1st International symposium

STNPD–2019
Science and Technology of Nano-Polycrystalline Diamond 201928 February - 2 March, Matsuyama, JapanGeodynamics Research Center, Ehime University
Supported by
Joint Usage/Research Center program, “PRIUS”
Grant-in-aid for Scientific Research in Innovative Areas,“Interaction and Coevolution of the Core and Mantle”

STNPD-2019
Science and Technology of Nano-Polycrystalline Diamond 2019
(STNPD-2019)

Scope:
Since the first report of synthesis of ultra-hard nano-polycrystalline diamond (NPD) in 2003 by
the Geodynamics Research Center (GRC) of Ehime University, efforts have been made to apply
this novel material to cutting-edge high-pressure researches in geoscience, physics, chemistry,materials science, etc., through a number of inter-laboratory collaborations with the GRC. We
will have an international symposium on the synthesis, physical properties, and applications of
NPD and relevant materials for further development of science and technology inhigh-pressure and related research fields, as well as for promotion of research collaborations
using NPD. We invite not only the NPD users but also those who are interested in using NPD
for their individual studies to this first international symposium on science and technology ofNPD to be held at the GRC in Matsuyama, where it was born. This symposium is supported by
the Joint Usage/Research Center program (“PRIUS”) run by the GRC and the Grant-in-aid for
Scientific Research in Innovative Areas (“Interaction and Coevolution of the Core and Mantle”).
Contents:
Information
Program for oral sessions
Program for poster session
List of participants-------- p.2-------- p.3-------- p.7-------- p.91

STNPD-2019
Venue:
Geodynamics Research Center, Ehime University, Matsuyama, Japan(30 min. from Matsuyama airport by taxi or 50 min. by bus + tram;
http://www.grc.ehime-u.ac.jp/en/about/access).
Date:
28 February - 2 March 2019(subsequent to the “PRIUS symposium”, mostly given in Japanese, 27-28 February).
Deadlines for contributed papers/posters and registration:
15 December 2018 (extended to 15 February 2019 for contributed poster presentation andregistration; registration can also be made on site except for unofficial dinner at March 1).
Registration fee:
Free of charge.
Banquet:5000 yen (on-site payment at the registration desk, cash only).
Unofficial Dinner:“Ginjiro” near Okaido. 5000 yen (on-site payment at the registration desk, cash only). p.5
Excursion to Uchiko-town:
2000 yen (on-site payment at the registration desk, cash only; including bus fair, lunch,drink).
Presentation:
30 minutes for keynote and 20 minutes for other speakers. Posters (should be prepared inEnglish) shall be displayed throughout the whole period of the symposium forpresentation/discussion with some core times. The poster should be in A0 size (about 90
cm X 120 cm), vertical (p.7-8).
Accommodation:
Many hotels are located in walking distance (15-20 minutes) from the GRC in the famous
Dogo onsen area and the Ohkaido downtown area. Most of the invited speakers will stay at
Daiwa Roynet Hotel (https://www.daiwaroynet.jp/ matsuyama/) near the entrance ofOhkaido
Organizing Committee:
Tetsuo Irifune (Chair) Hiroaki Ohfuji

Yoshio Kono

Fumitaro Ishikawa

Takeshi Sakai

Toru Shinmei

Akira Yamada(GRC members)

Masayuki Nishi

Contact:
Madoka Wada (GRC official)wada.madoka.oh@ehime-u.ac.jp
Tel +81-89-927-8165
2

STNPD-2019

Program for oral sessions[28 February]
13:30-15:00

1. Synthesis of NPD and related materials (Chair: H. Ohfuji)
KEYNOTE: Tetsuo Irifune (GRC, Ehime Univ.)“Synthesis, characterization, and application of NPD: An overview”
14:00-14:20 Masayuki Nishi (GRC, Ehime Univ.)“Polycrystalline diamond sintered from ultradispersed nanodiamonds”
14:20-14:40 Nico A. Gaida (Fac. Eng., Nagoya Univ.)“Transparent nanoceramics composed of birefringent crystals”
13:30-14:00

Norimasa Nishiyama (MSL, Tokyo Inst. Tech.)“Fabrication of transparent polycrystalline cubic silicon nitride and its physical properties”

