Eu(III)-organic framework as a multi-responsive photoluminescence sensor for efficient detection of 1-naphthol, Fe3+ and MnO4− in water
Zhao, Jiao-Jiao; Liu, Peng-Yu; Dong, Zhen-Peng; Liu, Zhi-Liang; Wang, Yan-Qin; Inorganica Chimica Acta 511 (2020) 119843–; doi:10.1016/j.ica.2020.119843

data_1564182
_publ_section_title
;
 Eu(III)-organic framework as a multi-responsive photoluminescence sensor
 for efficient detection of 1-naphthol, Fe3+ and MnO4&#x2212; in water
;
_journal_name_full               'Inorganica Chimica Acta'
_journal_page_first              119843
_journal_paper_doi               10.1016/j.ica.2020.119843
_journal_volume                  511
_journal_year                    2020
_chemical_formula_sum            'C42 H34 Eu3 N2 O21'
_chemical_formula_weight         1358.59
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   mixed
_cell_angle_alpha                104.512(2)
_cell_angle_beta                 93.874(3)
_cell_angle_gamma                101.256(3)
_cell_formula_units_Z            2
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_cell_length_b                   12.278(2)
_cell_length_c                   16.906(3)
_cell_measurement_reflns_used    5099
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.56
_cell_measurement_theta_min      2.16
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_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.991
_diffrn_measured_fraction_theta_max 0.941
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0222
_diffrn_reflns_av_unetI/netI     0.0491
_diffrn_reflns_Laue_measured_fraction_full 0.991
_diffrn_reflns_Laue_measured_fraction_max 0.941
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       15
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_diffrn_reflns_limit_l_min       -19
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_diffrn_reflns_point_group_measured_fraction_full 0.991
_diffrn_reflns_point_group_measured_fraction_max 0.941
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.622
_diffrn_reflns_theta_min         2.303
_exptl_absorpt_coefficient_mu    4.462
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.122
_exptl_crystal_description       block
_exptl_crystal_F_000             1314
_exptl_crystal_size_max          0.240
_exptl_crystal_size_mid          0.230
_exptl_crystal_size_min          0.220
_refine_diff_density_max         2.452
_refine_diff_density_min         -1.199
_refine_diff_density_rms         0.152
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_refine_ls_extinction_method     none
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_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     617
_refine_ls_number_reflns         9281
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.020
_refine_ls_R_factor_all          0.0444
_refine_ls_R_factor_gt           0.0335
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0264P)^2^+3.2857P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0683
_refine_ls_wR_factor_ref         0.0725
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                7798
_reflns_number_total             9281
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            ICA-2020-511-119843.cif
_cod_data_source_block           1
_cod_original_cell_volume        2126.0(6)
_cod_database_code               1564182
_shelx_estimated_absorpt_t_min   0.414
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_shelx_res_checksum              56015
_shelx_hkl_checksum              80352