Calixarenes with naphthalene units: calix[4]naphthalenes and hybrid[4]arenes
Boinski, T.; Cieszkowski, A.; Rosa, B.; Leśniewska, B.; Szumna, A.; New J. Chem. 40 (2016) 8892–; doi:10.1039/C6NJ01736C

data_7055775
_publ_section_title
;
 Calixarenes with naphthalene units: calix[4]naphthalenes and
 hybrid[4]arenes
;
_journal_issue                   10
_journal_name_full               'New J. Chem.'
_journal_page_first              8892
_journal_paper_doi               10.1039/C6NJ01736C
_journal_volume                  40
_journal_year                    2016
_chemical_formula_sum            'C53 H50 Cl2 O8'
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_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
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;
2016-08-13 deposited with the CCDC.
2016-09-02 downloaded from the CCDC.
;
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_cell_angle_gamma                82.019(4)
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_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measurement_device       'four-circle diffractometer'
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_diffrn_source                   'sealed X-ray tube'
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;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.35g (release 09-12-2014 CrysAlis171 .NET)
(compiled Dec  9 2014,15:38:47)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
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'Re-crystallisation from solvent: CH2Cl2'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0965P)^2^+1.4077P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                5928
_reflns_number_total             8567
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           TBnaft
_cod_depositor_comments          'Adding full bibliography for 7055775.cif.'
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