Role of Electron-Deficient Olefin Ligands in a Ni-Catalyzed Aziridine Cross-Coupling To Generate Quaternary Carbons.
Estrada, Jesús G; Williams, Wendy L.; Ting, Stephen I.; Doyle, Abigail G.; Journal of the American Chemical Society  (2020) –; doi:10.1021/jacs.0c02237

data_4134850
_publ_section_title
;
 Role of Electron-Deficient Olefin Ligands in a Ni-Catalyzed Aziridine
 Cross-Coupling To Generate Quaternary Carbons.
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_paper_doi               10.1021/jacs.0c02237
_journal_year                    2020
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_cell_length_b                   9.556(4)
_cell_length_c                   13.814(8)
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_computing_structure_refinement  'SHELXL-2014 (Sheldrick, 2014)'
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_diffrn_measured_fraction_theta_max 0.997
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_diffrn_reflns_limit_l_min       -21
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_diffrn_reflns_point_group_measured_fraction_max 0.997
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_diffrn_reflns_theta_max         33.291
_diffrn_reflns_theta_min         2.267
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_refine_ls_matrix_type           full
_refine_ls_number_parameters     219
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0564P)^2^+0.1654P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_database_code               4134850
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_shelxl_version_number           2014-3
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_shelx_hkl_checksum              34655