0.005 mø/L

Zinc(Z¡)
Foundational Limit: 5 mg/L;
Progressive Limit: I mg/L;
Aspirational Limit: 0.5 mp/L
Arsenic (As)Foundational Limit: 0.05 mg/L;
Progressive Limit: 0.01 mg/L;
Aspirational Limit: 0.005 ns/L
Cadmium( Cd )Foundatíonal Limit: 0.1 mg/L;
Progressive Limit: 0.05 mg/L;
Aspirational Limit: 0.01 ms/L

(Aspirational)

0.001

ND

ND

(Aspirational)(Aspirational)(Aspirational)

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

Lead( Pb )Foundational Limit : 0. I mg/L;
Progressíve Limit: 0.05 mg/L;
Asoírational Limit: 0.01 ms/L
Mercury (Hg)
Foundational Limit: 0.01 mg/L,
Progressíve Límit: 0.005 mg/L;
Aspirational Limít: 0.001 mp/L
Chromium VI( CrVI )Foundational Limit: 0.05 mg/L:
Progressive Limit: 0.005 mg/L;
Aspirational Limit: 0.001 ms/L
Cyanide( CN)
Foundational Limit: 0.2 mg/L;
Progressive Limit: 0.1 mg/L;
Aspirational Limit: 0.05 mø/L

ND

0.005

ND

(Aspirational)(Aspirational)(Aspirational)

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

The conlenl oflhis PDF filc is in accordancc wilh the original issucd repofs for refcrence

onliThis Test Repoñ cannot be reproduced, cxcept in full, without priorwilten pemission ofthe company.

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Technical Report:(68rÐ28e-0102
October 3 l, 2017
Page 9 of l7

2D) Azo Dves
Azo Dves
4,4' -Methylene-bis-(2-chloro-aniline)

lî07 luø/L)1002 (us/L)

ND
ND
ND
ND
ND
ND
ND
ND

4,4'-methylenedianiline

ND
ND

4.4'-Oxvdianiline

ND

4-Chloroaniline
3,3' -Dimethoxybenzidine
3,3' -Dimethylbenzidine
6-methoxy-m-toluidine (p-Cresidine)
2.4.5-Trimethvlaniline
4,4'-Thiodianiline

NT)

4-Aminoazobenzene

4-Methoxy-m-phenylenediamine
4.4' -Methvlene-di-o-toluidine

2,6-Xylidine
o-Anisidine
2-Naphthylamine
3.3'-Dichlorobenzidine
4-Aminodiohenvl
Benzidineo-Toluidine

2,4-Xylidine
4-Chloro-o-toluidine
4-Methvl-m-ohenvlenediamineo-Aminoazotoluene
5-nitro-o-toluidine

ND
ND
ND
NT)

ND
ND
ND
ND
ND

ND
ND
ND
ND
ND
ND
ND

Nf)
ND
ND
ND

Nf)

1003 (ms/ke)
NT)

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

ND

ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

ND
ND

I001

r002

I003

NT
NT
NT
NT
NT
NT
NT
NT
NT

NI)
ND
ND
ND
ND
ND
ND
ND
ND

ND
ND
ND

ND

NT

ND

Nf)

NT

ND
ND
ND

ND
ND
ND

NT)

ND
ND

NT)

ND
ND
ND
0.4

Others Priority Chemical Groups

2A) APs and APEOs
2B) Chlorobenzenes and Chlorotoluenes
2C) Chlorophenols
2E) Carcinoeenic Dves
2F) Disperse Dves
2G) Flame Ret¿rdants
2H) Glycols2l) Halogenated Solvents
2J) Orsanotin Comoounds

2K) Perfluorinated and PolyfluorinatedChemicals

2L) Phthalates
2M) Polv Aromatic Hvdrocarbons
2N) Volatile Orsanic Comnounds

NT
NT

ND

ND
ND
ND
ND

Remark t
Test method, reporting limit and list of chemical are summarized in tables of Appendix A.
ND = Not detected (Please refer to reporting limit shown in Appendix A.).
ppb: part(s) per billion.
NT = Not Tested

The content oflhis PDF lìlc is in a€ordance with the original issucd repots for rcfscncconly.
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Grlrrr|t!Ìtitr¡tr
Technical Report:(68r7)289-0102
October 3 l, 2017
Page l0 of 17

sss

APPENDIXA
Report LimitGroup

Substance (Testing
parameter)

CAS No.

Wastewater(ug/L)/(

Sludge(mg/kg)Name of the testing
method''(ppnÐ

Various (incl. 140-66-9,
1806 -26 4, 2'7 t93 -28-8)

50.2

Nonylphenol NP

Various (incl. 104-40-5,| 1066-49 -2, 2s I s 4 -52-3,
848s2- I s-3)

50.2

Nonylphenol Ethoxylates
OPEO (2-16)

Various (incl. 9002-93 - |9036-t9 -5, 68987-90-6)50.2Octylphenol OP, mixed
isomers

24. Alkylphenol(AP) andAlkylphenol
Ethoxylates(APEOs): including

all isomers

and Chlorotoluenes

2C. Chlorophenols

LCII{S(-MS)
OPEO/NPEO:

ISOl8857-2 or ASTM
D7065(LC/MS; GC/MS

Various (inc. 9016-45-9,

Nonylphenol Ethoxylates
NPEO (2-r8)

26027 -38 -3, 37 20 5 -87 - t,

Chlorobenzenel 08-90-7

Dichlorobenzene
Trichlorobenzene

Various
Various
Various

Tetrachlorobenzene
1,2-Dichlorobenzene
1.3-Dichlorobenzene

28. Chlorobenzenes

NP/OP: ISO 18857-2(modifieddichloromethane
extraction) or ASTM
D7065 (GC/MS or

0.2
0.2
0.2
0.2
0.2
0.2
0.2
o.2
0.2
0.2

0.1

684 12-5 4 - 4, 127 087 -87 -0)

95-50-ls4t-73-t

I .4-Dichlorobenzene

106-46-7

1,2,3 -Trichlorobenzene

8'7-6t-6

1,2,4-Trichlorobenzene
1.3.5-Trichlorobenzene
1.2.3.4-Tetrachlorobenzene
1.2.3.5-Tetr¿clorobenzene
1,2.4.5-Tetrachlorobenzene
Pentachlorobenzene
Hexachlorobenzene

t20-82-1

2-Chlorotoluene
3-Chlorotoluene
4-Chlorotoluene
2,3-Dichlorotoluene
2.4-Dichlorotoluene
2.5-Dichlorotoluene
2.6-Dichlorotoluene
3,4-Dichlorotoluene
3,5-Dichlorotoluene
2.3.4-Trichlorotoluene
2.3.6-Trichlorotoluene
2.4.5-Trichlorotoluene
2,4,6-Trichlorotoluene
3,4,5 -Trichlorotoluene
2-3 -4-5 -Tetrachlorotoluene
2.3.5.6-Tetrachlorotoluene
2.3.4.6-Tetrachlorotoluene

50.2

I 08-70-3

634-66-2
634-90-2
95-94-3
608-93-5

tt98-74-t
9s49-8
I 08-4 I -8

106-43-4
32768-54-0
9s-73-8
I 9398-6 l -9
1 I 8-69-4
95-75-0
25186-47-4
7359-72-O

2077-46-5

6639-30-l
23749-65-',l214'72-86-6
7605',7-12-O

29733-',70-8

87s-40-l

Pentachlorotoluene

877-n-22-Chlorophenol
3-Chloronhenol
4-Chloroohenol

95-57 -8
I 08-43-0

106-48-9

or LC/MSMS for
n=\,2)APEO l-18
0.1
0.1
0.1

0.t
0.1
0.1
0.1
0.1
0.1

0.2
0.2
0.2
0.2
0.2

0.1

0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.5
0.5
0.5

0.1

0.1
0.1

0.i
0.1
0.1
0.1
0.1
0.1

USEPA 82608,8270D.
Dichloromethane
extraction followed by
GC,{\4S

0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1

0.02s
0.02s
0.025

USEPA 8270 D
Solvent extraction,
derivatisation withThc conle¡l ofthis PDF lilc ¡s in accordåncc with the originål issued rcpols for referencc only.
This Tesl Repod cånnot bc rcproduccd, cxcept in full, wilhout prior willen pemission ofthe company.

