Synthesis and structure of the extended phosphazane ligand [(1,4-C6H4){N(μ-PN(t)Bu)2N(t)Bu}2](4.).
Sevilla, Raquel; Less, Robert J.; García-Rodríguez, Raúl; Bond, Andrew D.; Wright, Dominic S.; Dalton transactions (Cambridge, England : 2003) 45 (2016) 1868–1871; doi:10.1039/c5dt04393j

data_7037519
_publ_section_title
;
 Synthesis and structure of the extended phosphazane ligand
 [(1,4-C6H4){N(\m-PN(t)Bu)2N(t)Bu}2](4.).
;
_journal_issue                   5
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1868
_journal_page_last               1871
_journal_paper_doi               10.1039/c5dt04393j
_journal_volume                  45
_journal_year                    2016
_chemical_formula_moiety         'C30 H62 N8 P4'
_chemical_formula_sum            'C30 H62 N8 P4'
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_space_group_name_Hall           '-P 1'
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_audit_update_record
;
2015-11-04 deposited with the CCDC.
2015-12-02 downloaded from the CCDC.
;
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'HKL Denzo and Scalepack (Otwinowski & Minor, 1997)'
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_diffrn_measurement_device_type  'Nonius KappaCCD'
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+3.2317P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7037519--7037522.cif.'
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_cambridge_user_name             'Raquel Sevilla-Martin'
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_cambridge_supervisor_name       'Dominic Wright'
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