Nickelalactones with an allyl subunit - the effect of penta-coordination on structures and stability.
Freund, Robert R. A.; Görls, Helmar; Langer, Jens; Dalton transactions (Cambridge, England : 2003) 43 (2014) 13988–14000; doi:10.1039/c4dt01863j

data_7031737
_publ_section_title
;
 Nickelalactones with an allyl subunit - the effect of penta-coordination
 on structures and stability.
;
_journal_issue                   37
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              13988
_journal_page_last               14000
_journal_paper_doi               10.1039/c4dt01863j
_journal_volume                  43
_journal_year                    2014
_chemical_formula_moiety         'C34 H60 Ni P2, C4 H8 O'
_chemical_formula_sum            'C38 H68 Ni O P2'
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_cell_angle_gamma                90.00
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_cell_volume                     3620.82(9)
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_computing_data_collection       COLLECT
_computing_data_reduction        DENZO
_computing_molecular_graphics    SHELXTL/PC
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_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
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_diffrn_measured_fraction_theta_max 0.996
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_diffrn_measurement_method       'phi- + omega-scan'
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_exptl_absorpt_coefficient_mu    0.652
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            orange
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_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1448
_exptl_crystal_size_max          0.066
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0337P)^2^+2.8035P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     >2sigma(I)
_publcif_datablock.id            {a6f4d565-93b5-43ae-9e8e-7b43699d9bc8}
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_cod_depositor_comments
'Adding full bibliography for 7031730--7031737.cif.'
_cod_original_cell_volume        3620.75(9)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               7031737