Synthesis and Structure Determinations of Complexes Containing a Five-Membered Lactam Structure Based on Organohydrazido(2-) Ligands1
Hidetake Seino; Youichi Ishii; Masanobu Hidai; Inorganic Chemistry 36 (1997) 161–171; doi:10.1021/ic960778e

data_4323288
_publ_contact_author
;
   Hidai, Masanobu
   Department of Chemistry and Biotechnology, Graduate School of Engineering,
   the University of Tokyo, Tokyo, Hongo, Bunkyo-ku 113, Japan
;
_publ_contact_author_fax         ' +81 3-(5800)-6945 '
_publ_section_title
;
 Synthesis and Structure Determinations of Complexes Containing a
 Five-Membered Lactam Structure Based on Organohydrazido(2-) Ligands1
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              161
_journal_page_last               171
_journal_paper_doi               10.1021/ic960778e
_journal_volume                  36
_journal_year                    1997
_chemical_formula_sum            'C56 H52 B F5 N2 O P4 W'
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
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_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_audit_creation_date             'Wed Jun 19 09:22:50 1996'
_audit_creation_method           'from TEXRAY.INF file'
_cell_angle_alpha                90
_cell_angle_beta                 110.16(2)
_cell_angle_gamma                90
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_cell_length_a                   17.712(4)
_cell_length_b                   17.933(5)
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_cell_measurement_theta_min      25.21
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_computing_cell_refinement       'MSC/AFC Diffractometer Control'
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_diffrn_measurement_device       AFC7R
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_refine_ls_extinction_method     Zachariasen_type_2_Gaussian_isotropic
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_refine_ls_structure_factor_coef F
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_cod_data_source_block           '[WF(NNCH=CHCH2CO)(dppe)2][BF4]_(11a+BF4-)'
_cod_original_sg_symbol_H-M      'P 21/n '
_cod_original_formula_sum        'C56 H52 W N2 O P4 F5 B'
_cod_database_code               4323288