Neutral and Cationic Bis-Chelate Monoorganosilicon(IV) Complexes of 1-Hydroxy-2-pyridinone
Koch, James G.; Brennessel, William W.; Kraft, Bradley M.; Organometallics 36 (2017) 594–; doi:10.1021/acs.organomet.6b00796

data_4086930
_publ_section_title
;
 Neutral and Cationic Bis-Chelate Monoorganosilicon(IV) Complexes of
 1-Hydroxy-2-pyridinone
;
_journal_issue                   3
_journal_name_full               Organometallics
_journal_page_first              594
_journal_paper_doi               10.1021/acs.organomet.6b00796
_journal_volume                  36
_journal_year                    2017
_chemical_formula_moiety         'C17 H15 F N2 O4 Si'
_chemical_formula_sum            'C17 H15 F N2 O4 Si'
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_space_group_crystal_system      monoclinic
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_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
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_cell_measurement_theta_max      29.12
_cell_measurement_theta_min      2.68
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_diffrn_ambient_temperature      100.0(5)
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_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker SMART APEX II CCD platform'
_diffrn_measurement_method       '\w scans'
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_refine_ls_extinction_method     none
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_refine_ls_R_factor_all          0.0775
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0729P)^2^+0.2881P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 4086922--4086931.cif.'
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