Hydroxylammonium Sulfate
Mirceva, A.; Golic, L.; Acta Crystallographica Section C 51 (1995) 798–800; doi:10.1107/S0108270194013351

data_2003442
_publ_section_title
;
 Hydroxylammonium Sulfate
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              798
_journal_page_last               800
_journal_paper_doi               10.1107/S0108270194013351
_journal_volume                  51
_journal_year                    1995
_chemical_compound_source        ' recrystallization of the commercial product'
_chemical_formula_moiety         'H8 N2 O6 S1'
_chemical_formula_sum            'H8 N2 O6 S'
_chemical_formula_weight         164.14
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_type_scat_source           'Cromer & Mann (1968)'
_cell_angle_alpha                90.
_cell_angle_beta                 106.93(3)
_cell_angle_gamma                90.
_cell_formula_units_Z            4
_cell_length_a                   7.932(2)
_cell_length_b                   7.321(2)
_cell_length_c                   10.403(3)
_cell_measurement_reflns_used    45
_cell_measurement_temperature    293(1)
_cell_measurement_theta_max      13
_cell_measurement_theta_min      10
_cell_volume                     577.9(3)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.026
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            4180
_diffrn_reflns_theta_max         30
_diffrn_standards_decay_%        1.09
_diffrn_standards_interval_count 165
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.510
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.886
_exptl_crystal_density_meas      1.90(1)
_exptl_crystal_density_method    flotation
_exptl_crystal_description       'approximately prismatic'
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.41
_exptl_crystal_size_min          0.33
_refine_diff_density_max         0.24
_refine_diff_density_min         -0.52
_refine_ls_extinction_coef       'g = 2.9(3)'
_refine_ls_extinction_method     'Larson (1967)'
_refine_ls_goodness_of_fit_obs   0.363
_refine_ls_hydrogen_treatment    refall
_refine_ls_number_parameters     115
_refine_ls_number_reflns         1578
_refine_ls_R_factor_obs          0.026
_refine_ls_shift/esd_max         0.181
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      'Weighting scheme: empirical'
_refine_ls_wR_factor_obs         0.026
_reflns_number_observed          1520
_reflns_number_total             1688
_reflns_observed_criterion       I>2.5\s(I)
_cod_data_source_file            du1099.cif
_cod_data_source_block           du1099a
_cod_original_cell_volume        577.9(5)
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'H8 N2 O6 S1'
_cod_database_code               2003442