3-Hydroxy-2,6-dinitroacetophenone: an Unusual Substitution Pattern Resulting from Nitration of 3-Hydroxyacetophenone
Cristiano, M. L. S.; Johnstone, R. A. W.; Pratt, M. J.; Acta Crystallographica Section C 51 (1995) 2581–2583; doi:10.1107/S0108270195007451

data_2004257
_publ_section_title
;
 3-Hydroxy-2,6-dinitroacetophenone: an Unusual Substitution Pattern
 Resulting from Nitration of 3-Hydroxyacetophenone
;
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              2581
_journal_page_last               2583
_journal_paper_doi               10.1107/S0108270195007451
_journal_volume                  51
_journal_year                    1995
_chemical_formula_moiety         'C8 H6 N2 O6'
_chemical_formula_sum            'C8 H6 N2 O6'
_chemical_formula_weight         226.15
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_symmetry_cell_setting           monoclinic
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_audit_creation_method           'from TEXRAY.INF file'
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_cell_angle_gamma                90
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_cell_length_c                   9.392(2)
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_computing_cell_refinement       ' MSC/AFC Diffractometer Control Software'
_computing_data_collection
; MSC/AFC Diffractometer Control Software (Molecular
Structure Corporation, 1988)
;
_computing_data_reduction
' PROCESS TEXSAN (Molecular Structure Corporation, 1989)'
_computing_publication_material  'FINISH TEXSAN'
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_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   \y-scan
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_exptl_crystal_description       prism
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_exptl_crystal_size_mid          0.300
_exptl_crystal_size_min          0.300
_refine_diff_density_max         0.61916
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_refine_ls_extinction_method     Zachariasen_type_2_Gaussian_isotropic
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_refine_ls_structure_factor_coef F
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