Two alkali metal borates built by {Li@B<sub>14</sub>} and {B<sub>15</sub>} cluster units.
Li, Ming-Zhao; Qin, Dan; Chen, Juan; Wei, Qi; Yang, Guo-Yu; Dalton transactions (Cambridge, England : 2003) 54 (2025) 15468–15473; doi:10.1039/d5dt02076j

data_7719486
_publ_section_title
;
 Two alkali metal borates built by {Li@B<sub>14</sub>} and
 {B<sub>15</sub>} cluster units.
;
_journal_issue                   41
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              15468
_journal_page_last               15473
_journal_paper_doi               10.1039/d5dt02076j
_journal_volume                  54
_journal_year                    2025
_chemical_formula_moiety         'B15 K2 Li Na2 O25'
_chemical_formula_sum            'B15 K2 Li Na2 O25'
_chemical_formula_weight         693.27
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-C 2yc'
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_atom_sites_solution_primary     direct
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Olex2 1.5
(compiled 2025.04.05 svn.rf049d14d for OlexSys, GUI svn.r7205)
;
_audit_update_record
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2025-05-26 deposited with the CCDC.	2025-09-23 downloaded from the CCDC.
;
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_diffrn_reflns_point_group_measured_fraction_full 0.997
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0322P)^2^+2.2073P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0732
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d5dt02076j2.cif
_cod_data_source_block           1_CCDC1
_cod_depositor_comments
'Adding full bibliography for 7719485--7719486.cif.'
_cod_database_code               7719486
_shelxl_version_number           2013-4
_olex2_refinement_description
;
;
_shelx_res_checksum              28573
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_olex2_submission_special_instructions 'No special instructions were received'