Spin-State Versatility in a Series of Fe4 [2 ×2] Grid Complexes: Effects of Counteranions, Lattice Solvent, and Intramolecular Cooperativity.
Steinert, Markus; Schneider, Benjamin; Dechert, Sebastian; Demeshko, Serhiy; Meyer, Franc; Inorganic chemistry 55 (2016) 2363–2373; doi:10.1021/acs.inorgchem.5b02762

data_4347122
_publ_section_title
;
 Spin-State Versatility in a Series of Fe4 [2 \\times 2] Grid Complexes:
 Effects of Counteranions, Lattice Solvent, and Intramolecular
 Cooperativity.
;
_journal_issue                   5
_journal_name_full               'Inorganic chemistry'
_journal_page_first              2363
_journal_page_last               2373
_journal_paper_doi               10.1021/acs.inorgchem.5b02762
_journal_volume                  55
_journal_year                    2016
_chemical_formula_moiety
'C92 H56 Br4 Fe4 N24 4+, 4(F6 P -), C4 H8 O, C3 H7 N O'
_chemical_formula_sum            'C99 H71 Br4 F24 Fe4 N25 O2 P4'
_chemical_formula_weight         2765.72
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_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Stoe IPDS II'
_diffrn_measurement_method       \w
_diffrn_radiation_type           MoK\a
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_refine_ls_restrained_S_all      1.057
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0630P)^2^+61.3939P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_original_cell_volume        10060.3(5)
_cod_original_sg_symbol_H-M      'C 2/c'
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_shelx_res_checksum              6978
_shelx_hkl_checksum              25070