# ADRIA E. COLI PH (10 niveaux de pH)

## PLAQUE 1

### Temps de détection pour les 8 dilutions

$$ \text{pH} = 4.49 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>9.59234</td><td>9.81535</td><td>10.0473</td><td>0.05205</td><td>0.002709</td><td>369.132</td></tr><tr><td>2</td><td>8.86028</td><td>9.14120</td><td>9.4544</td><td>0.06796</td><td>0.004619</td><td>216.507</td></tr><tr><td>3</td><td>7.86054</td><td>8.30652</td><td>8.7845</td><td>0.10570</td><td>0.011172</td><td>89.513</td></tr><tr><td>4</td><td>7.54395</td><td>7.92549</td><td>8.3485</td><td>0.06526</td><td>0.004258</td><td>234.840</td></tr><tr><td>5</td><td>7.05708</td><td>7.28499</td><td>7.5178</td><td>0.05271</td><td>0.002778</td><td>359.950</td></tr><tr><td>6</td><td>6.63239</td><td>6.89667</td><td>7.1689</td><td>0.04352</td><td>0.001894</td><td>528.056</td></tr><tr><td>7</td><td>6.05006</td><td>6.35638</td><td>6.6914</td><td>0.07336</td><td>0.005382</td><td>185.791</td></tr><tr><td>8</td><td>5.64319</td><td>5.87331</td><td>6.1030</td><td>0.03729</td><td>0.001391</td><td>719.042</td></tr></tbody></table>

$$ \text{pH} = 4.78 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>8.38332</td><td>8.70383</td><td>9.03749</td><td>0.087767</td><td>.007703016</td><td>129.819</td></tr><tr><td>2</td><td>7.89173</td><td>8.18692</td><td>8.49079</td><td>0.080373</td><td>.006459896</td><td>154.801</td></tr><tr><td>3</td><td>7.42742</td><td>7.69414</td><td>7.96876</td><td>0.072629</td><td>.005274993</td><td>189.574</td></tr><tr><td>4</td><td>6.95431</td><td>7.19048</td><td>7.45716</td><td>0.057524</td><td>.003308973</td><td>302.209</td></tr><tr><td>5</td><td>6.49915</td><td>6.77439</td><td>7.05464</td><td>0.063546</td><td>.004038047</td><td>247.644</td></tr><tr><td>6</td><td>6.02969</td><td>6.30473</td><td>6.59122</td><td>0.064236</td><td>.004126254</td><td>242.351</td></tr><tr><td>7</td><td>5.54304</td><td>5.82349</td><td>6.12013</td><td>0.066016</td><td>.004358095</td><td>229.458</td></tr><tr><td>8</td><td>5.25799</td><td>5.48905</td><td>5.75482</td><td>0.040298</td><td>.001623940</td><td>615.786</td></tr></tbody></table>

$$ \text{pH} = 5.00 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>9.30410</td><td>9.67222</td><td>10.0649</td><td>0.11182</td><td>0.012503</td><td>79.978</td></tr><tr><td>2</td><td>8.73310</td><td>9.07103</td><td>9.4468</td><td>0.09576</td><td>0.009170</td><td>109.052</td></tr><tr><td>3</td><td>8.57756</td><td>8.91477</td><td>9.3086</td><td>0.09808</td><td>0.009619</td><td>103.962</td></tr><tr><td>4</td><td>7.95781</td><td>8.24587</td><td>8.5503</td><td>0.07950</td><td>0.006320</td><td>158.229</td></tr><tr><td>5</td><td>7.56413</td><td>7.85082</td><td>8.1685</td><td>0.08109</td><td>0.006575</td><td>152.084</td></tr><tr><td>6</td><td>6.93850</td><td>7.24839</td><td>7.5778</td><td>0.08577</td><td>0.007357</td><td>135.933</td></tr><tr><td>7</td><td>6.42903</td><td>6.76797</td><td>7.1343</td><td>0.09462</td><td>0.008953</td><td>111.690</td></tr><tr><td>8</td><td>6.10150</td><td>6.37227</td><td>6.6687</td><td>0.06488</td><td>0.004210</td><td>237.536</td></tr></tbody></table>

$$ \text{pH} = 5.17 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>8.32735</td><td>8.62873</td><td>8.94216</td><td>0.09037</td><td>0.008166</td><td>122.460</td></tr><tr><td>2</td><td>7.69704</td><td>8.03007</td><td>8.39594</td><td>0.10272</td><td>0.010552</td><td>94.766</td></tr><tr><td>3</td><td>7.23125</td><td>7.61120</td><td>8.00780</td><td>0.11414</td><td>0.013028</td><td>76.760</td></tr><tr><td>4</td><td>6.82486</td><td>7.15225</td><td>7.49659</td><td>0.09873</td><td>0.009748</td><td>102.586</td></tr><tr><td>5</td><td>6.29487</td><td>6.68668</td><td>7.10883</td><td>0.11964</td><td>0.014313</td><td>69.866</td></tr><tr><td>6</td><td>5.86425</td><td>6.19885</td><td>6.55680</td><td>0.10179</td><td>0.010362</td><td>96.510</td></tr><tr><td>7</td><td>5.54756</td><td>5.82587</td><td>6.11017</td><td>0.08269</td><td>0.006838</td><td>146.241</td></tr><tr><td>8</td><td>5.05297</td><td>5.29985</td><td>5.56421</td><td>0.06859</td><td>0.004705</td><td>212.555</td></tr></tbody></table>
## pH = 5.95

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>8.17522</td><td>8.51636</td><td>8.86893</td><td>0.10815</td><td>0.011696</td><td>85.502</td></tr><tr><td>2</td><td>8.04562</td><td>8.36180</td><td>8.68343</td><td>0.10360</td><td>0.010734</td><td>93.164</td></tr><tr><td>3</td><td>7.49608</td><td>7.73114</td><td>7.97022</td><td>0.07392</td><td>0.005464</td><td>183.028</td></tr><tr><td>4</td><td>7.02012</td><td>7.37640</td><td>7.75517</td><td>0.11459</td><td>0.013132</td><td>76.153</td></tr><tr><td>5</td><td>6.70131</td><td>7.00286</td><td>7.31245</td><td>0.09527</td><td>0.009077</td><td>110.167</td></tr><tr><td>6</td><td>6.22540</td><td>6.44678</td><td>6.67056</td><td>0.06940</td><td>0.004816</td><td>207.635</td></tr><tr><td>7</td><td>5.75474</td><td>6.01330</td><td>6.27824</td><td>0.08161</td><td>0.006660</td><td>150.140</td></tr><tr><td>8</td><td>5.34438</td><td>5.59302</td><td>5.85099</td><td>0.07898</td><td>0.006238</td><td>160.317</td></tr></tbody></table>

## pH = 6.51

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>9.19726</td><td>9.51110</td><td>9.8292</td><td>0.11195</td><td>0.01253</td><td>79.786</td></tr><tr><td>2</td><td>8.80054</td><td>9.15824</td><td>9.5235</td><td>0.12619</td><td>0.01592</td><td>62.795</td></tr><tr><td>3</td><td>8.64438</td><td>8.81728</td><td>8.9900</td><td>0.06320</td><td>0.00399</td><td>250.349</td></tr><tr><td>4</td><td>6.65373</td><td>8.40484</td><td>10.0907</td><td>0.64453</td><td>0.41542</td><td>2.407</td></tr><tr><td>5</td><td>7.41672</td><td>7.67140</td><td>7.9291</td><td>0.08780</td><td>0.00771</td><td>129.721</td></tr><tr><td>6</td><td>-1.29957</td><td>6.49723</td><td>13.2656</td><td>2.86977</td><td>8.23557</td><td>0.121</td></tr><tr><td>7</td><td>-1.98550</td><td>6.12183</td><td>13.2171</td><td>3.00033</td><td>9.00201</td><td>0.111</td></tr><tr><td>8</td><td>6.02428</td><td>6.29530</td><td>6.5689</td><td>0.09506</td><td>0.00904</td><td>110.652</td></tr></tbody></table>

## pH = 6.98

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>11.6662</td><td>12.0836</td><td>12.5022</td><td>0.15403</td><td>0.02373</td><td>42.1495</td></tr><tr><td>2</td><td>10.6165</td><td>12.5551</td><td>14.4583</td><td>0.74000</td><td>0.54760</td><td>1.8261</td></tr><tr><td>3</td><td>10.8577</td><td>11.8246</td><td>12.7822</td><td>0.36781</td><td>0.13529</td><td>7.3918</td></tr><tr><td>4</td><td>9.0649</td><td>11.2720</td><td>13.4191</td><td>0.84681</td><td>0.71709</td><td>1.3945</td></tr><tr><td>5</td><td>10.3416</td><td>11.6606</td><td>12.9679</td><td>0.51156</td><td>0.26169</td><td>3.8212</td></tr><tr><td>6</td><td>7.2547</td><td>10.1898</td><td>13.0155</td><td>1.12213</td><td>1.25918</td><td>0.7942</td></tr><tr><td>7</td><td>4.8543</td><td>9.4580</td><td>13.7785</td><td>1.74966</td><td>3.06131</td><td>0.3267</td></tr><tr><td>8</td><td>6.8856</td><td>10.4260</td><td>13.8949</td><td>1.37715</td><td>1.89655</td><td>0.5273</td></tr></tbody></table>

## pH = 7.43

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>14.7616</td><td>15.0783</td><td>15.3993</td><td>0.12013</td><td>0.01443</td><td>69.2965</td></tr><tr><td>2</td><td>13.5835</td><td>14.3527</td><td>15.1327</td><td>0.29416</td><td>0.08653</td><td>11.5564</td></tr><tr><td>3</td><td>14.2341</td><td>14.6486</td><td>15.0678</td><td>0.15830</td><td>0.02506</td><td>39.9064</td></tr><tr><td>4</td><td>11.9900</td><td>13.5680</td><td>15.1649</td><td>0.61157</td><td>0.37402</td><td>2.6737</td></tr><tr><td>5</td><td>11.7727</td><td>13.2323</td><td>14.6995</td><td>0.56501</td><td>0.31924</td><td>3.1324</td></tr><tr><td>6</td><td>10.5547</td><td>13.7298</td><td>17.0358</td><td>1.25836</td><td>1.58348</td><td>0.6315</td></tr><tr><td>7</td><td>11.8684</td><td>13.3514</td><td>14.8549</td><td>0.58174</td><td>0.33842</td><td>2.9549</td></tr><tr><td>8</td><td>12.5390</td><td>13.9656</td><td>15.4225</td><td>0.56327</td><td>0.31727</td><td>3.1519</td></tr></tbody></table>
## pH = 8.48

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>21.7893</td><td>22.8810</td><td>24.0321</td><td>0.43200</td><td>0.18662</td><td>5.35837</td></tr><tr><td>2</td><td>22.0491</td><td>24.6747</td><td>27.6377</td><td>1.09018</td><td>1.18849</td><td>0.84141</td></tr><tr><td>3</td><td>18.3271</td><td>21.2934</td><td>24.4363</td><td>1.19338</td><td>1.42416</td><td>0.70217</td></tr><tr><td>4</td><td>18.8953</td><td>22.3656</td><td>26.1274</td><td>1.41948</td><td>2.01493</td><td>0.49630</td></tr><tr><td>5</td><td>16.2401</td><td>22.1252</td><td>28.7087</td><td>2.45668</td><td>6.03530</td><td>0.16569</td></tr><tr><td>6</td><td>23.6643</td><td>26.8270</td><td>30.3457</td><td>1.31755</td><td>1.73595</td><td>0.57606</td></tr><tr><td>7</td><td>17.3568</td><td>20.7193</td><td>24.2096</td><td>1.35546</td><td>1.83727</td><td>0.54429</td></tr><tr><td>8</td><td>19.6844</td><td>22.3420</td><td>25.1030</td><td>1.07387</td><td>1.15319</td><td>0.86716</td></tr></tbody></table>

## pH = 9.03

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>33.5001</td><td>34.6456</td><td>35.8826</td><td>0.46335</td><td>0.21470</td><td>4.65774</td></tr><tr><td>2</td><td>39.7563</td><td>42.2190</td><td>45.1358</td><td>1.05084</td><td>1.10426</td><td>0.90559</td></tr><tr><td>3</td><td>32.5866</td><td>35.3114</td><td>38.4243</td><td>1.14577</td><td>1.31279</td><td>0.76174</td></tr><tr><td>4</td><td>36.8031</td><td>38.2447</td><td>39.7953</td><td>0.58790</td><td>0.34563</td><td>2.89325</td></tr><tr><td>5</td><td>35.6641</td><td>40.6019</td><td>46.7517</td><td>2.18990</td><td>4.79567</td><td>0.20852</td></tr><tr><td>6</td><td>34.0091</td><td>37.6166</td><td>41.6773</td><td>1.51875</td><td>2.30659</td><td>0.43354</td></tr><tr><td>7</td><td>32.0769</td><td>36.1112</td><td>40.6769</td><td>1.70330</td><td>2.90121</td><td>0.34468</td></tr><tr><td>8</td><td>37.0551</td><td>41.9477</td><td>47.5946</td><td>2.09558</td><td>4.39144</td><td>0.22772</td></tr></tbody></table>
# Caractéristiques du paramètre mumax pour chaque niveau de pH
et pour chaque méthode de régression

## OLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.11749</td><td>1.24013</td><td>1.36276</td><td>0.05012</td><td>0.00251</td><td>4.041</td></tr><tr><td>2</td><td>1.42727</td><td>1.49007</td><td>1.55287</td><td>0.02566</td><td>0.00066</td><td>1.722</td></tr><tr><td>3</td><td>1.32642</td><td>1.44218</td><td>1.55793</td><td>0.04731</td><td>0.00224</td><td>3.280</td></tr><tr><td>4</td><td>1.42414</td><td>1.48586</td><td>1.54759</td><td>0.02523</td><td>0.00064</td><td>1.698</td></tr><tr><td>5</td><td>1.45623</td><td>1.58378</td><td>1.71133</td><td>0.05213</td><td>0.00272</td><td>3.291</td></tr><tr><td>6</td><td>0.92073</td><td>1.21022</td><td>1.49970</td><td>0.11831</td><td>0.01400</td><td>9.776</td></tr><tr><td>7</td><td>0.60679</td><td>1.39060</td><td>2.17441</td><td>0.32033</td><td>0.10261</td><td>23.035</td></tr><tr><td>8</td><td>0.02713</td><td>1.84869</td><td>3.67025</td><td>0.74443</td><td>0.55418</td><td>40.268</td></tr><tr><td>9</td><td>-0.76373</td><td>0.09124</td><td>0.94622</td><td>0.34941</td><td>0.12209</td><td>382.950</td></tr><tr><td>10</td><td>-0.71249</td><td>-0.16642</td><td>0.37965</td><td>0.22317</td><td>0.04980</td><td>134.099</td></tr></tbody></table>

## WLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.11700</td><td>1.23985</td><td>1.36270</td><td>0.05020</td><td>0.00252</td><td>4.049</td></tr><tr><td>2</td><td>1.42704</td><td>1.48985</td><td>1.55266</td><td>0.02567</td><td>0.00066</td><td>1.723</td></tr><tr><td>3</td><td>1.32618</td><td>1.44201</td><td>1.55784</td><td>0.04734</td><td>0.00224</td><td>3.283</td></tr><tr><td>4</td><td>1.42402</td><td>1.48580</td><td>1.54759</td><td>0.02525</td><td>0.00064</td><td>1.699</td></tr><tr><td>5</td><td>1.45641</td><td>1.58418</td><td>1.71195</td><td>0.05222</td><td>0.00273</td><td>3.296</td></tr><tr><td>6</td><td>0.92100</td><td>1.21023</td><td>1.49946</td><td>0.11820</td><td>0.01397</td><td>9.767</td></tr><tr><td>7</td><td>0.60633</td><td>1.39039</td><td>2.17445</td><td>0.32043</td><td>0.10268</td><td>23.046</td></tr><tr><td>8</td><td>0.03010</td><td>1.84540</td><td>3.66069</td><td>0.74187</td><td>0.55037</td><td>40.201</td></tr><tr><td>9</td><td>-0.76408</td><td>0.09307</td><td>0.95021</td><td>0.35030</td><td>0.12271</td><td>376.395</td></tr><tr><td>10</td><td>-0.71254</td><td>-0.16686</td><td>0.37883</td><td>0.22301</td><td>0.04973</td><td>133.655</td></tr></tbody></table>

## IRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.15073</td><td>1.24779</td><td>1.34486</td><td>0.03967</td><td>0.00157</td><td>3.179</td></tr><tr><td>2</td><td>1.42885</td><td>1.47702</td><td>1.52520</td><td>0.01969</td><td>0.00039</td><td>1.333</td></tr><tr><td>3</td><td>1.37115</td><td>1.44343</td><td>1.51570</td><td>0.02954</td><td>0.00087</td><td>2.046</td></tr><tr><td>4</td><td>1.43881</td><td>1.48768</td><td>1.53655</td><td>0.01997</td><td>0.00040</td><td>1.342</td></tr><tr><td>5</td><td>1.46514</td><td>1.56854</td><td>1.67194</td><td>0.04226</td><td>0.00179</td><td>2.694</td></tr><tr><td>6</td><td>0.93466</td><td>1.19788</td><td>1.46109</td><td>0.10757</td><td>0.01157</td><td>8.980</td></tr><tr><td>7</td><td>0.70349</td><td>1.28348</td><td>1.86347</td><td>0.23703</td><td>0.05618</td><td>18.468</td></tr><tr><td>8</td><td>0.56452</td><td>1.87857</td><td>3.19261</td><td>0.53702</td><td>0.28839</td><td>28.587</td></tr><tr><td>9</td><td>-0.76733</td><td>0.13789</td><td>1.04311</td><td>0.36994</td><td>0.13686</td><td>268.285</td></tr><tr><td>10</td><td>-0.70921</td><td>-0.22838</td><td>0.25246</td><td>0.19651</td><td>0.03861</td><td>86.045</td></tr></tbody></table>
## DWLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.121</td><td>1.2394</td><td>1.358</td><td>0.048</td><td>0.00</td><td>3.898</td></tr><tr><td>2</td><td>1.430</td><td>1.4943</td><td>1.559</td><td>0.026</td><td>0.00</td><td>1.761</td></tr><tr><td>3</td><td>1.330</td><td>1.4450</td><td>1.560</td><td>0.047</td><td>0.00</td><td>3.245</td></tr><tr><td>4</td><td>1.425</td><td>1.4859</td><td>1.546</td><td>0.025</td><td>0.00</td><td>1.664</td></tr><tr><td>5</td><td>1.462</td><td>1.5858</td><td>1.709</td><td>0.050</td><td>0.00</td><td>3.181</td></tr><tr><td>6</td><td>1.333</td><td>1.4517</td><td>1.571</td><td>0.049</td><td>0.00</td><td>3.346</td></tr><tr><td>7</td><td>0.893</td><td>3.2661</td><td>5.639</td><td>0.970</td><td>0.94</td><td>29.695</td></tr><tr><td>8</td><td>1.053</td><td>2.7283</td><td>4.404</td><td>0.685</td><td>0.47</td><td>25.094</td></tr><tr><td>9</td><td>-259.611</td><td>19.0798</td><td>297.771</td><td>113.891</td><td>12971.12</td><td>596.920</td></tr><tr><td>10</td><td>-2.171</td><td>-0.8993</td><td>0.373</td><td>0.520</td><td>0.27</td><td>-57.805</td></tr></tbody></table>

## IDRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.15664</td><td>1.25521</td><td>1.35379</td><td>0.04028</td><td>0.00162</td><td>3.2092</td></tr><tr><td>2</td><td>1.43114</td><td>1.47924</td><td>1.52734</td><td>0.01966</td><td>0.00039</td><td>1.3289</td></tr><tr><td>3</td><td>1.36991</td><td>1.45074</td><td>1.53157</td><td>0.03303</td><td>0.00109</td><td>2.2769</td></tr><tr><td>4</td><td>1.44025</td><td>1.49065</td><td>1.54105</td><td>0.02060</td><td>0.00042</td><td>1.3817</td></tr><tr><td>5</td><td>1.47420</td><td>1.57718</td><td>1.68015</td><td>0.04208</td><td>0.00177</td><td>2.6682</td></tr><tr><td>6</td><td>1.00232</td><td>1.27571</td><td>1.54909</td><td>0.11172</td><td>0.01248</td><td>8.7576</td></tr><tr><td>7</td><td>0.82271</td><td>1.59001</td><td>2.35731</td><td>0.31357</td><td>0.09832</td><td>19.7211</td></tr><tr><td>8</td><td>0.90876</td><td>3.08374</td><td>5.25872</td><td>0.88883</td><td>0.79003</td><td>28.8233</td></tr><tr><td>9</td><td>-0.21334</td><td>0.92631</td><td>2.06596</td><td>0.46574</td><td>0.21691</td><td>50.2786</td></tr><tr><td>10</td><td>-0.83119</td><td>-0.35507</td><td>0.12104</td><td>0.19457</td><td>0.03786</td><td>-54.7973</td></tr></tbody></table>
# ADRIA E. COLI PH (10 niveaux de pH)

