A New Form of Triple-Stranded Helicate Found in Uranyl Complexes of Aliphatic α,ω-Dicarboxylates.
Thuéry, Pierre; Harrowfield, Jack; Inorganic chemistry 54 (2015) 10539–10541; doi:10.1021/acs.inorgchem.5b02348

data_4344437
_publ_section_title
;
 A New Form of Triple-Stranded Helicate Found in Uranyl Complexes of
 Aliphatic \a,\w-Dicarboxylates.
;
_journal_issue                   22
_journal_name_full               'Inorganic chemistry'
_journal_page_first              10539
_journal_page_last               10541
_journal_paper_doi               10.1021/acs.inorgchem.5b02348
_journal_volume                  54
_journal_year                    2015
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'SHELXTL (Sheldrick, 2008); PLATON (Spek, 2003)'
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'two \f and four \w scans with 2\% steps (341 frames)'
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;
 Flack x determined using 2119 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack   -0.044(3)
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_refine_ls_number_reflns         5196
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0352P)^2^+8.8576P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_depositor_comments
'Adding full bibliography for 4344436--4344441.cif.'
_cod_original_cell_volume        6023.0(2)
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