Silver nanofibers from the nanorods of one-dimensional organometallic coordination polymers
Akhbari, Kamran; Morsali, Ali; CrystEngComm 12 (2010) 3394–; doi:10.1039/c002740e

data_7212613
_publ_section_title
;
 Silver nanofibers from the nanorods of one-dimensional organometallic
 coordination polymers
;
_journal_issue                   11
_journal_name_full               CrystEngComm
_journal_page_first              3394
_journal_paper_doi               10.1039/c002740e
_journal_volume                  12
_journal_year                    2010
_chemical_formula_sum            'C40 H30 Ag2 O4'
_chemical_formula_weight         790.38
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                65.513(4)
_cell_angle_beta                 83.514(5)
_cell_angle_gamma                74.337(4)
_cell_formula_units_Z            2
_cell_length_a                   8.7099(5)
_cell_length_b                   14.3387(8)
_cell_length_c                   14.4473(8)
_cell_measurement_temperature    293(2)
_cell_volume                     1581.04(16)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0312
_diffrn_reflns_av_sigmaI/netI    0.0264
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            18369
_diffrn_reflns_theta_full        26.50
_diffrn_reflns_theta_max         26.50
_diffrn_reflns_theta_min         1.61
_exptl_absorpt_coefficient_mu    1.281
_exptl_crystal_density_diffrn    1.660
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             792
_refine_diff_density_max         2.739
_refine_diff_density_min         -1.819
_refine_diff_density_rms         0.082
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.035
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     415
_refine_ls_number_reflns         6526
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.035
_refine_ls_R_factor_all          0.0466
_refine_ls_R_factor_gt           0.0404
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0434P)^2^+2.9899P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1003
_refine_ls_wR_factor_ref         0.1036
_reflns_number_gt                5815
_reflns_number_total             6526
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c002740e.txt
_cod_data_source_block           morsali7
_cod_original_cell_volume        1581.04(15)
_cod_database_code               7212613