## PLAQUE 2

### Temps de détection pour les 8 dilutions

$$ \text{pH} = 4.48 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>23.8274</td><td>27.1015</td><td>30.4042</td><td>1.31259</td><td>1.72291</td><td>0.58042</td></tr><tr><td>2</td><td>26.9268</td><td>29.6942</td><td>32.5129</td><td>1.11173</td><td>1.23594</td><td>0.80910</td></tr><tr><td>3</td><td>27.3688</td><td>30.1158</td><td>32.9227</td><td>1.10373</td><td>1.21823</td><td>0.82086</td></tr><tr><td>4</td><td>28.1968</td><td>30.2160</td><td>32.2727</td><td>0.80726</td><td>0.65166</td><td>1.53454</td></tr><tr><td>5</td><td>28.4640</td><td>30.3519</td><td>32.2784</td><td>0.75220</td><td>0.56580</td><td>1.76741</td></tr><tr><td>6</td><td>30.1423</td><td>31.3294</td><td>32.5407</td><td>0.47075</td><td>0.22161</td><td>4.51250</td></tr><tr><td>7</td><td>30.6036</td><td>31.7771</td><td>32.9825</td><td>0.46470</td><td>0.21594</td><td>4.63088</td></tr><tr><td>8</td><td>32.2492</td><td>33.2350</td><td>34.2673</td><td>0.39040</td><td>0.15241</td><td>6.56132</td></tr></tbody></table>

$$ \text{pH} = 4.80 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>11.5952</td><td>12.1441</td><td>12.6874</td><td>0.20376</td><td>0.04152</td><td>24.0860</td></tr><tr><td>2</td><td>11.9670</td><td>13.2322</td><td>14.4691</td><td>0.47820</td><td>0.22867</td><td>4.3731</td></tr><tr><td>3</td><td>12.5118</td><td>14.1325</td><td>15.7107</td><td>0.61617</td><td>0.37967</td><td>2.6339</td></tr><tr><td>4</td><td>13.2324</td><td>14.9567</td><td>16.6352</td><td>0.65690</td><td>0.43152</td><td>2.3174</td></tr><tr><td>5</td><td>13.5526</td><td>15.9067</td><td>18.1588</td><td>0.89434</td><td>0.79984</td><td>1.2503</td></tr><tr><td>6</td><td>13.4653</td><td>16.7936</td><td>19.9575</td><td>1.27137</td><td>1.61638</td><td>0.6187</td></tr><tr><td>7</td><td>14.3898</td><td>17.7576</td><td>20.9589</td><td>1.28793</td><td>1.65876</td><td>0.6029</td></tr><tr><td>8</td><td>16.1799</td><td>18.4899</td><td>20.6877</td><td>0.87201</td><td>0.76040</td><td>1.3151</td></tr></tbody></table>

$$ \text{pH} = 5.02 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>9.9294</td><td>10.9443</td><td>11.9358</td><td>0.37956</td><td>0.14406</td><td>6.94137</td></tr><tr><td>2</td><td>10.5593</td><td>11.4679</td><td>12.3526</td><td>0.33630</td><td>0.11310</td><td>8.84195</td></tr><tr><td>3</td><td>9.5211</td><td>12.2623</td><td>14.8634</td><td>1.04060</td><td>1.08284</td><td>0.92350</td></tr><tr><td>4</td><td>11.0742</td><td>13.0635</td><td>14.9846</td><td>0.75644</td><td>0.57220</td><td>1.74764</td></tr><tr><td>5</td><td>10.0472</td><td>12.9074</td><td>15.6086</td><td>1.08328</td><td>1.17350</td><td>0.85215</td></tr><tr><td>6</td><td>12.2250</td><td>14.5063</td><td>16.6970</td><td>0.86829</td><td>0.75393</td><td>1.32638</td></tr><tr><td>7</td><td>9.2252</td><td>12.7953</td><td>16.1587</td><td>1.35779</td><td>1.84360</td><td>0.54242</td></tr><tr><td>8</td><td>14.6681</td><td>16.0988</td><td>17.4970</td><td>0.54219</td><td>0.29397</td><td>3.40173</td></tr></tbody></table>

$$ \text{pH} = 5.23 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>8.6464</td><td>9.2100</td><td>9.7623</td><td>0.20404</td><td>0.04163</td><td>24.0189</td></tr><tr><td>2</td><td>9.2135</td><td>9.7781</td><td>10.3359</td><td>0.20817</td><td>0.04333</td><td>23.0765</td></tr><tr><td>3</td><td>10.1367</td><td>10.8646</td><td>11.5752</td><td>0.26835</td><td>0.07201</td><td>13.8862</td></tr><tr><td>4</td><td>10.8287</td><td>11.5036</td><td>12.1668</td><td>0.24963</td><td>0.06232</td><td>16.0472</td></tr><tr><td>5</td><td>11.2620</td><td>12.0863</td><td>12.8876</td><td>0.30328</td><td>0.09198</td><td>10.8718</td></tr><tr><td>6</td><td>11.8866</td><td>12.7639</td><td>13.6203</td><td>0.32512</td><td>0.10570</td><td>9.4605</td></tr><tr><td>7</td><td>12.5988</td><td>13.6750</td><td>14.7150</td><td>0.39868</td><td>0.15895</td><td>6.2913</td></tr><tr><td>8</td><td>13.3510</td><td>14.3650</td><td>15.3530</td><td>0.37871</td><td>0.14342</td><td>6.9723</td></tr></tbody></table>
## pH = 5.78

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.4364</td><td>8.2777</td><td>9.1002</td><td>0.31199</td><td>0.097340</td><td>10.273</td></tr><tr><td>2</td><td>8.3347</td><td>8.6142</td><td>8.8936</td><td>0.10026</td><td>0.010053</td><td>99.474</td></tr><tr><td>3</td><td>8.8124</td><td>9.1210</td><td>9.4296</td><td>0.11286</td><td>0.012737</td><td>78.513</td></tr><tr><td>4</td><td>9.4241</td><td>9.6669</td><td>9.9092</td><td>0.08792</td><td>0.007729</td><td>129.377</td></tr><tr><td>5</td><td>9.8546</td><td>10.2400</td><td>10.6237</td><td>0.14063</td><td>0.019778</td><td>50.562</td></tr><tr><td>6</td><td>10.1097</td><td>10.8735</td><td>11.6258</td><td>0.28284</td><td>0.079996</td><td>12.501</td></tr><tr><td>7</td><td>10.6063</td><td>11.4345</td><td>12.2491</td><td>0.30806</td><td>0.094901</td><td>10.537</td></tr><tr><td>8</td><td>11.3806</td><td>11.7283</td><td>12.0745</td><td>0.12688</td><td>0.016099</td><td>62.114</td></tr></tbody></table>

## pH = 6.49

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.5907</td><td>7.7768</td><td>7.9633</td><td>0.06813</td><td>0.004641</td><td>215.457</td></tr><tr><td>2</td><td>7.8836</td><td>8.1838</td><td>8.4858</td><td>0.10913</td><td>0.011909</td><td>83.967</td></tr><tr><td>3</td><td>8.6396</td><td>8.7981</td><td>8.9567</td><td>0.05747</td><td>0.003302</td><td>302.821</td></tr><tr><td>4</td><td>9.0060</td><td>9.2502</td><td>9.4951</td><td>0.08942</td><td>0.007996</td><td>125.059</td></tr><tr><td>5</td><td>9.5969</td><td>9.7842</td><td>9.9716</td><td>0.06902</td><td>0.004764</td><td>209.889</td></tr><tr><td>6</td><td>10.1710</td><td>10.3688</td><td>10.5666</td><td>0.07233</td><td>0.005232</td><td>191.135</td></tr><tr><td>7</td><td>10.6908</td><td>10.8521</td><td>11.0134</td><td>0.05898</td><td>0.003479</td><td>287.474</td></tr><tr><td>8</td><td>10.9944</td><td>11.2402</td><td>11.4860</td><td>0.09057</td><td>0.008204</td><td>121.899</td></tr></tbody></table>

## pH = 7.04

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.4530</td><td>7.8589</td><td>8.2632</td><td>0.14927</td><td>0.022282</td><td>44.8787</td></tr><tr><td>2</td><td>7.9022</td><td>8.2756</td><td>8.6491</td><td>0.13761</td><td>0.018936</td><td>52.8106</td></tr><tr><td>3</td><td>8.3639</td><td>8.7360</td><td>9.1095</td><td>0.13633</td><td>0.018585</td><td>53.8073</td></tr><tr><td>4</td><td>8.8084</td><td>9.1894</td><td>9.5744</td><td>0.14006</td><td>0.019616</td><td>50.9778</td></tr><tr><td>5</td><td>9.3405</td><td>9.6920</td><td>10.0461</td><td>0.12787</td><td>0.016351</td><td>61.1578</td></tr><tr><td>6</td><td>9.8356</td><td>10.2490</td><td>10.6643</td><td>0.15153</td><td>0.022960</td><td>43.5540</td></tr><tr><td>7</td><td>10.3386</td><td>10.7094</td><td>11.0811</td><td>0.13576</td><td>0.018429</td><td>54.2610</td></tr><tr><td>8</td><td>10.9149</td><td>11.2240</td><td>11.5339</td><td>0.11317</td><td>0.012808</td><td>78.0762</td></tr></tbody></table>

## pH = 7.52

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.6731</td><td>7.8991</td><td>8.1238</td><td>0.07723</td><td>0.005965</td><td>167.640</td></tr><tr><td>2</td><td>8.0424</td><td>8.3226</td><td>8.6043</td><td>0.09630</td><td>0.009274</td><td>107.833</td></tr><tr><td>3</td><td>8.6089</td><td>8.8891</td><td>9.1696</td><td>0.09787</td><td>0.009579</td><td>104.393</td></tr><tr><td>4</td><td>9.0323</td><td>9.3600</td><td>9.6874</td><td>0.11436</td><td>0.013078</td><td>76.466</td></tr><tr><td>5</td><td>9.6874</td><td>9.9406</td><td>10.1948</td><td>0.08856</td><td>0.007843</td><td>127.497</td></tr><tr><td>6</td><td>9.7017</td><td>10.1221</td><td>10.5484</td><td>0.14510</td><td>0.021054</td><td>47.496</td></tr><tr><td>7</td><td>10.3988</td><td>10.7200</td><td>11.0433</td><td>0.11250</td><td>0.012657</td><td>79.009</td></tr><tr><td>8</td><td>10.9209</td><td>11.1621</td><td>11.4037</td><td>0.08427</td><td>0.007101</td><td>140.831</td></tr></tbody></table>
## pH = 8.54

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.8736</td><td>8.5659</td><td>9.3004</td><td>0.24451</td><td>0.059784</td><td>16.7268</td></tr><tr><td>2</td><td>8.2600</td><td>8.9425</td><td>9.6831</td><td>0.24387</td><td>0.059470</td><td>16.8151</td></tr><tr><td>3</td><td>8.6721</td><td>9.2898</td><td>9.9382</td><td>0.21696</td><td>0.047071</td><td>21.2445</td></tr><tr><td>4</td><td>9.2109</td><td>9.7925</td><td>10.4014</td><td>0.20401</td><td>0.041621</td><td>24.0262</td></tr><tr><td>5</td><td>9.7756</td><td>10.3450</td><td>10.9453</td><td>0.20045</td><td>0.040180</td><td>24.8881</td></tr><tr><td>6</td><td>10.2758</td><td>10.8638</td><td>11.4867</td><td>0.20751</td><td>0.043060</td><td>23.2231</td></tr><tr><td>7</td><td>10.8064</td><td>11.3179</td><td>11.8400</td><td>0.18040</td><td>0.032545</td><td>30.7270</td></tr><tr><td>8</td><td>11.1705</td><td>11.6735</td><td>12.1884</td><td>0.17443</td><td>0.030426</td><td>32.8666</td></tr></tbody></table>

## pH = 9.50

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>33.5001</td><td>34.6456</td><td>35.8826</td><td>0.46335</td><td>0.21470</td><td>4.65774</td></tr><tr><td>2</td><td>39.7563</td><td>42.2190</td><td>45.1358</td><td>1.05084</td><td>1.10426</td><td>0.90559</td></tr><tr><td>3</td><td>32.5866</td><td>35.3114</td><td>38.4243</td><td>1.14577</td><td>1.31279</td><td>0.76174</td></tr><tr><td>4</td><td>36.8031</td><td>38.2447</td><td>39.7953</td><td>0.58790</td><td>0.34563</td><td>2.89325</td></tr><tr><td>5</td><td>35.6641</td><td>40.6019</td><td>46.7517</td><td>2.18990</td><td>4.79567</td><td>0.20852</td></tr><tr><td>6</td><td>34.0091</td><td>37.6166</td><td>41.6773</td><td>1.51875</td><td>2.30659</td><td>0.43354</td></tr><tr><td>7</td><td>32.0769</td><td>36.1112</td><td>40.6769</td><td>1.70330</td><td>2.90121</td><td>0.34468</td></tr><tr><td>8</td><td>37.0551</td><td>41.9477</td><td>47.5946</td><td>2.09558</td><td>4.39144</td><td>0.22772</td></tr></tbody></table>
# Caractéristiques du paramètre mumax pour chaque niveau de pH
et pour chaque méthode de régression

## OLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.54750</td><td>0.88718</td><td>1.22686</td><td>0.13882</td><td>0.019271</td><td>15.647</td></tr><tr><td>2</td><td>0.73617</td><td>0.76351</td><td>0.79085</td><td>0.01117</td><td>0.000125</td><td>1.463</td></tr><tr><td>3</td><td>0.39229</td><td>0.89507</td><td>1.39785</td><td>0.20547</td><td>0.042220</td><td>22.956</td></tr><tr><td>4</td><td>0.87737</td><td>0.93540</td><td>0.99343</td><td>0.02372</td><td>0.000562</td><td>2.535</td></tr><tr><td>5</td><td>1.21257</td><td>1.31005</td><td>1.40754</td><td>0.03984</td><td>0.001587</td><td>3.041</td></tr><tr><td>6</td><td>1.29489</td><td>1.35346</td><td>1.41204</td><td>0.02394</td><td>0.000573</td><td>1.769</td></tr><tr><td>7</td><td>1.36915</td><td>1.42285</td><td>1.47654</td><td>0.02194</td><td>0.000482</td><td>1.542</td></tr><tr><td>8</td><td>1.36642</td><td>1.47705</td><td>1.58768</td><td>0.04521</td><td>0.002044</td><td>3.061</td></tr><tr><td>9</td><td>1.39032</td><td>1.48671</td><td>1.58310</td><td>0.03939</td><td>0.001552</td><td>2.650</td></tr><tr><td>10</td><td>-0.37965</td><td>0.16642</td><td>0.71249</td><td>0.22317</td><td>0.049803</td><td>134.099</td></tr></tbody></table>

## WLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.54691</td><td>0.88663</td><td>1.22635</td><td>0.13884</td><td>0.019275</td><td>15.659</td></tr><tr><td>2</td><td>0.73603</td><td>0.76339</td><td>0.79076</td><td>0.01118</td><td>0.000125</td><td>1.465</td></tr><tr><td>3</td><td>0.39141</td><td>0.89597</td><td>1.40052</td><td>0.20620</td><td>0.042519</td><td>23.014</td></tr><tr><td>4</td><td>0.87738</td><td>0.93542</td><td>0.99346</td><td>0.02372</td><td>0.000563</td><td>2.536</td></tr><tr><td>5</td><td>1.21246</td><td>1.31004</td><td>1.40762</td><td>0.03988</td><td>0.001590</td><td>3.044</td></tr><tr><td>6</td><td>1.29498</td><td>1.35349</td><td>1.41201</td><td>0.02391</td><td>0.000572</td><td>1.767</td></tr><tr><td>7</td><td>1.36908</td><td>1.42298</td><td>1.47687</td><td>0.02203</td><td>0.000485</td><td>1.548</td></tr><tr><td>8</td><td>1.36631</td><td>1.47686</td><td>1.58740</td><td>0.04518</td><td>0.002041</td><td>3.059</td></tr><tr><td>9</td><td>1.39007</td><td>1.48668</td><td>1.58330</td><td>0.03948</td><td>0.001559</td><td>2.656</td></tr><tr><td>10</td><td>-0.37883</td><td>0.16686</td><td>0.71254</td><td>0.22301</td><td>0.049733</td><td>133.655</td></tr></tbody></table>

## IRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.60504</td><td>0.88831</td><td>1.17158</td><td>0.11577</td><td>0.013402</td><td>13.0321</td></tr><tr><td>2</td><td>0.73723</td><td>0.76464</td><td>0.79204</td><td>0.01120</td><td>0.000125</td><td>1.4647</td></tr><tr><td>3</td><td>0.61562</td><td>0.90242</td><td>1.18923</td><td>0.11721</td><td>0.013738</td><td>12.9883</td></tr><tr><td>4</td><td>0.89683</td><td>0.93443</td><td>0.97202</td><td>0.01536</td><td>0.000236</td><td>1.6443</td></tr><tr><td>5</td><td>1.20079</td><td>1.29591</td><td>1.39102</td><td>0.03887</td><td>0.001511</td><td>2.9996</td></tr><tr><td>6</td><td>1.29463</td><td>1.34915</td><td>1.40367</td><td>0.02228</td><td>0.000496</td><td>1.6514</td></tr><tr><td>7</td><td>1.37518</td><td>1.41575</td><td>1.45633</td><td>0.01658</td><td>0.000275</td><td>1.1713</td></tr><tr><td>8</td><td>1.41293</td><td>1.47831</td><td>1.54369</td><td>0.02672</td><td>0.000714</td><td>1.8073</td></tr><tr><td>9</td><td>1.40358</td><td>1.48628</td><td>1.56897</td><td>0.03379</td><td>0.001142</td><td>2.2737</td></tr><tr><td>10</td><td>-0.27170</td><td>0.21585</td><td>0.70339</td><td>0.19925</td><td>0.039700</td><td>92.3111</td></tr></tbody></table>
## DWLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.66607</td><td>0.97843</td><td>1.29080</td><td>0.12765</td><td>0.01630</td><td>13.0467</td></tr><tr><td>2</td><td>0.72184</td><td>0.75381</td><td>0.78579</td><td>0.01307</td><td>0.00017</td><td>1.7333</td></tr><tr><td>3</td><td>0.74589</td><td>0.99026</td><td>1.23462</td><td>0.09986</td><td>0.00997</td><td>10.0846</td></tr><tr><td>4</td><td>0.87349</td><td>0.93511</td><td>0.99673</td><td>0.02518</td><td>0.00063</td><td>2.6928</td></tr><tr><td>5</td><td>1.22926</td><td>1.31506</td><td>1.40086</td><td>0.03506</td><td>0.00123</td><td>2.6663</td></tr><tr><td>6</td><td>1.29681</td><td>1.35463</td><td>1.41245</td><td>0.02363</td><td>0.00056</td><td>1.7443</td></tr><tr><td>7</td><td>1.36884</td><td>1.42162</td><td>1.47439</td><td>0.02157</td><td>0.00047</td><td>1.5171</td></tr><tr><td>8</td><td>1.37036</td><td>1.47524</td><td>1.58012</td><td>0.04286</td><td>0.00184</td><td>2.9053</td></tr><tr><td>9</td><td>1.39109</td><td>1.48657</td><td>1.58205</td><td>0.03902</td><td>0.00152</td><td>2.6248</td></tr><tr><td>10</td><td>-0.37276</td><td>0.89933</td><td>2.17143</td><td>0.51986</td><td>0.27026</td><td>57.8051</td></tr></tbody></table>

## IDRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.63013</td><td>0.95244</td><td>1.27475</td><td>0.13172</td><td>0.017349</td><td>13.8293</td></tr><tr><td>2</td><td>0.74078</td><td>0.76742</td><td>0.79406</td><td>0.01089</td><td>0.000119</td><td>1.4186</td></tr><tr><td>3</td><td>0.66979</td><td>0.97190</td><td>1.27401</td><td>0.12346</td><td>0.015243</td><td>12.7031</td></tr><tr><td>4</td><td>0.89506</td><td>0.93539</td><td>0.97571</td><td>0.01648</td><td>0.000272</td><td>1.7619</td></tr><tr><td>5</td><td>1.20302</td><td>1.29526</td><td>1.38751</td><td>0.03770</td><td>0.001421</td><td>2.9104</td></tr><tr><td>6</td><td>1.30080</td><td>1.35469</td><td>1.40859</td><td>0.02203</td><td>0.000485</td><td>1.6259</td></tr><tr><td>7</td><td>1.37651</td><td>1.41836</td><td>1.46022</td><td>0.01711</td><td>0.000293</td><td>1.2060</td></tr><tr><td>8</td><td>1.40990</td><td>1.48096</td><td>1.55202</td><td>0.02904</td><td>0.000843</td><td>1.9609</td></tr><tr><td>9</td><td>1.40808</td><td>1.49112</td><td>1.57415</td><td>0.03393</td><td>0.001151</td><td>2.2757</td></tr><tr><td>10</td><td>-0.12103</td><td>0.35508</td><td>0.83120</td><td>0.19457</td><td>0.037858</td><td>54.7961</td></tr></tbody></table>
# ADRIA L.M. PH (9 niveaux de pH)

## PLAQUE 1

### Temps de détection pour les 8 dilutions

$$ \text{pH} = 4.83 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>18.7203</td><td>19.0867</td><td>19.4534</td><td>0.14321</td><td>0.02051</td><td>48.7617</td></tr><tr><td>2</td><td>19.9332</td><td>20.3666</td><td>20.8003</td><td>0.16937</td><td>0.02869</td><td>34.8587</td></tr><tr><td>3</td><td>21.3987</td><td>21.8283</td><td>22.2581</td><td>0.16829</td><td>0.02832</td><td>35.3082</td></tr><tr><td>4</td><td>22.8250</td><td>23.0902</td><td>23.3554</td><td>0.10375</td><td>0.01076</td><td>92.8972</td></tr><tr><td>5</td><td>24.7293</td><td>25.2375</td><td>25.7457</td><td>0.20026</td><td>0.04010</td><td>24.9352</td></tr><tr><td>6</td><td>25.4934</td><td>25.8462</td><td>26.1990</td><td>0.13863</td><td>0.01922</td><td>52.0346</td></tr><tr><td>7</td><td>27.3005</td><td>27.8693</td><td>28.4374</td><td>0.22380</td><td>0.05009</td><td>19.9649</td></tr><tr><td>8</td><td>28.6542</td><td>29.5722</td><td>30.4888</td><td>0.36313</td><td>0.13186</td><td>7.5837</td></tr></tbody></table>

$$ \text{pH} = 5.03 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>14.9860</td><td>15.4654</td><td>15.9445</td><td>0.18671</td><td>0.034860</td><td>28.686</td></tr><tr><td>2</td><td>15.3774</td><td>15.7607</td><td>16.1444</td><td>0.14837</td><td>0.022015</td><td>45.425</td></tr><tr><td>3</td><td>16.2761</td><td>16.6767</td><td>17.0776</td><td>0.15533</td><td>0.024128</td><td>41.445</td></tr><tr><td>4</td><td>16.9406</td><td>17.3784</td><td>17.8173</td><td>0.16925</td><td>0.028646</td><td>34.909</td></tr><tr><td>5</td><td>18.1341</td><td>18.4088</td><td>18.6837</td><td>0.10610</td><td>0.011256</td><td>88.838</td></tr><tr><td>6</td><td>19.4381</td><td>19.8329</td><td>20.2277</td><td>0.15380</td><td>0.023655</td><td>42.274</td></tr><tr><td>7</td><td>20.6218</td><td>20.8452</td><td>21.0688</td><td>0.08628</td><td>0.007445</td><td>134.317</td></tr><tr><td>8</td><td>21.3358</td><td>21.5823</td><td>21.8289</td><td>0.09477</td><td>0.008980</td><td>111.353</td></tr></tbody></table>

$$ \text{pH} = 5.25 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>12.3001</td><td>12.6950</td><td>13.0902</td><td>0.15143</td><td>0.022932</td><td>43.6075</td></tr><tr><td>2</td><td>13.0532</td><td>13.5719</td><td>14.0922</td><td>0.19964</td><td>0.039858</td><td>25.0891</td></tr><tr><td>3</td><td>14.5042</td><td>14.8364</td><td>15.1686</td><td>0.12854</td><td>0.016522</td><td>60.5267</td></tr><tr><td>4</td><td>15.2333</td><td>15.6705</td><td>16.1074</td><td>0.16875</td><td>0.028478</td><td>35.1148</td></tr><tr><td>5</td><td>16.1480</td><td>16.6118</td><td>17.0752</td><td>0.17900</td><td>0.032040</td><td>31.2113</td></tr><tr><td>6</td><td>16.9878</td><td>17.2783</td><td>17.5688</td><td>0.11104</td><td>0.012331</td><td>81.0991</td></tr><tr><td>7</td><td>17.6368</td><td>17.9756</td><td>18.3148</td><td>0.12918</td><td>0.016688</td><td>59.9231</td></tr><tr><td>8</td><td>18.3225</td><td>18.7411</td><td>19.1609</td><td>0.15921</td><td>0.025349</td><td>39.4492</td></tr></tbody></table>

$$ \text{pH} = 6.05 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>9.7185</td><td>10.0832</td><td>10.4485</td><td>0.13620</td><td>0.018551</td><td>53.9063</td></tr><tr><td>2</td><td>10.3480</td><td>10.7636</td><td>11.1826</td><td>0.15375</td><td>0.023640</td><td>42.3005</td></tr><tr><td>3</td><td>11.0457</td><td>11.4493</td><td>11.8553</td><td>0.14916</td><td>0.022248</td><td>44.9476</td></tr><tr><td>4</td><td>11.8291</td><td>12.2552</td><td>12.6847</td><td>0.15764</td><td>0.024849</td><td>40.2424</td></tr><tr><td>5</td><td>12.4992</td><td>12.9202</td><td>13.3434</td><td>0.15553</td><td>0.024191</td><td>41.3378</td></tr><tr><td>6</td><td>13.2142</td><td>13.6137</td><td>14.0145</td><td>0.14746</td><td>0.021744</td><td>45.9904</td></tr><tr><td>7</td><td>14.0069</td><td>14.3480</td><td>14.6899</td><td>0.12584</td><td>0.015835</td><td>63.1524</td></tr><tr><td>8</td><td>14.7195</td><td>15.0420</td><td>15.3648</td><td>0.11890</td><td>0.014136</td><td>70.7407</td></tr></tbody></table>
## pH = 6.49

