Method and system for testing the dynamic interaction of coring fluid with earth material

A material sample representative of a subsurface formation is tested for its dynamic interaction with a coring fluid. The material sample is subjected to a pressurized and agitating coring fluid to simulate a coring operation. Thereafter the material sample is x-ray scanned to identify the extent of coring fluid invasion during the dynamic interaction of the material sample and the coring fluid.

BACKGROUND OF THE INVENTION 
This invention relates to the determination of certain lithological 
characteristics of a subsurface formation and more particularly to a 
method and system for testing a material sample representing the 
subsurface formation for its dynamic interaction characteristics with a 
coring fluid which might be utilized during a borehole operation for 
obtaining a core sample of such subsurface formation. 
In the production of minerals, specifically oil and gas, it is common to 
"engineer" the producing reservoir to improve the economic performance 
thereof. To do this, certain lithological properties of the reservoir must 
be determined, the two most important of these properties being the 
permeability and the porosity of the reservoir rock. Permeability is a 
measure of the ability of a material to transmit fluids through pore 
spaces of the mineral and is inversely proportional to the flow resistance 
offered by the material. Porosity of a material is defined as the ratio of 
the aggregate volume of its void or pore spaces to its gross bulk volume. 
In the case of an oil reservoir, porosity is a measure of the volume 
within the reservoir rock which is available for storing oil and gas. 
Normally, porosity and permeability, as well as other chemical or physical 
characteristics of an earth material, are determined from core samples by 
applying well-defined measurement procedures. 
Coring samples are ordinally taken by means of a core drill and the samples 
obtained are in the form of cylinders or cores. Drilling muds with a water 
or oil base are commonly used as coring fluids. These drilling muds are 
normally formulated to provide desired density and rheological properties 
which make them particularly suitable for use in coring wells. For 
example, drilling muds may be altered to increase the density by adding 
solid materials, such as barium sulfate, thereto. During the coring of a 
subsurface formation, contamination of a core sample by the drilling mud 
can readily occur. The core material, being porous, will be penetrated by 
the drilling mud filtrate under the pressure conditions present in the 
well. Depending on the size of the pore throats in the core material, mud 
solids (barite, clay minerals and rock cuttings) may also penetrate the 
core material. The extent of mud solids contamination of core samples must 
be taken into account when analyzing such core samples to identify certain 
subsurface formation lithological characteristics, such as porosity and 
permeability as examples. 
In view of the foregoing, it is an object of the present invention to 
simulate, or model, the dynamic interaction of coring fluid on a material 
sample representative of a select subsurface formation, both consolidated 
and unconsolidated, so as to provide a measure of the extent to which a 
coring fluid will invade a core sample from the select formation during a 
conventional coring operation. This and other objects of the present 
invention will become apparent from the following detailed description 
thereof. 
SUMMARY OF THE INVENTION 
The present invention is directed to a method and system for testing the 
dynamic interaction of a material sample representative of a subsurface 
formation and a coring fluid. The material sample is placed in a holder 
having an open upper end and a closed lower end with a fluid drain, such 
holder being comprised of a material permitting transmission of x-rays. 
The upper surface of the material sample is exposed directly to a coring 
fluid. A dynamic interaction is effected between the material sample and 
the coring fluid by pressurizing and agitating the coring fluid while in 
direct contact with the upper surface of the material sample. Coring fluid 
filtrate resulting from such a dynamic interaction is removed from the 
material sample by way of drainage through the fluid drain in the lower 
end of the holder. The material sample is thereafter scanned with x-rays 
through the holder. Computed tomographic images produced by the x-ray 
scanning provide a measure of the extent of the coring fluid invasion of 
the material sample from the density contrast created in the computed 
tomographic images by the presence of coring fluid solids in the material 
sample.

DESCRIPTION OF THE PREFERRED EMBODIMENT 
Before describing the method and system of the present invention relating 
to testing for the dynamic interaction of coring fluid on earth material 
of subsurface formations, a coring system which may be used for carrying 
out a subsurface coring operation will first be described in conjunction 
with FIG. 1. 
