Poly[[diaquabis(2,2'-bipyridine-κ^2^<i>N</i>,<i>N</i>')(μ~3~-5-hydroxyisophthalato-κ^5^<i>O</i>^1^,<i>O</i>^1'^:<i>O</i>^3^,<i>O</i>^3'^:<i>O</i>^3'^)(μ~3~-5-hydroxyisophthalato-κ^4^<i>O</i>^1^,<i>O</i>^1'^:<i>O</i>^3^:<i>O</i>^3'^)(μ~2~-5-hydroxyisophthalato-κ^3^<i>O</i>^1^,<i>O</i>^1'^:<i>O</i>^3^)didysprosium(III)] dihydrate]
Zhang, Yan-Lin; Acta Crystallographica Section E 67 (2011) m1473–m1474; doi:10.1107/S1600536811039080

data_2231926
_publ_section_title
;
 Poly[[diaquabis(2,2'-bipyridine-\k^2^<i>N</i>,<i>N</i>')(\m~3~-5-hydroxyisophthalato-\k^5^<i>O</i>^1^,<i>O</i>^1'^:<i>O</i>^3^,<i>O</i>^3'^:<i>O</i>^3'^)(\m~3~-5-hydroxyisophthalato-\k^4^<i>O</i>^1^,<i>O</i>^1'^:<i>O</i>^3^:<i>O</i>^3'^)(\m~2~-5-hydroxyisophthalato-\k^3^<i>O</i>^1^,<i>O</i>^1'^:<i>O</i>^3^)didysprosium(III)]
 dihydrate]
;
_journal_coeditor_code           HY2467
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1473
_journal_page_last               m1474
_journal_paper_doi               10.1107/S1600536811039080
_journal_volume                  67
_journal_year                    2011
_chemical_formula_iupac
'[Dy2 (C8 H4 O5)3 (C10 H8 N2)2 (H2 O)2] , 2H2 O'
_chemical_formula_moiety         'C44 H32 Dy2 N4 O17, 2(H2 O)'
_chemical_formula_sum            'C44 H36 Dy2 N4 O19'
_chemical_formula_weight         1249.77
_chemical_name_systematic
;
Poly[[diaquabis(2,2'-bipyridine-\k^2^<i>N</i>,<i>N</i>')(\m~3~-5-
hydroxyisophthalato-
\k^5^<i>O</i>^1^,<i>O</i>^1'^:<i>O</i>^3^,<i>O</i>^3'^:<i>O</i>^3'^)(\m~3~-
5-hydroxyisophthalato-
\k^4^<i>O</i>^1^,<i>O</i>^1'^:<i>O</i>^3^:<i>O</i>^3'^)(\m~2~-5-
hydroxyisophthalato-\k^3^<i>O</i>^1^,<i>O</i>^1'^:<i>O</i>^3^)didysprosium(III)]
dihydrate]
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                91.3100(10)
_cell_angle_beta                 103.1870(10)
_cell_angle_gamma                106.5050(10)
_cell_formula_units_Z            2
_cell_length_a                   11.3736(5)
_cell_length_b                   12.0349(6)
_cell_length_c                   17.8360(8)
_cell_measurement_reflns_used    7036
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      25.2
_cell_measurement_theta_min      2.34
_cell_volume                     2269.00(18)
_computing_cell_refinement       'SAINT (Bruker, 2007)'
_computing_data_collection       'APEX2 (Bruker, 2007)'
_computing_data_reduction        'SAINT (Bruker, 2007)'
_computing_molecular_graphics
'DIAMOND (Brandenburg, 1999) and SHELXTL (Sheldrick, 2008)'
_computing_publication_material  'SHELXTL (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.981
_diffrn_measured_fraction_theta_max 0.981
_diffrn_measurement_device_type  'Bruker APEXII CCD'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0201
_diffrn_reflns_av_sigmaI/netI    0.0371
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            11732
_diffrn_reflns_theta_full        25.20
_diffrn_reflns_theta_max         25.20
_diffrn_reflns_theta_min         1.77
_exptl_absorpt_coefficient_mu    3.352
_exptl_absorpt_correction_T_max  0.5396
_exptl_absorpt_correction_T_min  0.4879
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Bruker, 2001)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.829
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1224
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.21
_refine_diff_density_max         2.647
_refine_diff_density_min         -1.248
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.062
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     624
_refine_ls_number_reflns         8024
_refine_ls_number_restraints     252
_refine_ls_restrained_S_all      1.075
_refine_ls_R_factor_all          0.0398
_refine_ls_R_factor_gt           0.0347
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0438P)^2^+9.6294P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0910
_refine_ls_wR_factor_ref         0.0944
_reflns_number_gt                7052
_reflns_number_total             8024
_reflns_threshold_expression     >2\s(I)
_cod_data_source_file            hy2467.cif
_cod_data_source_block           I
_cod_database_code               2231926
_cod_database_fobs_code          2231926