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>8.7897</td><td>9.5541</td><td>10.3412</td><td>0.28368</td><td>0.080475</td><td>12.4262</td></tr><tr><td>2</td><td>9.5181</td><td>10.2179</td><td>10.9327</td><td>0.25865</td><td>0.066898</td><td>14.9482</td></tr><tr><td>3</td><td>10.1783</td><td>10.8946</td><td>11.6332</td><td>0.26368</td><td>0.069526</td><td>14.3831</td></tr><tr><td>4</td><td>10.7211</td><td>11.4640</td><td>12.2238</td><td>0.27476</td><td>0.075495</td><td>13.2460</td></tr><tr><td>5</td><td>11.7172</td><td>12.3381</td><td>12.9731</td><td>0.22762</td><td>0.051810</td><td>19.3012</td></tr><tr><td>6</td><td>12.4549</td><td>12.9987</td><td>13.5505</td><td>0.19856</td><td>0.039427</td><td>25.3635</td></tr><tr><td>7</td><td>13.0724</td><td>13.5750</td><td>14.0842</td><td>0.18149</td><td>0.032938</td><td>30.3597</td></tr><tr><td>8</td><td>13.8408</td><td>14.3657</td><td>14.8966</td><td>0.19306</td><td>0.037272</td><td>26.8300</td></tr></tbody></table>

## pH = 6.97

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>8.6740</td><td>9.3157</td><td>9.9792</td><td>0.23124</td><td>0.053473</td><td>18.7010</td></tr><tr><td>2</td><td>9.2111</td><td>9.9351</td><td>10.6977</td><td>0.26339</td><td>0.069375</td><td>14.4144</td></tr><tr><td>3</td><td>9.8959</td><td>10.5915</td><td>11.3147</td><td>0.25137</td><td>0.063185</td><td>15.8266</td></tr><tr><td>4</td><td>10.5040</td><td>11.2865</td><td>12.1251</td><td>0.28720</td><td>0.082486</td><td>12.1233</td></tr><tr><td>5</td><td>11.1978</td><td>12.0053</td><td>12.8692</td><td>0.29612</td><td>0.087690</td><td>11.4039</td></tr><tr><td>6</td><td>11.9869</td><td>12.7310</td><td>13.5204</td><td>0.27170</td><td>0.073821</td><td>13.5464</td></tr><tr><td>7</td><td>12.6909</td><td>13.3867</td><td>14.1141</td><td>0.25214</td><td>0.063575</td><td>15.7295</td></tr><tr><td>8</td><td>13.2534</td><td>14.0052</td><td>14.8057</td><td>0.27502</td><td>0.075636</td><td>13.2212</td></tr></tbody></table>

## pH = 7.48

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>8.3199</td><td>9.1647</td><td>10.0915</td><td>0.31387</td><td>0.09851</td><td>10.1508</td></tr><tr><td>2</td><td>9.0361</td><td>9.8719</td><td>10.7827</td><td>0.30946</td><td>0.09576</td><td>10.4425</td></tr><tr><td>3</td><td>9.5066</td><td>10.4484</td><td>11.4605</td><td>0.35046</td><td>0.12283</td><td>8.1416</td></tr><tr><td>4</td><td>10.2219</td><td>11.1645</td><td>12.1732</td><td>0.35001</td><td>0.12250</td><td>8.1630</td></tr><tr><td>5</td><td>10.9796</td><td>11.8508</td><td>12.8009</td><td>0.32268</td><td>0.10412</td><td>9.6039</td></tr><tr><td>6</td><td>11.6887</td><td>12.5029</td><td>13.3743</td><td>0.29864</td><td>0.08919</td><td>11.2123</td></tr><tr><td>7</td><td>12.2031</td><td>13.1286</td><td>14.1133</td><td>0.34264</td><td>0.11740</td><td>8.5178</td></tr><tr><td>8</td><td>12.9778</td><td>13.7903</td><td>14.6640</td><td>0.29875</td><td>0.08925</td><td>11.2043</td></tr></tbody></table>

## pH = 8.46

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>8.4392</td><td>9.4576</td><td>10.5121</td><td>0.38192</td><td>0.14586</td><td>6.8559</td></tr><tr><td>2</td><td>9.1314</td><td>10.1198</td><td>11.1526</td><td>0.36957</td><td>0.13658</td><td>7.3218</td></tr><tr><td>3</td><td>9.8943</td><td>10.8445</td><td>11.8334</td><td>0.35456</td><td>0.12571</td><td>7.9548</td></tr><tr><td>4</td><td>10.5935</td><td>11.5087</td><td>12.4711</td><td>0.34029</td><td>0.11580</td><td>8.6359</td></tr><tr><td>5</td><td>11.1211</td><td>12.1437</td><td>13.2420</td><td>0.38437</td><td>0.14774</td><td>6.7685</td></tr><tr><td>6</td><td>11.9403</td><td>12.8103</td><td>13.7103</td><td>0.32364</td><td>0.10474</td><td>9.5475</td></tr><tr><td>7</td><td>12.6397</td><td>13.4329</td><td>14.2435</td><td>0.29325</td><td>0.08600</td><td>11.6284</td></tr><tr><td>8</td><td>13.2123</td><td>14.1203</td><td>15.0854</td><td>0.33948</td><td>0.11524</td><td>8.6772</td></tr></tbody></table>

## pH = 9.03

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>9.3651</td><td>10.2192</td><td>11.0961</td><td>0.31651</td><td>0.10018</td><td>9.9824</td></tr><tr><td>2</td><td>9.7596</td><td>10.8415</td><td>12.0013</td><td>0.40628</td><td>0.16506</td><td>6.0584</td></tr><tr><td>3</td><td>11.0510</td><td>11.8171</td><td>12.5853</td><td>0.28623</td><td>0.08193</td><td>12.2060</td></tr><tr><td>4</td><td>11.0448</td><td>12.2183</td><td>13.5047</td><td>0.44583</td><td>0.19876</td><td>5.0311</td></tr><tr><td>5</td><td>12.0681</td><td>13.0330</td><td>14.0222</td><td>0.36242</td><td>0.13135</td><td>7.6132</td></tr><tr><td>6</td><td>12.5488</td><td>13.6103</td><td>14.7219</td><td>0.39734</td><td>0.15788</td><td>6.3341</td></tr><tr><td>7</td><td>13.4080</td><td>14.3288</td><td>15.3023</td><td>0.33977</td><td>0.11544</td><td>8.6621</td></tr><tr><td>8</td><td>14.1834</td><td>15.0761</td><td>16.0179</td><td>0.32904</td><td>0.10827</td><td>9.2363</td></tr></tbody></table>
# Caractéristiques du paramètre mumax pour chaque niveau de pH
et pour chaque méthode de régression

## OLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.42280</td><td>0.46122</td><td>0.49963</td><td>0.015699</td><td>.000246474</td><td>3.40393</td></tr><tr><td>2</td><td>0.62818</td><td>0.72480</td><td>0.82142</td><td>0.039487</td><td>.001559247</td><td>5.44804</td></tr><tr><td>3</td><td>0.71892</td><td>0.79297</td><td>0.86701</td><td>0.030261</td><td>.000915757</td><td>3.81624</td></tr><tr><td>4</td><td>0.96081</td><td>0.97123</td><td>0.98165</td><td>0.004259</td><td>.000018137</td><td>0.43849</td></tr><tr><td>5</td><td>0.96179</td><td>1.00577</td><td>1.04974</td><td>0.017970</td><td>.000322934</td><td>1.78674</td></tr><tr><td>6</td><td>0.99136</td><td>1.01450</td><td>1.03764</td><td>0.009459</td><td>.000089467</td><td>0.93235</td></tr><tr><td>7</td><td>1.02611</td><td>1.04593</td><td>1.06575</td><td>0.008101</td><td>.000065623</td><td>0.77450</td></tr><tr><td>8</td><td>1.02511</td><td>1.04180</td><td>1.05848</td><td>0.006818</td><td>.000046491</td><td>0.65449</td></tr><tr><td>9</td><td>0.94252</td><td>1.00433</td><td>1.06615</td><td>0.025263</td><td>.000638240</td><td>2.51544</td></tr></tbody></table>

## WLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.42281</td><td>0.46120</td><td>0.49959</td><td>0.015688</td><td>.000246123</td><td>3.40163</td></tr><tr><td>2</td><td>0.62791</td><td>0.72490</td><td>0.82189</td><td>0.039637</td><td>.001571057</td><td>5.46785</td></tr><tr><td>3</td><td>0.71872</td><td>0.79287</td><td>0.86702</td><td>0.030304</td><td>.000918304</td><td>3.82200</td></tr><tr><td>4</td><td>0.96078</td><td>0.97122</td><td>0.98166</td><td>0.004268</td><td>.000018215</td><td>0.43943</td></tr><tr><td>5</td><td>0.96165</td><td>1.00581</td><td>1.04997</td><td>0.018047</td><td>.000325695</td><td>1.79427</td></tr><tr><td>6</td><td>0.99132</td><td>1.01451</td><td>1.03769</td><td>0.009475</td><td>.000089772</td><td>0.93393</td></tr><tr><td>7</td><td>1.02605</td><td>1.04590</td><td>1.06575</td><td>0.008112</td><td>.000065803</td><td>0.77559</td></tr><tr><td>8</td><td>1.02509</td><td>1.04181</td><td>1.05853</td><td>0.006834</td><td>.000046707</td><td>0.65600</td></tr><tr><td>9</td><td>0.94238</td><td>1.00435</td><td>1.06631</td><td>0.025323</td><td>.000641230</td><td>2.52129</td></tr></tbody></table>

## IRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.43423</td><td>0.46021</td><td>0.48619</td><td>0.010618</td><td>.000112744</td><td>2.30722</td></tr><tr><td>2</td><td>0.63632</td><td>0.70351</td><td>0.77070</td><td>0.027459</td><td>.000754018</td><td>3.90319</td></tr><tr><td>3</td><td>0.72248</td><td>0.79102</td><td>0.85956</td><td>0.028011</td><td>.000784600</td><td>3.54108</td></tr><tr><td>4</td><td>0.96393</td><td>0.97138</td><td>0.97883</td><td>0.003044</td><td>.000009269</td><td>0.31342</td></tr><tr><td>5</td><td>0.97476</td><td>1.00594</td><td>1.03712</td><td>0.012741</td><td>.000162343</td><td>1.26661</td></tr><tr><td>6</td><td>0.99040</td><td>1.01210</td><td>1.03379</td><td>0.008866</td><td>.000078612</td><td>0.87603</td></tr><tr><td>7</td><td>1.02960</td><td>1.04512</td><td>1.06063</td><td>0.006341</td><td>.000040213</td><td>0.60676</td></tr><tr><td>8</td><td>1.02707</td><td>1.03972</td><td>1.05236</td><td>0.005167</td><td>.000026700</td><td>0.49699</td></tr><tr><td>9</td><td>0.95927</td><td>0.99856</td><td>1.03784</td><td>0.016055</td><td>.000257770</td><td>1.60785</td></tr></tbody></table>

## DWLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.42358</td><td>0.46387</td><td>0.50416</td><td>0.016465</td><td>.000271104</td><td>3.54954</td></tr><tr><td>2</td><td>0.63050</td><td>0.72367</td><td>0.81684</td><td>0.038075</td><td>.001449694</td><td>5.26137</td></tr><tr><td>3</td><td>0.72253</td><td>0.79644</td><td>0.87035</td><td>0.030203</td><td>.000912235</td><td>3.79227</td></tr><tr><td>4</td><td>0.96119</td><td>0.97132</td><td>0.98144</td><td>0.004138</td><td>.000017120</td><td>0.42598</td></tr><tr><td>5</td><td>0.96360</td><td>1.00668</td><td>1.04977</td><td>0.017606</td><td>.000309979</td><td>1.74893</td></tr><tr><td>6</td><td>0.99280</td><td>1.01539</td><td>1.03798</td><td>0.009232</td><td>.000085223</td><td>0.90918</td></tr><tr><td>7</td><td>1.02720</td><td>1.04649</td><td>1.06577</td><td>0.007881</td><td>.000062113</td><td>0.75311</td></tr><tr><td>8</td><td>1.02646</td><td>1.04333</td><td>1.06019</td><td>0.006892</td><td>.000047501</td><td>0.66059</td></tr><tr><td>9</td><td>0.94712</td><td>1.01052</td><td>1.07391</td><td>0.025907</td><td>.000671176</td><td>2.56374</td></tr></tbody></table>
IDRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.43237</td><td>0.46079</td><td>0.48921</td><td>0.011614</td><td>.000134886</td><td>2.52048</td></tr><tr><td>2</td><td>0.64091</td><td>0.70861</td><td>0.77631</td><td>0.027667</td><td>.000765436</td><td>3.90436</td></tr><tr><td>3</td><td>0.72409</td><td>0.79530</td><td>0.86652</td><td>0.029104</td><td>.000847021</td><td>3.65943</td></tr><tr><td>4</td><td>0.96387</td><td>0.97176</td><td>0.97964</td><td>0.003222</td><td>.000010382</td><td>0.33157</td></tr><tr><td>5</td><td>0.97668</td><td>1.00551</td><td>1.03434</td><td>0.011781</td><td>.000138801</td><td>1.17168</td></tr><tr><td>6</td><td>0.99166</td><td>1.01236</td><td>1.03307</td><td>0.008462</td><td>.000071609</td><td>0.83589</td></tr><tr><td>7</td><td>1.03007</td><td>1.04503</td><td>1.05999</td><td>0.006113</td><td>.000037371</td><td>0.58498</td></tr><tr><td>8</td><td>1.02685</td><td>1.04002</td><td>1.05320</td><td>0.005385</td><td>.000028994</td><td>0.51774</td></tr><tr><td>9</td><td>0.95897</td><td>1.00020</td><td>1.04143</td><td>0.016849</td><td>.000283887</td><td>1.68455</td></tr></tbody></table>
# ADRIA L.M. PH (9 niveaux de pH)

## PLAQUE 2

### Temps de détection pour les 8 dilutions

$$ \text{pH} = 4.48 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>16.6782</td><td>17.1173</td><td>17.5563</td><td>0.17048</td><td>0.029064</td><td>34.406</td></tr><tr><td>2</td><td>18.1964</td><td>18.7140</td><td>19.2309</td><td>0.20179</td><td>0.040721</td><td>24.557</td></tr><tr><td>3</td><td>19.1832</td><td>19.6149</td><td>20.0465</td><td>0.16817</td><td>0.028283</td><td>35.358</td></tr><tr><td>4</td><td>20.7319</td><td>21.0706</td><td>21.4092</td><td>0.13193</td><td>0.017407</td><td>57.450</td></tr><tr><td>5</td><td>21.9114</td><td>22.3245</td><td>22.7380</td><td>0.16050</td><td>0.025759</td><td>38.822</td></tr><tr><td>6</td><td>23.3757</td><td>23.7196</td><td>24.0637</td><td>0.13379</td><td>0.017900</td><td>55.864</td></tr><tr><td>7</td><td>24.3221</td><td>24.7754</td><td>25.2290</td><td>0.17608</td><td>0.031004</td><td>32.254</td></tr><tr><td>8</td><td>26.0201</td><td>26.2707</td><td>26.5214</td><td>0.09734</td><td>0.009476</td><td>105.531</td></tr></tbody></table>

$$ \text{pH} = 4.80 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>10.3105</td><td>11.0045</td><td>11.7069</td><td>0.26186</td><td>0.068570</td><td>14.5837</td></tr><tr><td>2</td><td>11.6557</td><td>11.9870</td><td>12.3192</td><td>0.12306</td><td>0.015143</td><td>66.0389</td></tr><tr><td>3</td><td>12.4676</td><td>12.8054</td><td>13.1437</td><td>0.12613</td><td>0.015909</td><td>62.8563</td></tr><tr><td>4</td><td>13.1346</td><td>13.5612</td><td>13.9893</td><td>0.16027</td><td>0.025687</td><td>38.9307</td></tr><tr><td>5</td><td>14.2534</td><td>14.6039</td><td>14.9550</td><td>0.13088</td><td>0.017131</td><td>58.3753</td></tr><tr><td>6</td><td>15.1389</td><td>15.4739</td><td>15.8089</td><td>0.12499</td><td>0.015623</td><td>64.0083</td></tr><tr><td>7</td><td>16.0538</td><td>16.4304</td><td>16.8066</td><td>0.14182</td><td>0.020113</td><td>49.7185</td></tr><tr><td>8</td><td>16.9083</td><td>17.2853</td><td>17.6638</td><td>0.14012</td><td>0.019634</td><td>50.9313</td></tr></tbody></table>

$$ \text{pH} = 5.02 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>9.6770</td><td>9.8943</td><td>10.1111</td><td>0.07866</td><td>0.006187</td><td>161.624</td></tr><tr><td>2</td><td>10.1313</td><td>10.4372</td><td>10.7437</td><td>0.11199</td><td>0.012541</td><td>79.740</td></tr><tr><td>3</td><td>10.6545</td><td>11.1113</td><td>11.5664</td><td>0.17013</td><td>0.028943</td><td>34.551</td></tr><tr><td>4</td><td>11.3068</td><td>11.7647</td><td>12.2212</td><td>0.16959</td><td>0.028762</td><td>34.768</td></tr><tr><td>5</td><td>11.3494</td><td>11.8036</td><td>12.2570</td><td>0.16834</td><td>0.028337</td><td>35.289</td></tr><tr><td>6</td><td>12.6444</td><td>13.2304</td><td>13.8114</td><td>0.21771</td><td>0.047399</td><td>21.098</td></tr><tr><td>7</td><td>11.1643</td><td>11.7258</td><td>12.2810</td><td>0.20576</td><td>0.042337</td><td>23.620</td></tr><tr><td>8</td><td>14.1302</td><td>14.7989</td><td>15.4628</td><td>0.24860</td><td>0.061803</td><td>16.180</td></tr></tbody></table>

$$ \text{pH} = 5.23 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>8.2588</td><td>8.5834</td><td>8.9086</td><td>0.11972</td><td>0.014334</td><td>69.7665</td></tr><tr><td>2</td><td>8.6842</td><td>9.1074</td><td>9.5276</td><td>0.15642</td><td>0.024468</td><td>40.8693</td></tr><tr><td>3</td><td>9.7320</td><td>10.2042</td><td>10.6715</td><td>0.17310</td><td>0.029962</td><td>33.3753</td></tr><tr><td>4</td><td>10.4292</td><td>10.8022</td><td>11.1746</td><td>0.13825</td><td>0.019112</td><td>52.3225</td></tr><tr><td>5</td><td>10.9923</td><td>11.4272</td><td>11.8597</td><td>0.16087</td><td>0.025879</td><td>38.6408</td></tr><tr><td>6</td><td>11.5399</td><td>12.0785</td><td>12.6117</td><td>0.19878</td><td>0.039513</td><td>25.3080</td></tr><tr><td>7</td><td>12.3710</td><td>13.0093</td><td>13.6383</td><td>0.23505</td><td>0.055248</td><td>18.1001</td></tr><tr><td>8</td><td>13.2221</td><td>13.5916</td><td>13.9586</td><td>0.13661</td><td>0.018662</td><td>53.5855</td></tr></tbody></table>
## pH = 6.03

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>6.9030</td><td>7.4994</td><td>8.1005</td><td>0.22653</td><td>0.05132</td><td>19.4868</td></tr><tr><td>2</td><td>3.7474</td><td>8.0200</td><td>12.6074</td><td>1.67610</td><td>2.80930</td><td>0.3560</td></tr><tr><td>3</td><td>3.9417</td><td>8.5407</td><td>13.4983</td><td>1.80788</td><td>3.26843</td><td>0.3060</td></tr><tr><td>4</td><td>4.4907</td><td>9.1669</td><td>14.2891</td><td>1.86688</td><td>3.48524</td><td>0.2869</td></tr><tr><td>5</td><td>8.8800</td><td>9.5458</td><td>10.2169</td><td>0.25185</td><td>0.06343</td><td>15.7656</td></tr><tr><td>6</td><td>9.7665</td><td>10.1639</td><td>10.5628</td><td>0.14856</td><td>0.02207</td><td>45.3107</td></tr><tr><td>7</td><td>10.2638</td><td>10.6887</td><td>11.1154</td><td>0.15887</td><td>0.02524</td><td>39.6195</td></tr><tr><td>8</td><td>10.5433</td><td>11.0510</td><td>11.5629</td><td>0.19021</td><td>0.03618</td><td>27.6383</td></tr></tbody></table>

