Dual Cobalt/Organophotoredox Catalysis for Diastereo- and Regioselective 1,2-Difunctionalization of 1,3-Diene Surrogates Creating Quaternary Carbon Centers
Xue, Sijing; Cristòfol, Àlex; Limburg, Bart; Zeng, Qian; Kleij, Arjan W.; ACS Catalysis 12 (2022) 3651–3659; doi:10.1021/acscatal.2c00660

data_4519382
_publ_section_title
;
 Dual Cobalt/Organophotoredox Catalysis for Diastereo- and Regioselective
 1,2-Difunctionalization of 1,3-Diene Surrogates Creating Quaternary
 Carbon Centers
;
_journal_issue                   6
_journal_name_full               'ACS Catalysis'
_journal_page_first              3651
_journal_page_last               3659
_journal_paper_doi               10.1021/acscatal.2c00660
_journal_volume                  12
_journal_year                    2022
_chemical_formula_sum            'C20 H26 O2'
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'shelXle (H&#x00FC;bschle, Sheldrick and Dittirch, 2011)'
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;
 Fullsphere data collection, phi and omega scans
;
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;
 CrysAlisPro 1.171.40.35a (Rigaku Oxford Diffraction, 2018)
 Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_density_diffrn    1.173
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_cod_original_cell_volume        1690.22(7)
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_shelx_estimated_absorpt_t_min   0.978
_shelx_estimated_absorpt_t_max   0.989
_shelx_res_checksum              52022
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