<i>catena</i>-Poly[bis(<i>O</i>,<i>O</i>'-diethyldithiophosphato-<i>S</i>)zinc(II)-μ-4,4'-bipyridyl-<i>N</i>:<i>N</i>']
Zhu, D.-L.; Yu, Y.-P.; Guo, G.-C.; Zhuang, H.-H.; Huang, J.-S.; Liu, Q.; Xu, Z.; You, X.-Z.; Acta Crystallographica Section C 52 (1996) 1963–1966; doi:10.1107/S010827019600368X

data_2005275
_publ_section_title
<i>catena</i>-Poly[bis(<i>O</i>,<i>O</i>'-diethyldithiophosphato-<i>S</i>)zinc(II)-\m-4,4'-bipyridyl-<i>N</i>:<i>N</i>']
_journal_issue                   8
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1963
_journal_page_last               1966
_journal_paper_doi               10.1107/S010827019600368X
_journal_volume                  52
_journal_year                    1996
_chemical_formula_iupac          '[Zn (C4 H10 O2 P S2)2 (C10 H8 N2)]'
_chemical_formula_moiety         'C18 H28 N2 O4 P2 S4 Zn'
_chemical_formula_sum            'C18 H28 N2 O4 P2 S4 Zn'
_chemical_formula_weight         592.03
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                103.18(3)
_cell_angle_beta                 93.98(4)
_cell_angle_gamma                110.49(3)
_cell_formula_units_Z            4
_cell_length_a                   15.328(7)
_cell_length_b                   15.621(6)
_cell_length_c                   12.427(4)
_cell_measurement_reflns_used    20
_cell_measurement_temperature    296
_cell_measurement_theta_max      6
_cell_measurement_theta_min      1.5
_cell_volume                     2677(2)
_diffrn_measurement_device       'Rigaku AFC-5R'
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.08
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            9819
_diffrn_reflns_theta_max         25
_diffrn_standards_decay_%        1.8
_diffrn_standards_interval_count 250
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    1.381
_exptl_absorpt_correction_T_max  0.9800
_exptl_absorpt_correction_T_min  0.7446
_exptl_absorpt_correction_type
'\y scans (TEXSAN; Molecular Structure Corporation, 1985)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.469
_exptl_crystal_description       prism
_exptl_crystal_size_max          0.55
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.25
_refine_diff_density_max         0.78
_refine_diff_density_min         -0.72
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   1.68
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     520
_refine_ls_number_reflns         6259
_refine_ls_R_factor_obs          0.055
_refine_ls_shift/esd_max         0.01
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/\s^2^(F)'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.070
_reflns_number_observed          6259
_reflns_number_total             9413
_reflns_observed_criterion       I>3\s(I)
_cod_data_source_file            mu1140.cif
_cod_data_source_block           mu1140a
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value '1/\s^2^(F)' was changed to
'calc'. New tag '_refine_ls_weighting_details' was created. The value
of the new tag was set to 'w = 1/\s^2^(F)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_database_code               2005275