## pH = 6.49

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.5907</td><td>7.7768</td><td>7.9633</td><td>0.06813</td><td>0.004641</td><td>215.457</td></tr><tr><td>2</td><td>7.8836</td><td>8.1838</td><td>8.4858</td><td>0.10913</td><td>0.011909</td><td>83.967</td></tr><tr><td>3</td><td>8.6396</td><td>8.7981</td><td>8.9567</td><td>0.05747</td><td>0.003302</td><td>302.821</td></tr><tr><td>4</td><td>9.0060</td><td>9.2502</td><td>9.4951</td><td>0.08942</td><td>0.007996</td><td>125.059</td></tr><tr><td>5</td><td>9.5969</td><td>9.7842</td><td>9.9716</td><td>0.06902</td><td>0.004764</td><td>209.889</td></tr><tr><td>6</td><td>10.1710</td><td>10.3688</td><td>10.5666</td><td>0.07233</td><td>0.005232</td><td>191.135</td></tr><tr><td>7</td><td>10.6908</td><td>10.8521</td><td>11.0134</td><td>0.05898</td><td>0.003479</td><td>287.474</td></tr><tr><td>8</td><td>10.9944</td><td>11.2402</td><td>11.4860</td><td>0.09057</td><td>0.008204</td><td>121.899</td></tr></tbody></table>

## pH = 7.04

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.4530</td><td>7.8589</td><td>8.2632</td><td>0.14927</td><td>0.022282</td><td>44.8787</td></tr><tr><td>2</td><td>7.9022</td><td>8.2756</td><td>8.6491</td><td>0.13761</td><td>0.018936</td><td>52.8106</td></tr><tr><td>3</td><td>8.3639</td><td>8.7360</td><td>9.1095</td><td>0.13633</td><td>0.018585</td><td>53.8073</td></tr><tr><td>4</td><td>8.8084</td><td>9.1894</td><td>9.5744</td><td>0.14006</td><td>0.019616</td><td>50.9778</td></tr><tr><td>5</td><td>9.3405</td><td>9.6920</td><td>10.0461</td><td>0.12787</td><td>0.016351</td><td>61.1578</td></tr><tr><td>6</td><td>9.8356</td><td>10.2490</td><td>10.6643</td><td>0.15153</td><td>0.022960</td><td>43.5540</td></tr><tr><td>7</td><td>10.3386</td><td>10.7094</td><td>11.0811</td><td>0.13576</td><td>0.018429</td><td>54.2610</td></tr><tr><td>8</td><td>10.9149</td><td>11.2240</td><td>11.5339</td><td>0.11317</td><td>0.012808</td><td>78.0762</td></tr></tbody></table>

## pH = 7.52

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.3452</td><td>7.6916</td><td>8.0391</td><td>0.12446</td><td>0.015490</td><td>64.5589</td></tr><tr><td>2</td><td>7.6581</td><td>8.1108</td><td>8.5698</td><td>0.16353</td><td>0.026742</td><td>37.3941</td></tr><tr><td>3</td><td>8.1979</td><td>8.6630</td><td>9.1320</td><td>0.16928</td><td>0.028656</td><td>34.8964</td></tr><tr><td>4</td><td>8.6564</td><td>9.1354</td><td>9.6178</td><td>0.17425</td><td>0.030363</td><td>32.9349</td></tr><tr><td>5</td><td>9.3718</td><td>9.7394</td><td>10.1091</td><td>0.13225</td><td>0.017491</td><td>57.1724</td></tr><tr><td>6</td><td>9.3707</td><td>9.9099</td><td>10.4601</td><td>0.19541</td><td>0.038184</td><td>26.1892</td></tr><tr><td>7</td><td>10.0513</td><td>10.5127</td><td>10.9781</td><td>0.16624</td><td>0.027635</td><td>36.1857</td></tr><tr><td>8</td><td>10.5326</td><td>10.9392</td><td>11.3491</td><td>0.14799</td><td>0.021901</td><td>45.6606</td></tr></tbody></table>
$$pH = 8.54$$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.4428</td><td>8.3979</td><td>9.4186</td><td>0.35440</td><td>0.12560</td><td>7.9619</td></tr><tr><td>2</td><td>7.8106</td><td>8.7942</td><td>9.8679</td><td>0.36903</td><td>0.13618</td><td>7.3432</td></tr><tr><td>3</td><td>8.2217</td><td>9.1183</td><td>10.0693</td><td>0.33140</td><td>0.10983</td><td>9.1051</td></tr><tr><td>4</td><td>8.7966</td><td>9.6240</td><td>10.4981</td><td>0.30519</td><td>0.09314</td><td>10.7364</td></tr><tr><td>5</td><td>9.3872</td><td>10.1790</td><td>11.0183</td><td>0.29256</td><td>0.08559</td><td>11.6832</td></tr><tr><td>6</td><td>9.8449</td><td>10.7026</td><td>11.6186</td><td>0.31814</td><td>0.10122</td><td>9.8799</td></tr><tr><td>7</td><td>10.3231</td><td>11.1282</td><td>11.9602</td><td>0.29672</td><td>0.08804</td><td>11.3584</td></tr><tr><td>8</td><td>10.7201</td><td>11.4914</td><td>12.2920</td><td>0.28195</td><td>0.07950</td><td>12.5793</td></tr></tbody></table>
# Caractéristiques du paramètre mumax pour chaque niveau de pH
et pour chaque méthode de régression

## OLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.51452</td><td>0.53712</td><td>0.55973</td><td>0.00924</td><td>0.000085</td><td>1.7200</td></tr><tr><td>2</td><td>0.74407</td><td>0.77125</td><td>0.79843</td><td>0.01111</td><td>0.000123</td><td>1.4404</td></tr><tr><td>3</td><td>0.44940</td><td>0.95962</td><td>1.46983</td><td>0.20851</td><td>0.043478</td><td>21.7289</td></tr><tr><td>4</td><td>0.88838</td><td>0.95089</td><td>1.01339</td><td>0.02555</td><td>0.000653</td><td>2.6865</td></tr><tr><td>5</td><td>1.27628</td><td>1.33379</td><td>1.39130</td><td>0.02350</td><td>0.000552</td><td>1.7621</td></tr><tr><td>6</td><td>1.29489</td><td>1.35346</td><td>1.41204</td><td>0.02394</td><td>0.000573</td><td>1.7688</td></tr><tr><td>7</td><td>1.36915</td><td>1.42285</td><td>1.47654</td><td>0.02194</td><td>0.000482</td><td>1.5423</td></tr><tr><td>8</td><td>1.36400</td><td>1.47744</td><td>1.59089</td><td>0.04636</td><td>0.002149</td><td>3.1380</td></tr><tr><td>9</td><td>1.39730</td><td>1.49686</td><td>1.59642</td><td>0.04069</td><td>0.001656</td><td>2.7182</td></tr></tbody></table>

## WLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.51452</td><td>0.53712</td><td>0.55972</td><td>0.00924</td><td>0.000085</td><td>1.7197</td></tr><tr><td>2</td><td>0.74390</td><td>0.77120</td><td>0.79849</td><td>0.01116</td><td>0.000124</td><td>1.4467</td></tr><tr><td>3</td><td>0.44874</td><td>0.96067</td><td>1.47259</td><td>0.20921</td><td>0.043770</td><td>21.7778</td></tr><tr><td>4</td><td>0.88836</td><td>0.95088</td><td>1.01339</td><td>0.02555</td><td>0.000653</td><td>2.6868</td></tr><tr><td>5</td><td>1.27617</td><td>1.33368</td><td>1.39120</td><td>0.02351</td><td>0.000553</td><td>1.7625</td></tr><tr><td>6</td><td>1.29498</td><td>1.35349</td><td>1.41201</td><td>0.02391</td><td>0.000572</td><td>1.7668</td></tr><tr><td>7</td><td>1.36908</td><td>1.42298</td><td>1.47687</td><td>0.02203</td><td>0.000485</td><td>1.5479</td></tr><tr><td>8</td><td>1.36385</td><td>1.47723</td><td>1.59060</td><td>0.04633</td><td>0.002147</td><td>3.1366</td></tr><tr><td>9</td><td>1.39709</td><td>1.49684</td><td>1.59658</td><td>0.04076</td><td>0.001662</td><td>2.7234</td></tr></tbody></table>

## IRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.51387</td><td>0.53105</td><td>0.54823</td><td>0.00702</td><td>0.000049</td><td>1.3220</td></tr><tr><td>2</td><td>0.75632</td><td>0.77218</td><td>0.78804</td><td>0.00648</td><td>0.000042</td><td>0.8395</td></tr><tr><td>3</td><td>0.65143</td><td>0.97443</td><td>1.29743</td><td>0.13200</td><td>0.017424</td><td>13.5465</td></tr><tr><td>4</td><td>0.91220</td><td>0.95455</td><td>0.99691</td><td>0.01731</td><td>0.000300</td><td>1.8134</td></tr><tr><td>5</td><td>1.27366</td><td>1.31990</td><td>1.36614</td><td>0.01890</td><td>0.000357</td><td>1.4317</td></tr><tr><td>6</td><td>1.29459</td><td>1.35186</td><td>1.40914</td><td>0.02341</td><td>0.000548</td><td>1.7315</td></tr><tr><td>7</td><td>1.37494</td><td>1.41574</td><td>1.45653</td><td>0.01667</td><td>0.000278</td><td>1.1776</td></tr><tr><td>8</td><td>1.41514</td><td>1.48014</td><td>1.54513</td><td>0.02656</td><td>0.000706</td><td>1.7946</td></tr><tr><td>9</td><td>1.41752</td><td>1.50287</td><td>1.58822</td><td>0.03488</td><td>0.001217</td><td>2.3209</td></tr></tbody></table>

## DWLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.51450</td><td>0.53659</td><td>0.55867</td><td>0.00903</td><td>0.000081</td><td>1.6820</td></tr><tr><td>2</td><td>0.74383</td><td>0.77197</td><td>0.80012</td><td>0.01150</td><td>0.000132</td><td>1.4899</td></tr><tr><td>3</td><td>0.60270</td><td>1.14842</td><td>1.69414</td><td>0.22302</td><td>0.049736</td><td>19.4194</td></tr><tr><td>4</td><td>0.89336</td><td>0.95368</td><td>1.01400</td><td>0.02465</td><td>0.000608</td><td>2.5847</td></tr><tr><td>5</td><td>1.26792</td><td>1.33234</td><td>1.39676</td><td>0.02633</td><td>0.000693</td><td>1.9759</td></tr><tr><td>6</td><td>1.29681</td><td>1.35463</td><td>1.41245</td><td>0.02363</td><td>0.000558</td><td>1.7443</td></tr><tr><td>7</td><td>1.36884</td><td>1.42162</td><td>1.47439</td><td>0.02157</td><td>0.000465</td><td>1.5171</td></tr><tr><td>8</td><td>1.36558</td><td>1.47670</td><td>1.58782</td><td>0.04541</td><td>0.002062</td><td>3.0751</td></tr><tr><td>9</td><td>1.39969</td><td>1.49942</td><td>1.59916</td><td>0.04076</td><td>0.001661</td><td>2.7182</td></tr></tbody></table>
IDRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.51480</td><td>0.53064</td><td>0.54648</td><td>0.00647</td><td>0.000042</td><td>1.2199</td></tr><tr><td>2</td><td>0.75483</td><td>0.77091</td><td>0.78699</td><td>0.00657</td><td>0.000043</td><td>0.8525</td></tr><tr><td>3</td><td>0.72524</td><td>1.04877</td><td>1.37229</td><td>0.13221</td><td>0.017480</td><td>12.6065</td></tr><tr><td>4</td><td>0.91227</td><td>0.95802</td><td>1.00378</td><td>0.01870</td><td>0.000350</td><td>1.9518</td></tr><tr><td>5</td><td>1.27438</td><td>1.31843</td><td>1.36249</td><td>0.01800</td><td>0.000324</td><td>1.3656</td></tr><tr><td>6</td><td>1.30080</td><td>1.35469</td><td>1.40859</td><td>0.02203</td><td>0.000485</td><td>1.6259</td></tr><tr><td>7</td><td>1.37651</td><td>1.41836</td><td>1.46022</td><td>0.01711</td><td>0.000293</td><td>1.2060</td></tr><tr><td>8</td><td>1.41179</td><td>1.48250</td><td>1.55321</td><td>0.02890</td><td>0.000835</td><td>1.9491</td></tr><tr><td>9</td><td>1.42473</td><td>1.50787</td><td>1.59101</td><td>0.03398</td><td>0.001154</td><td>2.2533</td></tr></tbody></table>
# ANNEXE 8

## ESTIMATIONS DES µmax OBTENUES

### A PARTIR DES DONNEES DE L'Institut Pasteur de Lille
# IPL L.M AW (6 taux de NaCl)

## PLAQUE 1

### Temps de détection pour les 8 dilutions

NaCl = 0.5%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>10.0709</td><td>10.8894</td><td>11.7392</td><td>0.30504</td><td>0.093051</td><td>10.7468</td></tr><tr><td>2</td><td>11.0402</td><td>11.8329</td><td>12.6515</td><td>0.29462</td><td>0.086799</td><td>11.5208</td></tr><tr><td>3</td><td>12.0309</td><td>12.7102</td><td>13.4129</td><td>0.25047</td><td>0.062733</td><td>15.9405</td></tr><tr><td>4</td><td>12.8505</td><td>13.6394</td><td>14.4723</td><td>0.29393</td><td>0.086395</td><td>11.5748</td></tr><tr><td>5</td><td>13.8237</td><td>14.5685</td><td>15.3481</td><td>0.27628</td><td>0.076329</td><td>13.1012</td></tr><tr><td>6</td><td>14.7130</td><td>15.4428</td><td>16.1985</td><td>0.26923</td><td>0.072485</td><td>13.7959</td></tr><tr><td>7</td><td>15.4910</td><td>16.1852</td><td>16.9023</td><td>0.25579</td><td>0.065429</td><td>15.2838</td></tr><tr><td>8</td><td>16.4629</td><td>17.1396</td><td>17.8357</td><td>0.24879</td><td>0.061899</td><td>16.1554</td></tr></tbody></table>

NaCl = 0.75%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>10.4045</td><td>11.0321</td><td>11.6827</td><td>0.23166</td><td>0.053668</td><td>18.6332</td></tr><tr><td>2</td><td>11.3659</td><td>12.0982</td><td>12.8535</td><td>0.27201</td><td>0.073988</td><td>13.5157</td></tr><tr><td>3</td><td>12.3112</td><td>12.9476</td><td>13.6037</td><td>0.23425</td><td>0.054875</td><td>18.2232</td></tr><tr><td>4</td><td>13.1722</td><td>13.8528</td><td>14.5641</td><td>0.25225</td><td>0.063630</td><td>15.7160</td></tr><tr><td>5</td><td>14.0440</td><td>14.6716</td><td>15.3174</td><td>0.23079</td><td>0.053265</td><td>18.7740</td></tr><tr><td>6</td><td>14.9842</td><td>15.6613</td><td>16.3591</td><td>0.24918</td><td>0.062091</td><td>16.1054</td></tr><tr><td>7</td><td>15.8854</td><td>16.5379</td><td>17.2154</td><td>0.24104</td><td>0.058101</td><td>17.2115</td></tr><tr><td>8</td><td>16.9019</td><td>17.4586</td><td>18.0308</td><td>0.20459</td><td>0.041858</td><td>23.8903</td></tr></tbody></table>

NaCl = 1%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>10.9081</td><td>11.3993</td><td>11.9043</td><td>0.17389</td><td>0.030237</td><td>33.0722</td></tr><tr><td>2</td><td>12.0847</td><td>12.5130</td><td>12.9561</td><td>0.15210</td><td>0.023135</td><td>43.2249</td></tr><tr><td>3</td><td>12.8749</td><td>13.3529</td><td>13.8531</td><td>0.16762</td><td>0.028096</td><td>35.5924</td></tr><tr><td>4</td><td>13.7192</td><td>14.2167</td><td>14.7321</td><td>0.17678</td><td>0.031253</td><td>31.9971</td></tr><tr><td>5</td><td>14.6788</td><td>15.1529</td><td>15.6402</td><td>0.16781</td><td>0.028160</td><td>35.5111</td></tr><tr><td>6</td><td>15.7342</td><td>16.0840</td><td>16.4448</td><td>0.12178</td><td>0.014831</td><td>67.4267</td></tr><tr><td>7</td><td>16.5077</td><td>16.9544</td><td>17.4149</td><td>0.15835</td><td>0.025074</td><td>39.8826</td></tr><tr><td>8</td><td>17.4523</td><td>17.9078</td><td>18.3757</td><td>0.16117</td><td>0.025975</td><td>38.4993</td></tr></tbody></table>
NaCl = 1.5%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>10.8859</td><td>11.3623</td><td>11.8501</td><td>0.16830</td><td>0.028326</td><td>35.3034</td></tr><tr><td>2</td><td>12.1308</td><td>12.5913</td><td>13.0715</td><td>0.16121</td><td>0.025988</td><td>38.4796</td></tr><tr><td>3</td><td>13.0061</td><td>13.4117</td><td>13.8244</td><td>0.14022</td><td>0.019662</td><td>50.8607</td></tr><tr><td>4</td><td>13.8419</td><td>14.3338</td><td>14.8479</td><td>0.17239</td><td>0.029719</td><td>33.6487</td></tr><tr><td>5</td><td>14.8162</td><td>15.2658</td><td>15.7300</td><td>0.15660</td><td>0.024525</td><td>40.7748</td></tr><tr><td>6</td><td>15.8258</td><td>16.2846</td><td>16.7597</td><td>0.16003</td><td>0.025609</td><td>39.0489</td></tr><tr><td>7</td><td>16.5984</td><td>17.1173</td><td>17.6634</td><td>0.18249</td><td>0.033303</td><td>30.0273</td></tr><tr><td>8</td><td>17.6435</td><td>18.0537</td><td>18.4779</td><td>0.14300</td><td>0.020448</td><td>48.9051</td></tr></tbody></table>

NaCl = 3%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>12.2734</td><td>12.7300</td><td>13.1996</td><td>0.15872</td><td>0.025193</td><td>39.6933</td></tr><tr><td>2</td><td>13.2981</td><td>13.6553</td><td>14.0177</td><td>0.12332</td><td>0.015208</td><td>65.7527</td></tr><tr><td>3</td><td>14.3525</td><td>14.6494</td><td>14.9498</td><td>0.10236</td><td>0.010478</td><td>95.4339</td></tr><tr><td>4</td><td>15.3361</td><td>15.7294</td><td>16.1323</td><td>0.13645</td><td>0.018618</td><td>53.7110</td></tr><tr><td>5</td><td>16.3151</td><td>16.6603</td><td>17.0178</td><td>0.11766</td><td>0.013844</td><td>72.2323</td></tr><tr><td>6</td><td>17.2471</td><td>17.6600</td><td>18.0803</td><td>0.14279</td><td>0.020389</td><td>49.0467</td></tr><tr><td>7</td><td>18.3395</td><td>18.6760</td><td>19.0248</td><td>0.11474</td><td>0.013166</td><td>75.9546</td></tr><tr><td>8</td><td>19.3020</td><td>19.6332</td><td>19.9745</td><td>0.11259</td><td>0.012678</td><td>78.8798</td></tr></tbody></table>

NaCl = 5%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>16.6728</td><td>17.0075</td><td>17.3442</td><td>0.12042</td><td>0.014501</td><td>68.9596</td></tr><tr><td>2</td><td>17.9783</td><td>18.3546</td><td>18.7352</td><td>0.13577</td><td>0.018433</td><td>54.2518</td></tr><tr><td>3</td><td>19.3049</td><td>19.6630</td><td>20.0288</td><td>0.12637</td><td>0.015969</td><td>62.6221</td></tr><tr><td>4</td><td>20.7060</td><td>21.0448</td><td>21.3876</td><td>0.11898</td><td>0.014156</td><td>70.6430</td></tr><tr><td>5</td><td>21.9541</td><td>22.2742</td><td>22.5974</td><td>0.11228</td><td>0.012607</td><td>79.3227</td></tr><tr><td>6</td><td>23.1696</td><td>23.6088</td><td>24.0594</td><td>0.15765</td><td>0.024854</td><td>40.2352</td></tr><tr><td>7</td><td>24.4959</td><td>24.9038</td><td>25.3177</td><td>0.14741</td><td>0.021728</td><td>46.0229</td></tr><tr><td>8</td><td>25.8750</td><td>26.2357</td><td>26.6027</td><td>0.13053</td><td>0.017039</td><td>58.6888</td></tr></tbody></table>
# Caractéristiques du paramètre mumax pour chaque taux de NaCl
et pour chaque méthode de régression

## OLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.75729</td><td>0.77766</td><td>0.79802</td><td>0.008321</td><td>.000069240</td><td>1.07002</td></tr><tr><td>2</td><td>0.74415</td><td>0.76237</td><td>0.78059</td><td>0.007446</td><td>.000055440</td><td>0.97666</td></tr><tr><td>3</td><td>0.73265</td><td>0.75476</td><td>0.77688</td><td>0.009038</td><td>.000081678</td><td>1.19741</td></tr><tr><td>4</td><td>0.70562</td><td>0.73398</td><td>0.76234</td><td>0.011590</td><td>.000134339</td><td>1.57913</td></tr><tr><td>5</td><td>0.69127</td><td>0.69644</td><td>0.70162</td><td>0.002115</td><td>.000004474</td><td>0.30371</td></tr><tr><td>6</td><td>0.52265</td><td>0.52602</td><td>0.52940</td><td>0.001378</td><td>.000001900</td><td>0.26201</td></tr></tbody></table>

## WLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.75727</td><td>0.77766</td><td>0.79805</td><td>0.008333</td><td>.000069435</td><td>1.07152</td></tr><tr><td>2</td><td>0.74410</td><td>0.76234</td><td>0.78057</td><td>0.007452</td><td>.000055531</td><td>0.97751</td></tr><tr><td>3</td><td>0.73257</td><td>0.75472</td><td>0.77686</td><td>0.009049</td><td>.000081886</td><td>1.19900</td></tr><tr><td>4</td><td>0.70554</td><td>0.73391</td><td>0.76228</td><td>0.011594</td><td>.000134426</td><td>1.57979</td></tr><tr><td>5</td><td>0.69126</td><td>0.69644</td><td>0.70163</td><td>0.002118</td><td>.000004487</td><td>0.30414</td></tr><tr><td>6</td><td>0.52264</td><td>0.52602</td><td>0.52940</td><td>0.001381</td><td>.000001906</td><td>0.26246</td></tr></tbody></table>

## IRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.76317</td><td>0.77764</td><td>0.79211</td><td>.005914333</td><td>.000034979</td><td>0.76055</td></tr><tr><td>2</td><td>0.74845</td><td>0.76320</td><td>0.77795</td><td>.006028194</td><td>.000036339</td><td>0.78986</td></tr><tr><td>3</td><td>0.73551</td><td>0.75372</td><td>0.77192</td><td>.007440883</td><td>.000055367</td><td>0.98723</td></tr><tr><td>4</td><td>0.71605</td><td>0.73940</td><td>0.76275</td><td>.009542321</td><td>.000091056</td><td>1.29055</td></tr><tr><td>5</td><td>0.69124</td><td>0.69621</td><td>0.70119</td><td>.002033779</td><td>.000004136</td><td>0.29212</td></tr><tr><td>6</td><td>0.52351</td><td>0.52667</td><td>0.52983</td><td>.001292316</td><td>.000001670</td><td>0.24537</td></tr></tbody></table>

## DWLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.75809</td><td>0.77861</td><td>0.79914</td><td>0.008389</td><td>.000070370</td><td>1.07739</td></tr><tr><td>2</td><td>0.74419</td><td>0.76187</td><td>0.77955</td><td>0.007226</td><td>.000052211</td><td>0.94842</td></tr><tr><td>3</td><td>0.73314</td><td>0.75525</td><td>0.77736</td><td>0.009035</td><td>.000081632</td><td>1.19630</td></tr><tr><td>4</td><td>0.70614</td><td>0.73439</td><td>0.76263</td><td>0.011543</td><td>.000133233</td><td>1.57175</td></tr><tr><td>5</td><td>0.69113</td><td>0.69629</td><td>0.70146</td><td>0.002111</td><td>.000004457</td><td>0.30319</td></tr><tr><td>6</td><td>0.52261</td><td>0.52599</td><td>0.52937</td><td>0.001381</td><td>.000001907</td><td>0.26252</td></tr></tbody></table>

## IDRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.76250</td><td>0.77813</td><td>0.79377</td><td>.006389453</td><td>.000040825</td><td>0.82113</td></tr><tr><td>2</td><td>0.74698</td><td>0.76189</td><td>0.77680</td><td>.006093198</td><td>.000037127</td><td>0.79975</td></tr><tr><td>3</td><td>0.73682</td><td>0.75538</td><td>0.77394</td><td>.007585326</td><td>.000057537</td><td>1.00417</td></tr><tr><td>4</td><td>0.71729</td><td>0.73977</td><td>0.76225</td><td>.009187385</td><td>.000084408</td><td>1.24192</td></tr><tr><td>5</td><td>0.69171</td><td>0.69651</td><td>0.70131</td><td>.001960443</td><td>.000003843</td><td>0.28147</td></tr><tr><td>6</td><td>0.52378</td><td>0.52687</td><td>0.52997</td><td>.001265561</td><td>.000001602</td><td>0.24020</td></tr></tbody></table>
# IPL L.M AW (4 taux de NaCl)

## PLAQUE 2

### Temps de détection pour les 8 dilutions

#### NaCl = 1%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>12.9530</td><td>13.3459</td><td>13.7534</td><td>0.13716</td><td>0.018812</td><td>53.1589</td></tr><tr><td>2</td><td>14.0201</td><td>14.4332</td><td>14.8574</td><td>0.14615</td><td>0.021360</td><td>46.8163</td></tr><tr><td>3</td><td>14.9221</td><td>15.3244</td><td>15.7334</td><td>0.14162</td><td>0.020056</td><td>49.8600</td></tr><tr><td>4</td><td>15.8859</td><td>16.3218</td><td>16.7744</td><td>0.15227</td><td>0.023185</td><td>43.1310</td></tr><tr><td>5</td><td>16.7726</td><td>17.2170</td><td>17.6756</td><td>0.15763</td><td>0.024846</td><td>40.2475</td></tr><tr><td>6</td><td>17.7279</td><td>18.1703</td><td>18.6249</td><td>0.15656</td><td>0.024512</td><td>40.7957</td></tr><tr><td>7</td><td>18.5346</td><td>19.0076</td><td>19.4987</td><td>0.16828</td><td>0.028318</td><td>35.3130</td></tr><tr><td>8</td><td>19.6795</td><td>20.0766</td><td>20.5703</td><td>0.13888</td><td>0.019287</td><td>51.8479</td></tr></tbody></table>

#### NaCl = 1.5%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>12.6146</td><td>13.1302</td><td>13.6601</td><td>0.18249</td><td>0.033301</td><td>30.0290</td></tr><tr><td>2</td><td>13.8575</td><td>14.2466</td><td>14.6459</td><td>0.13510</td><td>0.018252</td><td>54.7899</td></tr><tr><td>3</td><td>14.7908</td><td>15.1486</td><td>15.5116</td><td>0.12352</td><td>0.015256</td><td>65.5472</td></tr><tr><td>4</td><td>15.5879</td><td>16.1109</td><td>16.6611</td><td>0.18392</td><td>0.033827</td><td>29.5625</td></tr><tr><td>5</td><td>16.6345</td><td>17.0897</td><td>17.5642</td><td>0.15931</td><td>0.025381</td><td>39.3996</td></tr><tr><td>6</td><td>17.5639</td><td>18.0770</td><td>18.6138</td><td>0.17992</td><td>0.032371</td><td>30.8922</td></tr><tr><td>7</td><td>18.5968</td><td>19.1099</td><td>19.6490</td><td>0.18030</td><td>0.032510</td><td>30.7602</td></tr><tr><td>8</td><td>20.0158</td><td>20.4345</td><td>21.0255</td><td>0.14840</td><td>0.022024</td><td>45.4050</td></tr></tbody></table>

#### NaCl = 3%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>12.8865</td><td>13.5695</td><td>14.2806</td><td>0.25006</td><td>0.062528</td><td>15.9929</td></tr><tr><td>2</td><td>13.8695</td><td>14.5226</td><td>15.2133</td><td>0.23808</td><td>0.056682</td><td>17.6423</td></tr><tr><td>3</td><td>14.9781</td><td>15.5469</td><td>16.1448</td><td>0.20365</td><td>0.041472</td><td>24.1129</td></tr><tr><td>4</td><td>15.8214</td><td>16.5304</td><td>17.2669</td><td>0.25926</td><td>0.067217</td><td>14.8771</td></tr><tr><td>5</td><td>16.8141</td><td>17.4940</td><td>18.2126</td><td>0.24776</td><td>0.061384</td><td>16.2909</td></tr><tr><td>6</td><td>17.9491</td><td>18.5645</td><td>19.1998</td><td>0.22158</td><td>0.049097</td><td>20.3677</td></tr><tr><td>7</td><td>18.9026</td><td>19.6125</td><td>20.3532</td><td>0.25699</td><td>0.066046</td><td>15.1411</td></tr><tr><td>8</td><td>19.8669</td><td>20.5447</td><td>21.2484</td><td>0.24780</td><td>0.061407</td><td>16.2849</td></tr></tbody></table>

#### NaCl = 5%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>19.3968</td><td>19.7596</td><td>20.1261</td><td>0.13217</td><td>0.017469</td><td>57.2437</td></tr><tr><td>2</td><td>20.4026</td><td>20.7066</td><td>21.0126</td><td>0.11055</td><td>0.012221</td><td>81.8235</td></tr><tr><td>3</td><td>21.6411</td><td>22.0004</td><td>22.3631</td><td>0.13084</td><td>0.017119</td><td>58.4151</td></tr><tr><td>4</td><td>22.8871</td><td>23.4148</td><td>23.9618</td><td>0.19040</td><td>0.036251</td><td>27.5857</td></tr><tr><td>5</td><td>24.0608</td><td>24.5196</td><td>24.9877</td><td>0.16422</td><td>0.026967</td><td>37.0821</td></tr><tr><td>6</td><td>25.3892</td><td>25.8148</td><td>26.2498</td><td>0.15248</td><td>0.023251</td><td>43.0094</td></tr><tr><td>7</td><td>26.6082</td><td>27.0005</td><td>27.4004</td><td>0.14210</td><td>0.020191</td><td>49.5260</td></tr><tr><td>8</td><td>27.8193</td><td>28.2668</td><td>28.7247</td><td>0.16239</td><td>0.026371</td><td>37.9198</td></tr></tbody></table>
# Caractéristiques du paramètre mumax pour chaque taux de NaCl
et pour chaque méthode de régression

## OLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.71191</td><td>0.73085</td><td>0.74980</td><td>0.007742</td><td>.000059932</td><td>1.05925</td></tr><tr><td>2</td><td>0.64651</td><td>0.68008</td><td>0.71364</td><td>0.013718</td><td>.000188173</td><td>2.01706</td></tr><tr><td>3</td><td>0.67923</td><td>0.68892</td><td>0.69861</td><td>0.003962</td><td>.000015695</td><td>0.57506</td></tr><tr><td>4</td><td>0.54569</td><td>0.56036</td><td>0.57502</td><td>0.005992</td><td>.000035906</td><td>1.06936</td></tr></tbody></table>

## WLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.71188</td><td>0.73085</td><td>0.74982</td><td>0.007752</td><td>.000060097</td><td>1.06072</td></tr><tr><td>2</td><td>0.64661</td><td>0.68013</td><td>0.71364</td><td>0.013697</td><td>.000187601</td><td>2.01385</td></tr><tr><td>3</td><td>0.67919</td><td>0.68892</td><td>0.69865</td><td>0.003978</td><td>.000015821</td><td>0.57736</td></tr><tr><td>4</td><td>0.54572</td><td>0.56041</td><td>0.57509</td><td>0.006001</td><td>.000036010</td><td>1.07080</td></tr></tbody></table>

## IRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.71532</td><td>0.73074</td><td>0.74616</td><td>0.006301</td><td>.000039706</td><td>0.86231</td></tr><tr><td>2</td><td>0.66756</td><td>0.69208</td><td>0.71660</td><td>0.010020</td><td>.000100398</td><td>1.44779</td></tr><tr><td>3</td><td>0.68315</td><td>0.68985</td><td>0.69655</td><td>0.002738</td><td>.000007498</td><td>0.39694</td></tr><tr><td>4</td><td>0.54668</td><td>0.55802</td><td>0.56936</td><td>0.004635</td><td>.000021481</td><td>0.83058</td></tr></tbody></table>

## DWLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.71178</td><td>0.73055</td><td>0.74933</td><td>0.007674</td><td>.000058897</td><td>1.05050</td></tr><tr><td>2</td><td>0.64642</td><td>0.68007</td><td>0.71372</td><td>0.013752</td><td>.000189111</td><td>2.02211</td></tr><tr><td>3</td><td>0.67947</td><td>0.68908</td><td>0.69868</td><td>0.003925</td><td>.000015403</td><td>0.56955</td></tr><tr><td>4</td><td>0.54554</td><td>0.56036</td><td>0.57517</td><td>0.006054</td><td>.000036647</td><td>1.08032</td></tr></tbody></table>

## IDRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.71521</td><td>0.73071</td><td>0.74620</td><td>0.006331</td><td>.000040087</td><td>0.86648</td></tr><tr><td>2</td><td>0.66736</td><td>0.69234</td><td>0.71732</td><td>0.010209</td><td>.000104216</td><td>1.47450</td></tr><tr><td>3</td><td>0.68276</td><td>0.68985</td><td>0.69694</td><td>0.002898</td><td>.000008397</td><td>0.42006</td></tr><tr><td>4</td><td>0.54627</td><td>0.55816</td><td>0.57005</td><td>0.004859</td><td>.000023606</td><td>0.87048</td></tr></tbody></table>
# IPL E.C.187 AW (6 taux de NaCl)

## PLAQUE 1

### Temps de détection pour les 8 dilutions

#### NaCl = 0.5%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>6.9423</td><td>7.0725</td><td>7.2025</td><td>0.043552</td><td>.001896820</td><td>527.198</td></tr><tr><td>2</td><td>7.2923</td><td>7.4902</td><td>7.6879</td><td>0.067801</td><td>.004597027</td><td>217.532</td></tr><tr><td>3</td><td>7.9505</td><td>8.0767</td><td>8.2026</td><td>0.042204</td><td>.001781151</td><td>561.435</td></tr><tr><td>4</td><td>8.6535</td><td>8.8048</td><td>8.9556</td><td>0.050591</td><td>.002559461</td><td>390.707</td></tr><tr><td>5</td><td>9.2680</td><td>9.4511</td><td>9.6339</td><td>0.062700</td><td>.003931247</td><td>254.372</td></tr><tr><td>6</td><td>9.9763</td><td>10.1647</td><td>10.3524</td><td>0.064443</td><td>.004152919</td><td>240.794</td></tr><tr><td>7</td><td>10.6297</td><td>10.7641</td><td>10.8985</td><td>0.046059</td><td>.002121440</td><td>471.378</td></tr><tr><td>8</td><td>11.3255</td><td>11.4554</td><td>11.5858</td><td>0.043583</td><td>.001899440</td><td>526.471</td></tr></tbody></table>

#### NaCl = 0.75%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>6.9856</td><td>7.1027</td><td>7.2196</td><td>0.039176</td><td>.001534779</td><td>651.560</td></tr><tr><td>2</td><td>7.4810</td><td>7.6399</td><td>7.7989</td><td>0.053240</td><td>.002834465</td><td>352.800</td></tr><tr><td>3</td><td>8.0750</td><td>8.2463</td><td>8.4188</td><td>0.057570</td><td>.003314289</td><td>301.724</td></tr><tr><td>4</td><td>8.6826</td><td>8.8258</td><td>8.9697</td><td>0.046629</td><td>.002174243</td><td>459.930</td></tr><tr><td>5</td><td>9.2899</td><td>9.4908</td><td>9.6933</td><td>0.067541</td><td>.004561758</td><td>219.214</td></tr><tr><td>6</td><td>9.9343</td><td>10.0658</td><td>10.1978</td><td>0.042803</td><td>.001832098</td><td>545.822</td></tr><tr><td>7</td><td>10.5449</td><td>10.6865</td><td>10.8286</td><td>0.047493</td><td>.002255613</td><td>443.339</td></tr><tr><td>8</td><td>11.2918</td><td>11.4289</td><td>11.5664</td><td>0.045985</td><td>.002114592</td><td>472.904</td></tr></tbody></table>

#### NaCl = 1%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.2510</td><td>7.4405</td><td>7.6333</td><td>0.062089</td><td>.003855035</td><td>259.401</td></tr><tr><td>2</td><td>7.7105</td><td>7.8680</td><td>8.0268</td><td>0.051378</td><td>.002639742</td><td>378.825</td></tr><tr><td>3</td><td>8.4003</td><td>8.5567</td><td>8.7137</td><td>0.050909</td><td>.002591743</td><td>385.841</td></tr><tr><td>4</td><td>9.0373</td><td>9.1983</td><td>9.3599</td><td>0.054008</td><td>.002916869</td><td>342.833</td></tr><tr><td>5</td><td>9.7261</td><td>9.8814</td><td>10.0382</td><td>0.050685</td><td>.002568993</td><td>389.258</td></tr><tr><td>6</td><td>10.2716</td><td>10.4504</td><td>10.6301</td><td>0.060027</td><td>.003603214</td><td>277.530</td></tr><tr><td>7</td><td>10.9004</td><td>11.0894</td><td>11.2800</td><td>0.061657</td><td>.003801525</td><td>263.052</td></tr><tr><td>8</td><td>11.3831</td><td>11.5793</td><td>11.7771</td><td>0.064005</td><td>.004096620</td><td>244.104</td></tr></tbody></table>
NaCl = 1.5%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.8066</td><td>7.9895</td><td>8.1736</td><td>0.06144</td><td>0.003775</td><td>264.887</td></tr><tr><td>2</td><td>8.6328</td><td>8.7410</td><td>8.8492</td><td>0.03707</td><td>0.001374</td><td>727.777</td></tr><tr><td>3</td><td>9.0456</td><td>9.3009</td><td>9.5603</td><td>0.08618</td><td>0.007428</td><td>134.634</td></tr><tr><td>4</td><td>9.8175</td><td>10.0168</td><td>10.2181</td><td>0.06706</td><td>0.004497</td><td>222.366</td></tr><tr><td>5</td><td>10.6383</td><td>10.8246</td><td>11.0115</td><td>0.06395</td><td>0.004089</td><td>244.554</td></tr><tr><td>6</td><td>11.1993</td><td>11.3772</td><td>11.5571</td><td>0.05813</td><td>0.003379</td><td>295.961</td></tr><tr><td>7</td><td>11.7473</td><td>12.0667</td><td>12.3930</td><td>0.10812</td><td>0.011689</td><td>85.551</td></tr><tr><td>8</td><td>12.4720</td><td>12.6599</td><td>12.8494</td><td>0.06467</td><td>0.004182</td><td>239.133</td></tr></tbody></table>

NaCl = 3%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>10.9197</td><td>11.2086</td><td>11.5004</td><td>0.10289</td><td>0.010585</td><td>94.470</td></tr><tr><td>2</td><td>12.0193</td><td>12.1378</td><td>12.2564</td><td>0.04253</td><td>0.001809</td><td>552.905</td></tr><tr><td>3</td><td>12.7798</td><td>13.1041</td><td>13.4335</td><td>0.11411</td><td>0.013021</td><td>76.797</td></tr><tr><td>4</td><td>13.8520</td><td>14.0324</td><td>14.2129</td><td>0.06541</td><td>0.004278</td><td>233.761</td></tr><tr><td>5</td><td>15.1728</td><td>15.3701</td><td>15.5677</td><td>0.07276</td><td>0.005294</td><td>188.894</td></tr><tr><td>6</td><td>15.9629</td><td>16.1126</td><td>16.2626</td><td>0.05432</td><td>0.002950</td><td>338.952</td></tr><tr><td>7</td><td>16.7201</td><td>17.1443</td><td>17.5750</td><td>0.15335</td><td>0.023515</td><td>42.526</td></tr><tr><td>8</td><td>16.9627</td><td>17.6465</td><td>18.3167</td><td>0.24286</td><td>0.058982</td><td>16.954</td></tr></tbody></table>

NaCl = 5%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>19.7923</td><td>20.3861</td><td>20.9842</td><td>0.22904</td><td>0.05246</td><td>19.0625</td></tr><tr><td>2</td><td>21.4801</td><td>22.1157</td><td>22.7547</td><td>0.24551</td><td>0.06027</td><td>16.5913</td></tr><tr><td>3</td><td>22.8499</td><td>23.9662</td><td>25.0936</td><td>0.43486</td><td>0.18911</td><td>5.2880</td></tr><tr><td>4</td><td>24.4625</td><td>25.3744</td><td>26.2929</td><td>0.35475</td><td>0.12585</td><td>7.9459</td></tr><tr><td>5</td><td>26.2189</td><td>26.9533</td><td>27.6935</td><td>0.28467</td><td>0.08104</td><td>12.3397</td></tr><tr><td>6</td><td>27.7607</td><td>28.3620</td><td>28.9658</td><td>0.23156</td><td>0.05362</td><td>18.6493</td></tr><tr><td>7</td><td>29.4027</td><td>29.6848</td><td>29.9672</td><td>0.10848</td><td>0.01177</td><td>84.9825</td></tr><tr><td>8</td><td>30.2916</td><td>30.5692</td><td>30.8471</td><td>0.10647</td><td>0.01134</td><td>88.2130</td></tr></tbody></table>
# Caractéristiques du paramètre mumax pour chaque taux de NaCl
et pour chaque méthode de régression

## OLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.01658</td><td>1.07333</td><td>1.13008</td><td>0.023191</td><td>.000537841</td><td>2.16069</td></tr><tr><td>2</td><td>1.07956</td><td>1.12320</td><td>1.16684</td><td>0.017834</td><td>.000318044</td><td>1.58777</td></tr><tr><td>3</td><td>1.07764</td><td>1.12683</td><td>1.17603</td><td>0.020106</td><td>.000404236</td><td>1.78426</td></tr><tr><td>4</td><td>0.98848</td><td>1.02909</td><td>1.06969</td><td>0.016595</td><td>.000275399</td><td>1.61261</td></tr><tr><td>5</td><td>0.66205</td><td>0.71763</td><td>0.77320</td><td>0.022712</td><td>.000515840</td><td>3.16490</td></tr><tr><td>6</td><td>0.42618</td><td>0.46545</td><td>0.50472</td><td>0.016050</td><td>.000257601</td><td>3.44826</td></tr></tbody></table>

## WLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.01660</td><td>1.07350</td><td>1.13039</td><td>0.023253</td><td>.000540715</td><td>2.16613</td></tr><tr><td>2</td><td>1.07964</td><td>1.12331</td><td>1.16698</td><td>0.017849</td><td>.000318574</td><td>1.58893</td></tr><tr><td>3</td><td>1.07762</td><td>1.12684</td><td>1.17606</td><td>0.020116</td><td>.000404647</td><td>1.78515</td></tr><tr><td>4</td><td>0.98827</td><td>1.02895</td><td>1.06962</td><td>0.016623</td><td>.000276336</td><td>1.61557</td></tr><tr><td>5</td><td>0.66189</td><td>0.71747</td><td>0.77305</td><td>0.022714</td><td>.000515926</td><td>3.16586</td></tr><tr><td>6</td><td>0.42610</td><td>0.46535</td><td>0.50461</td><td>0.016043</td><td>.000257370</td><td>3.44744</td></tr></tbody></table>

## IRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.01569</td><td>1.05432</td><td>1.09295</td><td>0.015787</td><td>.000249237</td><td>1.49738</td></tr><tr><td>2</td><td>1.09733</td><td>1.13499</td><td>1.17265</td><td>0.015392</td><td>.000236920</td><td>1.35615</td></tr><tr><td>3</td><td>1.07574</td><td>1.11920</td><td>1.16267</td><td>0.017764</td><td>.000315558</td><td>1.58720</td></tr><tr><td>4</td><td>0.99997</td><td>1.02755</td><td>1.05512</td><td>0.011268</td><td>.000126979</td><td>1.09664</td></tr><tr><td>5</td><td>0.66612</td><td>0.70591</td><td>0.74570</td><td>0.016262</td><td>.000264468</td><td>2.30376</td></tr><tr><td>6</td><td>0.42617</td><td>0.45869</td><td>0.49120</td><td>0.013290</td><td>.000176614</td><td>2.89733</td></tr></tbody></table>

## DWLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.01686</td><td>1.07398</td><td>1.13110</td><td>0.023343</td><td>.000544873</td><td>2.17347</td></tr><tr><td>2</td><td>1.07980</td><td>1.12355</td><td>1.16729</td><td>0.017878</td><td>.000319621</td><td>1.59121</td></tr><tr><td>3</td><td>1.07708</td><td>1.12651</td><td>1.17593</td><td>0.020197</td><td>.000407936</td><td>1.79292</td></tr><tr><td>4</td><td>0.98867</td><td>1.02962</td><td>1.07057</td><td>0.016734</td><td>.000280018</td><td>1.62523</td></tr><tr><td>5</td><td>0.65854</td><td>0.71255</td><td>0.76655</td><td>0.022069</td><td>.000487039</td><td>3.09720</td></tr><tr><td>6</td><td>0.42801</td><td>0.46667</td><td>0.50533</td><td>0.015801</td><td>.000249659</td><td>3.38582</td></tr></tbody></table>

## IDRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.01658</td><td>1.05491</td><td>1.09325</td><td>0.015666</td><td>.000245416</td><td>1.48503</td></tr><tr><td>2</td><td>1.09871</td><td>1.13418</td><td>1.16964</td><td>0.014493</td><td>.000210050</td><td>1.27785</td></tr><tr><td>3</td><td>1.07536</td><td>1.12143</td><td>1.16749</td><td>0.018826</td><td>.000354437</td><td>1.67880</td></tr><tr><td>4</td><td>0.99700</td><td>1.02701</td><td>1.05701</td><td>0.012262</td><td>.000150347</td><td>1.19392</td></tr><tr><td>5</td><td>0.66924</td><td>0.70746</td><td>0.74568</td><td>0.015619</td><td>.000243938</td><td>2.20770</td></tr><tr><td>6</td><td>0.42668</td><td>0.45917</td><td>0.49165</td><td>0.013276</td><td>.000176242</td><td>2.89125</td></tr></tbody></table>
# IPL E.C.187 AW (6 taux de NaCl)

## PLAQUE 2

### Temps de détection pour les 8 dilutions

#### NaCl = 0.5%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.0931</td><td>7.2026</td><td>7.3128</td><td>0.034239</td><td>.001172289</td><td>853.032</td></tr><tr><td>2</td><td>7.5893</td><td>7.7446</td><td>7.9019</td><td>0.048736</td><td>.002375169</td><td>421.023</td></tr><tr><td>3</td><td>8.1358</td><td>8.2977</td><td>8.4628</td><td>0.050969</td><td>.002597819</td><td>384.938</td></tr><tr><td>4</td><td>8.8704</td><td>9.0042</td><td>9.1380</td><td>0.043462</td><td>.001888952</td><td>529.394</td></tr><tr><td>5</td><td>9.5008</td><td>9.6553</td><td>9.8100</td><td>0.051770</td><td>.002680109</td><td>373.119</td></tr><tr><td>6</td><td>10.2241</td><td>10.3340</td><td>10.4438</td><td>0.036791</td><td>.001353569</td><td>738.788</td></tr><tr><td>7</td><td>10.7080</td><td>10.8981</td><td>11.0908</td><td>0.062179</td><td>.003866197</td><td>258.652</td></tr><tr><td>8</td><td>11.4356</td><td>11.6217</td><td>11.8097</td><td>0.060770</td><td>.003692971</td><td>270.785</td></tr></tbody></table>

#### NaCl = 0.75%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.2956</td><td>7.4592</td><td>7.6242</td><td>0.051228</td><td>.002624282</td><td>381.057</td></tr><tr><td>2</td><td>7.9276</td><td>8.1070</td><td>8.2881</td><td>0.058568</td><td>.003430153</td><td>291.532</td></tr><tr><td>3</td><td>8.3781</td><td>8.5776</td><td>8.7786</td><td>0.065057</td><td>.004232395</td><td>236.273</td></tr><tr><td>4</td><td>8.9245</td><td>9.1317</td><td>9.3417</td><td>0.067771</td><td>.004592872</td><td>217.729</td></tr><tr><td>5</td><td>9.6352</td><td>9.8482</td><td>10.0633</td><td>0.069534</td><td>.004834945</td><td>206.828</td></tr><tr><td>6</td><td>10.3500</td><td>10.5277</td><td>10.7059</td><td>0.057812</td><td>.003342227</td><td>299.202</td></tr><tr><td>7</td><td>10.9535</td><td>11.1536</td><td>11.3567</td><td>0.065501</td><td>.004290316</td><td>233.083</td></tr><tr><td>8</td><td>11.5995</td><td>11.7631</td><td>11.9292</td><td>0.051402</td><td>.002642145</td><td>378.480</td></tr></tbody></table>

#### NaCl = 1%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.6504</td><td>7.8396</td><td>8.0303</td><td>0.061714</td><td>.003808624</td><td>262.562</td></tr><tr><td>2</td><td>8.1621</td><td>8.3419</td><td>8.5231</td><td>0.058644</td><td>.003439172</td><td>290.768</td></tr><tr><td>3</td><td>8.5904</td><td>8.8359</td><td>9.0902</td><td>0.077921</td><td>.006071696</td><td>164.699</td></tr><tr><td>4</td><td>9.3986</td><td>9.6126</td><td>9.8292</td><td>0.069944</td><td>.004892227</td><td>204.406</td></tr><tr><td>5</td><td>10.0674</td><td>10.3115</td><td>10.5632</td><td>0.077292</td><td>.005974020</td><td>167.391</td></tr><tr><td>6</td><td>10.5640</td><td>10.8612</td><td>11.1729</td><td>0.094916</td><td>.009009108</td><td>110.999</td></tr><tr><td>7</td><td>11.3158</td><td>11.5260</td><td>11.7407</td><td>0.066239</td><td>.004387671</td><td>227.911</td></tr><tr><td>8</td><td>12.2196</td><td>12.4234</td><td>12.6280</td><td>0.068385</td><td>.004676444</td><td>213.838</td></tr></tbody></table>
NaCl = 1.5%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>8.2051</td><td>8.3614</td><td>8.5191</td><td>0.05101</td><td>0.002602</td><td>384.35</td></tr><tr><td>2</td><td>9.0329</td><td>9.1205</td><td>9.2086</td><td>0.02855</td><td>0.000815</td><td>1227.08</td></tr><tr><td>3</td><td>9.4981</td><td>9.6333</td><td>9.7685</td><td>0.04527</td><td>0.002050</td><td>487.91</td></tr><tr><td>4</td><td>10.0593</td><td>10.2874</td><td>10.5213</td><td>0.07202</td><td>0.005187</td><td>192.78</td></tr><tr><td>5</td><td>10.9291</td><td>11.1075</td><td>11.2876</td><td>0.05824</td><td>0.003392</td><td>294.83</td></tr><tr><td>6</td><td>11.3364</td><td>11.5779</td><td>11.8216</td><td>0.07881</td><td>0.006212</td><td>160.99</td></tr><tr><td>7</td><td>12.1261</td><td>12.4363</td><td>12.7552</td><td>0.10218</td><td>0.010441</td><td>95.77</td></tr><tr><td>8</td><td>13.0477</td><td>13.2911</td><td>13.5379</td><td>0.08207</td><td>0.006736</td><td>148.46</td></tr></tbody></table>

NaCl = 3%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>10.2001</td><td>10.4631</td><td>10.7284</td><td>0.093601</td><td>.008761125</td><td>114.14</td></tr><tr><td>2</td><td>10.6626</td><td>10.8766</td><td>11.0921</td><td>0.073603</td><td>.005417440</td><td>184.59</td></tr><tr><td>3</td><td>12.1089</td><td>12.2279</td><td>12.3471</td><td>0.042729</td><td>.001825739</td><td>547.72</td></tr><tr><td>4</td><td>12.8677</td><td>13.0898</td><td>13.3122</td><td>0.081896</td><td>.006706879</td><td>149.10</td></tr><tr><td>5</td><td>13.8489</td><td>13.9297</td><td>14.0106</td><td>0.029008</td><td>.000841465</td><td>1188.40</td></tr><tr><td>6</td><td>14.5302</td><td>14.6807</td><td>14.8313</td><td>0.054014</td><td>.002917549</td><td>342.75</td></tr><tr><td>7</td><td>15.7724</td><td>16.0062</td><td>16.2407</td><td>0.085614</td><td>.007329749</td><td>136.43</td></tr><tr><td>8</td><td>16.1024</td><td>16.1723</td><td>16.2423</td><td>0.024427</td><td>.000596674</td><td>1675.96</td></tr></tbody></table>

NaCl = 5%

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>14.3675</td><td>14.6089</td><td>14.8505</td><td>0.09171</td><td>0.008411</td><td>118.887</td></tr><tr><td>2</td><td>16.0333</td><td>16.1604</td><td>16.2875</td><td>0.04860</td><td>0.002362</td><td>423.418</td></tr><tr><td>3</td><td>17.0473</td><td>17.2686</td><td>17.4901</td><td>0.08437</td><td>0.007118</td><td>140.497</td></tr><tr><td>4</td><td>18.0170</td><td>18.4310</td><td>18.8451</td><td>0.15871</td><td>0.025190</td><td>39.699</td></tr><tr><td>5</td><td>19.5369</td><td>19.8028</td><td>20.0687</td><td>0.10218</td><td>0.010441</td><td>95.772</td></tr><tr><td>6</td><td>20.5713</td><td>21.0968</td><td>21.6236</td><td>0.20168</td><td>0.040675</td><td>24.585</td></tr><tr><td>7</td><td>21.4664</td><td>21.6693</td><td>21.8721</td><td>0.07753</td><td>0.006012</td><td>166.344</td></tr><tr><td>8</td><td>22.2655</td><td>22.4839</td><td>22.7025</td><td>0.08267</td><td>0.006834</td><td>146.334</td></tr></tbody></table>
# Caractéristiques du paramètre mumax pour chaque taux de NaCl
et pour chaque méthode de régression

## OLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.04618</td><td>1.08506</td><td>1.12393</td><td>0.015887</td><td>.000252406</td><td>1.46419</td></tr><tr><td>2</td><td>1.05937</td><td>1.11588</td><td>1.17239</td><td>0.023095</td><td>.000533378</td><td>2.06966</td></tr><tr><td>3</td><td>0.97823</td><td>1.05477</td><td>1.13130</td><td>0.031279</td><td>.000978376</td><td>2.96549</td></tr><tr><td>4</td><td>0.93069</td><td>1.00125</td><td>1.07181</td><td>0.028835</td><td>.000831465</td><td>2.87991</td></tr><tr><td>5</td><td>0.68996</td><td>0.77693</td><td>0.86389</td><td>0.035542</td><td>.001263224</td><td>4.57468</td></tr><tr><td>6</td><td>0.53672</td><td>0.60111</td><td>0.66549</td><td>0.026312</td><td>.000692297</td><td>4.37719</td></tr></tbody></table>

## WLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.04621</td><td>1.08517</td><td>1.12413</td><td>0.015922</td><td>.000253522</td><td>1.46727</td></tr><tr><td>2</td><td>1.05913</td><td>1.11586</td><td>1.17259</td><td>0.023184</td><td>.000537501</td><td>2.07769</td></tr><tr><td>3</td><td>0.97837</td><td>1.05494</td><td>1.13152</td><td>0.031295</td><td>.000979373</td><td>2.96650</td></tr><tr><td>4</td><td>0.93081</td><td>1.00124</td><td>1.07166</td><td>0.028781</td><td>.000828346</td><td>2.87454</td></tr><tr><td>5</td><td>0.68989</td><td>0.77681</td><td>0.86372</td><td>0.035520</td><td>.001261656</td><td>4.57254</td></tr><tr><td>6</td><td>0.53676</td><td>0.60102</td><td>0.66528</td><td>0.026262</td><td>.000689669</td><td>4.36949</td></tr></tbody></table>

## IRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.04838</td><td>1.08159</td><td>1.11479</td><td>0.013570</td><td>.000184158</td><td>1.25468</td></tr><tr><td>2</td><td>1.07719</td><td>1.11525</td><td>1.15331</td><td>0.015555</td><td>.000241957</td><td>1.39475</td></tr><tr><td>3</td><td>0.99257</td><td>1.06552</td><td>1.13846</td><td>0.029812</td><td>.000888734</td><td>2.79785</td></tr><tr><td>4</td><td>0.95107</td><td>1.00506</td><td>1.05905</td><td>0.022066</td><td>.000486898</td><td>2.19546</td></tr><tr><td>5</td><td>0.70645</td><td>0.78564</td><td>0.86482</td><td>0.032361</td><td>.001047239</td><td>4.11908</td></tr><tr><td>6</td><td>0.54085</td><td>0.59797</td><td>0.65508</td><td>0.023341</td><td>.000544795</td><td>3.90337</td></tr></tbody></table>

## DWLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.04647</td><td>1.08559</td><td>1.12471</td><td>0.015986</td><td>.000255567</td><td>1.47261</td></tr><tr><td>2</td><td>1.06025</td><td>1.11640</td><td>1.17255</td><td>0.022946</td><td>.000526513</td><td>2.05535</td></tr><tr><td>3</td><td>0.97958</td><td>1.05576</td><td>1.13193</td><td>0.031131</td><td>.000969129</td><td>2.94868</td></tr><tr><td>4</td><td>0.93227</td><td>1.00276</td><td>1.07326</td><td>0.028808</td><td>.000829895</td><td>2.87285</td></tr><tr><td>5</td><td>0.69124</td><td>0.77877</td><td>0.86630</td><td>0.035771</td><td>.001279563</td><td>4.59326</td></tr><tr><td>6</td><td>0.54073</td><td>0.60381</td><td>0.66689</td><td>0.025778</td><td>.000664517</td><td>4.26923</td></tr></tbody></table>

## IDRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>1.04837</td><td>1.08248</td><td>1.11659</td><td>0.013940</td><td>.000194331</td><td>1.28781</td></tr><tr><td>2</td><td>1.07386</td><td>1.11520</td><td>1.15653</td><td>0.016892</td><td>.000285347</td><td>1.51473</td></tr><tr><td>3</td><td>1.00502</td><td>1.07279</td><td>1.14057</td><td>0.027698</td><td>.000767165</td><td>2.58184</td></tr><tr><td>4</td><td>0.95152</td><td>1.00910</td><td>1.06667</td><td>0.023528</td><td>.000553587</td><td>2.33163</td></tr><tr><td>5</td><td>0.72300</td><td>0.79638</td><td>0.86976</td><td>0.029989</td><td>.000899312</td><td>3.76562</td></tr><tr><td>6</td><td>0.55057</td><td>0.60746</td><td>0.66435</td><td>0.023249</td><td>.000540510</td><td>3.82724</td></tr></tbody></table>
# IPL LM PH (9 niveaux de pH)

## PLAQUE 1

### Temps de détection pour les 8 dilutions

$$ \text{pH} = 4.85 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>17.4501</td><td>17.7339</td><td>18.0178</td><td>0.11023</td><td>0.012150</td><td>82.305</td></tr><tr><td>2</td><td>19.6939</td><td>19.9124</td><td>20.1308</td><td>0.08567</td><td>0.007340</td><td>136.247</td></tr><tr><td>3</td><td>21.0895</td><td>21.4099</td><td>21.7302</td><td>0.12575</td><td>0.015814</td><td>63.236</td></tr><tr><td>4</td><td>22.3802</td><td>22.7979</td><td>23.2153</td><td>0.16373</td><td>0.026807</td><td>37.304</td></tr><tr><td>5</td><td>23.5241</td><td>23.8226</td><td>24.1211</td><td>0.11690</td><td>0.013666</td><td>73.174</td></tr><tr><td>6</td><td>25.5221</td><td>25.9387</td><td>26.3550</td><td>0.16395</td><td>0.026880</td><td>37.202</td></tr><tr><td>7</td><td>27.0064</td><td>27.4094</td><td>27.8122</td><td>0.15848</td><td>0.025115</td><td>39.817</td></tr><tr><td>8</td><td>28.3790</td><td>29.0536</td><td>29.7274</td><td>0.26589</td><td>0.070700</td><td>14.144</td></tr></tbody></table>

$$ \text{pH} = 5.09 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>13.2441</td><td>13.6112</td><td>13.9785</td><td>0.14283</td><td>0.020400</td><td>49.0187</td></tr><tr><td>2</td><td>14.1711</td><td>14.6132</td><td>15.0557</td><td>0.17232</td><td>0.029693</td><td>33.6780</td></tr><tr><td>3</td><td>15.6535</td><td>16.0869</td><td>16.5206</td><td>0.16891</td><td>0.028532</td><td>35.0483</td></tr><tr><td>4</td><td>16.6837</td><td>17.2603</td><td>17.8372</td><td>0.22533</td><td>0.050773</td><td>19.6957</td></tr><tr><td>5</td><td>18.0209</td><td>18.4609</td><td>18.9010</td><td>0.17192</td><td>0.029556</td><td>33.8338</td></tr><tr><td>6</td><td>18.7443</td><td>19.2674</td><td>19.7911</td><td>0.20419</td><td>0.041692</td><td>23.9856</td></tr><tr><td>7</td><td>19.7585</td><td>20.2978</td><td>20.8374</td><td>0.21075</td><td>0.044416</td><td>22.5142</td></tr><tr><td>8</td><td>21.0810</td><td>21.6214</td><td>22.1619</td><td>0.21168</td><td>0.044808</td><td>22.3173</td></tr></tbody></table>

$$ \text{pH} = 5.29 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>11.8243</td><td>12.3541</td><td>12.8839</td><td>0.20639</td><td>0.042598</td><td>23.4755</td></tr><tr><td>2</td><td>12.7016</td><td>13.3134</td><td>13.9254</td><td>0.23872</td><td>0.056989</td><td>17.5471</td></tr><tr><td>3</td><td>13.4614</td><td>14.1593</td><td>14.8592</td><td>0.27040</td><td>0.073119</td><td>13.6764</td></tr><tr><td>4</td><td>14.7152</td><td>15.3424</td><td>15.9696</td><td>0.24504</td><td>0.060043</td><td>16.6547</td></tr><tr><td>5</td><td>15.5923</td><td>16.1909</td><td>16.7898</td><td>0.23326</td><td>0.054410</td><td>18.3790</td></tr><tr><td>6</td><td>16.3559</td><td>17.0050</td><td>17.6547</td><td>0.25217</td><td>0.063588</td><td>15.7261</td></tr><tr><td>7</td><td>17.2797</td><td>17.9427</td><td>18.6068</td><td>0.25722</td><td>0.066160</td><td>15.1150</td></tr><tr><td>8</td><td>18.2067</td><td>18.7682</td><td>19.3328</td><td>0.21638</td><td>0.046822</td><td>21.3576</td></tr></tbody></table>
## pH = 6.12

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>8.7168</td><td>9.2021</td><td>9.6909</td><td>0.17947</td><td>0.032210</td><td>31.0465</td></tr><tr><td>2</td><td>9.7727</td><td>10.1907</td><td>10.6081</td><td>0.15585</td><td>0.024288</td><td>41.1722</td></tr><tr><td>3</td><td>10.2721</td><td>10.7949</td><td>11.3163</td><td>0.19367</td><td>0.037510</td><td>26.6596</td></tr><tr><td>4</td><td>10.9820</td><td>11.4829</td><td>11.9855</td><td>0.18613</td><td>0.034644</td><td>28.8654</td></tr><tr><td>5</td><td>11.9302</td><td>12.2395</td><td>12.5497</td><td>0.11326</td><td>0.012829</td><td>77.9501</td></tr><tr><td>6</td><td>12.7797</td><td>13.1362</td><td>13.4927</td><td>0.13223</td><td>0.017485</td><td>57.1916</td></tr><tr><td>7</td><td>13.1761</td><td>13.7766</td><td>14.3727</td><td>0.22323</td><td>0.049833</td><td>20.0669</td></tr><tr><td>8</td><td>14.2044</td><td>14.5763</td><td>14.9489</td><td>0.13717</td><td>0.018816</td><td>53.1457</td></tr></tbody></table>

## pH = 6.61

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.9083</td><td>8.6169</td><td>9.3565</td><td>0.25658</td><td>0.065832</td><td>15.1901</td></tr><tr><td>2</td><td>8.9289</td><td>9.6013</td><td>10.3004</td><td>0.24300</td><td>0.059049</td><td>16.9351</td></tr><tr><td>3</td><td>9.6094</td><td>10.2606</td><td>10.9470</td><td>0.23348</td><td>0.054511</td><td>18.3450</td></tr><tr><td>4</td><td>10.4035</td><td>11.0651</td><td>11.7500</td><td>0.23856</td><td>0.056910</td><td>17.5715</td></tr><tr><td>5</td><td>11.0409</td><td>11.7847</td><td>12.5788</td><td>0.27246</td><td>0.074236</td><td>13.4706</td></tr><tr><td>6</td><td>11.7532</td><td>12.4763</td><td>13.2418</td><td>0.26373</td><td>0.069555</td><td>14.3772</td></tr><tr><td>7</td><td>12.6525</td><td>13.3390</td><td>14.0726</td><td>0.24787</td><td>0.061439</td><td>16.2763</td></tr><tr><td>8</td><td>13.3311</td><td>14.0683</td><td>14.8581</td><td>0.27052</td><td>0.073183</td><td>13.6644</td></tr></tbody></table>

## pH = 7.05

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.8326</td><td>8.6993</td><td>9.6252</td><td>0.32152</td><td>0.10337</td><td>9.6736</td></tr><tr><td>2</td><td>8.6507</td><td>9.5021</td><td>10.4160</td><td>0.31275</td><td>0.09781</td><td>10.2237</td></tr><tr><td>3</td><td>9.4578</td><td>10.2346</td><td>11.0922</td><td>0.28528</td><td>0.08138</td><td>12.2877</td></tr><tr><td>4</td><td>10.0713</td><td>10.9745</td><td>11.9808</td><td>0.33832</td><td>0.11446</td><td>8.7368</td></tr><tr><td>5</td><td>10.8297</td><td>11.7021</td><td>12.6334</td><td>0.31956</td><td>0.10212</td><td>9.7928</td></tr><tr><td>6</td><td>11.5176</td><td>12.3538</td><td>13.2629</td><td>0.30921</td><td>0.09561</td><td>10.4591</td></tr><tr><td>7</td><td>12.1304</td><td>12.9908</td><td>13.9137</td><td>0.31594</td><td>0.09982</td><td>10.0184</td></tr><tr><td>8</td><td>12.9408</td><td>13.7916</td><td>14.7099</td><td>0.31342</td><td>0.09824</td><td>10.1797</td></tr></tbody></table>