@

GT!trET!I@IEI

Technical Report:(6817)289-0102
October 3 l, 2017
Page I 1 of 17

Report Linrit
Group

Substance (Testing
parameter)

CAS No.

Wastewater(uei L)/(

2.3-Dichloroohenol
2,4-Dichlorophenol
2.5-Dichloronhenol
2.6-Dichloroohenol
3.4-Dichlorophenol
3,5-Dichlorophenol
2.3-4-Trichloronhenol
2.3.5 -Trichloronhenol
2.3.6-Trichloronhenol
2.4.5 -Trichloroohenol
2.4.6-Trichloronhenol
3.4.5-Trichloronhenol
2.3.4.5-Tetrachloroohenol
2.3.4.6-Tetrachloroohenol
2,3,5,6-Tetrachlorophenol
Pentachloronhenol IPCPI
Tetrachlorophenol (TeCP)
4,4' -Methylene-bis-(2-chloro-aniline)
4,4'-methvlenedianiline

0.5

0.025

I 0 I -14-4

0.1

0.1

I 5950-66-0

933-78-8
933-75-5

95-95488-06-2
609- I 9-8
4901-s l -3

s8-90-2

0.025
0.025
0.025

0.025
0.025
0.025

0.025
0.025

0.1
0.1

4-Chloroaniline
3.3' -Dimethoxvbenzidine
3,3' -Dimethvlbenzidine
6-methoxy-m-toluidine (pCrssidine)
2.4.5 -Trimethvlaniline

to6-4'7-8

0.1

0.1

I I 9-90-4

0.1

0.1

tt9-93-7

0.1

0.1

120-'71-8

0.1

0.1

137 -17 -7

0.1

0.1

139-65-l
60-09-3

0.1
0.1

0.1
0.1

6 I s-0s-4

0.1

0.1

838-88-0

0.1

0.1

87-62-7
90-04-0
9 I -s9-8

0.1

0.1

0.1

0.1

0.1

0.1

9t-94-l

0.1

0.1

92-67-l0.1

4,4'-Methylene-d!otoluidine

92-87-5

0.1

0.1

95-5340.1

0.1

9s-68-1
95-69-2

0.1

0.1

0.1

0.1

phenvlenediamine

95-80-70.1

0.t

o-Aminoazotoluene
5-nitro-o-toluidine
C.I. Direct Black 38
C.I. Direct Blue 6
C.l. Acid Red 26

97-56-3
99-ss-8

0.1

0.1

0.1

0.1

1937 -37 -7

500

2602-46-2
3761-s3-3
569-61-9
573-58-0
632-99-5
247s-45-8s00
s00

4-Chloro-o-toluidine

4-Methyl-m-

C.l. Basic Red 9
C.l. Direct Red 28
C.I. Basic Violet l4
C.I. Disoerse Blue I

500
500
500
500

followed by GC/MS

0.02s
0.025

0.1

4-Aminoazobenzene
4-Methoxy-mnhenvlenediamine

KOH, acetic anhydride

0.02s

0.1

2.4-Xvlidine

Equivalent Concem

Various (incl. 25 167 -83 -3)

59 l-35-5

101-80-4o-Anisidine
2-Naohthvlamine
3,3' -Dichlorobenzidine
4-Aminodiphenyl
Benzidineo-Toluidine

Carcionogenic or

935-95-5
87-86-5

95-77 -2

Nanre ol'the testing
method

0.02s
0.025
0.025

t0t-77 -9

2.6-Xvlidine

28. Dyes-

0.025
0.025

0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5

4,4'-Oxydianiline

4,4'-Thiodianiline

2D. Dyes - Azo(Forming Restricted
Amines)576-24-9
t20-83-2
s83-78-8
87-65-0

Sludge(mg/kg)/(ppm¡EN 14362.
Reduction step with
Sodiumdithionite,solvent extraction,
GC/MS or LC/MS

Liquid Extraction
LCIMS

Thc contenl ofthis PDF file is in âccordan€e with lhe original issued repofs for refereûce only.
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@Technical Repof:(6817)289-0102
October 3 l, 20l7
Page 12 of l7

Report Linrit
Group

Substance (Testing
parame¿er)rilaste\Ã

CAS No.

ater(ugr¡¡7,247s-46-9

500I(withMichler's Ketone >0.lo/.\

2580-56-5

500I

569-64-2

500I

243'7-29-8500It0309-9s-2

500I82-28-0500I

I 19-15-35012222-97-8
12223-01-7

50
50
50
50
50
50
50
50
50
50
50
50
50
50
50

I
I
I
I

(sensitizing)

Disperse Yellow I
Disperse Blue 102
Disperse Blue 106
Disnerse Yellow 39
Disoerse Oranpe 37 I 59/7 6
Disperse Brown I
Disoerse Oranse I
Disperse Yellow 3
Disoerse Red I I
Disperse Red I
Disperse Red l7

Dispene Blue 7
Disoerse Blue 26
Disperse Yellow 49
Disperse Blue 35
Disperse Blue 124
Disperse Yellow 9
Disoerse Oranse 3
Disperse Blue 35

Tris(2-chloroethyl)ohosohate ITCEP)
Decabromodiphenyl ether(DecaBDEl

I 3301 -61 -6

233ss-64-8
258 I -69-3

2832-40-8
2872-48-2
2872-52-8
3r79-89-3

3t79-90-6
3860-63-7

54824-37-2
12222-75-2

6t951-5t-7
6373-73-s
730-40-55056524-77-7

5050

l i 5-96-8

5

I

I

I
I
I
I
I
1

I

I
I

I
I
I

tt63-19-5

5

t26-72-7

5

Pentabromodiphenyl ether(PentaBDE)

32534-8t-95Octabromodiphenyl ether(OctaBDE)

32s36-s2-0

5I

s4t2-25-9

5

I

545-55-1

5I

s9536-6s-l

5I

79-94-7

5I(HBCDD)

3t94-55-6

5I

2,2-Bis(bromomethyl)- 1,3propanediol ßBMP)3296-90-0

5I

Tris( 1,3-dichloroisopropvl) þhosohate

t3674-87-8

5Iohosohate IBIS/BDBPP)

Tris(aziridinyl)nhosohineoxide ITEPA)

Polybromobiphenyls
IPBBs)
Tetrabromobisphenol A(TBBPA)Hexabromocyclododecane

Liquid Extraction
LCIMS

1

Tris(2,3 -dibromopropyl)
phosphate 0RIS/TDBPP)

Bis(2,3-dibromopropyl)
2G. Flame
Retardants

12236-29-2

Name of'the testrng
method1(ppm)

C.I. Disperse Blue 3
C.l. Basic Btue 26

C.I. Basic Green
4lmalachite sreen chlorideì
C.I. Basic Green 4lmalachite øreen oxalatel
C.I. Basic Green
4(malachite ereen)
Disperse Orange I I

2F. Dyes-disperse

Sludgc'(nrgrkg)

TSO22032, USEPA527
and USEPA832lB.

Dichloromethane
extraction GC/MS or
LCll\4S(-MS)

The conlenl ofthis PDF filc is in accordancc wilh the original issucd repofs for reference only.
This Test Repon cannot bc rcproduced, except in full, without prior Mitcn pemission ofthe comparl

@

GIIEETII

EIETechnical Report:(6817)289-0102
October 31, 2017
Page 13 of 17

Report Lirnit
Group

Substance (Testing
paramstsr)

CAS No.

