Synthesis, structure and properties of [ethylpyridinium][Ni(mnt)2]: evidence for an unusual magnetically ordered ground state
Robertson, Neil; Bergemann, Christoph; Becker, Helmut; Agarwal, Prabhat; Julian, Stephen R.; Friend, Richard H.; Hatton, Nicholas J.; Underhill, Allan E.; Kobayashi, Akiko; Journal of Materials Chemistry 9 (1999) 1713–; doi:10.1039/a903007g

data_7213081
_publ_contact_author
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    ENTER NAME
 ENTER ADDRESS
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_publ_section_title
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 Synthesis, structure and properties of [ethylpyridinium][Ni(mnt)2]:
 evidence for an unusual magnetically ordered ground state
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_journal_issue                   8
_journal_name_full               'Journal of Materials Chemistry'
_journal_page_first              1713
_journal_paper_doi               10.1039/a903007g
_journal_volume                  9
_journal_year                    1999
_chemical_formula_sum            'C15 H10 N5 Ni S4'
_chemical_formula_weight         447.22
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
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_audit_creation_date             'Fri Mar 12 16:22:51 1999'
_audit_creation_method           'from TEXRAY.INF file'
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_cell_angle_gamma                99.65(1)
_cell_formula_units_Z            4
_cell_length_a                   13.055(3)
_cell_length_b                   16.915(3)
_cell_length_c                   10.772(2)
_cell_measurement_reflns_used    0
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_cell_volume                     2239.8(8)
_computing_data_reduction        teXsan
_computing_publication_material  teXsan
_computing_structure_refinement  teXsan
_diffrn_ambient_temperature      20.0
_diffrn_measurement_device       'Mac Science DIP-320'
_diffrn_radiation_detector       IP
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           'Mo K\a'
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_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       9
_diffrn_reflns_limit_l_min       0
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_diffrn_reflns_reduction_process 'Lp corrections applied'
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_diffrn_reflns_theta_min         0.00
_exptl_absorpt_coefficient_mu    1.246
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    1.326
_exptl_crystal_density_meas      ?
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_exptl_crystal_size_max          0.50
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_refine_diff_density_max         1.62
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_refine_ls_extinction_method     none
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_refine_ls_structure_factor_coef F
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_cod_depositor_comments
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The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_sg_symbol_H-M      'P -1         '
_cod_original_formula_sum        'C15 H10 N5 Ni S4 '
_cod_database_code               7213081