Solvothermal growth of a ruthenium metal-organic framework featuring HKUST-1 structure type as thin films on oxide surfaces
Olesia Kozachuk; Kirill Yusenko; Heshmat Noei; Yuemin Wang; Stephan Walleck; Thorsten Glaser; Roland Fischer; Chem.Commun. 47 (2011) 8509–; doi:10.1039/c1cc11107h

data_7106715
_publ_section_title
;
 Solvothermal growth of a ruthenium metal-organic framework featuring
 HKUST-1 structure type as thin films on oxide surfaces
;
_journal_name_full               Chem.Commun.
_journal_page_first              8509
_journal_paper_doi               10.1039/c1cc11107h
_journal_volume                  47
_journal_year                    2011
_chemical_formula_sum            'C6 O8 Ru2'
_chemical_formula_weight         402.20
_chemical_name_systematic
; 
?
;
_space_group_IT_number           225
_symmetry_cell_setting           cubic
_symmetry_space_group_name_Hall  '-F 4 2 3'
_symmetry_space_group_name_H-M   'F m -3 m'
_audit_creation_method           'Jana2006 Version : 23/10/2008'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            24
_cell_length_a                   26.553(3)
_cell_length_b                   26.553(3)
_cell_length_c                   26.553(3)
_cell_measurement_temperature    293
_cell_volume                     18722(4)
_computing_cell_refinement
'Jana2000 (Petricek, Dusek & Palatinus, 2000)'
_computing_data_collection       'Bruker D8'
_computing_molecular_graphics    'Diamond 3.2.'
_computing_publication_material
'Jana2000 (Petricek, Dusek & Palatinus, 2000) ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS'
_computing_structure_refinement
'Jana2000 (Petricek, Dusek & Palatinus, 2000)'
_computing_structure_solution    'FOX http://objcryst.sourceforge.net'
_diffrn_ambient_temperature      293
_diffrn_detector                 'position sensitive'
_diffrn_measurement_device       'Briker D8'
_diffrn_measurement_device_type  'Briker D8'
_diffrn_radiation_monochromator  'Goebel mirror'
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.54178
_diffrn_source                   X-ray
_diffrn_source_type              'Cu K\a'
_exptl_absorpt_process_details   Jana2006
_exptl_crystal_density_diffrn    0.856
_exptl_crystal_F_000             4512
_pd_char_colour                  black
_pd_instr_location
; 
?
;
_pd_meas_2theta_range_inc        0.014
_pd_meas_2theta_range_max        89.905
_pd_meas_2theta_range_min        5.000
_pd_meas_number_of_points        5987
_pd_meas_scan_method             step
_pd_proc_2theta_range_inc        0.014
_pd_proc_2theta_range_max        89.905
_pd_proc_2theta_range_min        5
_pd_proc_ls_background_function  '10 Legendre polynoms'
_pd_proc_ls_pref_orient_corr     none
_pd_proc_ls_profile_function     Pseudo-Voigt
_pd_proc_ls_prof_R_factor        0.0955
_pd_proc_ls_prof_wR_expected     0.0298
_pd_proc_ls_prof_wR_factor       0.1381
_pd_spec_mount_mode              transmission
_pd_spec_shape                   cylinder
_refine_ls_goodness_of_fit_all   4.60
_refine_ls_number_constraints    6
_refine_ls_number_parameters     29
_refine_ls_number_restraints     12
_refine_ls_R_factor_all          0.1823
_refine_ls_R_factor_gt           0.0951
_refine_ls_shift/su_max          0.1
_refine_ls_shift/su_mean         4.1764
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.1372
_refine_ls_wR_factor_ref         0.1761
_cod_data_source_file            c1cc11107h_1.txt
_cod_data_source_block           (I)
_cod_original_cell_volume        18722(3)
_cod_original_sg_symbol_Hall     '-F 4 2 3 '
_cod_database_code               7106715