Waslewater(ug/L)/(

Sludge(mg/kg)Name of the testing
method1(ppm)ITDCP)
Short chain chlorinatedparaffins (SCCPs)
Bis12-methoxvethvl)-ether

2H. Glycols

8ss3s-84-8

5

I I I -96-6
I l0-80-s

50

5

I 1 l-15-9

50
50

5

lt0-7l-450

52-methoxyethanol

109-86-4

2-methoxvethvlacetate

tt0-49-6

5
5

2-methoxvoroovlacetate
Triethylene glycol dimethyl70657 -70-4

50
50
50

tt2-49-2

50

5

107-06-2
75-09-2
79-01-6
127-t8-4
Various (incl. 993-16-8,

I
I

I

I
I
I

I

I

0.01

0.1

0.01

0.1

2-ethoxvethanol
2-ethoxyethvl acetate
Ethylene glycol dimethyl
ether

ether
I .2-Dichloroethane

2I. HalogenatedSolvents

Methylene Chloride
Trichloroethylene
Tetrachloroethvlene
Mono-, di and trimethvltin derivatives

7s3-73-t. I 066-4s-l)

5

US EPA 8270
Liquid Extraction

LC/MS

5

USEPA 82608
Headspace GC/MS or
Purgeand-Trap-GCA4S

Various (incl. 7 87 63 -54 -9,
Mono-, di- and tri-butyltin
derivatives

l r l8-46-3, 1002-53-5,
683- 18- 1 , 36&3-28-4,
5657 3 -85-4. 1461 -22-9\

2J. Organotin
Compounds

Mono-, di- and tri-phenyltin
derivatives

Mono-, di- and tri-octyltin
derivatives
Perfl uorooctanesulfonicacid (PFOS)

2K. Perfluorinatedand PolyfluorinatedChemicals (PFCs)

2L. Phthalates(including all otheresthers of phthalicacid)

Perfluoro-n-octanoic acid
IPFOA)
Perfl uorobutanesulfonicacid IPFBS)
Perfl uoro-n-hexanoic acid
IPFHxA)
8:2 FTOH
6:2 FTOH
Di-2-ethylhexyl phthalate
IDEHP)
Dimethoxyethyl phthalate
IDMEP)
Di-n-octyl phthalate
IDNOP)
Di-iso-decyl phthalate(DIDP)
Di-iso-nonyl phthalate(DINP)
Dì-n-hexyl phthalate(DnHP)
Dibutvl nhthalate IDBP)

Various (l 124-19-2,
101 1-95-6, 638t-06-2,
tt3s-99-s, 892-20-6,
639-58-7. 668-34-8)
Various (incl. 15231-44-4,
309 1 -25 -6, 944 t0 -0s -6,
3542-36-7 ,869-59-0,
2s87-76-0)

rso 17353
Derivatisation with
NaB(C2H5) GC,MS

0.01

0.1

0.01

0.1

3s5-46-4 ,432-s0-7

0.01

0.0s

335-6'7-U 335-95-5

0.01

0.05

29420-49-3, 2942043-3

0.01

0.05

301-24-4

0.01

0.05

678-39-7

647-42-7

I
I

0.5
0.5

I t7 -8t -7

l0I

I 17-82-8

l0I

I l7-84-0

l0

I

US EPA 8270D, ISO

26761-40-0

t0IDichloromethane
extraction GC/MS

28553-t2-0l0I84-75-3l0I

84-74-2

l0

I

DrN 38407-42(modified)
Ionic PFC:
Concentration or direct
injection, LC/MS(MS);Non-ionic PFC(FTOH): derivatisation

with acetic anhydride,
followed by GC/MS

I 8856The content ofthis PDF file is in accordancc with thc original issucd repols for rcfcrence only.
This Tcsl Rcpot cannot bc rcproduced, cxcept in full, withoul prior Mitien pcmission ofthe compâny.

@

EII TTI
gn¡ÍT
Technical Report:(6817)289-0102
October 3 1, 201 7
Page 14 of I 7

Report Limit(ìroupSubstance (Testing
parâmeteÐ

CAS )'lo.

Wasteu'ater(ugr¡¡4
Butyl benzyl phthalate

Sludge(mgikg)i(ppm)

8s-68-7l0

84-764t0

84-66-2l0

I 3 l -16-8

10(DIBP)

84-69-5l0Di-cyclohexyl phthalate(DCHP)

84-61-7l0

Di-iso-octyl phthalate(DIOP)

27ss4-26-3

l0I

68s1s-42-4

10I

7 l 888-89-6

l0

I

ßBP)
Dinonvl ohthalate (DNP)
Diethvl phthalate (DEP)
Di-n-propyl phthalate(DPRP)

Di-iso-butyl phthalate

1,2-benzenedicarboxylicacid, di-C7- I l-branched
and linearalkyl esters

Nanre o1'thr'testingn'ìethod(DHNUP)
1,2-benzenedicarboxylicacid, di-C6-8-branchedalkyl esters, C7-rich

IDIHP'I
Benzolalovrene lBaP)

2M. Poly Aromatic
Hydrocarbons(PaHs)

50-32-8I

I

Anthracene
Pyrene120-t2-7
129-00-0

I
I

I
I

BenzoIshilnervlene
Benzolelovrene

t9t-24-2

II

192-97-2

Indenol 1.2.3-cd.ìowene

I 93-39-5

I
I

I

BenzoIilfluoranthene
BenzoIblfluoranthene205-82-3
205-99-2
206-44-0
207-08-9

I

1

I

I

I

I

I
I

I

Fluoranthene

Benzolklfluoranthene
Acenaphthvlene
Chrysene
Dibenzla,h.lanth¡acene

Benzolalanthracene
Acenaphthene
Phenanthrene
Fluorene
Naphthalene
Benzene208-96-8

218-0i-9
53-70-3
56-55-3

I
I

I

I

I

8s-0 I -8
86-73-7II

9t-20-3

Xvlene1330-20-7

o-cresol9548-7(VoCs)

Þ-cresol

to6-44-5I

m-cresol

108-39-4

Total-NlA. Conventional
Parameters

pH
Color Im-r] (436nm;
525nm;620nm)
BOD5
Ammonium-N
Total-P

7t43-2

DrN 38407-39
Solvent extraction
GC/MS

I

83-32-92N. Volatile
Organic Compound

coD

I
I

I

I
I
I
I

Temnerature
TSS

I

1

I
I
0.1
0.1

ISO 11423-1

0.1

Headspace- or Purge-

0.1

and-Trap-GC/MS

i

0.1

N/A
N/A
N/A
N/A
N/A

N/A
N/A
N/A
N/A
N/A

N/A

N/A

N/A
N/A
N/A

N/A
N/A

N/A

Apply the standard
methods that best apply
to the region (ISO, EU,
US, China), please refer
toZDHC Wastewater
Guidelines for moredetails on the testing
method and the levels(Exceeded Foundational
Limit, Foundational,

The conlenl ofthis PDF file is in accordance with thc original issued rcpols for rcfscnce only.
This Test Repot cannot bc reproduced, except in full, without prior willcn pcmission oflhc companl

@G¡lTruI@¡E

Technical Report:(6817)28e-0r02
October 3 1, 20 l7
Page l5 of l7

Reporl Lirnit
Substance (Testing
paranrcter)Group

CAS No.

Wastewater(ug/L)/(

Sludge(ntgr¡g¡

Narne of thc testing
method'(ppm)AoX
Oil and Grease
PhenolColiform(bacteria/ I 00ml)
Persistent Foam

N/A
N/A
N/A
N/A
Not

N/A
N/A
N/A

visiblevisible

N/A
N/A

N/A

Progressive, andAspirational).

N/A
Not

ANIONS
SulfideSulfiteGroup

Substance ('Iesting
parameter)

CAS NoAntimonvl Sb )Cr total

7440-36-0
7440-47-3

Cobalrl Co )Copper( Cu )7440-484

lB. Conventional
METALSs,âter(me/L)lSilver Ao
Zinc( Zn\
Arsenic lAsl
Cadmiuml Cd )Leadl Pb I

7440-224

7439-92-l

0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.00010.001

Mercury (Hg)7439-97-6

0.00005

7440-50-8
7440-02-0

Nickel lNi)

Parameters -N/AReport Limit
Waste

7440-66-6
1440-18-2
7440-43-9

Chromium VI( CrVI )18540-29-9

0.001

Cyanide( CN-)

Various (incl. 57 -12-5)

0.02

Sludge Name of 'l'esting(mg/kg Methotl)/(ppm)N/A
N/A

VariousAcìd Digestion with

N/A

ICP analysis

N/A
N/A
N/A
N/A

0.1

please refer to ZDHC
Wastewater Guidelines
for more details on thetesting method and thelevels (Exceeded

Foundational Limit,
Foundational,
Progressive, andAsoirational).
Various
Solvent extraction andderivatisation followed
bv UV analvsis
With reference to

0.5

APHA 45OO CNB,C&E and followed
by UV analysis

Note / Key
ppb = part(s) per billion ; ppm - part(sO per million
U. S. EPA: United States Environmental Protection Agency

APHA: American Public Health Association
Comment 1: The report [(6817)289-0102] is sub-contracted to BVCPS (Shanghai, China) For Perfluorinated andPolyfluorinated Chemicals, Flame Retardants, Glycols & AOX Test.

