A dinuclear copper(II) complex of deprotonated <i>N</i>,<i>N</i>'-bis(<i>N</i>-propylglycyl)ethylenediamine
Tahirov, T.; Lu, T.-H.; Shu, K.; Chunmg, C.-S.; Huang, C.-C.; Hong, Y.-S.; Acta Crystallographica Section C 50 (1994) 204–206; doi:10.1107/S010827019300722X

data_2009429
_publ_section_title
;
 A dinuclear copper(II) complex of deprotonated
 <i>N</i>,<i>N</i>'-bis(<i>N</i>-propylglycyl)ethylenediamine
;
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              204
_journal_page_last               206
_journal_paper_doi               10.1107/S010827019300722X
_journal_volume                  50
_journal_year                    1994
_chemical_formula_moiety         'C24 H47 Cu2 N8 O6 , 2Cl1 O4'
_chemical_formula_sum            'C24 H54 Cl2 Cu2 N8 O14'
_chemical_formula_weight         876.784
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.
_cell_angle_beta                 94.260(10)
_cell_angle_gamma                90.
_cell_formula_units_Z            4
_cell_length_a                   9.4540(10)
_cell_length_b                   27.610(10)
_cell_length_c                   14.762(3)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    298(3)
_cell_measurement_theta_max      19.99
_cell_measurement_theta_min      5.44
_cell_volume                     3842.6(16)
_diffrn_measurement_device       'Nonius CAD-4'
_diffrn_measurement_method       \q/2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.053
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       32
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            7012
_diffrn_reflns_theta_max         24.9
_diffrn_standards_decay_%        .0
_diffrn_standards_interval_time  60
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    1.32
_exptl_absorpt_correction_T_max  0.695
_exptl_absorpt_correction_T_min  0.692
_exptl_absorpt_correction_type   'empirical (North, Phillips & Mathews, 1968)'
_exptl_crystal_colour            blue-violet
_exptl_crystal_density_diffrn    1.516
_exptl_crystal_description       parallelepiped
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.45
_exptl_crystal_size_min          0.38
_refine_diff_density_max         0.77
_refine_diff_density_min         -0.92
_refine_ls_goodness_of_fit_obs   1.77
_refine_ls_hydrogen_treatment    refU
_refine_ls_number_parameters     525
_refine_ls_number_reflns         4465
_refine_ls_R_factor_obs          0.058
_refine_ls_shift/esd_max         0.938
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      unit
_refine_ls_wR_factor_obs         0.061
_reflns_number_observed          4465
_reflns_number_total             6740
_reflns_observed_criterion       I>=2.5\s(I)
_cod_data_source_file            as1044.cif
_cod_data_source_block           as1044_structure_1_of_1
_cod_original_cell_volume        3843(2)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2009429