Catalytic Asymmetric Addition of Alkynylzinc Reagents to Nitrones
Konishi, Atsuko; Wei, Weilin; Kobayashi, Masato; Fujinami, Shuhei; Ukaji, Yutaka; Inomata, Katsuhiko; Chemistry Letters 36 (2007) 44–; doi:10.1246/cl.2007.44

data_8000160
_publ_section_title
;
 Catalytic Asymmetric Addition of Alkynylzinc Reagents to Nitrones
;
_journal_issue                   1
_journal_name_full               'Chemistry Letters'
_journal_page_first              44
_journal_paper_doi               10.1246/cl.2007.44
_journal_volume                  36
_journal_year                    2007
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_symmetry_space_group_name_H-M   'P 1'
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_cell_angle_beta                 91.046(5)
_cell_angle_gamma                99.929(6)
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_cell_measurement_temperature    123.2
_cell_measurement_theta_max      30.5
_cell_measurement_theta_min      3.1
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_diffrn_measured_fraction_theta_max 0.8144
_diffrn_measurement_device_type  'Rigaku/MSC Mercury CCD'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
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_diffrn_reflns_av_R_equivalents  0.012
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
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_exptl_absorpt_correction_type   none
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_exptl_crystal_colour            Colorless
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_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
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_exptl_crystal_size_mid          0.200
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_refine_ls_weighting_details     'w = 1/[\s^2^(Fo) + 0.00123|Fo|^2^]'
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