Microwave-Promoted, Metal- and Catalyst-Free Decarboxylative α,β-Difunctionlization of Secondary α-Amino Acids via Pseudo-Four-Component Reactions.
Manjappa, Kiran B.; Jhang, Wei-Fang; Huang, Shin-Yi; Yang, Ding-Yah; Organic letters 16 (2014) 5690–5693; doi:10.1021/ol5027574

data_1518118
_publ_section_title
;
 Microwave-Promoted, Metal- and Catalyst-Free Decarboxylative
 \a,\b-Difunctionlization of Secondary \a-Amino Acids via
 Pseudo-Four-Component Reactions.
;
_journal_issue                   21
_journal_name_full               'Organic letters'
_journal_page_first              5690
_journal_page_last               5693
_journal_paper_doi               10.1021/ol5027574
_journal_volume                  16
_journal_year                    2014
_chemical_formula_moiety         'C23 H19 N O3 S2'
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_cell_formula_units_Z            4
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_cell_measurement_reflns_used    2544
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_computing_cell_refinement
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CrysAlis RED, Oxford Diffraction Ltd., 
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Empirical absorption correction using spherical harmonics, 
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_refine_ls_structure_factor_coef Fsqd
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'calc w=1/[\s^2^(Fo^2^)+(0.0426P)^2^+0.7376P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_data_source_file            ol5027574_si_004.cif
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_cod_depositor_comments
'Adding full bibliography for 1518118--1518120.cif.'
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               1518118