Referring now to FIG. 1, a typical coring system of the prior art is shown 
in pictorial form obtaining a core sample 70 from a subsurface formation 
71 underlying formations 72 and 73. Drill pipe 74 extends from the surface 
rig 75 through a wellbore 76 to the subsurface formation of interest 71. 
By drilling into the formation 71 with a coring bit 77, the solid core 70 
of uncut formation enters the inner cylinder or core barrel of the coring 
bit 77. This solid core 70 is later removed from the core barrel at the 
earth's surface. For more details as to such a typical bottomhole coring 
operation reference may be had to U.S. patent application Ser. No. 
213,810, now U.S. Pat. No. 4,848,487 entitled "Method for Minimizing Mud 
Solids Invasion of Core Samples Obtained During Subsurface Coring", filed 
June 30, 1988 to Anderson, Sprunt, Wilson and Wooten, the teachings of 
which are incorporated herein by reference. 
As seen in FIG. 1, coring fluid flows out of the coring bit 77 as shown by 
the arrows 78. This coring fluid penetrates the formation just in front of 
the coring bit. In certain formations such as vuggy limestones and highly 
permeable sandstones, such coring fluid penetration can be a problem. A 
plurality of vugs 79, or pore spaces, in such formations are shown in FIG. 
1. As the drilling fluid penetrates the formation directly ahead of the 
coring bit, those vugs in the near vicinity of the coring bit are filled 
with the coring fluid as shown in the plurality of filled-in vugs 80. The 
coring fluid enters the core sample 70 before and as it is being drawn 
into the coring bit 77. Consequently the core sample is permeated with the 
coring fluid before any filter cake can form about the core sample. Mud 
solids in the coring fluid collect in the vugs 81 shown in the core sample 
70 due to dynamic filtration through the core sample. Such mud solids 
occupy pore space that in the petroleum reservoir is occupied by reservoir 
fluids and, as a foreign solid present in the sample of the reservoir 
formation, adversely affect all core analysis measurements of the samples. 
A common mud solid component in coring fluids is barite which is insoluble 
in most cleaning solutions. Barite is not easily removed from the occupied 
pore spaces of the core sample, either chemically or mechanically, by any 
of the typical cleaning methods mentioned above. 
It is therefore a specific aspect of the present invention to provide a 
method and system for testing for such unwanted invasion of whole mud 
solids into core samples of subsurface materials during coring operations. 
In accordance with this aspect of the invention, a material sample that is 
representative of a consolidated or unconsolidated subsurface formation is 
selected for testing as to its dynamic interaction characteristic with 
coring fluid, such testing being carried out by the use of the system 
shown in FIG. 2. 
Referring now to FIG. 2, a generally cylindrical hollow material sample 
holder 10 is open at an upper end 15 and contains a fluid drain centrally 
located in a lower closed end 17. Holder 10 is filled with a material 
sample 11 representative of a select consolidated or unconsolidated 
subsurface earth material to be tested for dynamic interaction with a 
coring fluid. 
Holder 10 is comprised of a generally cylindrical hollow fixture 12 
inserted within a generally cylindrical hollow adapter 13. Fixture 12 
contains a circumferential flange 14 about open upper end 15 and a fluid 
drain 16 in closed lower end 17. Adapter 13 contains a truncated fluid 
passageway 18 centrally located in a closed end 19. Passageway 18 is in 
fluid communication with drain 16 of fixture 12. Flange 14 of fixture 12 
is bored at 23 to receive a fastener 20 which extends through flange 14 
and threadably engages the upper end 21 of adapter 13. 
Adapter 13 includes a recess 24 along a portion of its lower end 19 which 
is covered by a bottom plate 25 to form a fluid channel 26 leading 
radially outwardly from the truncated fluid passagway 18. Adapter 13 
further includes a hole 27 bored through a portion of its upper surface 
which is also connected to fluid channel 26 covered by the bottom plate 25 
to form a fluid channel 29 leading upwardly along the length of adapter 13 
from the fluid channel 26. The open end of fluid channel 29 at the upper 
end 30 of adapter 13 is fitted with a tube member 31 which extends through 
a recess through flange 32. 