The conlent ofthis IDF file is ¡ì accordance wilh thc original issucd repols for rcfcrcncc only.
Th¡s Test Repot cannot be reproduced, exccpt ¡n full, wilhout prior wittcn pcmission oflhc company.

TEST REPORT
l:rlr¡r:utlr

nr:filrlGr
Technical Report(6817)284-0229

Ocfober 26,2017

Date Received

October 10, 20 I 7

Page I oflS

Factory lll, Devision ll; BANLADESH
Dhaka Region, BANGLADESH

Factory Company Name:
Factory Address:
Project No.:
Client Reference No.:
Sample Type:
Sample Pick Up Date:
Discharge Type:

Wastewater - Time-Weighted Composite Grab Samples*
October 10,2017
Direct Discharge
Factory Owned ETP
Yes
Octobsr I 1, 2017 To October 26,2017

Wastewater Discharge to:
On-Site Effluent Treatment Plant (ETP):
Test Period:
Sample Description:I00l) Incoming water
1002) Discharged Wastewater
1003) Sludge

R"EMARK

Ifthere are questions or concerns on this report, please contact the following persons:Generalenquiry

Mr. Abu Hanif, Mail: abu.hanif@bd.bureauveritas.com

InvoicingTechnical

Mr. Mahabubur Rahman, Mail: mahabubur.rahman@bd.bureauveritas.com

enquiry-Chemical

Mr. M. Nur Alam, Mail: nur.alam@bd.bureauveritas.com

This report shown the test result of the auxiliary chemical and/or raw material samples, which collected during paficular factory
audit. The results of this report shall not be used for any regulatory compliance purposes.

* The sampling is agreed with client.

BUREAU VERITAS
CONSUMER PRODUCTS SERVICES ( BANGLADESH ) LTD.

M.NURALAMSENIORMANAGER
ANALYTICAL LABORATORY

Prepared By:

Md. Abu Taher

Bure¿u Veritas
Consr¡mer Products Services (BD) Ltd,
Plot # ll0. DEPZ Extension Area
Ganakbaû. Savar. Dhaka. Bangladesh'fel: 88-02-770 I 464-6. Fax: 88-02-1 70 1 463

Erlail: ì:vcps.bd(1|bd.bureauveritas.conr
website: cps.bureauveritas.com
The content ofthis PDF file is in accordancc wilh the original issued repols for ref€renc€ only.
This Tcst RcpoÍ cannot bc reproduccd, cxccpl in full, without prior Millen pcmission oflhe company.

@G¡IEETT@IE

Technical Report:(6817)284-0229
October 26,2017
Page 2 of 18

Photo of the Sample/ Samnling LocationI00l) Incoming water

1002) Discharged Wastewater

1003) Sludge

The contc¡t oflhis PDF file is in âccordancc wilh the original issucd repots for reference only.
This Tcst Repon cannot be reproduced, except in füll, wilhoul p¡ior witten pemission ofthe company.

@

GIIEEIT

EilIE

Technical Report:(6817)284-0229
October 26,2017
Page 3 of 18

Executive Summarv
I A) Conventional Parameters

I00t

I002

I003

Temperature
TSS

COD
Total-N
pH Value
Color Im-rl
BODs
Ammonium-N
Total-PNA

See result in page

NA

5-8

AOX
Oil and Grease
PhenolColiform
Foam

ANIONS - Sutfide
ANIONS - Sulfite18) Conventional Parameters -METALS

a

a

o

ZDHC MRSL Substances

I001

I002

I003

2A) APs and APEOs

NT

o

o

2B) Chlorobenzenes and Chlorotoluenes

NT

o

o

2C) Chlorophenols

NT

o

o

2D) Azo Dyes

NT

o

o

2E) Carcinogenic Dyes

NT

o

o

2F) Disperse Dyes

NT

o

o

2G) Flame Retardants

NT

o

o

2H) Glycols

NT

o

o

2I) Halogenated Solvents

NT

o

o

2J) Organotin Compounds

NT

o

o

2K) Perfluorinated and Polyfluorinated Chemicals

NT

o

o

2L) Phthalates
2M) Poly Aromatic Hydrocarbons

NT

o

o

NT

o

o

2N) Volatile Organic Compounds

NT

o

o

Note / Key. - Detectedo - Not Detected
NT - Not Tested

NA- Not ApplicableThc contcnt ofthis PDF filc is in accordance with the original issucd repols forrefercnceonly.
Th¡s Tesl Repol cånnol bc reproduced, cxccpl in full, wilhoul priorwitl6 pemiss¡onof¡hc company.

BUREAUVE R ITAS

Technical Report:(6817)284-022e
October 26,2017
Page 4 of l8

Obiective
The environment samples were tested for below parameters.
IA) Conventional Parameters

I B) Conventional Parameters

2A) APs and APEOs- METALS

2B) Chlorobenzenes and Chlorotoluenes
2C) Chlorophenols
2D) Azo Dyes
2E) Carcinogenic Dyes
2F) Disperse Dyes
2G) Flame Retardants
2H) Glycols2l) Halogenated Solvents
2J) Organotin Compounds

2K) Perfluorinated and Polyfl uorinated Chemicals
2L) Phthalates
2M) Poly Aromatic Hydrocarbons
2N) Volatile Organic Compounds

Samuling Plan
Basically, three environment samples were sampled per factory, including l) Incoming water; 2) Discharged Wastewater and3) Sludge. Total number ofsample collected will be depended on the actual factory facilities and manufacturing processes.

Method of sampling used is time-weighted composite grab samples (agreed with client.). Composite sampling shall be
performed for no less than six hours, with no more than one hour between discrete samples. Each discrete sample shall be ofequal volume. Wastewater and freshwater samples should, as much as possible, be collected simultaneously, during the timethat PU is in normal operation. The sampling shall aim to analyse the snapshot of water quality characteristics of theoperating PU. Under no circumstance shall samples be taken during times when the production process is not running or thewastewater is diluted due to heavy rainfall, etc.

RemarkSampling procedure is with reference to below standards:
1) South Australia EPA Guidelines (June 2007), Regulatory Monitoring and Testing Water and Wastewater

Sampling.

2) Australia EPA (Victoria) Guideline (June 2009), Sampling and Analysis of Waters, Wastewaters, Soils
and Wastes.

3) ISO 5667-3:2003, Water Quality - Sampling - Part 3: Guidance on the Preservation and Handling of
Water Samples.

4) ASTM D3976-92 (Reapproved 2010), Standard Practice for Preparation of Sediment Samples for
Chemical Analysis.
Field data records are attached in Appendix B.

The contedt oflhis PDF lilc is in åccordance w¡lh the orig¡nal issued repots for reference only.
This Test Repod cannol be reproduccd cxcept in full, wilhout prior witler pemissio¡ ofthc eomp¡ny.

