Application Data
農薬の一斉分析(LC/MS) (2)No. 1102 1/2

SunShell C18 2.6 µm, 100 x 2.1 mm i.d.

Simultaneous Analysis of Pesticide (LC/MS) (2)PositiveSample No.
187

150

10050

1minSample
1. 1-Napthylacetamide
2. 3-oh-Carbofuran
3. Abamection
4. Acephate
5. Acetamiprid
6. Acibenzolar-s-methyl
7. Aldicarb
8. Aldoxycarb
9. Anilofos
10. Aramite
11. Atrazine
12. Azafenidin
13. Azamethiphos
14. Azimsulfuron
15. Azinphos-methyl
16. Azoxystrobin
17. Bendiocarb
18. Bensulfuron-methyl
19. Benzofenap20. Bitertanol
21. Boscalid
22. Bromacil
23. Butafenacil
24. Carbaryl
25. Carbofuran
26. Carboxin
27. Carpropamide
28. Chloridazon
29. Chlorimuron-ethyl
30. Chlorsulfuron
31. Chlorxuron
32. Chromafenozide

33. Chrothianidin
34. Cinosulfuron
35. Clodinafop acid
36. Clofentezine
37. Clomeprop
38. Cloquintocet-methyl
39. Cloransulam-methyl
40. Cumyruron
41. Cyanazine
42. Cyazofamid
43. Cycloate
44. Cycloprothrin
45. Cyclosulfamuron
46. Cyflufenamide
47. Cyproconazole
48. Cyprodinil
49. DDVP
50. Diallate
51. Dichlosulam
52. Diclomezine
53. Diclotopos
54. Difenoconazole
55. Diflubenzuron
56. Dimethirimol
57. Dimethoate
58. Dimethomorph
59. Dimeton-s-methyl
60. Diuron
61. Dymuron
62. Epoxiconazole
63. Ethametsulfuron-methyl

64. Ethoxysulfuron
65. Fenamidon
66. Fenamiphos
67. Fenbuconazole
68. Fenhexamid
69. Fenobucarb
70. Fenoxaprop-ethyl
71. Fenoxycarb
72. Fenpyroximate
73. Fensulfothion
74. Ferimzone
75. Flazasulfuron
76. Florasulam
77. Fluazifop
78. Flufenacet
79. Flufenoxuron
80. Flumetsulam
81. Fluridone
82. Flusilazole
83. Flutriahol
84. Foramsulfuron
85. Forchlofenuron
86. Fostiazate
87. Furametpyr
88. Furathiocarb
89. Halosulfuron-methyl90. Haloxyfop
91. Hexaconazole
92. Hexaflumuron
93. Hexazinon
94. Hexythiazox

95. Imazalil
96. Imazamethabenz-methyl
97. Imazaquin
98. Imazosulfuron
99. Imibenconazole debenzil
100. Imibenconazole
101. Imidacloprid
102. Indanofan
103. Indoxacarb
104. Iodosulfuron-methyl105. Iprovalicarb
106. Isoprocarb
107. Isoxaflutole
108. Isoxation-oxon109. Lactofen
110. Lenacil
111. Linuron
112. Lufenuron
113. Mepanipyrim
114. Mesosulfuron-methyl115. Methabenzthiazuron
116. Methamidofos
117. Methiocarb
118. Methomyl
119. Methoxyfenozide
120. Metosulam
121. Metsulfuron-methyl122. Mevinphos
123. Monocrotophos
124. Monolinuron
125. Myclobutanil

126. Naproanilide
127. Naptalam128. Norflurazon
129. Novaluron
130. Ometoate131. Oxadixyl132. Oxamyl133. Oxaziclomefone
134. Oxycarboxin
135. Pencycuron
136. Penoxsulam
137. Pentoxazone
138. Phenmedhipham139. Phosphamidone
140. Primicarb
141. Primisulfuron
142. Prohydrojasmon
143. Propaquizafop
144. Propoxur
145. Propoxycarbazone
146. Prosulfuron
147. Pyorquilon
148. Pyraclostrobin149. Pyrazolynate
150. Pyrazosulfuron-ethyl151. Pyriftalid
152. Quinoclamine
153. Quizalofop-ethyl154. Silafluofen
155. Simazine
156. Simeconazole

157. Simetryn158. Spinosyna
159. Spinosynd
160. Spiroxamine
161. Sulfentrazone
162. Sulfosulfuron
163. Tarlkoxydim
164. Tcmtb
165. Tebufenozide
166. Tebuthiuron
167. Teflubenzuron
168. Tetrachlorvinphos
169. Tetraconazole
170. Thiabendazole
171. Thiacloprid
172. Thiamethoxam
173. Thifensulfuron-methyl174. Thifluzamide
175. Thiodicarb
176. Tidiazuron
177. Tiradimenol
178. Tolfenpyrad179. Triasulfuron
180. Tribenuron
181. Tricyclazole
182. Tridemorph183. Trifloxysulfuron
184. Triflumuron
185. Triflusulfuron
186. Triticonazole
187. XMC

Application Data

No. 1102 2/2

Negativemin

By courtesy of AiSTI SCIENCE CO.,Ltd.

HPLC condition
Column: SunShell C18 2.6 µm, 100 x 2.1 mm
Mobile phase: A) 0.5 mM Ammonium acetate in H2OB) 0.5 mM Ammonium acetate in CH3OH
A/B = 95/5 – 1 min – 50/50 – 14 min – 2/98 – 5 min – 2/98 – 0.1 min – 95/5 – （Equilibrating,10 min）, v/v
Flow rate: 0.2 mL/min
Temperature: 40 oC
Detection: LC/MS/MS (QTRAP®4500: ESI, MRM)
Injection volume: 5 µL (STD 10ppb)