(5,5-Dimethyl-4,7-diazadecane-1,10-diamine-<i>N</i>,<i>N</i>',<i>N</i>'',<i>N</i>''')(perchlorato-<i>O</i>)copper(II) perchlorate
Tahirov, T. H.; Lu, T.-H.; Shu, K.; Chung, C.-S.; Acta Crystallographica Section C 50 (1994) 512–514; doi:10.1107/S010827019300959X

data_2009585
_publ_section_title
;(5,5-Dimethyl-4,7-diazadecane-1,10-diamine-<i>N</i>,<i>N</i>',<i>N</i>'',<i>N</i>''')(perchlorato-<i>O</i>)copper(II)
 perchlorate
;
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              512
_journal_page_last               514
_journal_paper_doi               10.1107/S010827019300959X
_journal_volume                  50
_journal_year                    1994
_chemical_formula_sum            'C10 H26 Cl2 Cu N4 O8'
_chemical_formula_weight         464.79
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.0
_cell_angle_beta                 91.050(10)
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   13.2970(10)
_cell_length_b                   13.8040(10)
_cell_length_c                   10.1360(10)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    298(3)
_cell_measurement_theta_max      16.31
_cell_measurement_theta_min      6.21
_cell_volume                     1860.2(3)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \q/2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.031
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            3446
_diffrn_reflns_theta_max         24.9
_diffrn_standards_decay_%        1
_diffrn_standards_interval_time  60
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    1.51
_exptl_absorpt_correction_T_max  0.9998
_exptl_absorpt_correction_T_min  0.9173
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            Blue-violet
_exptl_crystal_density_diffrn    1.66
_exptl_crystal_description       Parallelepiped
_exptl_crystal_size_max          0.24
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.19
_refine_diff_density_max         0.45
_refine_diff_density_min         -0.36
_refine_ls_extinction_coef       0.60(3)
_refine_ls_extinction_method     'Zachariasen (1968)'
_refine_ls_goodness_of_fit_obs   0.54
_refine_ls_hydrogen_treatment    refU
_refine_ls_number_parameters     298
_refine_ls_number_reflns         1987
_refine_ls_R_factor_obs          0.039
_refine_ls_shift/esd_max         0.668
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      unit
_refine_ls_wR_factor_obs         0.039
_reflns_number_observed          1987
_reflns_number_total             3251
_reflns_observed_criterion       I>=2.5\s(I)
_cod_data_source_file            as1066.cif
_cod_data_source_block           as1066_structure_1_of_1
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2009585