Patent ID: 8069549
Filing Date: 2011-12-06
Classification: B22F,H01L,H03H,Y10T

Abstract:
1. A method for sealing a quartz crystal device, in order to bond an upper substrate and a lower substrate with upper and lower surfaces, respectively, of an intermediate crystal plate in which a crystal resonator element and an outer frame are integrally connected to hermetically seal the crystal resonator element in a cavity defined between the upper substrate and the lower substrate, the method comprising: (a) applying a metallic thin film on each of upper and lower surfaces of the outer frame of the intermediate crystal plate, and a metallic thin film on a surface to be bonded with the outer frame of each of the upper substrate and the lower substrate; (b) applying a metal paste sealing material including an organic solvent and metallic particles to at least one of the metallic thin film on the upper surface of the outer frame and the metallic thin film of the upper substrate, and heating the metal paste sealing material to evaporate substantially all the organic solvent to form a primary sintered body having a porous structure with a Young's modulus of 9 to 16 GPa and a density of 10 to 17 g/cm wherein the metallic particles of the metal paste sealing material each have an average particle size from 0.1 to 1.0 μm, and the metal paste sealing material comprises the metallic particles in a proportion of from 88 to 93 percent by weight of the metal paste sealing material, the organic solvent in a proportion of from 5 to 15 percent by weight of the metal paste sealing material, and a resin material in a proportion of from 0.01 to 4.0 percent by weight of the metal paste sealing material, to hermetically seal the crystal resonator element; (c) applying the metal paste sealing material to at least one of the metallic thin film on the lower surface of the outer frame and the metallic thin film of the lower substrate, and heating the metal paste sealing material to evaporate substantially all the organic solvent to form a primary sintered body having a porous structure with a Young's modulus of 9 to 16 GPa and a density of 10 to 17 g/cm (d) placing the intermediate crystal plate and the upper substrate adjacent to each other while bringing one of the metallic thin films having the primary sintered bodies formed thereon into contact with the other of the metallic thin films, and applying pressure to the primary sintered bodies to densely recrystallize the metallic particles thereof to hermetically bond the intermediate crystal plate and the upper substrate in the outer frame; and (e) placing the intermediate crystal plate and the lower substrate adjacent to each other while bringing one of the metallic thin films having the primary sintered bodies formed thereon into contact with the other of the metallic thin films, and applying pressure to the primary sintered bodies to densely recrystallize the metallic particles thereof to hermetically bond the intermediate crystal plate and the lower substrate in the outer frame.