@Technical Report:(6817)284-022e
October 26,2017
Page 5 of 18

Test Result1A) Conventional Parameters
TemDerature

Test Method:

Measwement by thermometer

Tested ltemls)

Result

Unit

Conclusion

1002

33.7 (Foundational)

deg. C

DATA

Note:deg. C = degree Celsius (oC)Foundational Limit: A 15 / max. 35'C; Progressive Limit: A l0 / max. 30'C; Aspirational Limit: A 5 / max.25"C

Total Suspended Solids ITSS)
Test Method:

Reference to APHA 22"d Edition-2540D & ALPA 2540D

Tested ltem(s)Result

Unit

Conclusionr002

23 (Foundational)

ms/L

DATA

Note:

mg/L: milligram per liter
Foundational Limit: 50 mg/L; Progressive Limit: 15 mg/L; Aspirational Limit: 5 mg/L

Chemical Oxygen Demand (COD)

TestMethod:

Referenceto ALPA5220B &EPA'410.3

Tesfed ltem(s)Result

Unit

Conclusion

I002

80 ßrosressive)

mp/L

DATA

Note:
mg/L = milligram per liter
Foundational Limit: 150 mgll; Progressive Limit: 80 mg/L; Aspirational Limit: 40 mg/L

Total Nitrogen (Total-N)
Test Method:

Reference to APHA 22"d Editio¡2012,4500 N Org.B

Tested Item(s)Result

Unit

Conclusion

t002

16.3 (Foundational)

ms/L

DATA

Note:
mg/L = milligram per liter
Foundational Limit:20 mglL; Progressive Limit: l0 mg/L; Aspirational Limit: 5 mg/L

The contenl ollhis PDF file is in accordânce with the original i$ued repofs for reference only.
This Test Repol canûot be reproduced, except in full, w¡lhout pr¡orwillen pemission oflhe compåny.

ffià

w

ElEElI@
Technical Report:(6817)284-0229
October 26,2017
Page 6 of 18

oH Value
Test Method:

Reference to ALPA 4500-H+B & EPAI50.2

Unit

Result

Test ltem(s)1002Parameter
Temp. of sample
pH value ofsample

24des. C'7.3

DATA

Conclusion
Note:deg. C: degree Celsius ("C)

Temp.: Temperature
Limit: 6 - 9
Color [m''l (436nm: 525: 620nm)
Test

Method: ISO 7887: 2011(E), B

Tested ltem(s)Pârâm€ter
Trial (?':436 nm)
Trial (À=525 nm)
Trial (I:620 nm)

t002

pH

Result

Unit

Conclusion'7.3

5.1 (Foundational)

m-l

7.3

4.0 (Foundational)

m-l

t.)

2.3 (Foundational)

m-t

DATA
DATA
DATA

Note:
Foundational Limit: 7;5;3 m-r; Progressive Limit: 5;3;2 m-t; Aspirational Limit: 2;l;l m-lBiochemical Oxveen Demand (BODs)
Test Method:

Reference to APHA 22"d Edition-52108& ALPA 52108

Tested ltemlsl

Result

Unit

Conclusionr002

22 (Foundational)

ms/L

DATA

Note
mg/L = milligram per liter
Foundational Limit: 30 mg/L; Progressive Limit: 15 mg/L; Aspirational Limit: 5 mgll.

Ammonia Nitroqen
Test Method

Reference to APHA 22"d Edition2012,4500 NH¡ B.C

Tested ltem(s)Result

Unit

Conclusion

1002

9.0 (Foundational)

mg/L

DATA

Note:
mg/L : milligram per liter
Foundational Limit: l0 mg/L; Progressive Limit: I mg/L; Aspirational Limit: 0.5 mg/L
Thc @ntent oflhis PDF file is ¡n accordance with the originãl issued rcpofs for reference only.
This Tesl Repol caonot be rcproduced, cxccpl in full, withoul priorwitlen pemission ofthe company.

@

EI!f,EL
EI¡E
Technical Report:(6817)284-0229
Octobet 26,2017
Page 7 of 18

Total Phosohorus lTotal-P)
Test Method:

Reference to APHA 22nd Edition -4500-P.E (2012)

Tested Itemls)

Result

Unit

Conclusion

t002

0.8807 (Foundational)

rîc/L

DATA

Note:

mg/L: milligram per liter
Foundational Limit:3 m{L; Progressive Limit: 0.5 mgl[.; Aspirational Limit: 0.1 mgll.

Adsorbable Oreanic Haloeen (AOX)
Test Method:

Reference to HJ/T 83

Tested Itemls)

Result

Unit

Conclusionr002

2.0 (Foundational)

mE/L

DATA

Note:
mg/L = milligram per liter
Foundational Limit: 5 mgil; Progressive Limit: I mg/L; Aspirational Limit: 0.1 mg/L

Oil and Grease
Test Method

Reference to APHA,22nd Edition -5520 B (2012)

Tested Itemls)

Result

Unit

Conclusion

Í002

7 (Foundational)

rng/L

DATA

Note:

mg/L: milligram per liter
Foundational Limit: l0 mg/L; Progressive Limit: 2 mg/L; Aspirational Limit: 0.5 mg/L
PhenolTest Method

Reference to APHA 22nd Edition 2012, USEPA 420.1

Tested ltem(s)1002ResultBLQ GOQ: 0.01) (Progressive)

Unit

Conclusion

mE/L

DATA

Note:

mg/L: milligram per liter
Foundational Limit: 0.5 mg/L; Progressive Limit: 0.01 mg/L; Aspirational Limit: 0.001 mg/L

The conlentoflhis PDF file is in accordanc€ with lhe o¡iginâl issued repofs forreferencc only.
This Tesl Repol cânnot be reproduced, except iû full, without prior witren pcmission ofthe company.

ffià

w

GT!ÍEN
EIETechnical Report:(6817)284-0229
October 26,2017
Page I of 18

Coliform
Test Method

Reference to APHA 22"d Edition 2012,9221 B

Tested ltem(s)Resultt002

94 (Progressive)

Unit

MPN/
100 mL

Conclusion

DATA

Note:
bacteria/I00 mL: bacteria per 100 milliliters
Foundational Limit: 400 / 100 ml; Progressive Limit: 100 / 100 ml; Aspirational Limit: 25 / 100 ml;

Foam

:

Test Method

VisualTested ltemfs)

Resultt002

No Foam

Unit

Conclusion

DATA

ANIONS - Sulfide
Test Method¡ Reference to APHA 22nd Edition 2012, lS: 3025 Part 29

Tested Item(s)Result

Unit

Conclusiont002

BLQ @OQ: 1.0) (Exceed Foundational Limit)

ms/L

DATA

mg/L = milligram per liter
Foundational Limit: 0.5 mg/L; Progressive Limit: 0.05 mg/L; Aspirational Limit: 0.01 mg/L

ANIONS - Sulfite
Test Method

Reference to APHA 22nd Edition 2012,4500 SO¡ B

Tested Item(s)t002

Result
BLQ @OQ: 1.0) (Foundational)

Unit
mplL

Conclusion

DATA

Note:

mg/L: milligram per liter
Foundational Limil: 2 mglL; Progressive Limit: 0.5 mgll,; Aspirational Limit: 0.2 ngll,

The content oflhis PDF file is in accordånce with lhe original issued rcpots fot reftrence oÍly.
ThisTesl Repon cantrot be rcprcduced, except in full, withoul priormittfl pcmission ofthe compânf@EIIf,ETN
gffiETechnical Report:(6817)284-022e
October 26,2017
Page 9 of l8lB) Conventional Parameters - METALSHeaw Metals
Antimony( Sb )Foundational Limit: 0.1 mg/L,
Progressive Limit: 0.05 mg/L;
Asoirational Limit: 0.01 ms/L
Chromium( Cr ), total
Foundational Límit: 0.2 mg/L;
Progressive Limif : 0.1 mg/L;
Aspirational Limit: 0.05 mp/L
Cobalt( Co )Foundational Limil: 0.05 mg/L;
Progressive Limit: 0.02 mg/L;
Aspirational Limit: 0.01 mç/L
Copper( Cu )Foundational Limit: I mg/L;
Progressive Limit: 0.5 mg/L;
Asnirational Limit : 0.2 5 ms/L

l00l tus/L)

1002 (ms/L)

ND

ND(Aspirational)(Aspirational)

ND

0.039
(Aspirational)(Aspirational)

ND

ND(Aspirational)(Aspirational)

0.0s4(Aspirational)

0.019(Aspirational)

1003 (me/ks)

N/A

Nickel (Ni)Foundational Limit: 0.2 mg/L;
Progressive Limit: 0.1 mg/L;
Asoirational Limit: 0.05 ms/L
Silver (Ag)Foundational Limit: 0.1 mg/L;
Progressive Limit: 0.05 mg/L;
Asoírational Limit: 0.005 mø/L

