Meisserite, Na5(UO2)(SO4)3(SO3OH)(H2O), a new uranyl sulfate mineral from the Blue Lizard mine, San Juan County, Utah, USA
J. Plášil; A. R. Kampf; A. V. Kasatkin; J. Marty; R. Škoda; S. Silva; J. Čejka; Mineralogical Magazine 77 (2013) 2975–2988; doi:10.1180/minmag.2013.077.7.07

data_1513209
_publ_section_title
;
 Meisserite, Na5(UO2)(SO4)3(SO3OH)(H2O), a new uranyl sulfate mineral from
 the Blue Lizard mine, San Juan County, Utah, USA
;
_journal_issue                   7
_journal_name_full               'Mineralogical Magazine'
_journal_page_first              2975
_journal_page_last               2988
_journal_paper_doi               10.1180/minmag.2013.077.7.07
_journal_volume                  77
_journal_year                    2013
_chemical_compound_source
'From the Blue Lizard mine, San Juan County, Utah, USA'
_chemical_formula_sum            'H3 Na5 O19 S4 U'
_chemical_formula_weight         788.2
_chemical_name_mineral           Meisserite
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   difmap
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                102.864
_cell_angle_beta                 97.414
_cell_angle_gamma                91.461
_cell_formula_units_Z            2
_cell_length_a                   5.3232
_cell_length_b                   11.5105
_cell_length_c                   13.5562
_cell_measurement_temperature    293
_cell_volume                     801.743
_diffrn_ambient_temperature      293
_diffrn_measured_fraction_theta_full 0.99
_diffrn_measured_fraction_theta_max 0.99
_diffrn_radiation_probe          x-ray
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71075
_diffrn_reflns_av_R_equivalents  0.0274
_diffrn_reflns_av_sigmaI/netI    0.0224
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            13998
_diffrn_reflns_theta_full        27.47
_diffrn_reflns_theta_max         27.47
_diffrn_reflns_theta_min         3.11
_exptl_absorpt_coefficient_mu    10.883
_exptl_crystal_density_diffrn    3.264
_exptl_crystal_F_000             732
_refine_diff_density_max         0.78
_refine_diff_density_min         -0.78
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_gt    1.36
_refine_ls_goodness_of_fit_ref   1.34
_refine_ls_hydrogen_treatment    refall
_refine_ls_number_constraints    3
_refine_ls_number_parameters     274
_refine_ls_number_reflns         3627
_refine_ls_number_restraints     3
_refine_ls_R_factor_all          0.0215
_refine_ls_R_factor_gt           0.0180
_refine_ls_shift/su_max          0.0271
_refine_ls_shift/su_mean         0.0016
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     w=1/(\s^2^(I)+0.0004I^2^)
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.0439
_refine_ls_wR_factor_ref         0.0457
_reflns_number_gt                3306
_reflns_number_total             3627
_reflns_threshold_expression     I>3\s(I)
_cod_data_source_file            ciffile.cif.txt
_cod_data_source_block           I
_cod_original_cell_volume        801.7432
_cod_original_formula_sum        'H3 Na5 O19 S4 U1'
_cod_database_code               1513209
_cod_database_fobs_code          1513209