Synthesis of quinazolinone scaffolds <i>via</i> a zinc(II)-stabilized amidyl radical-promoted deaminative approach.
Manna, Subarna; Sahoo, Sangita; Rit, Arnab; Chemical communications (Cambridge, England) 60 (2024) 7097–7100; doi:10.1039/d4cc01554a

data_7133069
_publ_section_title
;
 Synthesis of quinazolinone scaffolds <i>via</i> a zinc(II)-stabilized
 amidyl radical-promoted deaminative approach.
;
_journal_issue                   55
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              7097
_journal_page_last               7100
_journal_paper_doi               10.1039/d4cc01554a
_journal_volume                  60
_journal_year                    2024
_chemical_formula_sum            'C26 H32 Br2.31 I1.69 N6 O2 Zn'
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_audit_update_record
;
2024-02-25 deposited with the CCDC.	2024-05-15 downloaded from the CCDC.
;
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'ORTEP3 (Farrugia, 1997) and Mercury (Bruno et al., 2002)'
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_diffrn_ambient_temperature      293(2)
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_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker Kappa Apex3 CMOS Diffractometer'
_diffrn_measurement_method       '\w scans'
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_exptl_absorpt_correction_type   multi-scan
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_exptl_crystal_colour            colourless
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0192P)^2^+0.6567P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_Friedel_coverage         0.000
_reflns_number_gt                4520
_reflns_number_total             5838
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d4cc01554a2.cif
_cod_data_source_block           newznbr
_cod_depositor_comments          'Adding full bibliography for 7133069.cif.'
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