Preparation, structural, Raman and impedance spectroscopic characterisation of the silver ion conductor (AgI)2Ag3SbS3
Nilges, Tom; Reiser, Sara; Hong, Jung Hoon; Gaudin, Etienne; Pfitzner, Arno; Physical Chemistry Chemical Physics 4 (2002) 5888–5894; doi:10.1039/b203556a

data_7205029
_publ_section_exptl_refinement   373K
_publ_section_title
;
 Preparation, structural, Raman and impedance spectroscopic
 characterisation of the silver ion conductor (AgI)2Ag3SbS3
;
_journal_coden_ASTM              PPCPFQ
_journal_issue                   23
_journal_name_full               'Physical Chemistry Chemical Physics'
_journal_page_first              5888
_journal_page_last               5894
_journal_paper_doi               10.1039/b203556a
_journal_volume                  4
_journal_year                    2002
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_cell_angle_beta                 90
_cell_angle_gamma                90
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_cell_length_b                   13.656(1)
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_cell_measurement_temperature    523
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_cell_measurement_wavelength     0.71073
_cell_volume                     1170.95(15)
_computing_cell_refinement       'Stoe CELL using 8000 reflections'
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_diffrn_measurement_device       'imaging plate system'
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_exptl_absorpt_correction_T_max  0.1678
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_exptl_absorpt_correction_type   gaussian
_exptl_crystal_colour            yellow
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_exptl_crystal_density_meas_temp 523
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     w=1/(\s^2^(I)+0.000484I^2^)
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_all         0.0678
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_reflns_limit_h_min              0
_reflns_limit_k_max              19
_reflns_limit_k_min              0
_reflns_limit_l_max              10
_reflns_limit_l_min              0
_reflns_number_observed          1052
_reflns_number_total             1814
_reflns_observed_criterion       2
_cod_data_source_file            b203556a.cif
_cod_data_source_block           523K
_cod_depositor_comments
;
The following automatic conversions were performed:
'_diffrn_radiation_probe' value 'X-ray' changed to 'x-ray' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

 Updated bibliographic information.

 Antanas Vaitkus,
 2019-10-03
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_cod_original_cell_volume        1170.9(2)
_cod_original_formula_sum        'Ag5 I2 Sb1 S3'
_cod_database_code               7205029