2,5-Bis-trimethylsilyl substituted boroles.
Heitkemper, Tobias; Naß, Leonard; Sindlinger, Christian P.; Dalton transactions (Cambridge, England : 2003) 49 (2020) 2706–2714; doi:10.1039/d0dt00393j

data_7703465
_publ_section_title
;
 2,5-Bis-trimethylsilyl substituted boroles.
;
_journal_issue                   8
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2706
_journal_page_last               2714
_journal_paper_doi               10.1039/d0dt00393j
_journal_volume                  49
_journal_year                    2020
_chemical_formula_sum            'C48 H70 Si2 Zr'
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_chemical_properties_physical    Air-sensitive,Moisture-sensitive
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_space_group_IT_number           2
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;
2020-01-10 deposited with the CCDC.	2020-02-06 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'Bruker Smart APEX II Quazar'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_type           AgK\a
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_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.149
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_exptl_crystal_recrystallization_method 'Re-crystallisation from solvent'
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0346P)^2^+2.8111P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0824
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_reflns_number_gt                14559
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_reflns_threshold_expression     'I > 2\s(I)'
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'Adding full bibliography for 7703465--7703474.cif.'
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