Multiple Bonds Between Main Group Elements and Transition Metals. 151.1 Trioxorhenium(VII) Alkoxide Complexes
Wolfgang A. Herrmann; William A. Wojtczak; Georg R. J. Artus; Fritz E. Kühn; Mike R. Mattner; Inorganic Chemistry 36 (1997) 465–471; doi:10.1021/ic951508j

data_4323296
_publ_contact_author
;                                                                               
       Georg Artus                                                     
                   
       Anorganisch-chemisches Institut der                                      
       Technischen Universit\"at M\"unchen                                      
       Lichtenbergstrasse 4                                                     
       D-85747 Garching                                                         
;
_publ_contact_author_email       'artus@zaphod.anorg.chemie.tu-muenchen.de '
_publ_contact_author_fax         ' 089 3209 3473 '
_publ_contact_author_phone       ' 089 3209 3143 '
_publ_section_title
;
 Multiple Bonds Between Main Group Elements and Transition Metals. 151.1
 Trioxorhenium(VII) Alkoxide Complexes
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              465
_journal_page_last               471
_journal_paper_doi               10.1021/ic951508j
_journal_volume                  36
_journal_year                    1997
_chemical_formula_sum            'C9 H21 O5 Re Si'
_chemical_formula_weight         423.55
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     heavy
_audit_creation_date             96-06-05
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_cell_angle_beta                 117.440
_cell_angle_gamma                90.000
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_cell_length_c                   12.485
_cell_measurement_reflns_used    250
_cell_measurement_temperature    193(4)
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_computing_cell_refinement       'CAD-4 software (Enraf-Nonius, 1989)'
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_computing_structure_solution    'SHELXS86 (Sheldrick, 1986)'
_diffrn_ambient_temperature      193(4)
_diffrn_measurement_device       '  Enraf-nonius CAD4 '
_diffrn_measurement_method       'omega scan'
_diffrn_radiation_monochromator  graphite
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_exptl_absorpt_coefficient_mu    8.53
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_exptl_crystal_colour            ' none '
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;
 H atoms placed geometrically after each cycle
;
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;
 Chebychev polynomial (Carruthers & Watkin, 1979)
;
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_cod_depositor_comments
;
The following automatic conversions were performed:

'_atom_sites_solution_hydrogens' value 'Geometric' was changed to
'geom'.

Automatic conversion script
Id: cif_fix_values 6452 2018-10-05 10:23:21Z andrius 
;
_cod_original_cell_volume        1438.64
_cod_original_sg_symbol_H-M      'P 1 21/c 1 '
_cod_original_formula_sum        ' C9 H21 Re1 Si1 O5 '
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