The optically clear compositions comprising PA1 (A) an organopolysiloxane which contains at least one monovalent SiC-bonded radical with primary, secondary and/or tertiary amino groups, PA1 (B) 0.01 to 1 part by weight per 100 parts by weight of organopolysiloxane (A) of a group of compounds consisting of water, methanol and ethanol and PA1 (C) 0.05 to 20 parts by weight of a solubilizing agent per 100 parts by weight of organopolysiloxane (A), chosen from a group consisting of PA2 (C1) C.sub.1 - to C.sub.19 -carboxylic acid C.sub.1 - to C.sub.12 -alkyl esters and -glycol esters, PA2 (C2) C.sub.3 - to C.sub.20 -alkanols and C.sub.3 - to C.sub.20 -alkanol-C.sub.1 - to C.sub.12 -alkoxylates and PA2 (C3) organosilicon compounds containing glycoside radicals.

FIELD OF INVENTION 
The present invention relates to optically clear compositions based on an 
organopolysiloxane containing aminoalkyl groups, water, an alkanol and a 
solubilizing agent and the preparation thereof. 
BACKGROUND OF INVENTION 
Organopolysiloxanes containing aminoalkyl groups are employed as textile 
treatment agents, in the cosmetics industry and as release agents. 
GB-A-20 36 052 describes organopolysiloxanes containing aminoalkyl groups 
which are formed when a polydimethylsiloxane containing terminal silanol 
groups and an alkoxysilane containing aminoalkyl groups are mixed at room 
temperature. However, the organopolysiloxane containing aminoalkyl groups 
prepared in this manner is cloudy since the alkanol formed as a 
condensation product and, optionally, water have limited solubility in the 
organopolysiloxane. On storage, further alkanol and water are formed 
during condensation reactions which proceed slowly, the siloxane chains 
are lengthened and an alkanol/water phase finally separates out. Accurate 
metering of the organopolysiloxane containing aminoalkyl groups is 
possible only after separation of the phases or emulsification thereof. 
The separating out of alkanol and water can be avoided if the mixture is 
heated during preparation, in order to complete the reaction and at the 
same time drive off the alkanol and water. The removal in vacuo of the 
methanol formed in the reaction of silanols with methoxysilane containing 
aminoalkyl groups is described in G. Helary and G. Sauvet, Eur. Polym, J. 
Volume 28, No. 1 pages 37 to 41, 1991. 
SUMMARY OF INVENTION 
The present invention is based on providing compositions with the least 
possible expenditure, compositions which are based on organopolysiloxane 
containing aminoalkyl groups wherein cloudiness does not occur during 
storage and the organopolysiloxane containing aminoalkyl groups can easily 
be metered. 
The present invention relates to optically clear compositions comprising: 
(A) an organopolysiloxane which contains at least one monovalent SiC-bonded 
radical with primary, secondary and/or tertiary amino groups, 
(B) 0.01 to 1 part by weight per 100 parts by weight of organopolysiloxane 
(A) of a group of compounds consisting of water, methanol and ethanol and 
(C) 0.05 to 20 parts by weight of a solubilizing agent per 100 parts by 
weight of organopolysiloxane (A), chosen from a group consisting of 
(C1) C.sub.1 - to C.sub.19 -carboxylic acid C.sub.1 - to C.sub.12 -alkyl 
esters and -glycol esters, 
(C2) C.sub.3 - to C.sub.20 -alkanols and C.sub.3 - to C.sub.20 
-alkanol-C.sub.1 - to C.sub.12 -alkoxylates and 
(C3) organosilicon compounds containing glycoside radicals. 
For most applications, the optically clear composition is processed as an 
aqueous emulsion. The solubilizing agents do not have a troublesome effect 
during the emulsification and fulfills the function of an emulsifier or an 
emulsifying auxiliary. A single compound can be employed as the 
solubilizing agent, and mixtures of different solubilizing agents can also 
be employed. 
In general no more than 0.5 part by weight per 100 parts by weight of 
organopolysiloxane (A) of compounds (B) which are chosen from water, 
methanol and ethanol are present in the optically clear compositions. 
