Activation of non-polar bonds by an electron-rich gallagermylene.
Bücker, Anna; Gehlhaar, Alexander; Wölper, Christoph; Schulz, Stephan; Chemical communications (Cambridge, England) 60 (2024) 2902–2905; doi:10.1039/d3cc06223f

data_7132689
_publ_section_title
;
 Activation of non-polar bonds by an electron-rich gallagermylene.
;
_journal_issue                   21
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              2902
_journal_page_last               2905
_journal_paper_doi               10.1039/d3cc06223f
_journal_volume                  60
_journal_year                    2024
_chemical_formula_sum            'C56 H71 Cl Ga Ge N2'
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_audit_update_record
;
2023-12-21 deposited with the CCDC.	2024-02-08 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'Bruker D8 KAPPA II (APEX II detector)'
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_diffrn_reflns_av_unetI/netI     0.0482
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_diffrn_reflns_limit_h_max       17
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_exptl_crystal_colour            colourless
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_refine_ls_extinction_method     none
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_refine_ls_R_factor_all          0.0704
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0612P)^2^+0.3058P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7132689--7132690.cif.'
_cod_database_code               7132689
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_shelx_estimated_absorpt_t_min   0.724
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_shelx_res_checksum              34856
_shelx_hkl_checksum              29905