14:40-15:00

15:00-15:50

Break & Poster

15:50-17:40

2. Features and physical properties (Chair: N. Nishiyama)
KEYNOTE: Yanbin Wang (GSECARS, Univ. Chicago)“The strength and plastic deformation of NPD”

15:50-16:20

Tsutomu Mashimo (Inst. Pulsed Power Sci., Kumamoto Univ.)“Shock-compression behavior and strength of diamond”
16:40-17:00 Hiroaki Ohfuji (GRC, Ehime Univ.)“Microstructure and crystallization mechanism of synthetic and natural NPDs”
17:00-17:20 Angelika Rosa (Mat. Extreme Cond., ESRF)“NPD: a key device for high quality XAS at extreme P/T conditions”
17:20-17:40 Fumitaro Ishikawa (Fac. Eng. & GRC, Ehime Univ.)“Impurity doping for electronic carrier control of diamond using high pressure and hightemperature technique”
16:20-16:40

17:40-18:20

Lab tour

18:30-20:30

Banquet: University cafeteria

3

STNPD-2019[1 March]
8:30-10:00

3. Applications to ultrahigh pressure generation (Chair: Y. Wang)
KEYNOTE: Takehiko Yagi (GCRC, Univ. Tokyo)“Ultra-high pressure generation using double stage diamond anvil technique and theproperties of nano polycrystalline diamond”
9:00-9:20 Takeshi Sakai (GRC, Ehime Univ.)“Equations of state at multi-megabar pressure”
9:20-9:40 Katsuya Shimizu (Kyokugen, Osaka Univ.)“Mbar-superconductivity and NPD”
9:40-10:00 Florent Occelli (CEA)
8:30-9:00“A new diamond anvil tip geometry aimed at reaching multi-Mbar pressures”
10:00-10:30

Break

10:30-12:00

4. Applications to X-ray spectroscopy under pressure (Chair: Y. Kono)
KEYNOTE: Max Wilke (Inst. Earth & Environ., Univ. Potsdam)“Using Nanopolycrystalline Diamonds for EXAFS on glass and melt at extreme conditions”11:00-11:20 Naoki Ishimatsu (Fac. Sci., Hiroshima Univ.)
10:30-11:00“Element-selective local structure studied by X-ray absorption spectroscopy using NPDanvils”
11:20-11:40 Saori Kawaguchi (JASRI, SPring-8)“Structure determination of liquid Fe-Ni-S alloys at high pressure”
11:40-12:00 Christele Sanloup (IMPMC, Sorbonne Université)“Incorporation of trace elements in magmas at depth”
12:00-13:00

Lunch

13:00-14:10

5. Applications to other high-pressure studies (Chair: N. Ishimatsu)
KEYNOTE: Yoshio Takano (NIMS)“Exploration of pressure induced superconductors using materials informatics”
13:30-13:50 Longjian Xie (BGI, Univ. Bayreuth)“Boron-doped diamond in multi-anvil apparatus and its implication for in-situ fallingsphere viscometry”
13:00-13:30

4

STNPD-2019
13:50-14:10

Hiroshi Fukui (Fac. Sci., Univ. Hyogo Pref.)“NPD applied to X-ray Raman Scattering and suggestions to improve the usability”
14:10-15:00

Break & Poster

15:00-18:00

A visit to Matsuyama castle or University museum~30 minute-walking from GRC, visiting the castle tower on the top of the hill. Anotheroption is to visit the Museum of Ehime Univ. on the campus, about 5 minutes from theGRC, where some NPD products are being displayed, including brilliant-cut NPD with adiameter of 1 cm and NPD with perfectly spherical shape of 7 mm diameter. Bothexcursions will be attended by some volunteer guides.

18:30-

Unofficial dinner“Ginjiro”, serving local cuisine of Ehime (near the Daiwa Roynet Hotel), about 5000 yen.

