Synthesis and structure of a new bulky bis(alkoxide) ligand on a terphenyl platform
Kurup, Sudheer S.; Nasser, Sandra; Ward, Cassandra L.; Groysman, Stanislav; Acta Crystallographica Section E 78 (2022) 92–96; doi:10.1107/S2056989021013438

data_2243964
_publ_section_title
;
 Synthesis and structure of a new bulky bis(alkoxide) ligand on a
 terphenyl platform
;
_journal_coeditor_code           JY2014
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              92
_journal_page_last               96
_journal_paper_doi               10.1107/S2056989021013438
_journal_volume                  78
_journal_year                    2022
_chemical_formula_iupac          'C36 H50 O2, C H2 Cl2'
_chemical_formula_moiety         'C36 H50 O2, C H2 Cl2'
_chemical_formula_sum            'C37 H52 Cl2 O2'
_chemical_formula_weight         599.68
_chemical_name_systematic
;
3,3'-([1,1':4',1''-Terphenyl]-2,2''-diyl)bis(2,2,4,4-tetramethylpentan-3-ol)
dichloromethane monosolvate
;
_space_group_crystal_system      triclinic
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Olex2 1.5
(compiled 2021.11.18 svn.ra9532c28 for OlexSys, GUI svn.r6429)
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SAINT (Bruker, 2016)
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APEX2 (Bruker, 2016)
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SAINT (Bruker, 2016)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>,  2009)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>,  2009)
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<i>SHELXL2018/3</i> (Sheldrick, 2015b)
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<i>SHELXT2018/2</i> (Sheldrick, 2015a)
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;
(SADABS; Krause <i>et al.</i>,  2015)
;
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0594P)^2^+0.6108P] where P=(Fo^2^+2Fc^2^)/3'
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