The Ordered [WO2F4]2- Anion
Margaret E. Welk; Alexander J. Norquist; Charlotte L. Stern; Kenneth R. Poeppelmeier; Inorganic Chemistry 40 (2001) 5479–5480; doi:10.1021/ic015554x

data_4320447
_publ_section_title
;
 The Ordered [WO2F4]2- Anion
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              5479
_journal_page_last               5480
_journal_paper_doi               10.1021/ic015554x
_journal_volume                  40
_journal_year                    2001
_chemical_formula_sum            'C32 H36 Cu F8 N6 O6 W2'
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_symmetry_cell_setting           monoclinic
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_cell_angle_gamma                90.00(1)
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_cell_length_c                   21.424(3)
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_cell_measurement_temperature    296.2
_cell_measurement_theta_max      0.0
_cell_measurement_theta_min      0.0
_cell_volume                     3755.7(13)
_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
_computing_data_reduction        'teXsan for Windows (MSC, 1997)'
_computing_publication_material  'teXsan for Windows (MSC, 1997)'
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;
SHELX97 (Sheldrick, 1997)
;
_diffrn_ambient_temperature      296.2
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_diffrn_radiation_detector       'scintillation counter'
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_diffrn_radiation_source         'Rigaku rotating anode'
_diffrn_radiation_type           'Mo K\a'
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_diffrn_reflns_limit_l_min       -28
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_diffrn_reflns_reduction_process 'Lp corrections applied'
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_diffrn_standards_decay_%        0.00
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_exptl_absorpt_correction_type   none
_exptl_crystal_colour            blue
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_refine_ls_R_factor_all          0.0201
_refine_ls_R_factor_gt           0.0200
_refine_ls_shift/su_max          2.0900
_refine_ls_shift/su_mean         0.0072
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo)]'
_refine_ls_weighting_scheme      sigma
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_cod_data_source_file            ic015554x_s.cif
_cod_data_source_block           '_s11j.cif'
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        3756(1)
_cod_original_sg_symbol_H-M      'C 2/c '
_cod_original_formula_sum        'C32 H36 Cu F8 N6 O6 W2 '
_cod_database_code               4320447