An efficient synthesis of chloro-aminocyclooctanediol and aminocyclooctanetriol: an unexpected acetolysis product
Karavaizoglu, Ufuk Nusret; Salamci, Emine; New Journal of Chemistry 44 (2020) 17976–17983; doi:10.1039/D0NJ02697B

data_7059985
_publ_section_title
;
 An efficient synthesis of chloro-aminocyclooctanediol and
 aminocyclooctanetriol: an unexpected acetolysis product
;
_journal_issue                   41
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              17976
_journal_page_last               17983
_journal_paper_doi               10.1039/D0NJ02697B
_journal_volume                  44
_journal_year                    2020
_chemical_formula_moiety         'C8 H14 Cl N3 O2'
_chemical_formula_sum            'C8 H14 Cl N3 O2'
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_symmetry_space_group_name_Hall  '-P 2ac 2ab'
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;
2020-02-29 deposited with the CCDC.	2020-09-14 downloaded from the CCDC.
;
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_computing_structure_refinement  'SHELXL-2013 (Sheldrick, 2013)'
_diffrn_ambient_temperature      296(2)
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_diffrn_measured_fraction_theta_max 1
_diffrn_measurement_device_type  'rigaku R-axis rapid S'
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_exptl_absorpt_correction_type   none
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_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0461P)^2^+2.3583P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7059985--7059986.cif.'
_cod_database_code               7059985
_shelx_estimated_absorpt_t_min   0.722
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