ND

0.010

(Aspirational)(Aspirational)

ND

ND(Aspirational)(Aspirational)

Zinc(Zn)
Foundational Limit: 5 mg/L;
Progressive Limit: I mg/L;
Aspirational Limit: 0.5 ms/L
Arsenic (As)Foundational Limil: 0.05 mg/L;
Progressive Limil: 0.01 mg/L;
Aspiralional Limit : 0.00 5 ms/L
Cadmium( Cd )Foundatíonal Limit: 0.1 mg/L;
Progressive Limit: 0.05 mg/L;
Asoirational Limít; 0.0I me/L
Lead( Pb )Foundational Limit: 0. I mg/L;
Progressive Limít: 0.05 mg/L;
Asoirational Limit: 0.01 ms/L
Mercury (Hg)
Foundalional Limit: 0.01 mg/L;
Progressive Limit: 0.005 mg/L;

Aspirational Limit: 0.001 mø/L
Chromium VI( CrVI )Foundational Limit: 0.05 mg/L,
Progressive Limit: 0.005 mg/L:Aspìrational Limit: 0.001 mp/L
Cyanide( CNI
Foundational Limit: 0.2 mg/L;
Progressive Limit : 0. I mg/L;
Aspirational Limit; 0.05 mF/L

0.00s

0.012

(Aspirational)(Aspirational)

ND

ND(Aspirational)(Aspirational)(Aspirational)

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

ND

ND

NT)

(Aspirational)(Aspirational)(Aspirational)

ND

NI)

NT)

(Aspirational)(Aspirational)(Aspirational)

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

ND

ND

ND

(Aspirational)(Aspirational)(Aspirational)

The øntcnt ofthis PDF file is in accordance with lhc original issucd repots for rcfercnce only.
This Test Repon cannot be reprcduce4 except in full, without prior wiltcn pemission ofthc company.

ffià

w

l:Íril:ül¡r@¡E

Technical Report:(6817)284-0229
October 26,2017
Page l0 of I 8

Others Priority Chemical Grouos

2A) APs and APEOs

28) Chlorobenzenes and Chlorotoluenes
2C) Chlorophenols
2D) Azo Dves
2E) Carcinosenic Dves
2F) Disoerse Dves
2G) Flame Retardants
2H) Glycols2l) Halosenated Solvents
2J) Orsanotin Comoounds
2K) Perfluorinated and PolyfluorinatedChemicals

2L) Phthalates
2M) Polv Aromatic Hvdrocarbons
2N) Volatile Organic Compounds

r001

I002

I003

NT
NT
NT
NT
NT
NT
NT
NT
NT
NT

ND
ND
ND
ND

ND
ND
ND
ND

NI)

NI)

ND
ND
ND
ND
ND

ND
ND
ND
ND
ND

NT

ND

ND

NT
NT
NT

ND
ND
ND

ND
ND
ND

Remark :Test method, reporting limit and list of chemical are summarized in tables of Appendix A.
ND = Not detected (Please refer to reporting limit shown in Appendix A.).
ppb = part(s) per billion.

NT: Not Tested

The coolentoflhis PDF file is ¡n accordaûce with the original issued repons for rcfscnce ooly.
This Tesl Repon cannot be reproduced, except in full, w¡lhout priorMillen pemission oflhe company.

@rilûril:tftr

ETIE

Technical Report:(6817)284-022e
October 26,2017
Page I I of 18

APPENDIXA
Report LimitGroup

Substance (Testing
parameter)

CAS No.

Wastcweter(uùL)t(0.2

Nonylphenol NP

Various (incl. 104-40-5,
t 1066-49 -2, 2s ts4 -s2-3,
84852- I 5-3)

5

0.2

NP/OP: ISO 18857-2(modifieddichloromethane
extraction) or ASTM
D7065 (GC/MS or

Nonylphenol Ethoxylates
oPEO (2-16)

Various (incl. 9002-93 - I,
9036-19-5, 68987-90-6)

5

0.2

OPEO,¡NPEO:
ISOl8857-2 or ASTM

Alkylphenol
Ethoxylates(APEOs): including

all isomers

Nonylphenol Ethoxylates
NPEO (2-18)

50.2

Chlorobenzene

I 08-90-7

0.1

Dichlorobenzene
Trichlorobenzene

I ,3-Dichlorobenzene

Various
Various
Various95-50-l
541-73-l

0.2
0.2
o.2

1.4-Dichlorobenzene

106-46-'7

1,2,3 -Trichlorobenzene

87 -6t-6

1,2,4-Trichlorobenzene
1,3,5-Trichlorobenzene
1.2.3.4-Tetrachlorobenzene

120-82-l

i.2.3.5-Tetraclorobenzene
1 .2.4.5 -Tetrachlorobenzene
Pentachlorobenzene
Hexachlorobenzene

and Chlorotoluenes

2-Chlorotoluene
3-Chlorotoluene
4-Chlorotoluene
2,3-Dichlorotoluene
2,4-Dichlorotoluene
2.5-Dichlorotoluene
2.6-Dichlorotoluene
3,4-Dichlorotoluene
3,5-Dichlorotoluene
2,3,4-Trichlorotoluene
2.3.6-Trichlorotoluene
2.4.5 -Trichlorotoluene
2.4.6-Trichlorotoluene
3,4,5-Trichlorotoluene
2,3,4,5 -Tetrachlorotoluene
2.3-5-6-Tetrachlorotoluene
2.3.4.6 -T etrachlorotoluene
Pentachlorotoluene

2C. Chlorophenols

2-Chlorophenol
3-Chloronhenol
4-Chloronhenol

108-70-3

634-66-2
634-90-2
95-94-3
608-93-5

tt98-74-l
95-49-8
I 08-4 l -8

106-43-4
32768-s4-0
95-73-8
r9398-6 l -9
I I 8-69-4

95-75-025t86-47 -4

7359-72-0
2077 -46-5

6639-30-t
23749-6s-7
21472-86-6
7 6057 -12-0
29733-70-8
87s-40- I
877 -tt-2

95-57-8
108-43-0
106-48-9

LC/MS(-MS)

D7065(LCIMS; GC/MSor LC/MSMS for

Various (inc. 9016-45-9,
26027 -38-3, 37 205 -87 - t,
684 t2- 54- 4, 127 087 -87 -0)

Tetrachlorobenzene
1,2-Dichlorobenzene

28. Chlorobenzenesl(ppm)

5

isomers(AP) and(m9ke)Name of the testing
methodVarious (incl. 140-66-9,
1806-264,27 t93-28-8)Octylphenol OP, mixed

24. Alkylphenol

Sludgen:\,2)APEO l-18

0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
o.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.2
0.5
0.5
0.5

0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1

USEPA 82608,8270D.
Dichloromethane
extraction followed by
GC/MS

0.1
0.1
0.1

0.i
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1

0.025
0.025
0.02s

USEPA 8270 D
Solvent extraction,
derivatisation with

The contcnl ofthis PDF fÌlc is irì accordaùce wilh the origirìal issued rcpors for refercncc only.
This Test Repol cã¡nol be rcproduced, exccpt iû full, wilhout prior witten pemission oflhc company.

@GIIÍETL@¡E

Technical Report:(6817)284-0229
October 26,2017
Page 12 of l8

Reporl l,inrit
Group

Substancc (Tcsting
paranreter)

CAS \o.

