Novel Two- and Three-Dimensional Organometallic-Organic Hybrid Materials Based on Polyphosphorus Complexes.
Attenberger, Bianca; Peresypkina, Eugenia V.; Scheer, Manfred; Inorganic chemistry 54 (2015) 7021–7029; doi:10.1021/acs.inorgchem.5b01048

data_4343460
_publ_section_title
;
 Novel Two- and Three-Dimensional Organometallic-Organic Hybrid Materials
 Based on Polyphosphorus Complexes.
;
_journal_issue                   14
_journal_name_full               'Inorganic chemistry'
_journal_page_first              7021
_journal_page_last               7029
_journal_paper_doi               10.1021/acs.inorgchem.5b01048
_journal_volume                  54
_journal_year                    2015
_chemical_formula_structural
'[(C5H5)2Mo2P2(CO)4Ag(C12H10N2)](Al(OC4F9)4)*0.075(CH2Cl2)*1.425(C6H6)'
_chemical_formula_sum            'C50.63 H28.7 Ag Al Cl0.15 F36 Mo2 N2 O8 P2'
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_chemical_name_systematic
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 ? 
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CrysAlisPro, Agilent Technologies,
Version 1.171.34.49 (release 20-01-2011 CrysAlis171 .NET)
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CrysAlisPro, Agilent Technologies,
Version 1.171.34.49 (release 20-01-2011 CrysAlis171 .NET)
(compiled Jan 20 2011,15:58:25)
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CrysAlisPro, Agilent Technologies,
Version 1.171.34.49 (release 20-01-2011 CrysAlis171 .NET)
(compiled Jan 20 2011,15:58:25)
;
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
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_diffrn_measured_fraction_theta_full 0.979
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CrysAlisPro, Agilent Technologies,
Version 1.171.34.49 (release 20-01-2011 CrysAlis171 .NET)
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Empirical absorption correction using spherical harmonics,
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_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.933
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_exptl_crystal_description       plate
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0774P)^2^+5.9698P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1290
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_reflns_number_gt                38016
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_cod_data_source_file            ic5b01048_si_002.cif
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The following automatic conversions were performed:
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Id: cif_correct_tags 3376 2015-05-07 07:48:27Z andrius 

 Adding full bibliography for 4343458--4343460.cif.
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_cod_original_cell_volume        12856.7(4)
_cod_original_formula_sum        'C50.63 H28.70 Ag Al Cl0.15 F36 Mo2 N2 O8 P2'
_cod_database_code               4343460