Diverse anion exchange of pliable [X<sub>2</sub>@Pd<sub>3</sub>L<sub>4</sub>]<sup>4+</sup> double cages: a molecular ruler for recognition of polyatomic anions.
Sarada, Ganguri; Kim, Ahreum; Kim, Dongwon; Jung, Ok-Sang; Dalton transactions (Cambridge, England : 2003) 49 (2020) 6183–6190; doi:10.1039/d0dt01027h

data_7704040
_publ_section_title
;
 Diverse anion exchange of pliable
 [X<sub>2</sub>@Pd<sub>3</sub>L<sub>4</sub>]<sup>4+</sup> double cages: a
 molecular ruler for recognition of polyatomic anions.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              6183
_journal_page_last               6190
_journal_paper_doi               10.1039/d0dt01027h
_journal_volume                  49
_journal_year                    2020
_chemical_formula_sum            'C106 H112 N18 O36 Pd3 S'
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_space_group_IT_number           13
_space_group_name_Hall           '-P 2yac'
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_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2020-04-06 deposited with the CCDC.	2020-04-09 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_diffrn_measured_fraction_theta_max 0.946
_diffrn_measurement_device_type  'Rayonix MX225HS CCD area detector'
_diffrn_measurement_method       'omega scan'
_diffrn_radiation_type           synchrotron
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_exptl_crystal_colour            colorless
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.2000P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2715
_refine_ls_wR_factor_ref         0.3063
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           NO3_6
_cod_depositor_comments
'Adding full bibliography for 7704033--7704041.cif.'
_cod_original_sg_symbol_H-M      'P 2/n'
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_shelx_res_checksum              96269
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