Structural versatility in hydrated rare earth(iii) 1,2-benzenedisulfonates
Deacon, Glen B.; Harika, Rita; Junk, Peter C.; Skelton, Brian W.; White, Allan H.; New Journal of Chemistry 31 (2007) 634–; doi:10.1039/b614681c

data_7052103
_publ_section_title
;
 Structural versatility in hydrated rare earth(iii)
 1,2-benzenedisulfonates
;
_journal_issue                   5
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              634
_journal_paper_doi               10.1039/b614681c
_journal_volume                  31
_journal_year                    2007
_chemical_formula_moiety         '2(C6 H16 Tb O12 S2), C6 H4 O6 S2,4(H2 O)'
_chemical_formula_sum            'C18 H44 O34 S6 Tb2'
_chemical_formula_weight         1314.76
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yb'
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_cell_angle_alpha                90.00000
_cell_angle_beta                 111.3270(10)
_cell_angle_gamma                90.00000
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_cell_length_b                   34.366(2)
_cell_length_c                   8.5388(4)
_cell_measurement_reflns_used    7947
_cell_measurement_temperature    150
_cell_measurement_theta_max      37.4
_cell_measurement_theta_min      2.3
_cell_volume                     2111.51(19)
_computing_cell_refinement       'Siemens SAINT (Siemens, 1995)'
_computing_data_collection       'Siemens SMART (Siemens, 1995)'
_computing_data_reduction        'xtal ADDREF SORTRF'
_computing_molecular_graphics    xtal
_computing_publication_material  'xtal BONDLA CIFIO'
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_diffrn_ambient_temperature      150
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_diffrn_measurement_device_type
;
Bruker SMART CCD diffractometer
;
_diffrn_measurement_method       '\w scans'
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_diffrn_radiation_type           'Mo K\a'
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_diffrn_reflns_limit_k_min       -58
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_diffrn_standards_decay_%        0
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_exptl_absorpt_coefficient_mu    3.725
_exptl_absorpt_correction_T_max  .79
_exptl_absorpt_correction_T_min  .63
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
SADABS; Sheldrick, 1996
;
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_exptl_crystal_description       prism
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_refine_ls_structure_factor_coef F
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;
w=1/(sig^2(F) + .0006F^2)
;
_refine_ls_weighting_scheme      calc
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_cod_original_cell_volume        2111.5(2)
_cod_original_sg_symbol_Hall     -p_2yb
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_cod_database_code               7052103