Please sign up whether:Group (1): Visit to Matsuyama castle at 15:00-18:00 before dinner.
Group (2): Stay at GRC or visit to University Museum, and gather at the entrance of GRC building at 17:50.
Groups (1) and (2) will meet at the north entrance of Okaido street at 18:10, and will move to:
Restaurant: Sennenn Japanese Restaurant Ginjiro (千年和食銀次郎)
Address: 3-7-15 NiBancho, Matsuyama, Ehime Prefecture<MAP>
Ehime University
Matsuyama Castle

Daiwa Roynet HotelOkaido

GinjiroContact information of Yoshio KONO, E-mail: kono.yoshio.rj@ehime-u.ac.jp
5

STNPD-2019[2 March]
9:00-10:30

6. New ideas and other applications (Chair: S. Pascarelli)
KEYNOTE: Yoshio Kono (GRC, Ehime Univ.)“Opposed-type double-stage cell for large volume experiments at >100 GPa and its
potential use of NPD”
9:30-9:50 Guillaume Morard (CNRS)“Pure iron phase diagram probed by multiple techniques”
9:50-10:10 Norimasa Ozaki (Fac. Eng., Osaka Univ.)“Study on shock-compressed nanopolycrystalline material”
10:10-10:30 Madhusoodhan Satish-Kumar (Fac. Sci., Niigata Univ.)
9:00-9:30“NPD as a carbon isotope standard for in situ analysis”
10:30-11:40

7. Discussion and future perspectives (Chair: T. Irifune)
KEYNOTE: Sakura Pascarelli (Mat. Extreme Cond., ESRF)“Use of Nanopolycrystalline Diamond Anvils overseas: scientific impact, present status andfuture needs”
11:00-11:40 Discussion
10:30-11:00

12:00-18:00

Excursion to Uchiko town
Historical town in Edo era (some 200 years ago), about one hour from Matsuyama by achartered bus (lunch box + drink will be served). The tour will be attended by somevolunteer guides.

18:00You are free6

STNPD-2019

Program for poster session

General Research Building I, 4F
Core time: 28 February, 15:00-15:50 / 1 March, 14:10-15:00
Display: from 2/28 (Thu) 12:30 pm. Please use “tools” on the table at front of Coffee space.
Remove: by 3/2 (Sat) 12:30 pm
Poster size: A0 size (about 90 x 120 cm), vertical (portrait style).

Poster no.

NameTitle

NPD-P01

Denis Mikhailenko

TEM characterization of carbon polymorphs in Ultra Highpressure rocks from Kokchetav massif (Northern Kazakhstan)

NPD-P02

Trishit Ruj

Early Martian crustal dynamics; Investigation from oldest
highland terrain

NPD-P03

Keyur De

Palaeostress regime responsible for crustal extension in Pyrrhae
Regio, MarsNPD-P04

Eleonora Kulik(1)Mechanical properties of polycrystalline perovskite- andilmenite-type MgSiO3

NPD-P05

Eleonora Kulik(2)Synthetic Mn-doped jadeite-creation of nanostructures byextreme

NPD-P06

Gréaux Steeve

Sound velocity of CaSiO3 suggests the presence of basaltic crustin the Earth’s lower mantle

NPD-P07

Nozomi Kondo

Major element composition of the Hadean crust: constrainsfrom Sm-Nd isotope systematics and high-pressure melting
experiments

NPD-P08

Xinguo Hong

Structural changes of GeO2 glass under high pressure using
NPD and single-crystalline diamond anvils

NPD-P09

Huiyang Gou

Revealing the structural and mechanical properties of Moborides

NPD-P10

Fumitoshi Iga

Material Design of Novel Rare-Earth Dodecaborides byHigh-Prssure Synthesis

NPD-P11
NPD-P12

Alena Krupp

Synthetic nanocomposite ceramics - tailored alternative(Astrid Holzheid)

materials of high-pressure minerals

Toshiki Hamatani

Development of Ultra-high Pressure’s Technique Using
Improved Toroidal Shaped Diamond Anvil

NPD-P13

Yuki Nakamoto

High pressure generation using nano-polycrystalline diamondanvils
7STNPD-2019
NPD-P14

Ryosuke Takeda

Generation of ultra-high pressures towards metallic hydrogenusing a double-stage diamond anvil cell

NPD-P15

Takehiro KunimotoHigh pressure generation to 90 GPa in Kawai-type multianvil
apparatus using nano-polycrystalline diamond anvils.

