R J Hill Laboratories Limited
1 Clyde Street
Private Bag 3205
Hamilton 3240, New Zealand

ANALYSISREPORT

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Client:Tel +64 7 858 2000
Fax +64 7 858 2001
Email mail@hill-labs.co.nz
Web www.hill-labs.co.nz

901964POPJv1Lab No:Dai company (H8560i):

1-2
1-2 Ichigayadai-machi, Shinjyuku-ku, Tokyo, Japan

2011-06-01

Date Registered:(yyyy-mm-dd)

Date Reported:(yyyy-mm-dd)

2011-06-08:

JC082-3814

Reference:

Sample Type: Food Additives and Supplements:
Hachi no tasuke (bee powder capsule)

Sample Name::

901964.1

Lab Number:

GC
Multiresidue GC Analysis (dried/oil Cat. C samples):
Analytes Detected:

None

These samples were collected by yourselves (or your agent) and analysed as received at the laboratory. This report must not be reproduced, except in full, without
the written consent of the signatory.
Refer to the following pages for method details, list of analytes screened and detection limits.

Hisashi Ito
Country Manager
Hill Laboratories
TEL 0476-48-8835
email: all@hill-labs.jp(Confirmation of Receipt)

Colin Ogle PhD
Client Services Manager - Food & Bioanalytical Division(ILAC)(IANZ)(ILAC-MRA)
This Laboratory is accredited by International Accreditation New Zealand (IANZ), which represents New Zealand in the International Laboratory Accreditation
Cooperation (ILAC). Through the ILAC Mutual Recognition Arrangement (ILAC-MRA) this accreditation is internationally recognised.
The tests reported herein have been performed in accordance with the terms of accreditation, with the exception of tests marked *, which are not accredited.

SUMMARY OF METHODS
The following table(s) gives a brief description of the methods used to conduct the analyses for this job. The detection limits given below are those attainable in a relatively clean sample type.
Detection limits may be higher for individual samples should insufficient sample be available, or if the sample type requires that dilutions be performed during analysis.

Sample Type: Food Additives and Supplements
Test

Method Description
GPC
GC-ECD/NPD

GC

Default Detection Limit,-Samples

1

GC-MS
230

Multiresidue GC Analysis (dried/oil Cat. Csamples)

Ethyl acetate extraction, GPC cleanup, GC-ECD/NPD analysis.
Confirmation by GC-MS.
This analytical method covers 230 analytes, as in following lists.
Note: The detection limits have been raised four fold to account fora dilution required during the analysis. Sample types that havebeen refined or concentrated necessitate a smaller sub-sample (5grams compared to 20 grams used for fresh or raw samples) to betaken for the analysis. This ensures the amounts of interferences
or co-extractives that may affect the analysis are kept to aminimum.
Analysis performed at Hill Laboratories - Food & BioanalyticalDivision, Waikato Innovation Park, Ruakura Lane, Hamilton.

Samples are held at the laboratory after reporting for a length of time depending on the preservation used and the stability of the analytes being tested. Once thestorage period is completed the samples are discarded unless otherwise advised by the client.

: 901964 v 1Lab No:

Hill Laboratories

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Detection Limits
Analytes

Detection Limit

Analytes

GC

Detection Limit

Multiresidue GC Analysis (dried/oil Cat. C samples)

0.08 mg/kg

0.04 mg/kg

Acephate

Cadusafos

0.04 mg/kg
Captafol

0.04 mg/kg
Captan0.08 mg/kg
Carbaryl

0.04 mg/kg
Carbofenothion

0.04 mg/kg
Atrazine-desethyl0.04 mg/kg
0.04 mg/kg
Carboxin

0.04 mg/kg

0.02 mg/kg

DDT

0.02 mg/kg

DDT
2,4'-DDT

0.12 mg/kg

Azaconazole

0.02 mg/kg

DDT

4,4'-DDE

Carbofuran

Atrazine-desisopropyl

0.02 mg/kg

DDT

2,4'-DDE

0.04 mg/kg
Atrazine

0.02 mg/kg

DDT

4,4'-DDD

0.02 mg/kg
Aldrin0.08 mg/kg

2,4'-DDD

0.04 mg/kg
Alachlor

Multiresidue GC Analysis (dried/oil Cat. C samples)

Cyprodinil

0.04 mg/kg
Acetochlor

Detection LimitGC

Multiresidue GC Analysis (dried/oil Cat. C samples)

0.02 mg/kg

DDT
4,4'-DDT

0.02 mg/kg

CIS

0.04 mg/kg

cis-Chlordane

0.08 mg/kg
Azinphos-methyl

TRANS

0.02 mg/kg

Deltamethrin (Tralomethrin)