Wastsw

alcr(ug/L)/(

Sludgc{Íìrgrkg)(

2,3-Dichlorophenol
2.4-Dichloroohenol
2.5-Dichloroohenol
2,6-Dichlorophenol
3,4-Dichlorophenol
3.5-Dichloronhenol
2.3.4-Trichloroohenol
2.3.5 -Trichloroohenol
2,3,6-Trichloroohenol
2,4,5 -Trichlorophenol
2.4.6-Trichloroohenol
3.4"5 -Trichloroohenol
2.3.4.5-Tetrachloroohenol
2,3,4,6-Tetrachlorophenol
2.3.5.6-Tetrachloronhenol
Pentachloroohenol IPCP)
Tetrachlorophenol (TeCP)
4,4' -Methylene-bis-(2-chloro-aniline)
4-4'-methvlenedianiline

4.4'-Oxvdianiline
4-Chloroaniline
3.3' -Dimethoxvbenzidine
3,3' -Dimethylbenzidine
6-methoxy-mtoluidine (pCresidine)
2,4,5-Trimethvlaniline

2D. Dyes - Azo(Forming Restricted
Amines)s83-78-8
87-65-0
95-77-2
59 I -35-5
15950-66-0

933-78-8
933-75-5

95-9s488-06-2
609- I 9-8

0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5

ppnt)

0.025
0.025

0.025
0.025

0.025
0.025
0.025

0.025
0.025

0.025
0.025

935-95-5
87-86-5

0.5
0.5
0.5
0.5
0.5

Various (incl. 25 167 -83-3)

0.5

0.025

101-r4-4

0.1

0.1

r0t-77 -9
I 0 l -80-4

0.1
0.1

0.1
0.1

490 l-s l-3

s8-90-2

0.025

0.02s
0.02s

t06-47 -8

0.1

0.1

t19-90-4

0.1

0.1

tt9-93-7

0.1

0.1

t20-7 t-8

0.1

0.1

t37 -17 -7

0.1

0.1

l 39-65- l

0.1

0.1

4-Aminoazobenzene
4-Methoxy-mohenvlenediamine
4,4'-Methylene-di-otoluidine

60-09-3

0.1

0.t

61 5-05-4

0.1

0.1

838-88-0

0.1

0.1
0.1

2.6-Xvlidine

87-62-70.1

o-Anisidine
2-Naphthvlamine
3,3' -Dichlorobenzidine
4-Aminodinhenvl
Benzidineo-Toluidine

90-04-00.1

9 l -59-8

0.1

0.1

9l-94-l

0.1

0.1

92-67 -t

0.1

92-87-50.1

0.1

9s-s340.1

0.1

95-68-r
95-69-2

0.1

0.1

0.1

0.1

phenvlenediamine

95-80-70.1

0.1

o-Aminoazotoluene
5-nitro-o-toluidine
C.l. Direct Black 38
C.L Direct Blue 6
C.I. Acid Red 26
C.l. Basic Red 9
C.I. Direct Red 28
C.I. Basic Violet l4

97 -56-3

99-55-8

0.1
0.1

0.1
0.1

t937 -37 -7

500

2602-46-2
3761-53-3
s69-61-9
573-58-0
632-99-s
2475-45-8

500
500
500

4-Chloro-o-toluidine

4-Methyl-m-

C.l. Disoerse Blue I

KOH, acetic anhydridefollowed by GC/MS

0.025
0.025

4.4'-Thiodianiline

2.4-Xvlidine

2E. DyesCarcionogenic or
Equivalent Concem

576-24-9
r20-83-2\lanre of the testing
methodEN 14362.
Reduction step with

Sodiumdithionite,solvent extraction,
GC/MS or LC/MS

Liquid Extraction
LCIMS

-500

s00
500

I

The contcnt ofthis PDF file is in accordance with the original issucd repons for refcrence only.
This Tcst Rcpot cannol bc reproduced, exccpt in full, w¡hout priorwiÍcn pcmission oflhc compa¡y.

@Technical Report:(6817)284-022e
October 26,2017
Page 13 oflS

Report LimitGroup

Substanoe (Testing
parameter)

CAS No.

Wastewater(u8/L)/(

Sludge(mgikg¡Narne of thc testing
nrethod,'(ppm)C.L Disperse Blue 3
C.l. Basic Blue 26

2475-46-9

500I(withMichler's Ketone >2580-s6-s

500I569-64-2

s00

I

2437-29-8500I10309-95-2

500I

82-28-0
I r9-15-3
12222-97-8
12223-0t-7
12236-29-2

500
50
50
50
50
50
50
50
50
50
50
50
50

I

0.t%)
C.L Basic Green
4lmalachite sreen chloride)
C.I. Basic Green 4lmalachite sreen oxalate)
C.L Basic Green
4lmalachite sreen)
Disnerse Oranse 1l

2F. Dyes-disperse(sensitizing)

Disperse Yellow I
Disoerce Blue 102
Disnerse Blue 106
Disoerse Yellow 39
Disperse Oranse 37 / 5917 6
Disperse Brown I
Disnerse Oranse I
Disnerse Yellow 3
Disperse Red 1l
Disperse Red I
Disperse Red l7
Disoerse Blue 7
Disperse Blue 26
Disperse Yellow 49
Disperse Blue 35
Disoerse Blue 124
Disoerse Yellow 9
Disoerse Oranse 3
Disperse Blue 35

Tris(2-chloroethyl)
phosphate ITCEP)
Decabromodiphenyl ether(DecaBDE)
Tris(2,3 -dibromopropyl)
ohosohate ffRIS/TDBPP)
Pentabromodiphenyl ether

lPentaBDE)
Octabromodiphenyl ether(OctaBDE)
Bis(2,3 -dibromopropyl)
2G. Flame

phosphate ßIS/BDBPP)

Retardants

Tris(aziridinyl)-13301-61-6

23355-64-8
2581-69-3
2832-40-8
2872-48-2
28'72-52-8

3179-89-3

3t79-90-6
3860-63-7
54824-37-2
12222-7s-2

6l9sl-st-7
6373-73-s
730-40-556524-77-7

50
50
50
50
50

I

I
I
I
I
I

I
I

I
I
I
I

I
t
I
I

I
I

50
50

1

I 15-96-85I

I 163-19-s

5

I

126-72-"/532534-81-9532536-52-0

55412-25-9

5

and USEPA832

Dichloromethane
extraction GC,MS or

tso 22032, usEPA527

phosphineoxide (TEPA)

545-55- I

5Polybromobiphenyls(PBBs)

59536-65- l

5I

79-94-7

5I3194-ss-6

5I

3296-90-0

5I

t3674-87 -8

5I

Tetrabromobisphenol A

OBBPA)
Hexabromocyclododecane

IHBCDD)
2,2-Bis(bromomethyl)- 1,3
nrooanediol IBBMPI
Tris( 1,3-dichloroisonroovl) nhosohate

Liquid Extraction
LC/MS

LCIMS(-MS)

The content oflhis PDF file is in accordancc with the original issued rcpofs lor refercnce only.
This Tcst Rcpon cannot be reproduced, cxcepl in lull, wilhout prior wrilten pemission oflhc compåny.

lB.

@

EI!ÍETI
EIIE
Technical Report:(6817)284-0229
October 26,2017
Page 14 of I 8

Report LimitGroup

Substance (Testing
parameter)

CAS No.

Wastewater

Sludge(!slL)/((mg/kg)/(ppm)

85535-84-8

5I

ttl-96-6

5

I I l-ls-9

50
50
50

n0-71-4

50

5

t09-86-4

570657-70-4

50
50
50

t12-49-2

50

5

107-06-2
7s-09-2

I
I
I
I

I

0.01

0.1

0.01

0.1

Name of the testing
method(TDCP)
Short chain chlorinatedparaffins (SCCPs)
Bis(2-methoxvethvl)-ether

2H. Glycols

2-ethoxvethanol
acetateEthylene glycol dimethyl
ether
2-methoxyethylacetate
2 -methoxvnronvlacetate

Triethylene glycol dimethyl
ether
1.2-Dichloroethane

2I. HalogenatedSolvenls

Mono-, di- and tri-butyltin
derivatives

acid)

5

r0lr-95-6,6381-06-2,
1 1 35-99-5, 892-20-6,

US EPA 8270
Liquid Extraction

LCIMS

5

I
I
I

USEPA 82608
Headspace GC/MS or
Purgeand-Trap-GC/MS

ISO 17353
Derivatisation with
NaB(C2H5) GC,MS

0.1

0.01

0.1

355-46-4 ,432-s0-7

0.01

0.05

33s-67-t/ 335-95-5

0.01

0.05

29420-49 -3, 29 420 -43 -3

0.01

0.05

307-24-4

0.0 r

0.05

678-39-7

I

647-42-7

I

0.5
0.5

ll7-8t-7

l01

I 17 -82-8

l0I

I I 7-84-0

10I

US EPA 8270D, ISO

2676t-40-0l0IDichloromsthane
extraction GCA4S(DINP)

