Patent ID: 7674450
Filing Date: 2010-03-09
Classification: C01G,C01P,C04B,Y10T

Abstract:
1. A process for the production of a valve metal oxide powder which comprises continuous reacting a fluoride-containing valve metal compound with a base in the presence of water at a temperature of at least 450° C. and calcination of the resultant product, wherein the fluoride-containing valve metal compound is employed as an aqueous solution at a concentration of 0.3 mol/l to 1.2 mol/l, based on the amount of valve metal, wherein the base is an aqueous ammonia solution with a concentration of 3 weight percent to 15 weight percent and the reaction is carried out continuously, wherein the volumetric flow ratios are adjusted such that the ratio of the volumetric flow rate of an aqueous solution of the fluoride-containing valve metal compound to the volumetric flow rate of the aqueous solution of the base is from 1:0.9 to 1:2, and wherein the molar concentration ratio of fluoride-containing valve metal compound, calculated as valve metal, to base is adjusted to from 1:5.6 to 1:8.5 and the, reaction is performed in a single reaction vessel.