Stabilization of Cu7 clusters in azide networks: syntheses, structures and magnetic behaviour.
Mistry, Subhradeep; Sutter, Jean-Pascal; Natarajan, Srinivasan; Dalton transactions (Cambridge, England : 2003) 45 (2016) 5140–5150; doi:10.1039/c5dt04387e

data_7038260
_publ_section_title
;
 Stabilization of Cu7 clusters in azide networks: syntheses, structures
 and magnetic behaviour.
;
_journal_issue                   12
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              5140
_journal_page_last               5150
_journal_paper_doi               10.1039/c5dt04387e
_journal_volume                  45
_journal_year                    2016
_chemical_formula_moiety         'C7 H22 Cu7 N47'
_chemical_formula_sum            'C7 H22 Cu7 N47'
_chemical_formula_weight         1209.49
_chemical_name_common            Mixedamine1
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
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_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2016-01-30 deposited with the CCDC.
2016-02-03 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_computing_cell_refinement       'CrysAlisPro CCD (Oxford Diffraction, 2009)'
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_diffrn_ambient_temperature      120(2)
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_diffrn_radiation_type           MoK\a
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_exptl_crystal_colour            Green
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0486P)^2^+34.2762P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                6532
_reflns_number_total             7511
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c5dt04387e2.cif
_cod_data_source_block           Compound_I
_cod_depositor_comments
'Adding full bibliography for 7038260--7038261.cif.'
_cod_database_code               7038260
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