28ss3-12-0

l0IDi-n-hexyl phthalate(DnHP)

84-7s-3

t0

I

Dibutvl phthalate IDBP

84-74-2l0Iacid IPFOS)

2L. Phthalates(including all otheresthers ofphthalic

753-'73-t.1066-45-l)
Various (incl. 787 63-54-9,
I I l8-46-3, i002-53-5,
683-t8-1,36@3-28-4,
5 657 3 -8s -4, t461 -22-9)

5

0.01

Perfl uorooctanesulfonicand PolyfluorinatedChemicals (PFCs)

127 -18-4

Various (incl. 993-16-8,

5

Various (1 124-19-2,
Mono-, di- and tri-phenyltin
derivatives

Mono-, di- and tri-octyltin
derivatives

2K. Perfluorinatedn0-49-6

79-0t-6
Tetrachloroethylene
Mono-, di- and trimethyltin derivatives

2J. Organotin
Compounds

l l 0-80-5

Perfluoro-n-octanoic acid
IPFOA)
Perfl uorobutanesulfonicacid IPFBSI
Perfl uoro-n-hexanoic acid
(PFHxA)
8:2 FTOH
6:2 FTOH
Di-2-ethylhexyl phthalate
IDEHP)
Dimethoxyethyl phthalate(DMEP)
Di-n-octyl phthalate(DNOP)
Di-iso-decyl phthalate(DIDP)

Diiso-nonyl phthalate639-58-7 .668-34-8)
Various (incl. 1523 I -44-4,
309 t -25 -6, 94410-05 -6,
3542-36-7 , 869-59-0,
2587-76-0)

DIN 38407-42(modified)
Ionic PFC:
Concentration or direct
injection, LC/MS(MS);Non-ionic PFC(FTOH): derivatisation

with acetic anhydride,
followed by GC/MS

I 88s6The conletrt otthis PDF file is itr ãccordancc with thc original issued rcpots for rcfercncc only.
This Tesl Repof cânnot be reproduced, cxccpl in lull, without prior witlen pcmission ofthe company.

@

EIIEEIIT

EIETechnical Report:(6817)284-0229
October 26,2017

Page15oflS
Report Lirnit(ìr'oup

Substance (Tcsting
paranretgr)(-AS \o.

Waste$

alef(ugi L)i(

Butyl benzyl phthalate(BBP)
Dinonvl nhthalate IDNP)
Diethvl nhthalate IDEP)
Di-n-propyl phthalate(DPRP)
Di-iso-butyl phthalate(DIBP)
Di-cyclohexyl phthalate(DCHP)
Di-iso-octyl phthalate(DIOP)
1,2-benzenedicarboxylicacid, di-C7-l l-branched
and linearalkyl esters

Sluclge(nrg/kg.)\ame o1'the testing
nrethod.'(ppm)85-68-7

l0I

84-76410

I

84-66-2

10I

l3 l-16-8

l0I

84-69-510I

84-6t-71027554-26-3

l0685t5-42-4

10

7 I 888-89-6

l050-32-8
120-12-7

I
I

II

I 29-00-0
19t-24-2
192-97-2

I

I

I

I
I
I

IDHNI]PI
1,2-benzenedicarboxylicacid, di-C6-8-branchedalkyl esters, C7-rich

IDIHP)
Benzolalovrene lBaP
Anthracene
Pwene

Benzolshilnervlene

I 93-39-5

2M. Poly Aromatic
Hydrocarbons

Benzolilfluoranthene
Benzolblfluoranthene

I

I

Benzolalanthracene

56-55-3

I1

83-32-9

I

85-01-8I
I

lA. Conventional

86-'/3-7

9t-20-37143-2t330-20-7

o-cresolp-cresol9548-7m-cresol
TemoeratureTSSl 08-39-4

COD

Parameters

I

Chrysene
DibenzIa.hl anthracene

Fluoranthene

Phenanthrene
Fluorene
Naohthalene
Benzene(VoCs)

II

205-82-3
20s-99-2
206-44-0
201-08-9
208-96-8
218-01-9s3-70-3(PaHs)

2N. Volatile
Organic Compound1

Total-NoH
Color [m-'] (436nm;
525nml 620nm)
BOD5
Ammonium-N
Total-P

106-44-5

I
I
I
I

I

I

I

I
I
I

I

I
0.1

I

Solvent extraction
GC/NfS

I
I
I

I
I
I
I
N/A

DIN 38407-39

0.1

rso 11423-l

0.1

Headspace- or Purge-

0.1
0.1

and-Trap-GC/MS

N/A
N/A

Apply the standard

N/A
N/A
N/A

N/A
N/A

N/A

N/A

N/A

N/A

N/A
N/A

N/A
N/A
N/A

to the region (ISO, EU,
US, China), please refer
toZDHC Wastewater
Guidelines for moredetails on the testing
method and the levels(Exceeded Foundational
Limit, Foundational,

N/A

methods that best apply

The content ofthis PDF file is in accordancc wilh the original issued repols for refsercc only.
This Tcst Repon cannot bc reprcduccd, exccpl in full, wilhoul prior wiltm pcmission oflhe compâny@Enririúrll

EIE

Technical Report:(6817\284-0229
October 26,2017
Page l6 of l8

Report l..irnit
Subslancc (T'esting
paralncter)(ìroup

CAS No.

Wasteu'
al er
(

AoX
Oil and Grease
PhenolColìform(bacteria/ I 00ml)
Persistent Foam

ug,L )¡t

Sludgc(nrgi kg)

Name ûl'thc testing
nrethod''(ppm)

N/A
N/A
N/A
N/A

N/A
N/A
N/A
N/A

Not
visible

Not

N/A
N/A

N/A

Progressive, andAspirational).

visibleANIONS
SulfideSulfiteSubstancc (Testing
paranreter)(ìrc)up

CAS No.

Chromiuml Cr ì. total
Cobalt( Co )Copper( Cu )METALS

SIudge(mg/kg)/(ppm)7440-36-0
7440-47-3

0.001
0.001

N/A

7440-484

N/A
N/A
N/A

N/A

Name of
Vlethod-l'csting

VariousAcid Digestion with
ICP analysis

Arsenic (As)Cadmiuml Cd )Leadl Pb )7440-66-6
7440-38-2
7440-43-9

0.001
0.001
0.001
0.001
0.001
0.001
0.0001

7439-92-t

0.001

I

Foundational Limit,
Foundational,

Mercury(Hg)'7439-97-6

0.00005

0.1

Progressive, and7440-50-8
7440-02-0

Nickel lNi)
Silver (As)Zinc( Zn\

lB. Conventionalìvater(mg/l-)/

Antimonvl Sb )Parameters -N/AReport LimitrÀ aste7440-224

Chromium VI( CrVI )18540-29-9

0.001

Cyanide( CNI

Various (incl. 57 -12-5)

0.02

N/A
N/A
I
I

please refer to ZDHC
Wastewater Guidelines
for more details on thetesting method and thelevels (Exceeded

Aspirational).
Various
Solvent extraction andderivatisation followed
bv UV analvsis
With reference to
0.5

APHA 45OO CN-

B,C&E and followed
bv UV analvsis

Note / Key
ppb = part(s) per billion ; ppm - part(sO per million
U. S. EPA = United States Environmental Protection Agency

APHA: American Public Health Association
Comment 1: The report [(6817)284-02291 is sub-contracted to BVCPS (Shanghai, China) For Perfluorinated andPolyfluorinated Chemicals, Flame Retardants, Glycols & AOX Test.
Comment 2: The report [(6817)284-0229] is sub-contracted to BVCPS (Chennai, India) For Phenol, Ammonium-N, TotalN, ANIONS - Sulfide, ANIONS - Sulfite & Coliform Test.

The contentofthis PDF filc is in accordancc with the original issued repots for refcrence only.
This Test Repon cannot be reprodüced, cxcept in full, wilhoul prior witten pemission ofthe company.