Hydrogen-Bonded Porous Coordination Polymers: Structural Transformation, Sorption Properties, and Particle Size from Kinetic Studies
Kazuhiro Uemura; Kazuya Saito; Susumu Kitagawa; Hidetoshi Kita; Journal of the American Chemical Society 128 (2006) 16122–16130; doi:10.1021/ja064152r

data_4111191
_publ_section_title
;
 Hydrogen-Bonded Porous Coordination Polymers: Structural Transformation,
 Sorption Properties, and Particle Size from Kinetic Studies
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              16122
_journal_page_last               16130
_journal_paper_doi               10.1021/ja064152r
_journal_volume                  128
_journal_year                    2006
_chemical_formula_sum            'C32 H22 Co N8 O4 S2'
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_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 104.6391(7)
_cell_angle_gamma                90
_cell_formula_units_Z            2
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_cell_length_b                   10.063(1)
_cell_length_c                   15.5356(4)
_cell_measurement_temperature    293.2
_cell_volume                     1720.0(4)
_computing_data_reduction        'teXsan Ver. 1.11'
_computing_publication_material  'teXsan Ver. 1.11'
_computing_structure_refinement  'teXsan Ver. 1.10'
_computing_structure_solution    SAPI91
_diffrn_measured_fraction_theta_full 0.9609
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_diffrn_measurement_device_type  'Rigaku/MSC Mercury CCD'
_diffrn_measurement_method       \w
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_exptl_crystal_size_min          0.200
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^) + (0.09000(Max(Fo^2^,0) + 2Fc^2^)/3)^2^]'
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