Novel ferrocenyl functionalised phosphinecarboxamides: synthesis, characterisation and coordination.
Navrátil, Michal; Faria, Erica N.; Panahy, Geve; Císařová, Ivana; Goicoechea, Jose M.; Štěpnička, Petr; Dalton transactions (Cambridge, England : 2003) 49 (2020) 8645–8651; doi:10.1039/d0dt01908a

data_7704654
_publ_section_title
;
 Novel ferrocenyl functionalised phosphinecarboxamides: synthesis,
 characterisation and coordination.
;
_journal_issue                   25
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              8645
_journal_page_last               8651
_journal_paper_doi               10.1039/d0dt01908a
_journal_volume                  49
_journal_year                    2020
_chemical_formula_moiety         'C20 H24 Cl2 Fe N O P Ru'
_chemical_formula_sum            'C20 H24 Cl2 Fe N O P Ru'
_chemical_formula_weight         553.19
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_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
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_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2020-05-26 deposited with the CCDC.	2020-06-10 downloaded from the CCDC.
;
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_cell_measurement_temperature    120(2)
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_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker D8 VENTURE Kappa Duo PHOTON 100 CMOS'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_monochromator  'Quazar Mo multilayer optic'
_diffrn_radiation_source         'I\mS micro-focus sealed tube'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0176P)^2^+1.9770P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                4245
_reflns_number_total             4784
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           mn135
_cod_depositor_comments
'Adding full bibliography for 7704652--7704657.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7704654
_shelx_shelxl_version_number     2014/7
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