Broad scope gold(i)-catalysed polyenyne cyclisations for the formation of up to four carbon-carbon bonds.
Rong, Zhouting; Echavarren, Antonio M.; Organic & biomolecular chemistry 15 (2017) 2163–2167; doi:10.1039/c7ob00235a

data_7155490
_publ_section_title
;
 Broad scope gold(i)-catalysed polyenyne cyclisations for the formation of
 up to four carbon-carbon bonds.
;
_journal_issue                   10
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              2163
_journal_page_last               2167
_journal_paper_doi               10.1039/c7ob00235a
_journal_volume                  15
_journal_year                    2017
_chemical_formula_sum            'C23 H27 N O4 S'
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_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
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_audit_update_record
;
2017-01-30 deposited with the CCDC.
2017-02-13 downloaded from the CCDC.
;
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;
 Fullsphere data collection, phi and omega scans
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; 
 SADABS Version 2008/1 Bruker-Nonius
 Blessing, Acta Cryst. (1995) A51 33-38
;
_exptl_crystal_colour            colourless
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0531P)^2^+0.8321P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_total             6481
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c7ob00235a2.cif
_cod_data_source_block           mo_zri185_0m
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4268 2015-11-12 08:31:59Z antanas 

 Adding full bibliography for 7155490--7155491.cif.
;
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               7155490
_shelx_estimated_absorpt_t_min   0.937
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_shelxl_version_number           2014-3
_shelx_res_checksum              65873