Patent ID: 7626052
Filing Date: 2009-12-01
Classification: C07B,C07C

Abstract:
1. A method for labeling synthesis, comprising: (a) Providing a UV reactor assembly comprising a high pressure reaction chamber, a UV spot light source with a light guide, wherein the light guide is used to provide photo irradiation of a reaction mixture through a window in the reaction chamber, (b) dissolving or reacting a base with alcohols or an alcohol solution in another solvent, (c) adding alkyl or aryl iodides to the solution of step (b) to give a reagent volume to be labeled, (d) introducing a [ (e) introducing at high pressure said reagent volume into the reaction chamber via the liquid inlet, (f) turning on the UV spot light source and waiting for a predetermined time while the labeling synthesis occur, and (g) collecting the [