Organic Amides as Suitable Precursors to Stabilize Stannylenes
Álvarez-Rodríguez, Lucía; Cabeza, Javier A.; García-Álvarez, Pablo; Polo, Diego; Organometallics 32 (2013) 3557–; doi:10.1021/om400476c

data_4089556
_publ_section_title
;
 Organic Amides as Suitable Precursors to Stabilize Stannylenes
;
_journal_issue                   12
_journal_name_full               Organometallics
_journal_page_first              3557
_journal_paper_doi               10.1021/om400476c
_journal_volume                  32
_journal_year                    2013
_chemical_formula_moiety         'C15 H36 N2 O Si2 Sn'
_chemical_formula_sum            'C15 H36 N2 O Si2 Sn'
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_cell_angle_beta                 96.0690(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
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_computing_cell_refinement
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CrysAlisPro, Agilent Technologies,
Version 1.171.35.19 (release 27-10-2011 CrysAlis171 .NET)
(compiled Oct 27 2011,15:02:11)
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_computing_data_collection
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CrysAlisPro, Agilent Technologies,
Version 1.171.35.19 (release 27-10-2011 CrysAlis171 .NET)
(compiled Oct 27 2011,15:02:11)
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_computing_data_reduction
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CrysAlisPro, Agilent Technologies,
Version 1.171.35.19 (release 27-10-2011 CrysAlis171 .NET)
(compiled Oct 27 2011,15:02:11)
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_computing_molecular_graphics    'PLATON (Spek, 2008)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 2008)'
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_computing_structure_solution    'SIR-97 (Giacovazzo, 1999)'
_diffrn_ambient_temperature      123(2)
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_diffrn_reflns_limit_l_min       -19
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_diffrn_reflns_theta_full        67.25
_diffrn_reflns_theta_max         67.25
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_exptl_absorpt_coefficient_mu    10.368
_exptl_absorpt_correction_T_max  1.00000
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_exptl_absorpt_correction_type   multi-scan
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CrysAlisPro, Agilent Technologies,
Version 1.171.35.19 (release 27-10-2011 CrysAlis171 .NET)
(compiled Oct 27 2011,15:02:11)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
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_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.325
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       fragment
_exptl_crystal_F_000             904
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_exptl_crystal_size_mid          0.1394
_exptl_crystal_size_min          0.1119
_refine_diff_density_max         0.485
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_refine_ls_extinction_method     none
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0323P)^2^+0.7559P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0565
_refine_ls_wR_factor_ref         0.0578
_reflns_number_gt                3695
_reflns_number_total             3911
_reflns_threshold_expression     >2\s(I)
_cod_data_source_file            om400476c_si_003.cif
_cod_data_source_block           xn12187-pga109
_cod_depositor_comments
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The following automatic conversions were performed:

data item '_symmetry_cell_setting' value 'MONOCLINIC' was changed to
'monoclinic' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/ACS/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4089556