Platinum(IV) Analogues of AMD473 (cis-[PtCl2(NH3)(2-picoline)]): Preparative, Structural, and Electrochemical Studies
Battle, Andrew R.; Choi, Robin; Hibbs, David E.; Hambley, Trevor W.; Inorganic Chemistry 45 (2006) 6317–6322; doi:10.1021/ic060273g

data_4332352
_publ_section_title
;
 Platinum(IV) Analogues of AMD473 (cis-[PtCl2(NH3)(2-picoline)]):&#x00A0;
 Preparative, Structural, and Electrochemical Studies
;
_journal_issue                   16
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              6317
_journal_page_last               6322
_journal_paper_doi               10.1021/ic060273g
_journal_volume                  45
_journal_year                    2006
_chemical_formula_moiety         'C6 H10 Cl2 N2 Pt '
_chemical_formula_sum            'C6 H10 Cl2 N2 Pt'
_chemical_formula_weight         376.15
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_audit_creation_date             19102-05-09
_audit_creation_method           'by teXsan v1.8'
_audit_update_record
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?
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_cell_measurement_theta_max      0.0
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_cell_volume                     974.32(16)
_computing_cell_refinement       'd*TREK (MSC, 1996-1998)'
_computing_data_collection       'd*TREK (MSC, 1996-1998)'
_computing_data_reduction        'd*TREK (MSC, 1996-1998)'
_computing_publication_material  'teXsan (MSC, 1992-1997)'
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_computing_structure_solution
;
SHELXS86 (Sheldrick, 1985)
;
_diffrn_ambient_temperature      293.2
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_diffrn_reflns_limit_l_min       -14
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_refine_ls_extinction_expression 'equ(3) Acta Cryst.(1968) A24, p213.'
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo)]'
_refine_ls_weighting_scheme      sigma
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_refine_ls_wR_factor_ref         0.0222
_reflns_number_gt                1957
_reflns_number_total             2444
_reflns_threshold_expression     I>2.50\s(I)
_cod_data_source_file            ic060273gsup1.cif
_cod_data_source_block           rsc1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        974.3(1)
_cod_original_sg_symbol_H-M      'P 21/c     '
_cod_original_formula_sum        'C6 H10 Cl2 N2 Pt '
_cod_database_code               4332352