Spirocyclic tin salicyl alcoholates - a combined experimental and theoretical study on their structures, <sup>119</sup>Sn NMR chemical shifts and reactivity in thermally induced twin polymerization.
Kitschke, Philipp; Preda, Ana-Maria; Auer, Alexander A.; Scholz, Sebastian; Rüffer, Tobias; Lang, Heinrich; Mehring, Michael; Dalton transactions (Cambridge, England : 2003) 48 (2018) 220–230; doi:10.1039/c8dt03695k

data_7048223
_publ_section_title
;
 Spirocyclic tin salicyl alcoholates - a combined experimental and
 theoretical study on their structures, <sup>119</sup>Sn NMR chemical
 shifts and reactivity in thermally induced twin polymerization.
;
_journal_issue                   1
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'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              220
_journal_page_last               230
_journal_paper_doi               10.1039/c8dt03695k
_journal_volume                  48
_journal_year                    2018
_chemical_formula_moiety         'C28 H44 O6 S2 Sn, 2(C2 H6 O S)'
_chemical_formula_sum            'C32 H56 O8 S4 Sn'
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2018-08-07 deposited with the CCDC.
2018-11-22 downloaded from the CCDC.
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET)
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET)
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CrysAlisPro, Agilent Technologies,
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Empirical absorption correction using spherical harmonics,
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_exptl_crystal_colour            colourless
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_refine_ls_number_restraints     0
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_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0355P)^2^+0.6806P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                3266
_reflns_number_total             3266
_reflns_threshold_expression     'I > 2\s(I)'
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