Hydrolysis of phosphodiester with hydroxo- or carboxylate-bridged dinuclear Ni(ii) and Cu(ii) complexes
Yamaguchi, Kazuya; Akagi, Fumio; Suzuki, Shinnichiro; Fujinami, Shuhei; Suzuki, Masatatsu; Shionoya, Mitsuhiko; Chemical Communications  (2001) 375–; doi:10.1039/b008994j

data_7114744
_publ_section_title
;
 Hydrolysis of phosphodiester with hydroxo- or carboxylate-bridged
 dinuclear Ni(ii) and Cu(ii) complexes
;
_journal_issue                   4
_journal_name_full               'Chemical Communications'
_journal_page_first              375
_journal_paper_doi               10.1039/b008994j
_journal_year                    2001
_chemical_formula_sum            'C46 H59 Cl2 N6 Ni2 O16 P'
_chemical_formula_weight         1171.28
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2yn'
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_audit_creation_date             2000-10-31
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_cell_angle_alpha                90
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_cell_angle_gamma                90
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_cell_length_a                   13.5091(4)
_cell_length_b                   20.927(1)
_cell_length_c                   18.0299(9)
_cell_measurement_reflns_used    0
_cell_measurement_temperature    138.2
_cell_measurement_theta_max      0.0
_cell_measurement_theta_min      0.0
_cell_volume                     5064.6(4)
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_computing_publication_material  teXsan
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_diffrn_measurement_device       'unknown QUANTUM'
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_diffrn_radiation_detector       CCD
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_diffrn_reflns_limit_l_min       -14
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_diffrn_reflns_reduction_process 'Lp corrections applied'
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_diffrn_reflns_theta_min         1.13
_diffrn_standards_decay_%        0.00
_diffrn_standards_interval_count 0
_diffrn_standards_number         0
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_exptl_absorpt_correction_type   none
_exptl_crystal_colour            Colorless
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_exptl_crystal_density_meas      ?
_exptl_crystal_description       Prism
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_refine_ls_shift/su_max          0.0007
_refine_ls_shift/su_mean         0.0000
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\\s^2^(Fo) + 0.00189|Fo|^2^]'
_refine_ls_weighting_scheme      sigma
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_cod_data_source_file            b008994j.txt
_cod_data_source_block           '[Ni2(Me4tpdp)(DPP)(MeOH)2](ClO4)2'
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_sg_symbol_H-M      'P 21/n     '
_cod_original_formula_sum        'C46 H59 Cl2 N6 O16 Ni2 P '
_cod_database_code               7114744