Preferably, the organopolysiloxane (A) in the composition contains at least 
one siloxane unit of the formula 
EQU R.sup.1.sub.a Q.sub.b SiO.sub.(4-a-b)/2 (I) 
and all other siloxane units have the formula 
EQU R.sup.1.sub.c SiO.sub.(4-c)/2 (II) 
in which 
R.sup.1 is identical or different monovalent optionally fluorine-, 
chlorine- or bromine-substituted C.sub.1 - to C.sub.18 -hydrocarbon 
radicals, hydrogen atoms, C.sub.1 - to C.sub.12 - alkoxy or hydroxyl 
radicals or alkylglycol radicals, 
Q is a group of the formula 
EQU --R.sup.2 --[NR.sup.3 (CH.sub.2).sub.m ].sub.d N(R.sup.3).sub.2 (III) 
in which 
R.sup.2 is a divalent C.sub.1 - to C.sub.18 -hydrocarbon radical, 
R.sup.3 is a hydrogen atom or an optionally fluorine-, chlorine- or 
bromine- or C.sub.1 - to C.sub.5 -alkoxy-substituted C.sub.1 - to C.sub.18 
-hydrocarbon radical, 
a has the values 0, 1, or 2, 
b has the values 1, 2 or 3, 
c has the values 0, 1, 2 or 3, 
d has the values 0, 1, 2, 3 or 4 and 
m has the values 2, 3, 4, 5 or 6 
and the sum of a+b is not more than 4. 
The C.sub.3 - to C.sub.12 -alkoxy radicals R.sup.1 are of such low 
reactivity that the C.sub.3 - to C.sub.12 -alkanols formed therefrom by 
condensation with silanol groups or hydrolysis with water can be obtained 
only in a very small mount. Furthermore, these alkanols dissolve readily 
in the organopolysiloxane (A) and are themselves solubilizing agents (C1). 
Examples of C.sub.1 - to C.sub.18 -hydrocarbon radicals are alkyl radicals, 
such as the methyl, ethyl, n-propyl, iso-propyl, n-butyl, iso-butyl, 
tert-butyl, n-pentyl, iso-pentyl, neo-pentyl and tert-pentyl radical; 
hexyl radicals, such as the n-hexyl radical; heptyl radicals, such as the 
n-heptyl radical; octyl radicals, such as the n-octyl radical and the 
isooctyl radicals, such as the 2,2,4-trimethylpentyl radical; nonyl 
radicals, such as the n-nonyl radical; decyl radicals, such as the n-decyl 
radical; dodecyl radicals, such as n-dodecyl radical; cycloalkyl radicals, 
such as cyclopentyl, cyclohexyl and cycloheptyl radicals and 
methylcyclohexyl radicals; aryl radicals, such as the phenyl and the 
naphthyl radicals; alkaryl radicals, such as o-, m- and p-tolyl radicals, 
xylyl radicals and ethylphenyl radicals; and aralkyl radicals, such as the 
benzyl radical and the .alpha.- and the .beta.-phenylethyl radical. 
The above hydrocarbon radicals R.sup.1 optionally contain an aliphatic 
double bond. Examples are alkenyl radicals, such as the vinyl, allyl, 
5-hexen-1-yl, E-4-hexen-1-yl, Z-4-hexen-1-yl, 2-(3-cyclohexenyl)-ethyl and 
cyclododeca-4,8-dienyl radical. Preferred radicals R.sup.1 with an 
aliphatic double bond are the vinyl, allyl and 5-hexen-1-yl radical. 
Preferably, not more than 1% of the hydrocarbon radicals R.sup.1 contain a 
double bond. 
Examples of C.sub.1 - to C.sub.18 -hydrocarbon radicals which are 
substituted by fluorine, chlorine or bromine atoms are the 
3,3,3-trifluoro-n-propyl radical, the 2,2,2,2',2',2'-hexafluoroisopropyl 
radical, the heptafluoroisopropyl radical and the o-, m- and 
p-chlorophenyl radical. 
Examples of the divalent C.sub.1 to C.sub.18 -hydrocarbon radicals R.sup.2 
are saturated straight- or branched-chain or cyclic alkylene radicals, 
such as the methylene and ethylene radical, as well as propylene, 
butylene, pentylene, hexylene, 2-methylpropylene, cyclohexylene and 
octadecylene radicals or unsaturated alkylene or arylene radicals, such as 
the hexenylene radical and phenylene radicals, the n-propylene radical and 
the 2-methylpropylene radical being more preferred. 
The alkoxy radicals are the alkyl radicals described above bonded via an 
oxygen atom. The examples of alkyl radicals also apply in their full scope 
to the alkoxy radical R.sup.1. 
