Heavier pnictinidene gold(i) complexes.
Kořenková, Monika; Kremláček, Vít; Erben, Milan; Jirásko, Robert; De Proft, Frank; Turek, Jan; Jambor, Roman; RůŽička, Aleš; Císařová, Ivana; Dostál, Libor; Dalton transactions (Cambridge, England : 2003) 47 (2018) 14503–14514; doi:10.1039/c8dt03022g

data_7047560
_publ_section_title
;
 Heavier pnictinidene gold(i) complexes.
;
_journal_issue                   41
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              14503
_journal_page_last               14514
_journal_paper_doi               10.1039/c8dt03022g
_journal_volume                  47
_journal_year                    2018
_chemical_formula_moiety         'C43.25 H59.25 Au Bi N4, B F4'
_chemical_formula_sum            'C43.25 H59.25 Au B Bi F4 N4'
_chemical_formula_weight         1127.95
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   mixed
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_audit_update_record
;
2018-09-04 deposited with the CCDC.
2018-09-14 downloaded from the CCDC.
;
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_computing_cell_refinement       'COLLECT and DENZO'
_computing_data_collection
'COLLECT (Hooft, 1998) and DENZO (Otwinowski & Minor, 1997)'
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_computing_structure_solution    'SIR92 (Altomare et al., 1994)'
_diffrn_ambient_temperature      150(1)
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_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measurement_device_type  'Bruker Nonius KappaCCD area detector'
_diffrn_measurement_method       '\f and \w scans to fill the Ewald sphere'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
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_diffrn_reflns_av_unetI/netI     0.0863
_diffrn_reflns_Laue_measured_fraction_full 0.997
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_diffrn_reflns_limit_l_min       -25
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;
Gaussian integration (Coppens, 1970)
;
_exptl_crystal_colour            colourless
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0566P)^2^+34.3493P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_total             10147
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c8dt03022g2.cif
_cod_data_source_block           7
_cod_depositor_comments
'Adding full bibliography for 7047556--7047562.cif.'
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_shelx_res_checksum              25258