Ethyl 5-methyl-3-[11-(pyridin-2-yl)-6,11-dihydro-6,11-epoxydibenzo[<i>b</i>,<i>e</i>]oxepin-6-yl]isoxazole-4-carboxylate: a bicyclic acetal from the rearrangement of an anthracenyl isoxazole
Weaver, Matthew J.; Campbell, Michael J.; Li, Chun; Natale, Nicholas R.; Acta Crystallographica Section E 76 (2020) 1818–1822; doi:10.1107/S2056989020014358

data_2243674
_publ_section_title
;
 Ethyl
 5-methyl-3-[11-(pyridin-2-yl)-6,11-dihydro-6,11-epoxydibenzo[<i>b</i>,<i>e</i>]oxepin-6-yl]isoxazole-4-carboxylate:
 a bicyclic acetal from the rearrangement of an anthracenyl isoxazole
;
_journal_coeditor_code           HB7949
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              1818
_journal_page_last               1822
_journal_paper_doi               10.1107/S2056989020014358
_journal_volume                  76
_journal_year                    2020
_chemical_formula_iupac          'C26 H20 N2 O5'
_chemical_formula_moiety         'C26 H20 N2 O5'
_chemical_formula_sum            'C26 H20 N2 O5'
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_chemical_name_systematic
'Ethyl 5-methyl-3-[11-(pyridin-2-yl)-6,11-dihydro-6,11-epoxydibenzo[<i>b</i>,<i>e</i>]oxepin-6-yl]isoxazole-4-carboxylate'
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
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;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
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;
SAINT (Bruker, 2016)
;
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APEX3 (Bruker, 2016)
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SAINT (Bruker, 2016)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>,  2009)
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publCIF (Westrip, 2010)
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ShelXL (Sheldrick, 2015)
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ShelXS (Sheldrick, 2008)
;
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;
(SADABS; Krause <i>et al.</i>,  2015)
;
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'w=1/[\s^2^(Fo^2^)+(0.0476P)^2^+2.6861P] where P=(Fo^2^+2Fc^2^)/3'
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