NPD-P16

Yu Nishihara

Effect of pressure on electromotive force of type-R
thermocouple

NPD-P17

Yoshinori Tange

Time‐resolved XFEL observation of shock‐wave propagating
material

NPD-P18

Rei Fukuda

Epitaxial formation of pyramidal structure on CVD diamond byhigh pressure and high temperature treatment

NPD-P19

Toru Shinmei

NPD and other novel material synthesis at GRC usinglarge-volume multianvil apparatus

NPD-P20

Nadezda Chertkova

A compact diamond anvil cell for in situ spectroscopic
measurements at high pressures and high temperatures

NPD-P21

Hirokazu Kadobayashi

Time-resolved x-ray diffraction and Raman studies of the phasetransition mechanisms of methane hydrate

Hideaki Kawamura

Decomposition of magnesite in the presence of reduced C-H-O
fluid under upper mantle conditions

STNPD-2019
Or al session

Freespace
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5 6 7 8 1049Coffee
space

8

StepWCStep

NPD-P22

STNPD-2019

List of participants
No.

NameAffiliation

E-mail1

CHERTKOVA, Nadezda

GRC, Ehime University

chertkova.nadezda.sj@ehime-u.ac.jp

2

DE, Keyur

Presidency University

de.keyur@gmail.com

3

FUJINO, Kiyoshi

4

FUKUDA, Rei

5

FUKUI, Hiroshi

6

GAIDA, Nico Alexander

Graduate School of Science,
Hokkaido University
Graduate School of Science andEngineering, Ehime University
Graduate School of Material
Science, University of Hyogo
Graduate School of Engineering,
Nagoya University

kfujino@sci.hokudai.ac.jp

f863001x@mails.cc.ehime-u.ac.jp

fukuih@sci.u-hyogo.ac.jp

gaida@mp.pse.nagoya-u.ac.jp

Center for High Pressure Science &7

GOU, Huiyang

Technology Advanced Researchhuiyang.gou@hpstar.ac.cn(HPSTAR)8GRÉAUX, Steeve

GRC, Ehime University

greaux@sci.ehime-u.ac.jp

Center for Science and Technology
9

HAMATANI, Toshiki

under Extreme Conditions, Osaka

hamatani@hpr.stec.es.osaka-u.ac.jp

University
Department of Environment
10

HIRAI, Hisako

Systems, Faculty of Geo-environmehiraihisako777@gmail.com

ntal Science, Rissho University
11

HOLZHEID, Astrid

Institute of Geosciences, Kiel
University

astrid.holzheid@ifg.uni-kiel.deCenter for High Pressure Science &12

HONG, Xinguo

Technology Advanced Research

xinguo.hong@gmail.com(HPSTAR)
13

ICHIDA, Yoshio

Graduate School of Engineering,
Utsunomiya University
9

ichida@cc.utsunomiya-u.ac.jp

STNPD-2019
Graduate School of Science and

14

IGA, Fumitoshi

15

INOUE, Toru

16

IRIFUNE, Tetsuo

GRC, Ehime University

irifune@dpc.ehime-u.ac.jp

17

ISHIKAWA, Fumitaro

GRC, Ehime University

ishikawa@ee.ehime-u.ac.jp

18

ISHIMATSU, Naoki

19

KADOBAYASHI,
Hirokazu

Engineering, Ibaraki University
Graduate School of Science,Hiroshima University

Graduate School of Science,
Hiroshima University

fumitoshi.iga.sciphys@vc.ibaraki.ac.jp

toinoue@hiroshima-u.ac.jp

ishimatsunaoki@hiroshima-u.ac.jp

GRC, Ehime University

kadobayashi.hirokazu.at@ehime-u.ac.jp

GRC, Ehime University

kakizawa@sci.ehime-u.ac.jp

20

KAKIZAWA, Sho

21

KAWAGUCHI, Saori

22

KAWAMURA, Hideaki

GRC, Ehime University

kawamura@sci.ehime-u.ac.jp

23

KIMURA, Masaki

GRC, Ehime University

kimura.masaki.mj@ehime-u.ac.jp

24

KONDO, Nozomi

GRC, Ehime University

kondo.nozomi.xg@ehime-u.ac.jp

25

KONO, Yoshio

GRC, Ehime University

kono.yoshio.rj@ehime-u.ac.jp

26

KULIK, Eleonora

27

KUNIMOTO, Takehiro

GRC, Ehime University

kunimoto@sci.ehime-u.ac.jp

28

KURIO, Ayako

Syntekinfo@syntek.co.jp

MADHUSOODHAN,

Graduate School of Science andSatish-Kumar

Technology, Niigata University

29

Japan Synchrotron Radiation
Research Institute (JASRI)

