Use of crown ethers to isolate intermediates in ammonia-borane dehydrocoupling reactions.
Less, Robert J.; García-Rodríguez, Raúl; Simmonds, Hayley R.; Allen, Lucy K.; Bond, Andrew D.; Wright, Dominic S.; Chemical communications (Cambridge, England) 52 (2016) 3650–3652; doi:10.1039/c6cc00088f

data_7118675
_publ_section_title
;
 Use of crown ethers to isolate intermediates in ammonia-borane
 dehydrocoupling reactions.
;
_journal_issue                   18
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              3650
_journal_page_last               3652
_journal_paper_doi               10.1039/c6cc00088f
_journal_volume                  52
_journal_year                    2016
_chemical_absolute_configuration unk
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_chemical_formula_sum            'C24 H56 Al B Cl4 N2 O12'
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_space_group_name_Hall           'P -2yac'
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_audit_update_record
;
2015-12-18 deposited with the CCDC.
2016-01-29 downloaded from the CCDC.
;
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0998P)^2^+6.2086P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_depositor_comments
'Adding full bibliography for 7118673--7118675.cif.'
_cod_database_code               7118675
_cambridge_user_name             'Rob Less'
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_cambridge_supervisor_crsid      dsw1000
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_shelx_estimated_absorpt_t_min   0.339
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_shelx_res_checksum              59624