Competitive isomerization and catalyst decomposition during ring-closing metathesis
Killeen, Charles; Liu, Jie; Zijlstra, Harmen S.; Maass, Florian; Piers, James; Adams, Reid; Oliver, Allen; McIndoe, J. Scott; Catalysis Science & Technology 13 (2023) 4000–4008; doi:10.1039/D3CY00065F

data_1569292
_publ_section_title
;
 Competitive isomerization and catalyst decomposition during ring-closing
 metathesis
;
_journal_issue                   13
_journal_name_full               'Catalysis Science &amp; Technology'
_journal_page_first              4000
_journal_page_last               4008
_journal_paper_doi               10.1039/D3CY00065F
_journal_volume                  13
_journal_year                    2023
_chemical_formula_moiety         'C14 H28 N, F6 P'
_chemical_formula_sum            'C14 H28 F6 N P'
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_chemical_name_systematic        'dibutyldiallylammonium hexafluorophosphate'
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_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
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_audit_update_record
;
2022-10-21 deposited with the CCDC.	2023-06-02 downloaded from the CCDC.
;
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_computing_molecular_graphics    'Bruker XP (Bruker, 2015)'
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_diffrn_measurement_device_type  'Bruker APEX-II'
_diffrn_measurement_method       'combination of \w and \f-scans '
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_point_group_measured_fraction_full 1.000
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'Re-crystallisation from solvent: Ethanol'
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0379P)^2^+0.8483P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_depositor_comments
'Adding full bibliography for 1569291--1569292.cif.'
_cod_original_cell_volume        1771.4(4)
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               1569292
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_shelx_res_checksum              37076
_shelx_hkl_checksum              97082