Synthesis of quinolinyl-based pincer copper(ii) complexes: an efficient catalyst system for Kumada coupling of alkyl chlorides and bromides with alkyl Grignard reagents.
Pandiri, Hanumanprasad; Gonnade, Rajesh G.; Punji, Benudhar; Dalton transactions (Cambridge, England : 2003) 47 (2018) 16747–16754; doi:10.1039/c8dt03210f

data_7047828
_publ_section_title
;
 Synthesis of quinolinyl-based pincer copper(ii) complexes: an efficient
 catalyst system for Kumada coupling of alkyl chlorides and bromides with
 alkyl Grignard reagents.
;
_journal_issue                   46
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              16747
_journal_page_last               16754
_journal_paper_doi               10.1039/c8dt03210f
_journal_volume                  47
_journal_year                    2018
_chemical_formula_moiety         'C15 H18 Cl Cu N3 O'
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_symmetry_space_group_name_Hall  '-C 2yc'
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;
2018-03-27 deposited with the CCDC.
2018-10-19 downloaded from the CCDC.
;
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_diffrn_measurement_device       '\k-geometry diffractometer'
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0258P)^2^+3.8293P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_total             4633
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_cod_data_source_file            c8dt03210f2.cif
_cod_data_source_block           mo_HP_CuSb_230117_0m
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'MULTI-SCAN' changed to
'multi-scan' according to
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 

 Adding full bibliography for 7047827--7047830.cif.
;
_cod_database_code               7047828
_shelx_shelxl_version_number     2014/7
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_shelx_res_checksum              69740