Patent ID: 7145003
Filing Date: 2006-12-05
Classification: C07D

Abstract:
1. A process for synthesizing the compound 1,5-Dinosyl-3,3,7,7-tetrakis(difluoramino) octahydro-1,5-diazocine (DNTDFD), comprising: reacting tetrahydro-1,5-bis(4-nitrobenzenesulfonyl)-1,5-diazocine-3,7-(2H, 6H) dione with HNF2/oleum, in the presence of a diluent and absorbent for the reagent difluoramine, initially approximately between −5 and 0 degrees C.; and allowing a temperature to rise to between 10 degrees C. and ambient temperature during said reaction, to yield crude DNTDFD.