Controllable Synthesis of Covalent Porphyrinic Cages with Varying Sizes via Template-Directed Imine Condensation Reactions.
Ding, Huimin; Wu, Xiaojun; Zeller, Matthias; Xie, Yunpeng; Wang, Cheng; The Journal of organic chemistry 80 (2015) 9360–9364; doi:10.1021/acs.joc.5b01781

data_4031489
_publ_section_title
;
 Controllable Synthesis of Covalent Porphyrinic Cages with Varying Sizes
 via Template-Directed Imine Condensation Reactions.
;
_journal_issue                   18
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              9360
_journal_page_last               9364
_journal_paper_doi               10.1021/acs.joc.5b01781
_journal_volume                  80
_journal_year                    2015
_chemical_formula_moiety
'C130 H112 N18 Zn2, 5.786(C H Cl3), 3.214(C3 H6 O)'
_chemical_formula_sum            'C145.43 H137.07 Cl17.36 N18 O3.21 Zn2'
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;  
SHELXL-2014/7 (Sheldrick, 2014), 
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;
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0793P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                4595
_reflns_number_total             12530
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           11_MZ
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3271 2015-04-21 07:52:19Z andrius 

 Adding full bibliography for 4031489--4031490.cif.
;
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