Tri-<i>tert</i>-butyl 3,3',3''-(aminomethanetriyl)tripropanoate
Weber, Edwin; Langer, Joachim; Seichter, Wilhelm; Acta Crystallographica Section E 63 (2007) o2064–o2065; doi:10.1107/S1600536807012615

data_2213543
_publ_section_title
;
 Tri-<i>tert</i>-butyl 3,3',3''-(aminomethanetriyl)tripropanoate
;
_journal_coeditor_code           SI2006
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o2064
_journal_page_last               o2065
_journal_paper_doi               10.1107/S1600536807012615
_journal_volume                  63
_journal_year                    2007
_chemical_formula_iupac          'C22 H41 N O6'
_chemical_formula_moiety         'C22 H41 N O6'
_chemical_formula_sum            'C22 H41 N O6'
_chemical_formula_weight         415.56
_chemical_name_systematic
;
Tri-tert-butyl 3,3',3"-(aminomethanetriyl)tripropanoate
;
_space_group_IT_number           33
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_symmetry_space_group_name_H-M   'P n a 21'
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_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
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_cell_measurement_reflns_used    9475
_cell_measurement_temperature    93(2)
_cell_measurement_theta_max      32.48
_cell_measurement_theta_min      3.31
_cell_volume                     2443.65(15)
_computing_cell_refinement       'SAINT-NT (Bruker, 2004)'
_computing_data_collection       'SMART (Bruker, 2004)'
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_computing_structure_solution    'SHELXS97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      93(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker SMART CCD area-detector'
_diffrn_measurement_method       '\f and \w'
_diffrn_radiation_monochromator  graphite
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_exptl_crystal_colour            colourless
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_exptl_crystal_description       irregular
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0693P)^2^+0.1594P] where P=(Fo^2^+2Fc^2^)/3'
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