Structure of Sr~3~V~10~O~28~.22H~2~O
Nieto, J. M.; Salagre, P.; Medina, F.; Sueiras, J. E.; Solans, X.; Acta Crystallographica Section C 49 (1993) 1879–1881; doi:10.1107/S0108270193003361

data_2001193
_publ_section_title
;
 Structure of Sr~3~V~10~O~28~.22H~2~O
;
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1879
_journal_page_last               1881
_journal_paper_doi               10.1107/S0108270193003361
_journal_volume                  49
_journal_year                    1993
_chemical_formula_sum            'H44 O50 Sr3 V10'
_chemical_formula_weight         1616.60
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.0
_cell_angle_beta                 109.55(2)
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   18.839(2)
_cell_length_b                   12.7190(10)
_cell_length_c                   18.743(2)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    298
_cell_measurement_theta_max      14
_cell_measurement_theta_min      8
_cell_volume                     4232.2(9)
_diffrn_measurement_device       'Philips PW-1100'
_diffrn_measurement_method       \w
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.021
_diffrn_reflns_limit_h_max       24
_diffrn_reflns_limit_h_min       -24
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            4300
_diffrn_reflns_theta_max         30
_diffrn_standards_decay_%        0
_diffrn_standards_interval_time  120
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    6.383
_exptl_absorpt_correction_T_max  0.40
_exptl_absorpt_correction_T_min  0.37
_exptl_absorpt_correction_type   DIFABS
_exptl_crystal_colour            Ochre
_exptl_crystal_density_diffrn    2.536
_exptl_crystal_description       Prism
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.1
_refine_diff_density_max         0.6
_refine_diff_density_min         -0.4
_refine_ls_number_parameters     302
_refine_ls_number_reflns         3462
_refine_ls_R_factor_obs          0.031
_refine_ls_shift/esd_max         0.1
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = [\s^2^F~o~+0.0016F~o~^2^]^-1^'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.033
_reflns_number_observed          3462
_reflns_observed_criterion       I>2.5\s(I)
_cod_data_source_file            mu1037.cif
_cod_data_source_block           mu1037_structure_1_of_1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value '[\s^2^F~o~+0.0016F~o~^2^]^-1^'
was changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to 'w =
[\s^2^F~o~+0.0016F~o~^2^]^-1^'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        4232.0(10)
_cod_database_code               2001193