Tricationic analogues of boroxines and polyborate anions
Alessandro Del Grosso; Ewan Clark; Nicholas Montoute; Michael Ingleson; Chem.Commun. 48 (2012) 7589–; doi:10.1039/c2cc32605a

data_7108034
_publ_section_title
;
 Tricationic analogues of boroxines and polyborate anions
;
_journal_name_full               Chem.Commun.
_journal_page_first              7589
_journal_paper_doi               10.1039/c2cc32605a
_journal_volume                  48
_journal_year                    2012
_chemical_formula_moiety         'C20 H20 Al4 B3 Br10 N4 O3'
_chemical_formula_sum            'C20 H20 Al4 B3 Br10 N4 O3'
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_chemical_name_systematic
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?
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_cell_formula_units_Z            4
_cell_length_a                   10.3692(3)
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_cell_measurement_temperature    100(2)
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CrysAlis RED, Oxford Diffraction Ltd.,
Version 1.171.33.52 (release 06-11-2009 CrysAlis171 .NET)
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_computing_data_collection
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CrysAlis CCD, Oxford Diffraction Ltd.,
Version 1.171.33.52 (release 06-11-2009 CrysAlis171 .NET)
(compiled Nov 6 2009,16:24:50)
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_computing_data_reduction
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CrysAlis RED, Oxford Diffraction Ltd.,
Version 1.171.33.52 (release 06-11-2009 CrysAlis171 .NET)
(compiled Nov 6 2009,16:24:50)
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_computing_molecular_graphics    'SHELXL-97 (Sheldrick, 1997)'
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_diffrn_ambient_temperature      100(2)
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_diffrn_measurement_device_type  'Oxford Diffraction XCalibur 2'
_diffrn_measurement_method       'phi and omega'
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CrysAlisPro, Agilent Technologies,
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Empirical absorption correction using spherical harmonics,
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_exptl_crystal_colour            colorless
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_exptl_crystal_density_method    'not measured'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0453P)^2^+2.0625P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_database_code               7108034