The alkylglycol radicals R.sup.1 preferably have the formula 
EQU --R.sup.2 --[O(CHR.sup.3).sub.d ].sub.n OR.sup.4 (IV) 
in which 
R.sup.2, R.sup.3 and d have the above meanings, 
n is from 1 to 100 and 
R.sup.4 is a hydrogen atom, a radical R.sup.3 or a group of the formula 
##STR1## 
in which R.sup.5 is the radical R.sup.3 or O--R.sup.3. 
Preferably, in the above formulae (I) to (IV), 
R.sup.1 is a methyl, phenyl, C.sub.1 - to C.sub.3 -alkoxy or hydroxyl 
radical or a radical of the formula (IV), 
R.sup.2 is a divalent C.sub.2 - to C.sub.6 -hydrocarbon radical, 
R.sup.3 is a hydrogen atom or a methyl radical, 
a has the values 0 or 1, 
b has the value 1, 
c has the values 2 or 3 and 
d has the value 1. 
Linear polydimethylsiloxanes which optionally contain C.sub.1 - to C.sub.3 
-alkoxy or hydroxyl end groups are more preferred. In these 
polymethylsiloxanes, Q is preferably an H.sub.2 N(CH.sub.2).sub.2 
NH(CH.sub.2).sub.3 - or H.sub.2 N(CH.sub.2).sub.2 NHCH.sub.2 
CH(CH.sub.3)CH.sub.2 - group. 
The ratio of siloxane units of formula (I) to siloxane units of formula 
(II) is preferably 1:10 to 30,000, in particular 1:20 to 300. The amine 
contents are preferably 0.01 to 2 mequivalents/g, in particular 0.1 to 0.7 
mequivalents/g, measured as the consumption of 1N hydrochloric acid in 
ml/g of organopolysiloxane (A) during titration to the neutral point. 
One type of organopolysiloxane (A) can be employed. However, it is also 
possible to employ a mixture of at least two different types of 
organopolysiloxane (A). 
The organopolysiloxane (A) or a mixture of at least two different types of 
organopolysiloxane (A) preferably has an average viscosity of 20 to 
100,000 mPa.s, in particular 20 to 10,000 mPa.s, at 25.degree. C. 
The composition preferably comprises 0.1 to 10 parts by weight, in 
particular 0.5 to 3 parts by weight, of solubilizing agent (C) per 100 
parts by weight of organopolysiloxane (A). 
The organopolysiloxanes are prepared from 
(E) compounds which are chosen from 
(E1) organosilanes which contain at least one monovalent SiC-bonded radical 
with primary, secondary and/or tertiary amino groups and at least one 
C.sub.1 - to C.sub.4 -alkoxy group and 
(E2) organopolysiloxanes which contain at least one monovalent SiC-bonded 
radical with primary, secondary and/or tertiary amino groups and at least 
one C.sub.1 - to C.sub.4 -alkoxy and/or silanol group and 
(F) compounds which are chosen from 
(F1) organosilanes which contain at least one C.sub.1 - to C.sub.4 -alkoxy 
group and 
(F2) organopolysiloxanes which contain at least one C.sub.1 - to C.sub.4 
-alkoxy group and/or silanol group. 
The organosilanes (E1) preferably have the formula 
EQU Q.sub.e R.sup.6.sub.f SiR.sup.1.sub.(4-e-f) (V) 
in which 
R.sup.6 is a C.sub.1 - to C.sub.2 -alkoxy radical, 
e has the values 1, 2 or 3, preferably 1, 
f has the values 1, 2 or 3 and with the proviso that the sum of e+f is not 
more than 4, and Q and R.sup.1 have the above meanings. 
Preferably, the organopolysiloxane (E2) contains at least one siloxane unit 
of above formula (I) and at least one siloxane unit of the formula 
EQU R.sup.1.sub.g R.sup.6.sub.h HO.sub.i SiO.sub.(4-g-h)/2 (VI) 
and all other siloxane units have the above formula (II), wherein 
g has the values 0, 1 or 2, 
h has the values 1, 2 or 3 and 
i has the values 0 or 1, with the proviso that the sum of g, h and i is not 
more than 3, and Q, R.sup.1 and R.sup.6 have the above meanings. 
The organosilanes (F1) preferably have the formula 
EQU R.sup.6.sub.j SiR.sup.1.sub.(4-j) (VII) 
in which 
j has the values 1, 2, 3 or 4 and 
R.sup.1 and R.sup.6 have the above meanings. 
Preferably, the organopolysiloxanes (F2) contain at least one siloxane unit 
of above formula (VI) and all other siloxane units have the above formula 
(II). 
