Influence of steric hindrance on the 1,4- <i>versus</i> 1,6-Michael addition: synthesis of furans and pentasubstituted benzenes.
Rana, Shally; Shaw, Ranjay; Pratap, Ramendra; Organic & biomolecular chemistry 22 (2024) 5361–5373; doi:10.1039/d4ob00686k

data_7159964
_publ_section_title
;
 Influence of steric hindrance on the 1,4- <i>versus</i> 1,6-Michael
 addition: synthesis of furans and pentasubstituted benzenes.
;
_journal_issue                   26
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              5361
_journal_page_last               5373
_journal_paper_doi               10.1039/d4ob00686k
_journal_volume                  22
_journal_year                    2024
_chemical_formula_moiety         'C16 H13 Cl N2 O S'
_chemical_formula_sum            'C16 H13 Cl N2 O S'
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_audit_update_record
;
2019-12-30 deposited with the CCDC.	2024-06-05 downloaded from the CCDC.
;
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_computing_structure_solution    'SHELXL-2016/6 (Sheldrick, 2016)'
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_refine_ls_R_factor_gt           0.0454
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0447P)^2^+0.8316P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_total             2626
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7159964--7159965.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7159964
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