Oxidation of Complexes by (O2CPh)2 and (ER)2 (E = S, Se), Including Structures of Pd(CH2CH2CH2CH2)(SePh)2(bpy) (bpy = 2,2'-Bipyridine) and MMe2(SePh)2(L2) (M = Pd, Pt; L2= bpy, 1,10-Phenanthroline) and C...O and C...E Bond Formation at Palladium(IV)
Allan J. Canty; Hong Jin; Brian W. Skelton; Allan H. White; Inorganic Chemistry 37 (1998) 3975–3981; doi:10.1021/ic9715005

data_4322927
_publ_contact_author
;
     A.J.Canty
     University of Tasmania
     Chemistry Department
     P.O. Box 252C
     Hobart
     Tasmania, Tasmania
;
_publ_contact_author_email       Allan.Canty@utas.edu.au
_publ_contact_author_fax         036_2262_858
_publ_contact_author_phone       036_2262_162
_publ_section_title
;
 Oxidation of Complexes by (O2CPh)2 and (ER)2 (E = S, Se), Including
 Structures of Pd(CH2CH2CH2CH2)(SePh)2(bpy) (bpy = 2,2'-Bipyridine) and
 MMe2(SePh)2(L2) (M = Pd, Pt; L2= bpy, 1,10-Phenanthroline) and C...O and
 C...E Bond Formation at Palladium(IV)
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              3975
_journal_page_last               3981
_journal_paper_doi               10.1021/ic9715005
_journal_volume                  37
_journal_year                    1998
_chemical_formula_analytical     'C26 H24 N2 Pt Se2'
_chemical_formula_moiety         '[(C12H8N2)(CH3)2(C6H5Se)2Pt]'
_chemical_formula_sum            'C26 H24 N2 Pt Se2'
_chemical_formula_weight         717.49
_chemical_name_systematic
'[Dimethyl(1,10-phenanthroline)bis(selenophenolato)platinum(IV)]'
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_cell_angle_beta                 90.00000
_cell_angle_gamma                90.00000
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_computing_publication_material  xtal_BONDLA_CIFIO
_computing_structure_refinement  xtal_CRYLSQ
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_diffrn_reflns_limit_k_min       -19
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_diffrn_reflns_limit_l_min       -35
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_diffrn_reflns_theta_min         1.68
_diffrn_standards_decay_%        0
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_exptl_crystal_colour            orange
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_exptl_crystal_F_000             2720
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_refine_diff_density_max         0.99
_refine_diff_density_min         -.966
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_refine_ls_extinction_expression Eq22_p292_"Cryst._Comp."_Munksgaard_1970
_refine_ls_extinction_method     Zachariasen
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_refine_ls_goodness_of_fit_obs   1.078
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_refine_ls_R_factor_all          .074
_refine_ls_R_factor_obs          .036
_refine_ls_shift/esd_max         .074
_refine_ls_shift/esd_mean        .004
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         .058
_refine_ls_wR_factor_obs         .043
_reflns_d_resolution_high        .712
_reflns_d_resolution_low         12.117
_reflns_limit_h_max              19
_reflns_limit_h_min              0
_reflns_limit_k_max              19
_reflns_limit_k_min              0
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_reflns_limit_l_min              0
_reflns_number_observed          2098
_reflns_number_total             3531
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_cod_data_source_file            ic9715005_5.cif
_cod_data_source_block           iptsep
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_hydrogen_treatment' value 'constrained' was replaced with
the value 'constr' as specified in the replacement file
'src/cod-tools/trunk/data/replacement-values/replacement_values.lst'.

Automatic conversion script
Id: cif_fix_values 5376 2017-05-30 11:51:03Z andrius 
;
_cod_original_cell_volume        4838(6)
_cod_original_sg_symbol_Hall     -i_4ad
_cod_original_sg_symbol_H-M      'I 41/a'
_cod_database_code               4322927