Poly[[{μ~3~-tris[2-(4-phenyl-1,2,3-triazol-1-yl)ethyl]amine}silver(I)] hexafluoridophosphate]
Ohi, Hiromi; Shimizu, Mayumi; Obata, Makoto; Funabiki, Takuzo; Yano, Shigenobu; Acta Crystallographica Section E 64 (2008) m1256–m1257; doi:10.1107/S1600536808028298

data_2219505
_publ_section_title
;
 Poly[[{\m~3~-tris[2-(4-phenyl-1,2,3-triazol-1-yl)ethyl]amine}silver(I)]
 hexafluoridophosphate]
;
_journal_coeditor_code           BT2780
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1256
_journal_page_last               m1257
_journal_paper_doi               10.1107/S1600536808028298
_journal_volume                  64
_journal_year                    2008
_chemical_formula_iupac          '[Ag (C30 H30 N10)] P F6'
_chemical_formula_moiety         'C30 H30 Ag N10 +, F6 P -'
_chemical_formula_sum            'C30 H30 Ag F6 N10 P'
_chemical_formula_weight         783.47
_chemical_name_systematic
;
Poly[[{\m~3~-tris[2-(4-phenyl-1,2,3-triazol-1-yl)ethyl]amine}silver(I)]
hexafluoridophosphate]
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.0000
_cell_angle_beta                 112.646(5)
_cell_angle_gamma                90.0000
_cell_formula_units_Z            4
_cell_length_a                   14.893(3)
_cell_length_b                   14.935(3)
_cell_length_c                   15.735(3)
_cell_measurement_reflns_used    9566
_cell_measurement_temperature    193.1
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      4.0
_cell_volume                     3230.1(11)
_computing_cell_refinement       'CrystalClear (Rigaku/MSC & Rigaku, 2006)'
_computing_data_collection       'CrystalClear (Rigaku/MSC & Rigaku, 2006)'
_computing_data_reduction
'CrystalStructure (Rigaku/MSC & Rigaku, 2006)'
_computing_molecular_graphics    'ORTEP3 (Burnett & Johnson, 1996)'
_computing_publication_material
'CrystalStructure (Rigaku/MSC & Rigaku, 2006)'
_computing_structure_refinement  'CRYSTALS (Betteridge <i>et al.</i>,  2003)'
_computing_structure_solution    'SIR97 (Altomare <i>et al.</i>,  1999)'
_diffrn_detector_area_resol_mean 7.31
_diffrn_measured_fraction_theta_full 0.988
_diffrn_measured_fraction_theta_max 0.988
_diffrn_measurement_device_type  'Rigaku Mercury'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71070
_diffrn_reflns_av_R_equivalents  0.075
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            31971
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_exptl_absorpt_coefficient_mu    0.746
_exptl_absorpt_correction_T_max  0.963
_exptl_absorpt_correction_T_min  0.776
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(Jacobson, 1998)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.611
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       platelet
_exptl_crystal_F_000             1584.00
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.05
_refine_diff_density_max         3.48
_refine_diff_density_min         -2.33
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.034
_refine_ls_hydrogen_treatment    refall
_refine_ls_number_parameters     463
_refine_ls_number_reflns         7326
_refine_ls_number_restraints     0
_refine_ls_R_factor_gt           0.0537
_refine_ls_shift/su_max          0.0000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     'w = 1/[1.0000\s(Fo^2^)]/(4Fo^2^)'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.0552
_reflns_number_gt                4647
_reflns_number_total             7326
_reflns_threshold_expression     F^2^>2\s(F^2^)
_cod_data_source_file            bt2780.cif
_cod_data_source_block           I
_cod_original_cell_volume        3230.2(12)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2219505
_cod_database_fobs_code          2219505