Activation of Carbon Monoxide by (Me3tpa)Rh and (Me3tpa)Ir
Dzik, Wojciech I.; Smits, Jan M. M.; Reek, Joost N. H.; de Bruin, Bas; Organometallics 28 (2009) 1631–; doi:10.1021/om801142y

data_4068884
_publ_contact_author
;
        Dr. B. de Bruin
        Department of Homogeneous Catalysis
        Van 't Hoff Institute for Molecular Sciences
        University of Amsterdam
        Nieuwe Achtergracht 166
        1018 WV Amsterdam
        The Netherlands
;
_publ_section_title
;
 Activation of Carbon Monoxide by (Me3tpa)Rh and (Me3tpa)Ir
;
_journal_issue                   6
_journal_name_full               Organometallics
_journal_page_first              1631
_journal_paper_doi               10.1021/om801142y
_journal_volume                  28
_journal_year                    2009
_chemical_formula_sum            'C22 H24 F6 N4 O3 P Rh'
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_cell_angle_beta                 81.380(6)
_cell_angle_gamma                79.582(6)
_cell_formula_units_Z            4
_cell_length_a                   8.2853(7)
_cell_length_b                   13.8246(12)
_cell_length_c                   22.4016(14)
_cell_measurement_reflns_used    724
_cell_measurement_temperature    208(2)
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_computing_data_collection
;
Nonius "Collect" program suite (Nonius, 1999)
;
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Nonius "EvalCCD" program suite (Duisenberg, 1998)
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_computing_molecular_graphics
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PLATON (Spek, 2003)
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DIRDIF (Beurskens et al., 1996),
PATTY (Beurskens et al., 1987)
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_refine_ls_structure_factor_coef Fsqd
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;
w=1/[\s^2^(Fo^2^)+(0.0216P)^2^+4.6866P] where P=(Fo^2^+2Fc^2^)/3
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.0743
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_reflns_number_gt                9637
_reflns_number_observed          9637
_reflns_number_total             11163
_reflns_observed_criterion       >2sigma(I)
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_cod_data_source_block           WOJ04
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Automatic conversion script
Id: cif_correct_tags 1440 2010-10-19 06:21:57Z saulius 

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Automatic conversion script
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