0.04 mg/kg

Demeton-S-methyl0.04 mg/kg

Diazinon

0.04 mg/kg

Dichlobenil

0.04 mg/kg

Dichlofenthion

0.04 mg/kg

Dichlofluanid

0.04 mg/kg

Dichloran

0.04 mg/kg

Dichlorvos

0.04 mg/kg

Dicofol

0.04 mg/kg

Dicrotophos

0.04 mg/kg

Dieldrin

0.04 mg/kg

Difenoconazole

0.08 mg/kg

Diflufenican

0.08 mg/kg

Dimethenamid

0.04 mg/kg

Dimethoate

0.04 mg/kg

Dimethomorph

0.04 mg/kg

Dimethylvinphos

0.04 mg/kg

Dinocap

0.04 mg/kg

Dioxabenzofos

0.04 mg/kg

Diphenylamine-S-

trans-chlordane

0.08 mg/kg
Azoxystrobin

0.04 mg/kg

0.04 mg/kg

Chlorfenvinphos

0.04 mg/kg
Bendiocarb

0.04 mg/kg

Chlorfluazuron

0.04 mg/kg
Benodanil

0.04 mg/kg

Chlorobenzilate

0.04 mg/kg
Benoxacor

0.04 mg/kg

Chlorothalonil

0.02 mg/kg

BHC
alpha-BHC

0.12 mg/kg

Chlorpropham

0.02 mg/kg

BHC
beta-BHC

0.2 mg/kg

Chlorpyrifos

0.02 mg/kg-BHC
gamma-BHC (Lindane)

0.04 mg/kg

Chlorpyrifos-methyl

0.02 mg/kg

BHC
delta-BHC

0.02 mg/kg

Chlorthal-dimethyl0.04 mg/kg
Bifenox0.04 mg/kg

Chlortoluron

0.04 mg/kg
Bifenthrin

0.04 mg/kg

Chlozolinate

0.04 mg/kg
Bitertanol

0.04 mg/kg

Clomazone

0.04 mg/kg
Bromacil

0.08 mg/kg

Coumaphos

0.04 mg/kg
Bromophos-ethyl0.04 mg/kg

Cyanazine

0.04 mg/kg
Bromopropylate

0.04 mg/kg

Cyanophos

0.04 mg/kg
Bupirimate

0.2 mg/kg

Cyfluthrin

0.04 mg/kg
Buprofezin

0.04 mg/kg

Cyhalothrin

0.04 mg/kg
Butachlor

0.08 mg/kg

Cypermethrin

0.04 mg/kg
Butamifos

0.12 mg/kg
0.04 mg/kg

ChlorfenapyrBenalaxyl

Cyproconazole: 901964 v 1
Lab No:Analytes

GC

Hill Laboratories

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Analytes

Detection Limit

Analytes

GC

Detection Limit

Analytes

GC

Multiresidue GC Analysis (dried/oil Cat. C samples)

Multiresidue GC Analysis (dried/oil Cat. C samples)

0.2 mg/kg

0.04 mg/kg

Disulfoton

Fensulfothion

0.04 mg/kg
FenvalerateI

0.04 mg/kg
Fluazifop-butyl

II0.02 mg/kg

0.04 mg/kg

0.04 mg/kg
Malathion

0.02 mg/kg

0.08 mg/kg
Fludioxonil

0.08 mg/kg
Mepronil

0.02 mg/kg
Endrin0.2 mg/kg
LinuronFlucythrinateEndosulfan sulfate

0.04 mg/kg
Leptophos

0.02 mg/kg

Endosulfan II

0.04 mg/kg
Kresoxim-methyl0.04 mg/kg

Endosulfan I

0.08 mg/kg

0.08 mg/kg
Fenthion

Edifenphos

Multiresidue GC Analysis (dried/oil Cat. C samples)

Isoprocarb

0.08 mg/kg
DiuronDetection Limit

GC

0.04 mg/kg

0.08 mg/kg

Fluometuron

0.02 mg/kg
Endrin Aldehyde

Metalaxyl (Mefenoxam)

