Metal Nitrite: A Powerful Oxidizing Reagent
Baidya, Mahiuddin; Yamamoto, Hisashi; Journal of the American Chemical Society 133 (2011) 13880–13882; doi:10.1021/ja206736q

data_4106738
_publ_section_title
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 Metal Nitrite: A Powerful Oxidizing Reagent
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_journal_coden_ASTM              JACSAT
_journal_issue                   35
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              13880
_journal_page_last               13882
_journal_paper_doi               10.1021/ja206736q
_journal_volume                  133
_journal_year                    2011
_chemical_formula_sum            'C12 H21 N O2'
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_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
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_cell_angle_beta                 100.109(11)
_cell_angle_gamma                104.700(11)
_cell_formula_units_Z            2
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_cell_length_b                   8.188(6)
_cell_length_c                   13.970(10)
_cell_measurement_temperature    100(2)
_cell_volume                     590.7(7)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.957
_diffrn_measured_fraction_theta_max 0.957
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_theta_full        28.25
_diffrn_reflns_theta_max         28.25
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_exptl_absorpt_coefficient_mu    0.080
_exptl_absorpt_correction_T_max  0.9905
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_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.038
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     137
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0876P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ja206736q_si_003.cif
_cod_data_source_block           baid04s
_cod_depositor_comments
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 Updated bibliographic information.

 Antanas Vaitkus,
 2019-10-11
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_cod_original_cell_volume        590.6(7)
_cod_database_code               4106738