Etude de la phenylhydrazone du 3-benzoyl-1-methylindole
Toupet, L.; Soufiaoui, M.; Carrie, R.; Acta Crystallographica Section C 49 (1993) 2143–2145; doi:10.1107/S0108270193005190

data_2001175
_publ_section_title
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 Etude de la phenylhydrazone du 3-benzoyl-1-methylindole
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_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              2143
_journal_page_last               2145
_journal_paper_doi               10.1107/S0108270193005190
_journal_volume                  49
_journal_year                    1993
_chemical_formula_sum            'C22 H19 N3'
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_cell_angle_beta                 90
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_cell_measurement_theta_max      12
_cell_measurement_theta_min      9
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_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       '\w/2\q, t~max~ = 60 s'
_diffrn_radiation_type           MoK\a
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_diffrn_standards_decay_%        0.3
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_exptl_absorpt_coefficient_mu    0.070
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_exptl_crystal_description       prism
_exptl_crystal_size_max          0.25
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_refine_ls_extinction_method     none
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_refine_ls_hydrogen_treatment    noref
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_refine_ls_R_factor_obs          0.038
_refine_ls_shift/esd_max         0.3
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(I)+(0.04F~o~^2^)^2^]^-1/2^'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.039
_reflns_number_observed          1730
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_reflns_observed_criterion       I>3\s(I)
_cod_data_source_file            pa1035.cif
_cod_data_source_block           pa1035_structure_1_of_1
_cod_depositor_comments
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The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value
'1/[\s^2^(I)+(0.04F~o~^2^)^2^]^-1/2^' was changed to 'calc'. New tag
'_refine_ls_weighting_details' was created. The value of the new tag
was set to 'w = 1/[\s^2^(I)+(0.04F~o~^2^)^2^]^-1/2^'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
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_cod_database_code               2001175