Stoichiometry of lanthanide(iii) complexes with tripodal aminophosphonic ligands ‒ a new solution to an old problem
Janicki, Rafał; Gałęzowska, Joanna; Mondry, Anna; Inorganic Chemistry Frontiers 4 (2017) 1200–; doi:10.1039/C7QI00191F

data_4349707
_publ_section_title
;
 Stoichiometry of lanthanide(iii) complexes with tripodal aminophosphonic
 ligands -- a new solution to an old problem
;
_journal_issue                   7
_journal_name_full               'Inorganic Chemistry Frontiers'
_journal_page_first              1200
_journal_paper_doi               10.1039/C7QI00191F
_journal_volume                  4
_journal_year                    2017
_chemical_formula_sum            'C21 H74 Eu N19 O24 P4'
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_audit_update_record
;
2017-04-03 deposited with the CCDC.
2017-05-15 downloaded from the CCDC.
;
_cell_angle_alpha                105.889(8)
_cell_angle_beta                 94.515(7)
_cell_angle_gamma                90.629(7)
_cell_formula_units_Z            2
_cell_length_a                   11.9255(11)
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_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.21 (release 14-08-2012 CrysAlis171 .NET)
(compiled Sep 14 2012,17:21:16)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.21 (release 14-08-2012 CrysAlis171 .NET)
(compiled Sep 14 2012,17:21:16)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.21 (release 14-08-2012 CrysAlis171 .NET)
(compiled Sep 14 2012,17:21:16)
;
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
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_diffrn_ambient_temperature      100(2)
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_exptl_crystal_colour            colourless
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0565P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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