Dramatic Structural Rearrangements in Porous Coordination Networks
Javier Martí-Rujas; Nazrul Islam; Daisuke Hashizume; Fujio Izumi; Makoto Fujita; Masaki Kawano; Journal of the American Chemical Society 133 (2011) 5853–5860; doi:10.1021/ja109160a

data_4105934
_publ_section_title
;
 Dramatic Structural Rearrangements in Porous Coordination Networks
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              5853
_journal_page_last               5860
_journal_paper_doi               10.1021/ja109160a
_journal_volume                  133
_journal_year                    2011
_chemical_formula_sum            'C18 H12 Cl4 N6 Zn2'
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_chemical_name_systematic
;
 ?
;
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_cell_length_b                   9.403(3)
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_cell_measurement_temperature    85(1)
_cell_measurement_theta_max      22.91
_cell_measurement_theta_min      2.14
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_computing_cell_refinement       'Bruker SAINT'
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_computing_molecular_graphics    'Bruker XP'
_computing_publication_material  'Bruker SHELXTL'
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_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      85(1)
_diffrn_detector_area_resol_mean 8.366
_diffrn_measured_fraction_theta_full 0.939
_diffrn_measured_fraction_theta_max 0.939
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_monochromator  'focusing mirror'
_diffrn_radiation_source         'fine-focus rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
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_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -11
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_diffrn_reflns_limit_k_min       -12
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_diffrn_reflns_theta_max         28.78
_diffrn_reflns_theta_min         1.89
_diffrn_standards_decay_%        none
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_exptl_crystal_colour            colorless
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_refine_ls_extinction_method     none
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_refine_ls_R_factor_all          0.0922
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_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0267P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_database_code               4105934