The organopolysiloxanes (E2) and (F2) preferably have an average viscosity 
of 10 to 100,000 mPa.s, preferably 20 to 10,000 mPa.s, in particular 50 to 
1000 mPa.s, at 25.degree. C. 
The organopolysiloxanes (A) are preferably prepared at 0.degree. C. to 
50.degree. C., in particular at 10.degree. C. to 30.degree. C. 
The reaction time in which 99 mole % of the starting compound (E) and (F) 
have reacted to give organopolysiloxanes (A) is usually 1 hour to 20 days, 
in particular 12 hours to 3 days. 
Preferably, 0.1 to 10 parts by weight, in particular 0.5 to 3 parts by 
weight, of solubilizing agent (C) are added per 100 parts by weight of 
starting compounds (E) and (F). 
The optically clear compositions are preferably prepared by reacting the 
starting compounds (E) and (F) in the presence of 
(C) 0.01 to 20 parts by weight of the solubilizing agent described above 
per 100 parts by weight of starting compounds (E) and (F). 
In this embodiment, the starting compounds (E) and (F) can be mixed with 
the solubilizing agent (C) and the optically clear compositions then form 
during storage and transportation. It is possible for the reaction mixture 
of the starting compounds (E) and (F) with the solubilizing agent (C) to 
be introduced directly into vessels, such as canisters, drums or tanks. 
After the required reaction time at the required reaction temperature, the 
optically clear compositions which have formed can be further processed. 
The required reaction time can be met on the transportation route or 
during warehousing. 
Thereafter, the starting compounds (E) and (F) can be present in small 
amounts in the optically clear compositions. As long as the reaction of 
the starting compounds (E) and (F) has not yet been concluded completely, 
alkanols having 1 to 4 carbon atoms and/or water are still formed. 
One water molecule is formed in the condensation reaction between two 
silanol groups. One alkanol molecule is formed in the condensation 
reaction between one silanol group and one alkoxy group. In the 
condensation reaction between two alkoxy groups, one water molecule is 
required and two alkanol molecules are formed. 
If the compounds (E) and (F) employed contain more alkoxy groups than 
silanol groups, water must be added. The amounts of water required are so 
low that, because of the solubilizing agent (C) employed, they are 
homogeneously miscible with the compounds (E) and (F). A maximum of 0.3, 
in particular 0.1, part by weight per 100 parts by weight of compounds (E) 
and (F) is sufficient. 
The organopolysiloxanes (E2) and F2) preferably contain silanol groups, 
since the reaction between silanol groups and alkoxy groups proceeds 
rapidly. 
The optically clear compositions can also be prepared by mixing 
(A) an organopolysiloxane which contains at least one monovalent SiC-bonded 
radical with primary, secondary and/or tertiary amino groups, and 
(B) 0.01 to 1 part by weight per 100 parts by weight of organopolysiloxane 
(A), comprising an alkanol having 1 to 4 carbon atoms and, optionally, 
water, with 
(C) 0.05 to 5 parts by weight of the solubilizing agent described above per 
100 parts by weight of organopolysiloxane (A). 
The cloudy mixtures of components (A) and (B) become clear again by this 
procedure. 
The C.sub.1 - to C.sub.19 -carboxylic acid C.sub.1 - to C.sub.12 -alkyl 
esters and -glycol esters (C1) employed as the solubilizing agent (C) 
preferably have the formula 
##STR2## 
in which R.sup.7 is a C.sub.1 - to C.sub.18 -alkyl radical, 
R.sup.8 is a hydrogen atom or a C.sub.1 - to C.sub.6 -alkyl radical, 
k has the values 1, 2 or 3 and 
l has the values 0 or 1 to 20. 
R.sup.7 is preferably straight-chain and has 1 to 19 carbon atoms. R.sup.8 
is preferably a straight-chain alkyl radical and has 1 to 6 carbon atoms. 
k preferably has the value 2. The value of 1 is preferably 0 or 1 to 5. 
The C.sub.3 - to C.sub.20 -alkanols and C.sub.3 - to C.sub.20 
-alkanol-C.sub.1 - to C.sub.12 -alkoxylates (C2) preferably have the 
formula 
EQU R.sup.7 --CH.sub.2 CH.sub.2 --[O(CH.sub.2).sub.k ].sub.u OH (IX) 
u has the values 0 or 1 to 20 and 
k and R.sup.7 have the above meanings. 
R.sup.7 preferably has 4 to 14 carbon atoms. 
