General sulfone construction via sulfur dioxide surrogate control
Chen, Shihao; Li, Yaping; Wang, Ming; Jiang, Xuefeng; Green Chemistry 22 (2020) 322–326; doi:10.1039/C9GC03841H

data_7239713
_publ_section_title
;
 General sulfone construction via sulfur dioxide surrogate control
;
_journal_issue                   2
_journal_name_full               'Green Chemistry'
_journal_page_first              322
_journal_page_last               326
_journal_paper_doi               10.1039/C9GC03841H
_journal_volume                  22
_journal_year                    2020
_chemical_formula_sum            'C23 H20 O4 S Se'
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_space_group_name_Hall           '-P 2ybc'
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_audit_update_record
;
2019-06-08 deposited with the CCDC.	2019-12-05 downloaded from the CCDC.
;
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_computing_cell_refinement       'Bruker SAINT'
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_diffrn_radiation_monochromator  graphite
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_diffrn_reflns_limit_l_min       -21
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_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
 SADABS-2014/5 - Bruker AXS area detector scaling and absorption correction 
;
_exptl_crystal_colour            colorless
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0630P)^2^+1.7153P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1134
_refine_ls_wR_factor_ref         0.1229
_reflns_Friedel_coverage         0.000
_reflns_number_gt                3940
_reflns_number_total             4875
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c9gc03841h2.cif
_cod_data_source_block           a
_cod_depositor_comments
;Adding full bibliography for 7239713--7239714.cif.

 Adding full bibliography for 7239713--7239714.cif.
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7239713
_shelx_shelxl_version_number     2016/6
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_shelx_estimated_absorpt_t_max   0.833
_shelx_res_checksum              5718