Structural and magnetic properties of oxyquinolinate clusters of cobalt(ii) and manganese(ii) and serendipitous intake of carbonate during synthesis.
Khakhlary, Prithiviraj; E Anson, Christopher; Mondal, Abhishake; Powell, Annie K.; Baruah, Jubaraj B.; Dalton transactions (Cambridge, England : 2003) 44 (2015) 2964–2969; doi:10.1039/c4dt02999b

data_7033528
_publ_section_title
;
 Structural and magnetic properties of oxyquinolinate clusters of
 cobalt(ii) and manganese(ii) and serendipitous intake of carbonate during
 synthesis.
;
_journal_issue                   7
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2964
_journal_page_last               2969
_journal_paper_doi               10.1039/c4dt02999b
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety         'C54 H36 Cl2 Co4 N6 O6'
_chemical_formula_sum            'C54 H36 Cl2 Co4 N6 O6'
_chemical_formula_weight         1171.51
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2014-12-19 deposited with the CCDC.
2015-01-07 downloaded from the CCDC.
;
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_cell_measurement_theta_max      21.66
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_cell_volume                     2477.33(17)
_computing_cell_refinement       'Bruker SMART'
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_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
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_diffrn_measured_fraction_theta_max 0.986
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0631P)^2^+1.1308P] where P=(Fo^2^+2Fc^2^)/3'
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'Adding full bibliography for 7033526--7033528.cif.'
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