From serendipitous assembly to controlled synthesis of 3d-4f single-molecule magnets.
Ledezma-Gairaud, M; Grangel, L.; Aromí, G; Fujisawa, T.; Yamaguchi, A.; Sumiyama, A.; Sañudo, E C; Inorganic chemistry 53 (2014) 5878–5880; doi:10.1021/ic500418e

data_1516252
_publ_section_title
;
 From serendipitous assembly to controlled synthesis of 3d-4f
 single-molecule magnets.
;
_journal_issue                   12
_journal_name_full               'Inorganic chemistry'
_journal_page_first              5878
_journal_page_last               5880
_journal_paper_doi               10.1021/ic500418e
_journal_volume                  53
_journal_year                    2014
_chemical_formula_moiety         '[C6H16N]3, [C138 H192 O33 Mn6 Gd]'
_chemical_formula_sum            'C156 H240 Gd Mn6 N3 O33'
_chemical_formula_weight         3171.27
_chemical_name_systematic
;
 ?
;
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_diffrn_ambient_temperature      101(2)
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_diffrn_measurement_device_type  'Bruker Smart APEX II'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
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_diffrn_radiation_type           MoK\a
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_exptl_absorpt_correction_type   multi-scan
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_exptl_crystal_colour            BROWN
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_platon_squeeze_details
;
;
_refine_diff_density_max         1.113
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_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1071P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            ic500418e_si_004.cif
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_cod_depositor_comments
'Adding full bibliography for 1516250--1516252.cif.'
_cod_original_cell_volume        20014(6)
_cod_database_code               1516252
_shelx_estimated_absorpt_t_min   0.835
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_shelx_res_checksum              16288
_shelx_hkl_checksum              77681