[2-(1<i>H</i>-Indol-4-yl)ethyl]dipropylamine
Wang, De-Cai; Pan, Hua-Yang; Song, Jun-Song; Wei, Ping; Ou-yang, Ping-Kai; Acta Crystallographica Section E 68 (2012) o1502–; doi:10.1107/S1600536812015474

data_2234712
_publ_section_title
;
 [2-(1<i>H</i>-Indol-4-yl)ethyl]dipropylamine
;
_journal_coeditor_code           LD2053
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o1502
_journal_paper_doi               10.1107/S1600536812015474
_journal_volume                  68
_journal_year                    2012
_chemical_formula_iupac          'C16 H24 N2'
_chemical_formula_moiety         'C16 H24 N2'
_chemical_formula_sum            'C16 H24 N2'
_chemical_formula_weight         244.37
_chemical_name_systematic
;
[2-(1<i>H</i>-Indol-4-yl)ethyl]dipropylamine
;
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_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
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_cell_length_a                   12.1100(9)
_cell_length_b                   15.5996(12)
_cell_length_c                   16.0253(12)
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_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      13
_cell_measurement_theta_min      9
_cell_volume                     3027.4(4)
_computing_cell_refinement       'CAD-4 EXPRESS (Enraf--Nonius, 1994)'
_computing_data_collection       'CAD-4 EXPRESS (Enraf--Nonius, 1994)'
_computing_data_reduction        'XCAD4 (Harms & Wocadlo, 1995)'
_computing_molecular_graphics    'SHELXTL (Sheldrick, 2008)'
_computing_publication_material  'SHELXTL (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.991
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'Enraf--Nonius CAD-4'
_diffrn_measurement_method       \w/2\q
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_diffrn_standards_interval_count 200
_diffrn_standards_interval_time  2
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_exptl_absorpt_correction_T_max  0.9937
_exptl_absorpt_correction_T_min  0.9814
_exptl_absorpt_correction_type   psi-scan
_exptl_absorpt_process_details   '(North et al., 1968)'
_exptl_crystal_colour            white
_exptl_crystal_density_diffrn    1.072
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
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_refine_ls_R_factor_all          0.1464
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_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0390P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     I>2\s(I)
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