Lead and tin β-diketiminato amido/anilido complexes: competitive nucleophilic reactivity at the β-diketiminato γ-carbon.
Harris, Lisa A.-M.; Tam, Eric C. Y.; Coles, Martyn P.; Fulton, J. Robin; Dalton transactions (Cambridge, England : 2003) 43 (2014) 13803–13814; doi:10.1039/c4dt01714e

data_7031971
_publ_section_title
;
 Lead and tin \b-diketiminato amido/anilido complexes: competitive
 nucleophilic reactivity at the \b-diketiminato \g-carbon.
;
_journal_issue                   36
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              13803
_journal_page_last               13814
_journal_paper_doi               10.1039/c4dt01714e
_journal_volume                  43
_journal_year                    2014
_chemical_compound_source        'synthesis as described'
_chemical_formula_moiety         'C41 H59 N3 Pb1'
_chemical_formula_sum            'C41 H59 N3 Pb'
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;
 ?
;
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_cell_measurement_temperature    173(2)
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_cell_measurement_wavelength     0.71073
_cell_volume                     1909.24(5)
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'HKL Denzo and Scalepack (Otwinowski & Minor 1997)'
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;
        [c.f. r.h. blessing, acta cryst. (1995), a51, 33-38]
;
_exptl_crystal_colour            Yellow
_exptl_crystal_density_diffrn    1.393
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_exptl_crystal_description       Needles
_exptl_crystal_F_000             816
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_refine_ls_matrix_type           full
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_refine_ls_number_reflns         8691
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_refine_ls_R_factor_all          0.0305
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_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
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'calc w=1/[\s^2^(Fo^2^)+(0.0112P)^2^+2.2486P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0478
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_reflns_number_gt                7920
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_reflns_threshold_expression     >2sigma(I)
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_cod_data_source_block           (5)-jun309
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'Adding full bibliography for 7031968--7031975.cif.'
_cod_database_code               7031971