Phosphido-bis(borane) complexes of the alkaline earth metals.
Izod, Keith; Watson, James M.; Harrington, Ross W.; Clegg, William; Dalton transactions (Cambridge, England : 2003) 50 (2021) 1019–1024; doi:10.1039/d0dt03895d

data_7706214
_publ_section_title
;
 Phosphido-bis(borane) complexes of the alkaline earth metals.
;
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'Dalton transactions (Cambridge, England : 2003)'
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_journal_paper_doi               10.1039/d0dt03895d
_journal_volume                  50
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_chemical_formula_moiety         'C42 H92 B4 Ca O4 P2 Si4'
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2020-12-03 deposited with the CCDC.	2020-12-14 downloaded from the CCDC.
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CrysAlisPro, Oxford Diffraction Ltd.,
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CrysAlisPro, Oxford Diffraction Ltd.,
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CrysAlisPro, Oxford Diffraction Ltd.,
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'Oxford Diffraction Gemini A Ultra diffractometer'
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_diffrn_source                   'Enhance (Mo) X-ray Source'
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CrysAlisPro, Oxford Diffraction Ltd.,
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Empirical absorption correction using spherical harmonics,
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_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.087
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       lath
_exptl_crystal_F_000             2008
_exptl_crystal_recrystallization_method
'Re-crystallisation from solvent: toluene and THF'
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0453P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_gt                3590
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'Adding full bibliography for 7706210--7706214.cif.'
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_shelx_shelxl_version_number     2018/3
_shelx_estimated_absorpt_t_min   0.889
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