Synthesis of Substituted Trinaphthylenes.
Rüdiger, Elias C; Rominger, Frank; Steuer, Lena; Bunz, Uwe H. F.; The Journal of organic chemistry 81 (2016) 193–196; doi:10.1021/acs.joc.5b02481

data_4036528
_publ_section_title
;
 Synthesis of Substituted Trinaphthylenes.
;
_journal_issue                   1
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              193
_journal_page_last               196
_journal_paper_doi               10.1021/acs.joc.5b02481
_journal_volume                  81
_journal_year                    2016
_chemical_formula_sum            'C45 H48 Cl6 O6'
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_chemical_name_common            '2 in paper'
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_diffrn_measured_fraction_theta_max 0.970
_diffrn_measurement_device_type  'Bruker APEX area detector'
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_diffrn_source                   'sealed tube'
_exptl_absorpt_coefficient_mu    0.446
_exptl_absorpt_correction_T_max  0.9542
_exptl_absorpt_correction_T_min  0.8950
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
Sheldrick, G. M. (2008). <i>SADABS</i>. University of G\"ottingen, Germany.
;
_exptl_crystal_colour            colourless
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_refine_ls_extinction_method     none
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_refine_ls_number_reflns         5692
_refine_ls_number_restraints     873
_refine_ls_restrained_S_all      1.025
_refine_ls_R_factor_all          0.1117
_refine_ls_R_factor_gt           0.0697
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0452P)^2^+4.4136P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1417
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_reflns_threshold_expression     'I > 2\s(I)'
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_shelx_shelxl_version_number     2014/7
_shelx_estimated_absorpt_t_min   0.928
_shelx_estimated_absorpt_t_max   0.944
_shelx_res_checksum              32219
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