Reaction of an allylstannylene with adamantyl phosphaalkyne.
Krebs, K. M.; Jamin, J.; Wesemann, L.; Dalton transactions (Cambridge, England : 2003) 45 (2016) 5933–5936; doi:10.1039/c5dt03792a

data_7037037
_publ_section_title
;
 Reaction of an allylstannylene with adamantyl phosphaalkyne.
;
_journal_issue                   14
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              5933
_journal_page_last               5936
_journal_paper_doi               10.1039/c5dt03792a
_journal_volume                  45
_journal_year                    2016
_chemical_formula_sum            'C110.15 H161.65 P2 Sn2'
_chemical_formula_weight         1785.15
_chemical_name_systematic
;
 ?
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2015-09-25 deposited with the CCDC.
2015-10-20 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_number            70071
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_exptl_crystal_colour            yellow
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0711P)^2^+8.7223P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1275
_refine_ls_wR_factor_ref         0.1455
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c5dt03792a2.cif
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_cod_depositor_comments          'Adding full bibliography for 7037037.cif.'
_cod_database_code               7037037
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