Powder study of poly[(μ~2~-2,2-dimethylpropane-1,3-diyl diisocyanide)-μ~2~-iodido-silver(I)]
Rukiah, Mwaffak; Al-Ktaifani, Mahmoud; Acta Crystallographica Section C 65 (2009) m135–m138; doi:10.1107/S0108270109004661

data_2017013
_publ_section_title
;
 Powder study of poly[(\m~2~-2,2-dimethylpropane-1,3-diyl
 diisocyanide)-\m~2~-iodido-silver(I)]
;
_journal_coeditor_code           GT3002
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m135
_journal_page_last               m138
_journal_paper_doi               10.1107/S0108270109004661
_journal_volume                  65
_journal_year                    2009
_chemical_formula_iupac          '[Ag I (C7 H10 N2)]'
_chemical_formula_moiety         'C7 H10 Ag I N2'
_chemical_formula_structural     'Ag (C N C H2(C H3)2C H2 N C)] I'
_chemical_formula_sum            'C7 H10 Ag I N2'
_chemical_formula_weight         356.94
_chemical_name_systematic
;poly[(\m~2~-2,2-dimethylpropane-1,3-diyl
 diisocyanide)-\m~2~-iodido-silver(I)]
;
_space_group_IT_number           61
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            8
_cell_length_a                   16.1168(2)
_cell_length_b                   17.1119(2)
_cell_length_c                   7.68115(7)
_cell_measurement_temperature    298
_cell_volume                     2118.38(4)
_computing_cell_refinement       'GSAS (Larsen & Von Dreele, 2004)'
_computing_data_collection       'WinXPOW (Stoe & Cie, 1999)'
_computing_data_reduction        'WinXPOW (Stoe & Cie, 1999)'
_computing_molecular_graphics    'PLATON (Spek, 2009)'
_computing_publication_material  'GSAS (Larsen & Von Dreele, 2004)'
_computing_structure_refinement  'GSAS (Larsen & Von Dreele, 2004)'
_computing_structure_solution    'FOX (Favre-Nicolin & \<Cern\'y, 2002)'
_diffrn_ambient_temperature      295
_diffrn_measurement_device_type  'Stoe STADI P transmission'
_diffrn_radiation_monochromator  'Ge 111'
_diffrn_radiation_type           'Cu K\a1'
_diffrn_radiation_wavelength     1.5406
_exptl_absorpt_coefficient_mu    37.72
_exptl_absorpt_correction_T_max  0.25777
_exptl_absorpt_correction_T_min  0.20911
_exptl_absorpt_correction_type   cylinder
_exptl_absorpt_process_details
;
GSAS absorption/surface roughness correction: function number 5.
Flat-plate sample in transmission geometry. Absorption correction
term (\m.r) = 0.62300. Correction is not refined.
;
_exptl_crystal_density_diffrn    2.238
_exptl_crystal_F_000             1328.0
_refine_diff_density_max         0.662
_refine_diff_density_min         -0.508
_refine_ls_goodness_of_fit_all   1.24
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     96
_refine_ls_number_restraints     40
_refine_ls_shift/su_max          0.01
_refine_ls_shift/su_mean         0.00
_reflns_number_total             876
_cod_data_source_file            gt3002.cif
_cod_data_source_block           I
_cod_original_cell_volume        2118.38(6)
_cod_database_code               2017013