Institute of Geosciences, Kiel
University

10

sao.kawaguchi@spring8.or.jp

eleonorakulik@gmail.com

satish@geo.sc.niigata-u.ac.jp

STNPD-2019
30

MASHIMO, Tsutomu

31

MATSUMOTO, Ryo

Institute of Pulsed Power Science,Kumamoto University
National Institute for Materials
Science (NIMS)

nishiyama.n.ae@m.titech.ac.jp

MATSUMOTO.Ryo@nims.go.jp

Sobolev Institute of Geology and32

MIKHAILENKO, DenisМinerаlоgу, Siberian Вrаnсh of themikhailenkodenis@gmail.com

Russian Academy of Sciences
33

MORARD, Guillaume

IMPMC CNRS

guillaume.morard@upmc.fr

Center for Science and Technology
34

NAKAMOTO, Yuki

under Extreme Conditions, Osaka

nakamoto@stec.es.osaka-u.ac.jp

University
35

NISHI, Masayuki

GRC, Ehime University

nishi@sci.ehime-u.ac.jp

36

NISHIHARA, Yu

GRC, Ehime University

yunishi@sci.ehime-u.ac.jp

Laboratory for Materials and37

NISHIYAMA, Norimasa

Structures, Tokyo Institute ofnishiyama.n.ae@m.titech.ac.jp

Technology38

OCCELLI, Florent

CEA

florent.occelli@cea.fr

39

OHFUJI, Hiroaki

GRC, Ehime University

ohfuji@sci.ehime-u.ac.jp

40

OZAKI, Norimasa

41

PASCARELLI, Sakura

42

ROSA, Angelika

Graduate School of engineering,Osaka University
European Synchrotron Radiation
Facility (ESRF)
European Synchrotron Radiation
Facility (ESRF)

norimasa.ozaki@eie.eng.osaka-u.ac.jp

sakura@esrf.fr

angelika.rosa@esrf.fr

Department of Earth and Planetary
43

RUJ, Trishit

Science, School of Science, The
University of Tokyo11trishitruj@gmail.com

STNPD-2019
44

SAKAI, Takeshi

GRC, Ehime University

45

SANLOUP, Chrystele

Sorbonne Universitè

sakai@sci.ehime-u.ac.jp
chrystele.sanloup@sorbonne-universite.
frCenter for Science and Technology
46

SHIMIZU, Katsuya

under Extreme Conditions, Osakashimizu@stec.es.osaka-u.ac.jp

University
47

SHINMEI, Toru

48

TAKANO, Yoshihiko

GRC, Ehime University
National Institute for Materials
Science (NIMS)

shinmei@sci.ehime-u.ac.jp

TAKANO.Yoshihiko@nims.go.jp

Center for Science and Technology
49

TAKEDA, Ryosuke

under Extreme Conditions, Osaka

takeda@hpr.es.osaka-u.ac.jp

University50TAMAROVA, Anastasia

51

TANGE, Yoshinori

52

WANG, Yanbin

53

WILKE, Max

54

XIE, Longjian

55

YAGI, Takehiko

Moscow State University
Japan Synchrotron Radiation
Research Institute (JASRI)GSECARS, University of Chicago
Universität Potsdam, Institut fürGeowissenschaftenBayerisches Geoinstitut, University
Bayreuth
Graduate School of Science, The
University of Tokyo12

dragon.of.rainbow@yandex.ru

yoshinori.tange@spring8.or.jp

wang@cars.uchicago.edu

wilkem@uni-potsdam.de

Longjian.Xie@uni-bayreuth.deyagi@eqchem.s.u-tokyo.ac.jp