Rich Structural Chemistry in New Alkali Metal Yttrium Tellurites: Three-Dimensional Frameworks of NaYTe4O10, KY(TeO3)2, RbY(TeO3)2, and a Novel Variant of Hexagonal Tungsten Bronze, CsYTe3O8.
Kim, Youngkwon; Lee, Dong Woo; Ok, Kang Min; Inorganic chemistry 54 (2015) 389–395; doi:10.1021/ic502724n

data_4341953
_publ_section_title
;
 Rich Structural Chemistry in New Alkali Metal Yttrium Tellurites:
 Three-Dimensional Frameworks of NaYTe4O10, KY(TeO3)2, RbY(TeO3)2, and a
 Novel Variant of Hexagonal Tungsten Bronze, CsYTe3O8.
;
_journal_issue                   1
_journal_name_full               'Inorganic chemistry'
_journal_page_first              389
_journal_page_last               395
_journal_paper_doi               10.1021/ic502724n
_journal_volume                  54
_journal_year                    2015
_chemical_formula_sum            'Na O10 Te4 Y'
_chemical_formula_weight         782.3
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_symmetry_space_group_name_Hall  '-P 4ac 2b'
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_atom_sites_solution_primary     direct
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_cell_angle_gamma                90
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_cell_length_b                   8.9337(2)
_cell_length_c                   13.4854(3)
_cell_measurement_temperature    298(2)
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_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 1
_diffrn_measured_fraction_theta_max 1
_diffrn_measurement_device_type  'Bruker SMART Breeze'
_diffrn_measurement_method       CCD
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0542
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_diffrn_reflns_limit_l_min       -17
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_diffrn_reflns_theta_min         3.021
_exptl_absorpt_coefficient_mu    16.123
_exptl_absorpt_correction_T_max  0.69
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_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details
; 
 SADABS(Blessing, 1995) 
;
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    4.828
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
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_exptl_crystal_size_max          0.042
_exptl_crystal_size_mid          0.026
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_refine_ls_restrained_S_all      1.101
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0139P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                588
_reflns_number_total             675
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            ic502724n_si_002.cif
_cod_data_source_block           NaYTe4O10
_cod_depositor_comments
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The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'EMPIRICAL' changed to
'empirical' according to
/home/saulius/struct/COD-crude-data--automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2935 2014-11-11 08:27:57Z andrius 

 Adding full bibliography for 4341953--4341956.cif.
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_cod_original_cell_volume        1076.28(5)
_cod_original_sg_symbol_H-M      'P 42/n b c'
_cod_database_code               4341953