Microwave-assisted ionothermal synthesis of a water-stable Eu-coordination polymer: a Ba(2+) ion detector and fluorescence thermometer.
Wang, Ze-Ping; Hu, Bing; Qi, Xing-Hui; Shen, Nan-Nan; Huang, Xiao-Ying; Dalton transactions (Cambridge, England : 2003) 45 (2016) 8745–8752; doi:10.1039/c6dt00641h

data_7039009
_publ_section_title
;
 Microwave-assisted ionothermal synthesis of a water-stable
 Eu-coordination polymer: a Ba(2+) ion detector and fluorescence
 thermometer.
;
_journal_issue                   21
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              8745
_journal_page_last               8752
_journal_paper_doi               10.1039/c6dt00641h
_journal_volume                  45
_journal_year                    2016
_chemical_formula_moiety         'C16 H8 Eu O12, C10 H19 N2'
_chemical_formula_sum            'C26 H27 Eu N2 O12'
_chemical_formula_weight         711.45
_chemical_name_systematic
;
 ?
;
_space_group_crystal_system      orthorhombic
_space_group_IT_number           60
_space_group_name_Hall           '-P 2n 2ab'
_space_group_name_H-M_alt        'P b c n'
_symmetry_space_group_name_Hall  '-P 2n 2ab'
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_atom_sites_solution_hydrogens   mixed
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2016-01-31 deposited with the CCDC.
2016-04-11 downloaded from the CCDC.
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
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_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0566
_diffrn_reflns_av_unetI/netI     0.0792
_diffrn_reflns_Laue_measured_fraction_full 0.999
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_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.102
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_diffrn_source                   'Enhance (Mo) X-ray Source'
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CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
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Empirical absorption correction using spherical harmonics,
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_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.671
_exptl_crystal_description       block
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_refine_ls_number_restraints     1025
_refine_ls_restrained_S_all      0.949
_refine_ls_R_factor_all          0.0792
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0332P)^2^+2.5000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0808
_refine_ls_wR_factor_ref         0.0951
_reflns_Friedel_coverage         0.000
_reflns_number_gt                4142
_reflns_number_total             6193
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c6dt00641h2.cif
_cod_data_source_block           x
_cod_depositor_comments
'Adding full bibliography for 7039009--7039010.cif.'
_cod_database_code               7039009
_shelxl_version_number           2014-3
_shelx_res_checksum              12116