The organosilicon compounds (C3) containing glycoside radicals are 
preferably built up from units of the formula 
##STR3## 
in which v has the values 0, 1, 2 or 3, 
o has the values 0, 1, 2 or 3 and 
R.sup.9 is a radical of the formula 
EQU Z--[(CH.sub.2).sub.k O].sub.u --R.sup.2 -- (XI) 
wherein 
Z is a glycoside radical which is built up from 1 to 10, preferably 1 to 4, 
in particular 1 or 2, monosaccharide units and 
R.sup.1, R.sup.2, k and u have the above meanings, with the proviso that 
the sum of v and o is less than or equal to 3, and the organosilicon 
compound of units of formula (X) contains at least one radical R.sup.9 per 
molecule. 
Examples of monosaccharides from which the glycoside radicals Z can be 
built up are hexoses and pentoses, such as glucose, fructose, galactose, 
mannose, talose, allose, altrose, idose, arabinose, xylose, lyxose and 
ribose, glucose being more preferred. 
Examples of alkylene radicals are methylene, ethylene, propylene, butylene, 
pentylene, hexylene, heptylene, octylene, nonylene, decylene and 
octadecylene radicals. 
The radical R.sup.2 is preferably linear alkylene radicals having 2 to 20 
carbon atoms, more preferably linear alkylene radicals having 2 to 8 
carbon atoms, in particular the n-propylene radical. 
Examples of radicals R.sup.9 are G--CH.sub.2 CH.sub.2 CH.sub.2 --, 
G--(CH.sub.2 CH.sub.2 O)--CH.sub.2 CH.sub.2 CH.sub.2 --, G--(CH.sub.2 
CH.sub.2 O).sub.2 --CH.sub.2 CH.sub.2 CH.sub.2 --, 
##STR4## 
in which G is a glucoside radical (C.sub.6 H.sub.11 O.sub.6 --), 
##STR5## 
in which G.sub.2 is a glycoside radical built up from two glucose units. 
The radical R.sup.9 is preferably G--CH.sub.2 CH.sub.2 CH.sub.2 --, 
G--(CH.sub.2 CH.sub.2 O)--CH.sub.2 CH.sub.2 CH.sub.2 --, 
G.sub.2 --CH.sub.2 CH.sub.2 --CH.sub.2 --, 
and 
G.sub.2 --(CH.sub.2 CH.sub.2 O)--CH.sub.2 CH.sub.2 CH.sub.2 --, 
where 
G--(CH.sub.2 CH.sub.2 O)--CH.sub.2 CH.sub.2 CH.sub.2 --, 
and 
G.sub.2 --(CH.sub.2 CH.sub.2 O)--CH.sub.2 CH.sub.2 CH.sub.2 --, are more 
preferred and G is a glucoside radical (C.sub.5 H.sub.11 O.sub.6 --), and 
G.sub.2 is a glucoside radical built up from two glucose units. 
The organosilicon compounds containing glycoside radicals are preferably 
those of the formula 
EQU R.sup.9.sub.q R.sup.1.sub.3-p SiO--[(SiR.sup.1 R.sup.9 O).sub.r 
--(SiR.sup.1.sub.2 O).sub.s ].sub.t --SiR.sup.1.sub.3-q R.sup.9.sub.x 
(XII) 
in which 
R.sup.1 and R.sup.9 have the above mentioned meaning, 
q is 0 or 1, 
r is 0 or a number from 1 to 200, preferably 0 or a number from 1 to 100, 
more preferably 0 or a number from 1 to 50, 
s is 0 or a number from 1 to 1000, preferably 0 or a number from 1 to 500, 
more preferably 0 or a number from 1 to 100 and 
t is 0 or a number from 1 to 1200, preferably 0 or a number from 1 to 600, 
more preferably 0 or a number from 1 to 100, 
with the proviso that the compound of formula (XII) contains at least one 
radical R.sup.9. 
If r in the organosilicon compounds containing glycoside radicals, of 
formula (XII), is on average other than 0, q is preferably 0. 
If x in the organosilicon compounds containing glycoside radicals, of 
formula (XII), is on average other than 0, r is preferably 0. 
Although not shown by formula (XII), up to 10 mole % of the 
diorganosiloxane units can be replaced by other siloxane units, such as 
R.sup.1 SiO.sub.3/2, R.sup.6 SiO.sub.3/2 and/or SiO.sub.4/2 units, in 
which R.sup.1 and R.sup.6 have the above meaning. 
