Topochemical Transketalization Reaction Driven by Hydrogen Bonding
Kana M. Sureshan; Tomohiro Murakami; Tomomi Miyasou; Yutaka Watanabe; Journal of the American Chemical Society 126 (2004) 9174–9175; doi:10.1021/ja0483847

data_4112804
_publ_section_title
;
 Topochemical Transketalization Reaction Driven by Hydrogen Bonding
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              9174
_journal_page_last               9175
_journal_paper_doi               10.1021/ja0483847
_journal_volume                  126
_journal_year                    2004
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_cell_angle_beta                 100.65(1)
_cell_angle_gamma                99.14(1)
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_cell_length_c                   9.790(1)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    296.2
_cell_measurement_theta_max      29.8
_cell_measurement_theta_min      28.8
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_computing_cell_refinement       'MSC/AFC Diffractometer Control'
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_diffrn_measurement_method       w-2q
_diffrn_radiation_type           'Cu Ka'
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_diffrn_reflns_limit_h_min       0
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_diffrn_reflns_theta_max         60.04
_diffrn_standards_decay_%        18.44
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
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_exptl_absorpt_correction_T_min  0.761
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_exptl_crystal_size_mid          0.250
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_refine_diff_density_min         -0.21
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[s^2^(Fo^2^) + (0.05000(Max(Fo^2^,0) + 2Fc^2^)/3)^2^]'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     F^2^>2.0s(F^2^)
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_cod_data_source_block           master_file_afc7*.xtl
_cod_original_sg_symbol_Hall     '-P 1 '
_cod_original_sg_symbol_H-M      'P -1 '
_cod_original_formula_sum        'C12 H20 O6 '
_cod_database_code               4112804