## pH = 7.54

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.9187</td><td>8.9866</td><td>10.1189</td><td>0.40229</td><td>0.16184</td><td>6.17890</td></tr><tr><td>2</td><td>8.9193</td><td>9.8317</td><td>10.8255</td><td>0.34190</td><td>0.11690</td><td>8.55454</td></tr><tr><td>3</td><td>9.4655</td><td>10.4866</td><td>11.5943</td><td>0.38581</td><td>0.14885</td><td>6.71804</td></tr><tr><td>4</td><td>10.2359</td><td>11.1625</td><td>12.1527</td><td>0.34382</td><td>0.11821</td><td>8.45950</td></tr><tr><td>5</td><td>10.9939</td><td>11.9107</td><td>12.9192</td><td>0.34534</td><td>0.11926</td><td>8.38506</td></tr><tr><td>6</td><td>11.7074</td><td>12.6368</td><td>13.6575</td><td>0.34979</td><td>0.12235</td><td>8.17303</td></tr><tr><td>7</td><td>12.2337</td><td>13.2667</td><td>14.3923</td><td>0.39122</td><td>0.15305</td><td>6.53363</td></tr><tr><td>8</td><td>13.0284</td><td>14.0317</td><td>15.1239</td><td>0.37978</td><td>0.14423</td><td>6.93325</td></tr></tbody></table>
$$pH = 8.47$$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>8.2083</td><td>9.3785</td><td>10.6451</td><td>0.44557</td><td>0.19853</td><td>5.03704</td></tr><tr><td>2</td><td>9.0835</td><td>10.1419</td><td>11.2815</td><td>0.39834</td><td>0.15868</td><td>6.30213</td></tr><tr><td>3</td><td>9.7293</td><td>10.7963</td><td>11.9340</td><td>0.40313</td><td>0.16251</td><td>6.15334</td></tr><tr><td>4</td><td>10.5064</td><td>11.5438</td><td>12.6476</td><td>0.39151</td><td>0.15328</td><td>6.52413</td></tr><tr><td>5</td><td>10.9578</td><td>12.3455</td><td>13.9008</td><td>0.54223</td><td>0.29401</td><td>3.40119</td></tr><tr><td>6</td><td>11.7119</td><td>13.0525</td><td>14.5427</td><td>0.52156</td><td>0.27202</td><td>3.67617</td></tr><tr><td>7</td><td>12.4357</td><td>13.7084</td><td>15.1029</td><td>0.49141</td><td>0.24148</td><td>4.14106</td></tr><tr><td>8</td><td>13.4523</td><td>14.4378</td><td>15.4985</td><td>0.37084</td><td>0.13752</td><td>7.27170</td></tr></tbody></table>

$$pH = 8.90$$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>9.2879</td><td>10.3543</td><td>11.4742</td><td>0.40548</td><td>0.16442</td><td>6.08213</td></tr><tr><td>2</td><td>10.2849</td><td>11.2596</td><td>12.2731</td><td>0.36877</td><td>0.13599</td><td>7.35340</td></tr><tr><td>3</td><td>10.9269</td><td>12.0231</td><td>13.1893</td><td>0.41960</td><td>0.17607</td><td>5.67962</td></tr><tr><td>4</td><td>11.5814</td><td>12.6843</td><td>13.8510</td><td>0.42096</td><td>0.17720</td><td>5.64322</td></tr><tr><td>5</td><td>12.4126</td><td>13.4910</td><td>14.6347</td><td>0.41214</td><td>0.16986</td><td>5.88728</td></tr><tr><td>6</td><td>13.0719</td><td>14.1609</td><td>15.3102</td><td>0.41515</td><td>0.17235</td><td>5.80208</td></tr><tr><td>7</td><td>13.8459</td><td>14.9219</td><td>16.0577</td><td>0.41024</td><td>0.16829</td><td>5.94200</td></tr><tr><td>8</td><td>14.5591</td><td>15.6850</td><td>16.8585</td><td>0.42896</td><td>0.18401</td><td>5.43459</td></tr></tbody></table>
# Caractéristiques du paramètre mumax pour chaque taux de NaCl
et pour chaque méthode de régression

## OLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.40998</td><td>0.44016</td><td>0.47035</td><td>0.012337</td><td>.000152191</td><td>2.80273</td></tr><tr><td>2</td><td>0.57085</td><td>0.60764</td><td>0.64443</td><td>0.015037</td><td>.000226109</td><td>2.47465</td></tr><tr><td>3</td><td>0.72195</td><td>0.74902</td><td>0.77609</td><td>0.011062</td><td>.000122362</td><td>1.47683</td></tr><tr><td>4</td><td>0.87248</td><td>0.91527</td><td>0.95805</td><td>0.017487</td><td>.000305784</td><td>1.91056</td></tr><tr><td>5</td><td>0.86949</td><td>0.90327</td><td>0.93704</td><td>0.013802</td><td>.000190502</td><td>1.52804</td></tr><tr><td>6</td><td>0.93372</td><td>0.96428</td><td>0.99484</td><td>0.012488</td><td>.000155957</td><td>1.29509</td></tr><tr><td>7</td><td>0.94371</td><td>0.97233</td><td>1.00095</td><td>0.011697</td><td>.000136815</td><td>1.20296</td></tr><tr><td>8</td><td>0.93174</td><td>0.95453</td><td>0.97732</td><td>0.009314</td><td>.000086748</td><td>0.97575</td></tr><tr><td>9</td><td>0.89037</td><td>0.92316</td><td>0.95595</td><td>0.013400</td><td>.000179562</td><td>1.45154</td></tr></tbody></table>

## WLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.40991</td><td>0.44014</td><td>0.47037</td><td>0.012355</td><td>.000152651</td><td>2.80711</td></tr><tr><td>2</td><td>0.57079</td><td>0.60765</td><td>0.64451</td><td>0.015064</td><td>.000226915</td><td>2.47900</td></tr><tr><td>3</td><td>0.72180</td><td>0.74895</td><td>0.77610</td><td>0.011095</td><td>.000123101</td><td>1.48143</td></tr><tr><td>4</td><td>0.87242</td><td>0.91523</td><td>0.95803</td><td>0.017493</td><td>.000306004</td><td>1.91133</td></tr><tr><td>5</td><td>0.86938</td><td>0.90313</td><td>0.93689</td><td>0.013793</td><td>.000190253</td><td>1.52726</td></tr><tr><td>6</td><td>0.93362</td><td>0.96426</td><td>0.99489</td><td>0.012519</td><td>.000156730</td><td>1.29832</td></tr><tr><td>7</td><td>0.94364</td><td>0.97230</td><td>1.00096</td><td>0.011714</td><td>.000137207</td><td>1.20473</td></tr><tr><td>8</td><td>0.93167</td><td>0.95451</td><td>0.97734</td><td>0.009332</td><td>.000087091</td><td>0.97770</td></tr><tr><td>9</td><td>0.89023</td><td>0.92307</td><td>0.95592</td><td>0.013424</td><td>.000180214</td><td>1.45431</td></tr></tbody></table>

## IRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.41568</td><td>0.43866</td><td>0.46165</td><td>0.009394</td><td>.000088243</td><td>2.14146</td></tr><tr><td>2</td><td>0.57814</td><td>0.60753</td><td>0.63693</td><td>0.012013</td><td>.000144313</td><td>1.97735</td></tr><tr><td>3</td><td>0.72690</td><td>0.74757</td><td>0.76823</td><td>0.008446</td><td>.000071329</td><td>1.12975</td></tr><tr><td>4</td><td>0.87667</td><td>0.91060</td><td>0.94452</td><td>0.013864</td><td>.000192215</td><td>1.52253</td></tr><tr><td>5</td><td>0.88005</td><td>0.90586</td><td>0.93167</td><td>0.010548</td><td>.000111262</td><td>1.16442</td></tr><tr><td>6</td><td>0.94369</td><td>0.96612</td><td>0.98856</td><td>0.009168</td><td>.000084053</td><td>0.94895</td></tr><tr><td>7</td><td>0.94677</td><td>0.97147</td><td>0.99617</td><td>0.010094</td><td>.000101892</td><td>1.03906</td></tr><tr><td>8</td><td>0.93793</td><td>0.95561</td><td>0.97329</td><td>0.007226</td><td>.000052212</td><td>0.75614</td></tr><tr><td>9</td><td>0.89938</td><td>0.92808</td><td>0.95677</td><td>0.011727</td><td>.000137531</td><td>1.26362</td></tr></tbody></table>

## DWLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.40940</td><td>0.44057</td><td>0.47174</td><td>0.012737</td><td>.000162224</td><td>2.89096</td></tr><tr><td>2</td><td>0.57056</td><td>0.60725</td><td>0.64393</td><td>0.014993</td><td>.000224785</td><td>2.46899</td></tr><tr><td>3</td><td>0.72280</td><td>0.74950</td><td>0.77620</td><td>0.010913</td><td>.000119088</td><td>1.45600</td></tr><tr><td>4</td><td>0.87247</td><td>0.91570</td><td>0.95892</td><td>0.017666</td><td>.000312073</td><td>1.92920</td></tr><tr><td>5</td><td>0.87009</td><td>0.90420</td><td>0.93831</td><td>0.013941</td><td>.000194342</td><td>1.54176</td></tr><tr><td>6</td><td>0.93485</td><td>0.96534</td><td>0.99583</td><td>0.012460</td><td>.000155264</td><td>1.29079</td></tr><tr><td>7</td><td>0.94454</td><td>0.97399</td><td>1.00345</td><td>0.012037</td><td>.000144896</td><td>1.23587</td></tr><tr><td>8</td><td>0.93488</td><td>0.95586</td><td>0.97684</td><td>0.008574</td><td>.000073515</td><td>0.89701</td></tr><tr><td>9</td><td>0.89142</td><td>0.92447</td><td>0.95752</td><td>0.013508</td><td>.000182461</td><td>1.46114</td></tr></tbody></table>
IDRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.41651</td><td>0.44022</td><td>0.46393</td><td>0.009689</td><td>.000093874</td><td>2.20090</td></tr><tr><td>2</td><td>0.57858</td><td>0.60732</td><td>0.63606</td><td>0.011745</td><td>.000137941</td><td>1.93389</td></tr><tr><td>3</td><td>0.72845</td><td>0.74846</td><td>0.76847</td><td>0.008178</td><td>.000066878</td><td>1.09264</td></tr><tr><td>4</td><td>0.87725</td><td>0.91027</td><td>0.94329</td><td>0.013495</td><td>.000182121</td><td>1.48255</td></tr><tr><td>5</td><td>0.88094</td><td>0.90581</td><td>0.93068</td><td>0.010165</td><td>.000103328</td><td>1.12220</td></tr><tr><td>6</td><td>0.94451</td><td>0.96764</td><td>0.99078</td><td>0.009454</td><td>.000089387</td><td>0.97706</td></tr><tr><td>7</td><td>0.94796</td><td>0.97254</td><td>0.99712</td><td>0.010044</td><td>.000100892</td><td>1.03281</td></tr><tr><td>8</td><td>0.93813</td><td>0.95523</td><td>0.97234</td><td>0.006990</td><td>.000048859</td><td>0.73175</td></tr><tr><td>9</td><td>0.90018</td><td>0.92893</td><td>0.95768</td><td>0.011750</td><td>.000138071</td><td>1.26494</td></tr></tbody></table>
# IPL LM PH (8 niveaux de pH)

## PLAQUE 2

### Temps de détection pour les 8 dilutions

$$ \text{pH} = 5.10 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>12.7381</td><td>13.1037</td><td>13.4697</td><td>0.14093</td><td>0.019861</td><td>50.3491</td></tr><tr><td>2</td><td>13.5171</td><td>13.9455</td><td>14.3747</td><td>0.16589</td><td>0.027521</td><td>36.3362</td></tr><tr><td>3</td><td>14.7714</td><td>15.2031</td><td>15.6352</td><td>0.16741</td><td>0.028028</td><td>35.6791</td></tr><tr><td>4</td><td>16.2196</td><td>16.5626</td><td>16.9056</td><td>0.13343</td><td>0.017803</td><td>56.1717</td></tr><tr><td>5</td><td>17.2068</td><td>17.6209</td><td>18.0353</td><td>0.16137</td><td>0.026040</td><td>38.4024</td></tr><tr><td>6</td><td>17.9719</td><td>18.3827</td><td>18.7940</td><td>0.15962</td><td>0.025478</td><td>39.2493</td></tr><tr><td>7</td><td>19.6994</td><td>20.0661</td><td>20.4339</td><td>0.14261</td><td>0.020339</td><td>49.1675</td></tr><tr><td>8</td><td>20.3655</td><td>20.8327</td><td>21.3033</td><td>0.18064</td><td>0.032632</td><td>30.6451</td></tr></tbody></table>

$$ \text{pH} = 5.32 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>11.1960</td><td>11.6906</td><td>12.1865</td><td>0.19078</td><td>0.036397</td><td>27.4745</td></tr><tr><td>2</td><td>12.1696</td><td>12.7319</td><td>13.2947</td><td>0.21763</td><td>0.047363</td><td>21.1135</td></tr><tr><td>3</td><td>12.9589</td><td>13.6458</td><td>14.3335</td><td>0.26643</td><td>0.070983</td><td>14.0879</td></tr><tr><td>4</td><td>13.8630</td><td>14.4537</td><td>15.0455</td><td>0.22828</td><td>0.052113</td><td>19.1891</td></tr><tr><td>5</td><td>14.8151</td><td>15.3943</td><td>15.9748</td><td>0.22433</td><td>0.050322</td><td>19.8719</td></tr><tr><td>6</td><td>15.9352</td><td>16.4288</td><td>16.9229</td><td>0.19144</td><td>0.036647</td><td>27.2871</td></tr><tr><td>7</td><td>16.8719</td><td>17.3599</td><td>17.8482</td><td>0.18923</td><td>0.035809</td><td>27.9263</td></tr><tr><td>8</td><td>17.5362</td><td>18.0983</td><td>18.6615</td><td>0.21675</td><td>0.046979</td><td>21.2862</td></tr></tbody></table>

$$ \text{pH} = 6.14 $$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th> poids</th></tr></thead><tbody><tr><td>1</td><td>8.6383</td><td>9.1331</td><td>9.6336</td><td>0.18199</td><td>0.033119</td><td>30.1938</td></tr><tr><td>2</td><td>9.6868</td><td>10.0215</td><td>10.3563</td><td>0.12334</td><td>0.015214</td><td>65.7298</td></tr><tr><td>3</td><td>10.2011</td><td>10.6171</td><td>11.0346</td><td>0.15357</td><td>0.023584</td><td>42.4011</td></tr><tr><td>4</td><td>11.0620</td><td>11.4335</td><td>11.8056</td><td>0.13596</td><td>0.018486</td><td>54.0959</td></tr><tr><td>5</td><td>11.7297</td><td>12.0920</td><td>12.4552</td><td>0.13367</td><td>0.017867</td><td>55.9683</td></tr><tr><td>6</td><td>12.4053</td><td>12.8074</td><td>13.2102</td><td>0.14829</td><td>0.021991</td><td>45.4727</td></tr><tr><td>7</td><td>13.1108</td><td>13.5590</td><td>14.0081</td><td>0.16531</td><td>0.027327</td><td>36.5938</td></tr><tr><td>8</td><td>13.8139</td><td>14.2655</td><td>14.7197</td><td>0.16563</td><td>0.027434</td><td>36.4515</td></tr></tbody></table>
## pH = 6.61

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.9851</td><td>8.6975</td><td>9.4731</td><td>0.25974</td><td>0.067462</td><td>14.8231</td></tr><tr><td>2</td><td>8.7765</td><td>9.3821</td><td>10.0267</td><td>0.21423</td><td>0.045895</td><td>21.7886</td></tr><tr><td>3</td><td>9.3795</td><td>10.0357</td><td>10.7299</td><td>0.23572</td><td>0.055562</td><td>17.9978</td></tr><tr><td>4</td><td>10.1126</td><td>10.7661</td><td>11.4819</td><td>0.23465</td><td>0.055063</td><td>18.1611</td></tr><tr><td>5</td><td>10.8752</td><td>11.5338</td><td>12.2304</td><td>0.23654</td><td>0.055952</td><td>17.8724</td></tr><tr><td>6</td><td>11.5785</td><td>12.1851</td><td>12.8363</td><td>0.21555</td><td>0.046462</td><td>21.5231</td></tr><tr><td>7</td><td>12.1594</td><td>12.8244</td><td>13.5321</td><td>0.23960</td><td>0.057406</td><td>17.4198</td></tr><tr><td>8</td><td>12.8296</td><td>13.4829</td><td>14.1942</td><td>0.23385</td><td>0.054688</td><td>18.2855</td></tr></tbody></table>

## pH = 7.06

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.8673</td><td>8.7281</td><td>9.6503</td><td>0.31981</td><td>0.10228</td><td>9.7773</td></tr><tr><td>2</td><td>8.6095</td><td>9.4829</td><td>10.4196</td><td>0.32069</td><td>0.10284</td><td>9.7237</td></tr><tr><td>3</td><td>9.4619</td><td>10.2423</td><td>11.1054</td><td>0.28686</td><td>0.08229</td><td>12.1527</td></tr><tr><td>4</td><td>10.0310</td><td>10.8777</td><td>11.8021</td><td>0.31380</td><td>0.09847</td><td>10.1555</td></tr><tr><td>5</td><td>10.7593</td><td>11.5692</td><td>12.4431</td><td>0.29831</td><td>0.08899</td><td>11.2377</td></tr><tr><td>6</td><td>11.4084</td><td>12.2139</td><td>13.0707</td><td>0.29451</td><td>0.08674</td><td>11.5290</td></tr><tr><td>7</td><td>12.1899</td><td>13.0023</td><td>13.9062</td><td>0.29958</td><td>0.08975</td><td>11.1423</td></tr><tr><td>8</td><td>12.8234</td><td>13.6946</td><td>14.6573</td><td>0.32490</td><td>0.10556</td><td>9.4734</td></tr></tbody></table>

## pH = 7.55

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>7.8891</td><td>8.9175</td><td>10.0254</td><td>0.38717</td><td>0.14990</td><td>6.67094</td></tr><tr><td>2</td><td>8.7019</td><td>9.6873</td><td>10.7484</td><td>0.36708</td><td>0.13475</td><td>7.42139</td></tr><tr><td>3</td><td>9.3192</td><td>10.3654</td><td>11.4875</td><td>0.39297</td><td>0.15443</td><td>6.47547</td></tr><tr><td>4</td><td>10.2485</td><td>11.1576</td><td>12.1564</td><td>0.34222</td><td>0.11711</td><td>8.53870</td></tr><tr><td>5</td><td>10.8332</td><td>11.7404</td><td>12.7176</td><td>0.33800</td><td>0.11425</td><td>8.75298</td></tr><tr><td>6</td><td>11.5038</td><td>12.4168</td><td>13.3919</td><td>0.33867</td><td>0.11470</td><td>8.71852</td></tr><tr><td>7</td><td>12.1854</td><td>13.1251</td><td>14.1569</td><td>0.35361</td><td>0.12504</td><td>7.99743</td></tr><tr><td>8</td><td>12.8946</td><td>13.7938</td><td>14.7676</td><td>0.33595</td><td>0.11286</td><td>8.86041</td></tr></tbody></table>

## pH = 8.42

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>8.1983</td><td>9.3268</td><td>10.5384</td><td>0.42786</td><td>0.18307</td><td>5.46246</td></tr><tr><td>2</td><td>8.9398</td><td>10.0336</td><td>11.2004</td><td>0.41334</td><td>0.17085</td><td>5.85300</td></tr><tr><td>3</td><td>9.7517</td><td>10.7411</td><td>11.7860</td><td>0.37197</td><td>0.13836</td><td>7.22727</td></tr><tr><td>4</td><td>10.4808</td><td>11.4984</td><td>12.6035</td><td>0.38471</td><td>0.14800</td><td>6.75655</td></tr><tr><td>5</td><td>11.1478</td><td>12.1654</td><td>13.2607</td><td>0.38294</td><td>0.14664</td><td>6.81929</td></tr><tr><td>6</td><td>11.7961</td><td>12.9220</td><td>14.1423</td><td>0.42900</td><td>0.18404</td><td>5.43359</td></tr><tr><td>7</td><td>12.6418</td><td>13.6855</td><td>14.8111</td><td>0.39666</td><td>0.15734</td><td>6.35584</td></tr><tr><td>8</td><td>13.1666</td><td>14.1832</td><td>15.2528</td><td>0.38145</td><td>0.14551</td><td>6.87248</td></tr></tbody></table>
$$pH = 8.85$$

<table><thead><tr><th>Dil</th><th>tinf</th><th>t0</th><th>tsup</th><th>écart-type</th><th>variance</th><th>poids</th></tr></thead><tbody><tr><td>1</td><td>9.1132</td><td>10.1704</td><td>11.2852</td><td>0.40017</td><td>0.16014</td><td>6.24462</td></tr><tr><td>2</td><td>9.7844</td><td>10.8162</td><td>11.8939</td><td>0.38866</td><td>0.15106</td><td>6.61999</td></tr><tr><td>3</td><td>10.5678</td><td>11.6179</td><td>12.7439</td><td>0.39789</td><td>0.15832</td><td>6.31644</td></tr><tr><td>4</td><td>11.3883</td><td>12.3345</td><td>13.3390</td><td>0.35668</td><td>0.12722</td><td>7.86039</td></tr><tr><td>5</td><td>12.0888</td><td>13.0550</td><td>14.0796</td><td>0.36400</td><td>0.13249</td><td>7.54748</td></tr><tr><td>6</td><td>12.6062</td><td>13.6882</td><td>14.8323</td><td>0.41015</td><td>0.16822</td><td>5.94450</td></tr><tr><td>7</td><td>13.4182</td><td>14.4792</td><td>15.6034</td><td>0.40260</td><td>0.16208</td><td>6.16963</td></tr><tr><td>8</td><td>14.1029</td><td>15.1269</td><td>16.2011</td><td>0.38658</td><td>0.14945</td><td>6.69142</td></tr></tbody></table>
# Caractéristiques du paramètre mumax pour chaque taux de NaCl
et pour chaque méthode de régression

## OLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.56740</td><td>0.60678</td><td>0.64617</td><td>0.016096</td><td>.000259077</td><td>2.65266</td></tr><tr><td>2</td><td>0.72490</td><td>0.75070</td><td>0.77651</td><td>0.010547</td><td>.000111250</td><td>1.40501</td></tr><tr><td>3</td><td>0.92671</td><td>0.95381</td><td>0.98091</td><td>0.011075</td><td>.000122666</td><td>1.16118</td></tr><tr><td>4</td><td>0.97699</td><td>1.00211</td><td>1.02723</td><td>0.010268</td><td>.000105424</td><td>1.02460</td></tr><tr><td>5</td><td>0.95781</td><td>0.98433</td><td>1.01085</td><td>0.010839</td><td>.000117487</td><td>1.10117</td></tr><tr><td>6</td><td>0.97550</td><td>0.99969</td><td>1.02388</td><td>0.009886</td><td>.000097731</td><td>0.98890</td></tr><tr><td>7</td><td>0.94453</td><td>0.97565</td><td>1.00678</td><td>0.012721</td><td>.000161821</td><td>1.30383</td></tr><tr><td>8</td><td>0.94698</td><td>0.96848</td><td>0.98999</td><td>0.008789</td><td>.000077251</td><td>0.90753</td></tr></tbody></table>

## WLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.56738</td><td>0.60671</td><td>0.64604</td><td>0.016074</td><td>.000258367</td><td>2.64933</td></tr><tr><td>2</td><td>0.72480</td><td>0.75063</td><td>0.77647</td><td>0.010558</td><td>.000111471</td><td>1.40654</td></tr><tr><td>3</td><td>0.92661</td><td>0.95372</td><td>0.98082</td><td>0.011077</td><td>.000122694</td><td>1.16143</td></tr><tr><td>4</td><td>0.97692</td><td>1.00208</td><td>1.02724</td><td>0.010284</td><td>.000105751</td><td>1.02622</td></tr><tr><td>5</td><td>0.95776</td><td>0.98428</td><td>1.01079</td><td>0.010836</td><td>.000117418</td><td>1.10091</td></tr><tr><td>6</td><td>0.97534</td><td>0.99962</td><td>1.02390</td><td>0.009923</td><td>.000098457</td><td>0.99263</td></tr><tr><td>7</td><td>0.94447</td><td>0.97556</td><td>1.00665</td><td>0.012705</td><td>.000161411</td><td>1.30231</td></tr><tr><td>8</td><td>0.94696</td><td>0.96845</td><td>0.98994</td><td>0.008783</td><td>.000077140</td><td>0.90690</td></tr></tbody></table>

## IRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.57562</td><td>0.60867</td><td>0.64171</td><td>0.013506</td><td>.000182412</td><td>2.21895</td></tr><tr><td>2</td><td>0.72498</td><td>0.75019</td><td>0.77541</td><td>0.010305</td><td>.000106184</td><td>1.37359</td></tr><tr><td>3</td><td>0.93340</td><td>0.95234</td><td>0.97128</td><td>0.007740</td><td>.000059905</td><td>0.81272</td></tr><tr><td>4</td><td>0.98648</td><td>1.00312</td><td>1.01975</td><td>0.006798</td><td>.000046212</td><td>0.67768</td></tr><tr><td>5</td><td>0.96128</td><td>0.98128</td><td>1.00128</td><td>0.008175</td><td>.000066828</td><td>0.83308</td></tr><tr><td>6</td><td>0.99009</td><td>1.00667</td><td>1.02324</td><td>0.006775</td><td>.000045895</td><td>0.67297</td></tr><tr><td>7</td><td>0.94954</td><td>0.96827</td><td>0.98699</td><td>0.007653</td><td>.000058574</td><td>0.79042</td></tr><tr><td>8</td><td>0.95305</td><td>0.96949</td><td>0.98593</td><td>0.006718</td><td>.000045126</td><td>0.69290</td></tr></tbody></table>

## DWLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.56741</td><td>0.60691</td><td>0.64641</td><td>0.016142</td><td>.000260555</td><td>2.65967</td></tr><tr><td>2</td><td>0.72449</td><td>0.74989</td><td>0.77529</td><td>0.010379</td><td>.000107714</td><td>1.38401</td></tr><tr><td>3</td><td>0.92771</td><td>0.95575</td><td>0.98380</td><td>0.011461</td><td>.000131356</td><td>1.19916</td></tr><tr><td>4</td><td>0.97701</td><td>1.00235</td><td>1.02769</td><td>0.010354</td><td>.000107208</td><td>1.03299</td></tr><tr><td>5</td><td>0.95801</td><td>0.98558</td><td>1.01316</td><td>0.011268</td><td>.000126961</td><td>1.14325</td></tr><tr><td>6</td><td>0.97686</td><td>1.00122</td><td>1.02558</td><td>0.009954</td><td>.000099079</td><td>0.99417</td></tr><tr><td>7</td><td>0.94554</td><td>0.97748</td><td>1.00942</td><td>0.013051</td><td>.000170339</td><td>1.33521</td></tr><tr><td>8</td><td>0.94690</td><td>0.96862</td><td>0.99034</td><td>0.008876</td><td>.000078776</td><td>0.91632</td></tr></tbody></table>
IDRLS

<table><thead><tr><th>Obs</th><th>mulow</th><th>mu</th><th>muup</th><th>ecmu</th><th>vmu</th><th>cvmu</th></tr></thead><tbody><tr><td>1</td><td>0.57466</td><td>0.60949</td><td>0.64433</td><td>0.014236</td><td>.000202661</td><td>2.33569</td></tr><tr><td>2</td><td>0.72421</td><td>0.74995</td><td>0.77570</td><td>0.010522</td><td>.000110703</td><td>1.40297</td></tr><tr><td>3</td><td>0.93247</td><td>0.95201</td><td>0.97154</td><td>0.007984</td><td>.000063743</td><td>0.83864</td></tr><tr><td>4</td><td>0.98848</td><td>1.00469</td><td>1.02090</td><td>0.006624</td><td>.000043883</td><td>0.65935</td></tr><tr><td>5</td><td>0.96100</td><td>0.98061</td><td>1.00022</td><td>0.008013</td><td>.000064214</td><td>0.81718</td></tr><tr><td>6</td><td>0.99018</td><td>1.00653</td><td>1.02287</td><td>0.006680</td><td>.000044619</td><td>0.66364</td></tr><tr><td>7</td><td>0.94771</td><td>0.96777</td><td>0.98784</td><td>0.008199</td><td>.000067228</td><td>0.84723</td></tr><tr><td>8</td><td>0.95231</td><td>0.96993</td><td>0.98755</td><td>0.007200</td><td>.000051846</td><td>0.74237</td></tr></tbody></table>
# ANNEXE 9

## PROCEDURE SAS

POUR CALCULER LES ESTIMATIONS DE $\mu_{max}$

AVEC 5 METHODES DE REGRESSION
*/************** REGMACRO00.SAS *****************************/;

/* programme pour exploiter en une seule fois */;

/* toutes les plaques 1 de six taux de NaCl */;

/* au moyen des regressions : */;

/* OLS, WLS , IRLS ,DWLS, IDRLS */;

/* Exemple avec les donnees adria ecoli aw plaquel */;

;

title;

options linesize=85 ps=31000;

**** macroprocedure MREG pour seuiller les fichiers ***/;

**** et calculer les temps de seuil ***/;

%macro mreg(f1=1,f2=1,k1=1,k2=1);

%do i=&f1 %to &f2;

data resul&i;xlow=0; x0=0 ;xup=0 ;sp=0; sp2=0; poids=0;

%end;

%do i=&f1 %to &f2;

data don&i; informat "d:\previus\bioscreen\adria\datarap1\ecawp1_&i..txt";

input t d1-d8;

%end;

%do i=&f1 %to &f2;

data comp&i;set don&i;

%if &i=1 %then %do; dlow1=0.25 ; dup1=0.65 ; seuil1=1000/60;%end;

%if &i=2 %then %do; dlow2=0.25 ; dup2=0.65 ; seuil2=1000/60;%end;

%if &i=3 %then %do; dlow3=0.30 ; dup3=0.70 ; seuil3=1000/60;%end;

%if &i=4 %then %do; dlow4=0.30 ; dup4=0.70 ; seuil4=1000/60;%end;

%if &i=5 %then %do; dlow5=0.25 ; dup5=0.70 ; seuil5=1000/60;%end;

%if &i=6 %then %do; dlow6=0.20 ; dup6=0.70 ; seuil6=2000/60;%end;

%end;

%do i=&f1 %to &f2;

%do k=&k1 %to &k2 ;

data d00; set comp&i;

t=t/60 ;

if t > seuil&i then delete ;

data don&i&k;merge d00(keep=t d&k dlow&i dup&i);

if d&k < dlow&i then delete ;

if d&k > dup&i then delete ;

%end;

%end;

%do i=&f1 %to &f2;

%do k=&k1 %to &k2 ;

data prev1;set comp&i(keep=dlow&i dup&i);

dens0=(dlow&i+dup&i)/2;

data prev2;set prev1;if _N_ > 1 then delete;
d00=dens0;
proc reg data=don&i&k outest=coeff noprint;
model d&k=t;
data coeff2 ; set coeff(keep=_RMSE_ INTERCEPT T) ;
rename _RMSE_ = s INTERCEPT=b0 T=b1 ;
data prev3; merge prev2 coeff2; x0=(d00-b0)/b1 ;

data conf; set prev3(keep=x0 s b1);
proc means data=don&i&k noprint mean n var; var t;
output out=desc mean=moy n=n var=var;
data proba ; set desc(keep=n) ;
fisher=finv(0.95,2,n-2);fisher=sqrt(2*fisher) ;
data conf2; merge conf desc proba;sxx=var*(n-1);

pp=b1*b1-(fisher*fisher*s*s)/sxx ;
qq=2*((fisher*fisher*s*s*moy/sxx)-(b1*b1*x0));
rr=(b1*b1*x0*x0)-(fisher*fisher*s*s)*((n+1)/n)-
(fisher*fisher*s*s*moy*moy/sxx) ;
delta=qq*qq-4*pp*rr;rac=sqrt delta) ;

xlow=((-qq)-rac)/(2*pp) ;
xup=((-qq)+rac)/(2*pp) ;

sp=(xup-xlow)/(2*fisher) ; sp2=sp*sp; poids=1/sp2;

data res1; set conf2(keep=xlow x0 xup sp sp2 poids);
proc append base data= res1 ;
%end;
%end;
%do i=&f1 %to &f2;
data final&i ; set resul&i ; if _n_ =1 then delete ;
proc print data=final&i ;
%end;
%mend;

%mreg(f1=1,f2=6,k1=1,k2=8);
run;

*/**** fin de la macroprocedure MREG *********/;

*/**** constitution du fichier des valeurs ***/;
*/**** de la reponse et de leurs poids ********/;

data repy; input y wy; cards;

12.00 102.266
11.31 102.033
10.62 101.879
9.93 101.510
9.23 101.022
8.54 101.022
7.85 101.022
7.16 100.090
;

*/*******************************************************************/;
/* macroprocedure OLS (regression ordinaire) */;

%macro OLS(f1=1,f2=1);

data rols0;mulow=0; mu=0 ;muup=0 ;ecmu=0; vmu=0; cvmu=0;

%do i=&f1 %to &f2;

data regols;merge final&i(keep=x0) repy(keep=y);
proc reg data=regols outest=coef1 tableout noprint;
model y=x0/influence;
data par1&i ;set coef1(keep=x0) ; if _n_ ^=1 then delete;
x0=-x0;rename x0=mu;
data ect1&i ;set coef1(keep=x0) ;if _n_^=2 then delete;
rename x0=ecmu;
data bal&i ;set coef1(keep=x0) ;if _n_^=5 then delete;
x0=-x0;rename x0=muup;
data bb1&i ;set coef1(keep=x0) ;if _n_^=6 then delete;
x0=-x0;rename x0=mulow;
data rols1&i; merge bb1&i par1&i bal&i ect1&i ;
vmu=ecmu*ecmu;cvmu=100*(ecmu/mu);
proc append base=rols0 data= rols1&i ;
%end;

data rols2 ; set rols0 ; if _n_ =1 then delete ;
proc print data=rols2 ;

%mend;

%OLS(f1=1,f2=6);
run;

*/********************************************************************/

/* macroprocedure WLS (regression ponderee sur Y) */;

%macro WLS(f1=1,f2=1);

data rwls0;mulow=0; mu=0 ;muup=0 ;ecmu=0; vmu=0; cvmu=0;

%do i=&f1 %to &f2;

data regwls;merge final&i(keep=x0) repy(keep=y wy);
proc reg data=regwls outest=coef2 tableout noprint;
model y=x0/influence;
weight wy;

data par2&i ;set coef2(keep=x0) ; if _n_ ^=1 then delete;
x0=-x0 ;rename x0=mu;
data ect2&i ;set coef2(keep=x0) ;if _n_^=2 then delete;
rename x0=ecmu;
data ba2&i ;set coef2(keep=x0) ;if _n_^=5 then delete;
x0=-x0 ;rename x0=muup;
data bb2&i ;set coef2(keep=x0) ;if _n_^=6 then delete;
x0=-x0 ;rename x0=mulow;
data rwls1; merge bb2&i par2&i ba2&i ect2&i;
vmu=ecmu*ecmu;cvmu=(ecmu/mu)*100;
```sas
proc append base=rwls0 data= rwls1;
end;

data rwls2; set rwls0; if _n_ =1 then delete;
proc print data=rwls2;
end;

%WLS(f1=1,f2=6);
run;
```

```
/*****************************************************************/;
```

```
/** macroprocedure IRLS ( ponderee sur Y) **/;
```

```sas
%macro IRLS(f1=1, f2=1);

data rirls0; mulow=0; mu=0; muup=0; ecmu=0; vmu=0; cvmu=0;

do i=&f1 %to &f2;

data regirls&i; merge final&i(keep=x0) repy(keep=y wy);
data transit&i; set regirls&i;

%do k=1 %to 10;
proc reg data=transit&i noprint;
  model y=x0 /r;
  weight wy;
  output out=rirls1&k r=r stdr=stdr;
  data rirls2&k; set rirls1&i(keep=r stdr);
  wy=r/stdr; wy=2/(1+wy**2);
  data transit&i; merge regirls&i(keep=x0 y) rirls2&k(keep=wy);
%end;

proc reg data=transit&i outest=coef3 tableout noprint;
  model y=x0/influence;
  weight wy;
  data par3&i; set coef3(keep=x0) if _n_^=1 then delete;
  x0=-x0; rename x0=mu;
  data ect3&i; set coef3(keep=x0) if _n_^=2 then delete;
  rename x0=ecmu;
  data ba3&i; set coef3(keep=x0) if _n_^=5 then delete;
  x0=-x0; rename x0=muup;
  data bb3&i; set coef3(keep=x0) if _n_^=6 then delete;
  x0=-x0; rename x0=mulow;
  data rirls3; merge bb3&i par3&i ba3&i ect3&i;
  vmu=ecmu*ecmu; cvmu=100*(ecmu/mu);

proc append base=rirls0 data=rirls3;
end;

data rirls4; set rirls0; if _n_ =1 then delete;
proc print data=rirls4;
end;
```
2.447
;

*/**********fin de constitution des fichiers***********/;

*/************** regression DWLS.SAS *******************/;

%macro WNLS(f1=1, f2=1);

data rwnls0;mulow=0; mu=0;muup=0;ecmu=0;vmu=0; cvmu=0;

%do i=&f1 %to &f2 ;

data donx&i ;set final&i(keep=x0 poids);
rename x0=xobs; rename poids=wx;

data d1&i;merge donx&i dony;

data d11&i; set d1&i(keep=wx wy);
wxn=sqrt(wx) ; wyn=sqrt(wy) ;

data d2&i ; merge d1&i(keep=xobs yobs) d11&i(keep=wxn wyn) ;
xw=xobs*wxn ; yw=yobs*wyn ;

data d31&i ; set d2&i(keep=xw) ; rename xw= rep ;
data d32&i ; set d2&i(keep=yw) ; rename yw= rep ;
data d4&i ; set d31&i d32&i ;

data d52&i; merge d51 d11&i(keep=wxn) ;
%do k=1 %to 8;xw&k=wxn*x&k ;%end;

data d54&i ; set d52&i(keep=xw1-xw8) d53 ;

data d62&i; merge d61 d11&i(keep=wyn) ;
%do k=1 %to 8;yw&k=wyn*y&k ;%end;

data d64&i ; set d63 d62&i(keep=yw1-yw8) ;

data d7&i; merge d54&i d64&i ;

data tot&i ; merge d4&i(keep=rep) d7&i(keep=xw1-xw8 yw1-yw8);

proc NLIN data=tot&i outest=coef noitprint;

parms a1= 7
a2= 7
a3= 8
a4= 8
a5= 9
a6= 9
a7= 10
a8= 15
b= 16
c = -1;

model rep=a1*xw1+a2*xw2+a3*xw3+a4*xw4+a5*xw5+a6*xw6+a7*xw7+a8*xw8
+ (b+c*a1)*yw1 +(b+c*a2)*yw2 +(b+c*a3)*yw3 + (b+c*a4)*yw4
+ (b+c*a5)*yw5 +(b+c*a6)*yw6 +(b+c*a7)*yw7 + (b+c*a8)*yw8 ;
```sas
der.a1=xw1+c*yw1;
der.a2=xw2+c*yw2;
der.a3=xw3+c*yw3;
der.a4=xw4+c*yw4;
der.a5=xw5+c*yw5;
der.a6=xw6+c*yw6;
der.a7=xw7+c*yw7;
der.a8=xw8+c*yw8;
der.b =yw1+yw2+yw3+yw4+yw5+yw6+yw7+yw8;
der.c =a1*yw1+a2*yw2+a3*yw3+a4*yw4+a5*yw5+a6*yw6+a7*yw7+a8*yw8;

data rwnls1&i; set coef(keep=c); if _n_ > 1 then delete;
c=-c ;rename c=mu;
data rwnls2&i; set coef(keep=c); if _n_ ^=11 then delete;
c=sqrt(c);rename c=ecmu;
data rwnls4&i; merge rwnls1&i(keep=mu) rwnls2&i(keep=ecmu) quantile;
mulow=mu-tstud*ecmu; muup=mu+tstud*ecmu; vmu=ecmu*ecmu; cvmu=100*(ecmu/mu);
data rwnls5; merge rwnls4&i(keep=mulow) rwnls4&i(keep=mu) rwnls4&i(keep=muup)
rwnls4&i(keep=ecmu) rwnls4&i(keep=vmu) rwnls4&i(keep=cvmu);
proc append base=rwnls0 data=rwnls5;

%end;

data rwnls6; set rwnls0; if _n_ =1 then delete;
proc print data=rwnls6;

%mend;

%WNLS(f1=1,f2=6);

run;

/*****************************************************************/;
```

```sas
/*****************************************************************/;
%macro IRWNLS(f1=1,f2=1,k1=1,k2=1);

data rils0;mulow=0; mu=0 ;muup=0 ;ecmu=0; vmu=0; cvmu=0;

%do j=&f1 %to &f2 ;

data donx&j ;set final&j(keep=x0 poids);
rename x0=xobs; rename poids=wx;

data d1&j;merge donx&j dony;

data transit; set d1&j;

%do i=&k1 %to &k2;

data d11&j&i; set transit(keep=wx wy);
wxn=sqrt(wx) ; wyn=sqrt(wy) ;

data d2&j&i ; merge transit(keep=xobs yobs) d11&j&i(keep=wxn wyn) ;
xw=xobs*wxn ; yw=yobs*wyn ;

data d31&j&i ; set d2&j&i(keep=xw) ; rename xw=rep ;
data d32&j&i ; set d2&j&i(keep=yw) ; rename yw=rep ;
```
data d4&j&i ; set d31&j&i d32&j&i ;

data d52&j&i; merge d51 d11&j&i(keep=wxn) ;
%do k=1 %to 8;xw&k=wxn*x&k ;%end;

data d54&j&i ; set d52&j&i(keep=xw1-xw8) d53 ;

data d62&j&i; merge d61 d11&j&i(keep=wyn) ;
%do k=1 %to 8;yw&k=wyn*y&k ;%end;

data d64&j&i ; set d63 d62&j&i(keep=yw1-yw8) ;

data d7&j&i; merge d54&j&i d64&j&i ;

data tot&j&i ; merge d4&j&i(keep=rep) d7&j&i(keep=xw1-xw8 yw1-yw8);

proc NLIN data=tot&j&i outest=coef noprint noitprint;

parms a1= 7
a2= 7
a3= 8
a4= 8
a5= 9
a6= 9
a7= 10
a8= 15
b = 16
c = -1;

model rep=a1*xw1+a2*xw2+a3*xw3+a4*xw4+a5*xw5+a6*xw6+a7*xw7+a8*xw8
+ (b+c*a1)*yw1 +(b+c*a2)*yw2 +(b+c*a3)*yw3 + (b+c*a4)*yw4
+ (b+c*a5)*yw5 +(b+c*a6)*yw6 +(b+c*a7)*yw7 + (b+c*a8)*yw8 ;

der.a1=xw1+c*yw1 ;
der.a2=xw2+c*yw2 ;
der.a3=xw3+c*yw3 ;
der.a4=xw4+c*yw4 ;
der.a5=xw5+c*yw5 ;
der.a6=xw6+c*yw6 ;
der.a7=xw7+c*yw7 ;
der.a8=xw8+c*yw8 ;
der.b =yw1+yw2+yw3+yw4+yw5+yw6+yw7+yw8 ;
der.c =a1*yw1+a2*yw2+a3*yw3+a4*yw4+a5*yw5+a6*yw6+a7*yw7+a8*yw8 ;

output out=rul1&j&i student=resstud ;

data rul2&j&i ; set rul1&j&i(keep=resstud);
poids=2/(1+resstud**2);
data rulx&j&i; set rul2&j&i ; if _n_ > 8 then delete ; rename poids=wx;
data ruly&j&i; set rul2&j&i ; if _n_ < 9 then delete ; rename poids=wy;

data transit ;
merge d1&j(keep=xobs yobs) rulx&j&i(keep=wx) ruly&j&i(keep=wy);
data rils1&j&i; set coef(keep=c); if _n_ > 1 then delete ;
c=-c ; rename c=mu;
data rils2&j&i; set coef(keep=c); if _n_ ^=11 then delete ;
c=sqrt(c); rename c=ecmu;
data rils4&j&i; merge rils1&j&i(keep=mu) rils2&j&i(keep=ecmu) quantile;
mulow=mu-tstud*ecmu ; muup=mu+tstud*ecmu ; vmu=ecmu*ecmu; cvmu=100*(ecmu/mu);
data rils5; merge rils4&j&i(keep=mulow) rils4&j&i(keep=mu)
rils4&j&i(keep=muup) rils4&j&i(keep=ecmu) rils4&j&i(keep=vmu)

rils4&j&i(keep=cvmu);

%end;

proc append base=rils0 data=rils5;

%end;

data rils6; set rils0; if _n_ =1 then delete ;

proc print data=rils6;

%mend;

%IRWNLS(f1=1,f2=6,k1=1,k2=20);

run;

/******************************************************************/;

quit; run;

/******************************************************************/;