Double butterfly-shaped octanuclear dysprosium clusters: structure, magnetism and assembly mechanism
Li, Yun-Lan; Huang, Zhong-Ming; Wang, Hai-Ling; Zhu, Zhong-Hong; Liang, Fu-Pei; Zou, Hua-Hong; CrystEngComm 25 (2023) 225–232; doi:10.1039/D2CE01506D

data_7245922
_publ_section_title
;
 Double butterfly-shaped octanuclear dysprosium clusters: structure,
 magnetism and assembly mechanism
;
_journal_issue                   2
_journal_name_full               CrystEngComm
_journal_page_first              225
_journal_page_last               232
_journal_paper_doi               10.1039/D2CE01506D
_journal_volume                  25
_journal_year                    2023
_chemical_formula_sum            'C78 H134 Dy8 N20 O46'
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_space_group_name_Hall           '-P 1'
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_audit_update_record
;
2022-11-04 deposited with the CCDC.	2022-11-28 downloaded from the CCDC.
;
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_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
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_diffrn_measurement_device_type  'XtaLAB Synergy, Dualflex, HyPix'
_diffrn_radiation_type           CuK\a
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_diffrn_reflns_point_group_measured_fraction_full 0.998
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_diffrn_reflns_theta_max         75.784
_diffrn_reflns_theta_min         2.705
_exptl_absorpt_coefficient_mu    30.668
_exptl_crystal_colour            brown
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_exptl_crystal_description       block
_exptl_crystal_F_000             1638
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_refine_ls_extinction_method     none
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1958P)^2^+1.3300P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           20220113-lfp-lyl-4942-2
_cod_depositor_comments
'Adding full bibliography for 7245922--7245923.cif.'
_cod_original_cell_volume        2628.60(8)
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_shelx_shelxl_version_number     2014/7
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