The optically clear compositions can also comprise basic catalysts and 
acidic catalysts which promote the condensation and the equilibration 
reaction. Examples of basic and acidic catalysts are alkali metal 
hydroxides, in particular potassium hydroxide and cesium hydroxide, alkali 
metal alcoholates, quaternary ammonium hydroxides, such as 
tetramethylammonium hydroxide, benzyltrimethylammonium hydroxide and 
benzyltriethylammonium hydroxide, benzyltrimethylammonium butylate, 
.beta.-hydroxyethyltrimethylammonium 2-ethylhexoate, quaternary 
phosphonium hydroxides, such as tetra-n-butylphosphonium hydroxide and 
tri-n-butyl-3-[tris-(trimethylsiloxy) silyl]-n-propylphosphonium 
hydroxide, alkali metal siloxanolates and ammonium organosiloxanolates, 
such as benzyltrimethylammonium methylsiloxanolate, hydrofluoric acid, 
boron fluoride and ammonium fluorides such as cetylamine hydrofluoride. 
The basic catalysts and acidic catalysts which promote the condensation and 
the equilibration reaction can already be mixed with the compounds (E) and 
(F) during preparation of the optically clear compositions. Preferably, 
not more than 5, in particular not more than 2, parts by weight of basic 
or acidic catalysts are present per 100 parts by weight of 
organopolysiloxane (A) or compounds (E) and (F). 
The optically clear compositions can comprise additives for particular 
purposes, for example for use as textile treatment compositions, in 
addition to the above constituents. Suitable additives are biocides, such 
as fungicides, bactericides, algicides and microbicides, thickeners, 
antifreezes, antistatics, dyestuffs, flameproofing agents and organic 
plasticizers. 
In the following examples, unless stated otherwise in each case, 
a) all the amounts data are based on the weight; 
b) all the pressures are 0.10 MPa (absolute); 
c) all the temperatures are 20.degree. C.

EXAMPLE 1 
In each case 98 parts by weight of a polydimethylsiloxane oil with terminal 
hydroxyl groups and having a viscosity of 70 mPa. s at 25.degree. C. were 
mixed with 2 parts by weight of a silane of the formula 
EQU CH.sub.3 (CH.sub.3 O).sub.2 SiY (XlII) 
and the mixture was stored at 20.degree. C. After the time stated below, 
clouding occurred. 
Silane 1:Y=--(CH.sub.2).sub.3 --NH(CH.sub.2).sub.3 CH.sub.3 ; clouding 
after 17 days. 
Silane 2:Y---(CH.sub.2).sub.3 --NHCH.sub.3 ; clouding after 10 days. 
Silane 3:Y=--(CH.sub.2).sub.3 --NH--(CH.sub.2).sub.3 --OCH.sub.3 ; clouding 
after 24 days. 
Silane 4:Y=--(CH.sub.2).sub.3 --NH--(CH.sub.2).sub.2 --N(CH.sub.3).sub.2 ; 
clouding after 20 days. 
Silane 5:Y=--(CH.sub.2).sub.3 --NH(cyclohexyl); clouding after 20 days. 
Silane 6:Y=--(CH.sub.2).sub.3 --NH--(CH.sub.2).sub.2 --NH.sub.2 ; clouding 
after 21 days. 
Two days after clouding had occurred, the mixtures were mixed with 1 part 
by weight of iso-tridecyl-diethylene glycol ether. The mixtures became 
optically clear after a few minutes. 
EXAMPLE 2 
The mixtures prepared in Example 1 were mixed with 10 parts by weight of 
iso-tridecanol 2 days after clouding had occurred. The mixtures became 
optically clear after a few minutes. 
EXAMPLE 3 
The mixtures prepared in Example 1 were mixed with 10 parts by weight of 
iso-propyl palmitate 2 days after clouding had occurred. The mixtures 
became optically clear after a few minutes. 
EXAMPLE 4 
The mixtures prepared in Example 1 were mixed with 10 parts by weight of 
ethylglycol acetate 2 days after clouding had occurred. The mixtures 
became optically clear after a few minutes. 
EXAMPLE 5 
In each case 98 parts by weight of a polydimethylsiloxane oil with terminal 
hydroxyl groups and having a viscosity of 70 mPa.s at 25.degree. C. were 
mixed with 2 parts by weight of the silane 6 described in Example 1 and 
with the solubilizing agents stated in Examples 1 to 4 above, in the 
amounts stated, and the mixture was stored at 20.degree. C. for 40 days. 
The mixtures remained optically clear.