Study of the relationship between magnetic field and dielectric properties in two ferromagnetic complexes
Yang, Li; Li, Jing; Pu, Tian-Cheng; Kong, Ming; Zhang, Jing; Song, You; RSC Adv. 7 (2017) 47913–; doi:10.1039/C7RA08695D

data_7229317
_publ_section_title
;
 Study of the relationship between magnetic field and dielectric
 properties in two ferromagnetic complexes
;
_journal_issue                   76
_journal_name_full               'RSC Adv.'
_journal_page_first              47913
_journal_paper_doi               10.1039/C7RA08695D
_journal_volume                  7
_journal_year                    2017
_chemical_formula_sum            'C8 H14 Cr N Ni O12'
_chemical_formula_weight         426.91
_space_group_crystal_system      trigonal
_space_group_IT_number           163
_space_group_name_Hall           '-P 3 2c'
_space_group_name_H-M_alt        'P -3 1 c'
_symmetry_space_group_name_Hall  '-P 3 2c'
_symmetry_space_group_name_H-M   'P -3 1 c'
_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2016/6
_audit_update_record
;
2017-03-21 deposited with the CCDC.
2017-10-09 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            2
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_cell_length_c                   13.5314(10)
_cell_measurement_reflns_used    6423
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.518
_cell_measurement_theta_min      2.881
_cell_volume                     781.26(7)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
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_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0314
_diffrn_reflns_av_unetI/netI     0.0149
_diffrn_reflns_Laue_measured_fraction_full 1.000
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_diffrn_reflns_limit_h_max       10
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_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -17
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_diffrn_reflns_point_group_measured_fraction_full 1.000
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_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.518
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_exptl_absorpt_coefficient_mu    1.961
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_exptl_absorpt_correction_T_min  0.621
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            Black-green
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_refine_ls_R_factor_all          0.0330
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_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0239P)^2^+1.1914P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_database_code               7229317
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