0.08 mg/kg

Methacrifos

0.04 mg/kg

Methamidophos

0.04 mg/kg

Methidathion

0.04 mg/kg

Methiocarb

0.08 mg/kg

Methoxychlor

0.04 mg/kg

Metolachlor

0.04 mg/kg

Metribuzin

0.02 mg/kg

Mevinphos

0.02 mg/kg

Monocrotophos

0.02 mg/kg

Myclobutanil

0.04 mg/kg

Naled

0.04 mg/kg

Napropamide

0.12 mg/kg

Nitrofen

0.12 mg/kg

Nitrothal-isopropyl

0.04 mg/kg

Norflurazon

0.04 mg/kg

Omethoate0.04 mg/kg

Oxadiazon

0.04 mg/kg

Oxadixyl

0.04 mg/kg

Oxychlordane

0.04 mg/kg

Oxyfluorfen

0.04 mg/kg

Flusilazole

0.02 mg/kg
Endrin ketone

0.08 mg/kg

Flutriafol

0.04 mg/kg

EPN

0.08 mg/kg

EPN

0.08 mg/kg

Folpet0.08 mg/kg
Epoxiconazole

0.04 mg/kg

EPTC

0.08 mg/kg

Fonofos

EPTC

0.02 mg/kg

Furalaxyl0.04 mg/kg
Esfenvalerate

0.04 mg/kg

Furathiocarb

0.08 mg/kg
Esprocarb

0.04 mg/kg

Halfenprox

0.04 mg/kg
Ethion0.04 mg/kg

Haloxyfop-methyl0.04 mg/kg
Ethoprophos

0.04 mg/kg

Heptachlor

0.08 mg/kg
Etridiazole

0.04 mg/kg

Heptachlor epoxide

0.04 mg/kg
Etrimfos

0.12 mg/kg

Hexachlorobenzene

0.04 mg/kg
Famphur

0.08 mg/kg

Hexaconazole

0.04 mg/kg
Fenamiphos

0.04 mg/kg

Hexazinone

0.04 mg/kg
Fenarimol

0.04 mg/kg

Hexythiazox

0.04 mg/kg
Fenchlorphos

0.04 mg/kg

Imazalil

0.04 mg/kg
Fenitrothion

0.12 mg/kg

Indoxacarb

0.08 mg/kg
Fenobucarb

0.04 mg/kg

Iodofenphos

0.08 mg/kg
Fenoxaprop-ethyl0.04 mg/kg

Iprobenfos

0.04 mg/kg
Fenpiclonil

0.02 mg/kg

Iprodione

0.04 mg/kg
Fenpropathrin

0.04 mg/kg
Fenpropimorph

0.04 mg/kg

Isazophos

0.04 mg/kg

Isofenphos
Paclobutrazol: 901964 v 1
Lab No:Hill Laboratories

4/5
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Analytes

Detection Limit

Analytes

GC

Detection Limit

Multiresidue GC Analysis (dried/oil Cat. C samples)

0.04 mg/kg

0.08 mg/kg

Parathion-ethyl

Pyraclofos

0.08 mg/kg
Pyrazoxyfen

0.12 mg/kg
Pyrethrin

0.04 mg/kg
Pyrifenox

0.04 mg/kg
Pyrimethanil

0.04 mg/kg
Trifluralin0.08 mg/kg

0.08 mg/kg
Pyriproxyfen

0.08 mg/kg
Vinclozolin

0.08 mg/kg
Phosalone

0.08 mg/kg
Trifloxystrobin

0.04 mg/kg

Phorate0.04 mg/kg
Triazophos

0.04 mg/kg

Phenthoate

0.08 mg/kg
Triallate

0.04 mg/kg

Permethrin

0.04 mg/kg
Triadimefon

0.04 mg/kg

Pendimethalin

0.04 mg/kg

0.04 mg/kg
Pyrazophos

Penconazole

Multiresidue GC Analysis (dried/oil Cat. C samples)

Tolylfluanid

0.04 mg/kg
Parathion-methyl

Detection LimitGC

Multiresidue GC Analysis (dried/oil Cat. C samples)

0.04 mg/kg
Quinalphos

0.04 mg/kg
Phosmet0.04 mg/kg
Quintozene

0.04 mg/kg
Phosphamidon

0.04 mg/kg
Quizalofop-ethyl0.08 mg/kg
Piperonyl-butoxide

0.04 mg/kg
Simazine

0.04 mg/kg
Pirimicarb

0.08 mg/kg
Simetryn

0.04 mg/kg
Pirimiphos-methyl0.04 mg/kg
Sulfentrazone

0.04 mg/kg
Prochloraz

0.04 mg/kg
Sulfotep

0.04 mg/kg
Procymidone

0.04 mg/kg
Tebuconazole

0.04 mg/kg
Profenofos

0.04 mg/kg
Tebufenpyrad

0.04 mg/kg
Prometryn

0.04 mg/kg
Terbacil

0.08 mg/kg
Propachlor

0.04 mg/kg
Terbufos

0.04 mg/kg
Propanil

0.04 mg/kg
Terbumeton

0.04 mg/kg
Propaphos

0.04 mg/kg
Terbuthylazine

0.2 mg/kg
Propargite

0.04 mg/kg
Terbuthylazine-desethyl0.04 mg/kg
Propazine

0.08 mg/kg
Terbutryn

0.04 mg/kg
Propetamphos

0.04 mg/kg
Tetrachlorvinphos

0.04 mg/kg
Propham

0.04 mg/kg
Tetradifon

0.04 mg/kg
Propiconazole

0.04 mg/kg
Thenylchlor

0.08 mg/kg
Propoxur

0.04 mg/kg
Thiobencarb

0.04 mg/kg
Propyzamide

0.08 mg/kg
Thiometon

0.04 mg/kg
Prothiofos

0.04 mg/kg
Tolclofos-methyl: 901964 v 1
Lab No:AnalytesGC

Hill Laboratories

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