When affixed together as shown in FIG. 2, the fixture 12 and adapter 13 
with its base plate 25 comprise the generally cylindrical material sample 
holder 10. The outside diameter of holder 10 permits its slidable 
insertion into a generally cylindrical hollow test cell 34. Test cell 34 
is closed at a lower end 35 and is sealed at an upper open end 36 by a 
cover 37. With the holder 10 inserted into the lower portion of test cell 
34, an upper chamber 38 is formed which is filled with a select coring 
fluid. Since the upper end 15 of fixture 12 of holder 10 is open, the 
coring fluid will be in direct contact with the upper surface of material 
sample 11. 
To test the dynamic interaction of the coring fluid and the material 
sample, it is necessary to agitate the coring fluid and at the same time 
provide suitable pressure conditions within the chamber 38 so that the 
coring fluid interaction with the material sample will simulate, or model, 
the dynamic interaction that such a coring fluid and material sample would 
experience in a subsurface coring operation. Accordingly, the coring fluid 
is pressurized from a suitable gas pressure supply by means of a 
passageway 40 through cover 37. Agitation to the coring fluid is supplied 
by any suitable mixer 41 suspended within the coring fluid and driven by a 
mechanical drive 42 through cover 37. In the alternative, the coring fluid 
could be agitated by continuously circulating the coring fluid or even by 
shaking the test cell 34 as examples. 
As the dynamic interaction takes place between the coring fluid and 
material sample, coring fluid invades material sample. Coring fluid solids 
remain in the pore spaces of the material sample while coring fluid 
filtrate passes from the lower end of the material sample through the 
drain 16, the truncated passageway 18, the channels 26 and 29 and up the 
tube 31 through a passageway in the cover 37 to a filtrate collection unit 
(not shown). 
Upon termination of the dynamic interaction testing of the coring fluid and 
material sample, the holder 10 is removed from the test cell 34 and the 
material sample x-ray scanned to identify the extent of coring fluid 
invasion of the material sample from a density contrast created in 
computed tomographic images produced from such x-ray scanning. It is a 
specific feature of the present invention to subject the material sample 
to x-rays without disturbing the material sample by its being removed from 
the holder 10. This is carried out by providing a fixture 12 which 
comprises a material that allows for the transmission of x-rays, such as 
aluminum, acrylic or teflon as examples. Fixture 12 is removed from 
adapter 13 by disengaging fastener 20 and then placed in the computer 
tomography (CT) scanning system of FIG. 3. 
Referring to FIG. 3, X-ray energy provided by the x-ray tube 50 passes 
through the material sample 11 and fixture 12 (not shown) and falls on the 
detector array 51. Rotation of fixture 11 within the x-ray fan beam 52 is 
provided by suitable gantry means (not shown). In an alternative 
embodiment, the material sample 11 may remain stationary and the gantry 
may be used to rotate the x-ray tube 50 and detector 51 about the material 
sample. In medical applications, CT scanning rates are usually in the 
order of 2 to 9 seconds. However, patient dose limitations are of no 
concern in the present application, and scan times of the core sample can 
be up to 30 seconds per scan. The output of the detector 51 is passed 
through the data processing unit 55 to the display unit 56. After a 
desired number of translations are completed for a core sample slice, the 
sample is indexed one slice-width through the x-ray fan beam to place the 
next adjacent sample slice within the path of the x-ray fan beam. In this 
manner, a 3-D tomographic presentation is made of the entire sample by 
compositing the cross-sectional view of each of the scan slices. Such a CT 
scanning system, while not forming a part of the present invention, is 
used in accordance with the method of the present invention to quantify 
the coring fluid solid content in the material sample and thereby identify 
the extent of coring fluid invasion of the material sample having taken 
place during the dynamic interaction testing of the coring fluid and the 
material sample. For more details as to such a CT scanning system, 
reference may be made to U.S. Pat. Nos. 4,649,483 to Dixon; 4,688,238 to 
Sprunt et al.; 4,722,095 to Muegge et al. and 4,782,501 to Dixon, the 
teachings of which are incorporated herein by reference. 
Having now described a preferred embodiment of the present invention, it is 
to be understood that various modifications and changes may be made 
thereto without departing from the spirit and scope of the invention as 
set forth in the appended claims.