Synthesis and structural properties of the first bismuth(iii) telluroether complex
Levason, William; Hill, Nicholas J.; Reid, Gillian; Journal of the Chemical Society, Dalton Transactions  (2002) 4316–; doi:10.1039/b209321a

data_7012254
_publ_section_title
;
 Synthesis and structural properties of the first bismuth(iii)
 telluroether complex
;
_journal_issue                   23
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              4316
_journal_paper_doi               10.1039/b209321a
_journal_year                    2002
_chemical_formula_moiety         'C7 H8 Bi Br3 Te '
_chemical_formula_structural     '[BiBr3(PhTeMe)]'
_chemical_formula_sum            'C7 H8 Bi Br3 Te'
_chemical_formula_weight         668.43
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
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_symmetry_space_group_name_Hall  '-P 2yn'
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_cell_length_b                   6.7592(2)
_cell_length_c                   22.5808(8)
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_cell_measurement_theta_max      0.0
_cell_measurement_theta_min      0.0
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_computing_cell_refinement       'Nonius Kappa CCD Diffractometer Control'
_computing_data_collection       'Nonius Kappa CCD Diffractometer Control'
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'teXsan for Windows version 1.06 (MSC, 1997-1999)'
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'teXsan for Windows version 1.06 (MSC, 1997-1999)'
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'teXsan for Windows version 1.06 (MSC, 1997-1999)'
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;
SHELX97 (Sheldrick, 1997)
;
_diffrn_ambient_temperature      120.0(1)
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_diffrn_radiation_monochromator  graphite
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_diffrn_radiation_type           'Mo K\a'
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_diffrn_reflns_limit_k_max       7
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_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            5253
_diffrn_reflns_reduction_process 'Lp corrections applied'
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_diffrn_reflns_theta_min         3.15
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_exptl_absorpt_process_details
'SORTAV, R H Blessing, J. Appl. Cryst., 1997, 30, 421-426.'
_exptl_crystal_colour            orange-red
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_exptl_crystal_size_mid          0.06
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_refine_ls_structure_factor_coef F
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_reflns_threshold_expression     I>2.00\s(I)
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_cod_original_cell_volume        1272.18(6)
_cod_original_sg_symbol_H-M      'P 21/n     '
_cod_original_formula_sum        'C7 H8 Bi Br3 Te '
_cod_database_code               7012254