Correction to Palladium-Catalyzed Synthesis of Dibenzophosphole Oxides via Intramolecular Dehydrogenative Cyclization
Yoichiro Kuninobu; Takuya Yoshida; Kazuhiko Takai; Journal of Organic Chemistry 77 (2012) 9436–9436; doi:10.1021/jo3021506

data_4027621
_publ_section_title
;
 Correction to Palladium-Catalyzed Synthesis of Dibenzophosphole Oxides
 via Intramolecular Dehydrogenative Cyclization
;
_journal_name_full               'Journal of Organic Chemistry'
_journal_page_first              9436
_journal_page_last               9436
_journal_paper_doi               10.1021/jo3021506
_journal_volume                  77
_journal_year                    2012
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_cell_length_b                   11.528(3)
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_cell_measurement_theta_max      27.48
_cell_measurement_theta_min      3.32
_cell_volume                     1653.5(7)
_computing_cell_refinement       CrystalClear
_computing_data_collection       'CrystalClear (Rigaku, ????)'
_computing_data_reduction        CrystalClear
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_computing_structure_solution    'Il Milione (Burla, et al., 2007)'
_diffrn_ambient_temperature      153
_diffrn_detector_area_resol_mean 7.111
_diffrn_measured_fraction_theta_full 0.991
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'Rigaku Saturn724'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71075
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_diffrn_reflns_limit_l_max       20
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_diffrn_reflns_theta_full        27.46
_diffrn_reflns_theta_max         27.47
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_exptl_absorpt_coefficient_mu    0.170
_exptl_absorpt_correction_T_max  0.966
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_exptl_absorpt_correction_type   multi-scan
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_exptl_crystal_size_max          0.300
_exptl_crystal_size_mid          0.200
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_refine_ls_extinction_method     none
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_refine_ls_shift/su_max          0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^)+(0.0691P)^2^+0.7884P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1479
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_cod_data_source_file            jo3021506_si_001.cif
_cod_data_source_block           145-11427
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