Mono- and di-cationic hydrido boron compounds.
Ghadwal, Rajendra S.; Schürmann, Christian J; Andrada, Diego M.; Frenking, Gernot; Dalton transactions (Cambridge, England : 2003) 44 (2015) 14359–14367; doi:10.1039/c5dt02237a

data_7035694
_publ_section_title
;
 Mono- and di-cationic hydrido boron compounds.
;
_journal_issue                   32
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              14359
_journal_page_last               14367
_journal_paper_doi               10.1039/c5dt02237a
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety
'2(C56 H82 B N4), 2(C2 F6 N O4 S2), 3(C6 H5 F)'
_chemical_formula_sum            'C67 H89.5 B F7.5 N5 O4 S2'
_chemical_formula_weight         1246.36
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_hydrogens   mixed
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_audit_update_record
;
2015-07-06 deposited with the CCDC.
2015-07-07 downloaded from the CCDC.
;
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'SHELXT (G.M.Sheldrick,Acta Cryst.(2015)A71,3-8)'
_diffrn_ambient_temperature      100(2)
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_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Bruker Smart APEX II Quazar'
_diffrn_measurement_method       'omega scans'
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0853P)^2^+2.8427P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7035694--7035697.cif.'
_cod_original_cell_volume        3269.0(13)
_cod_original_formula_sum        'C67 H89.50 B F7.50 N5 O4 S2'
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_shelx_res_checksum              56055