Two 2D multiresponsive luminescence coordination polymers for selective sensing of Fe3+, CrVI anions and TNP in aqueous medium
Zhou, Ai-Mei; Wei, Han; Gao, Wei; Liu, Jie-Ping; Zhang, Xiu-Mei; CrystEngComm 21 (2019) 5185–; doi:10.1039/C9CE01045A

data_7233295
_publ_section_title
;
 Two 2D multiresponsive luminescence coordination polymers for selective
 sensing of Fe3+, CrVI anions and TNP in aqueous medium
;
_journal_issue                   34
_journal_name_full               CrystEngComm
_journal_page_first              5185
_journal_paper_doi               10.1039/C9CE01045A
_journal_volume                  21
_journal_year                    2019
_chemical_formula_sum            'C14 H20 Cd N2 O11'
_chemical_formula_weight         504.72
_space_group_crystal_system      triclinic
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_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2019-06-25 deposited with the CCDC.    2019-07-31 downloaded from the CCDC.
;
_cell_angle_alpha                70.6260(10)
_cell_angle_beta                 77.550(3)
_cell_angle_gamma                74.2340(10)
_cell_formula_units_Z            2
_cell_length_a                   7.4640(7)
_cell_length_b                   10.1801(9)
_cell_length_c                   13.3769(11)
_cell_measurement_reflns_used    995
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      26.054
_cell_measurement_theta_min      2.858
_cell_volume                     913.95(14)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
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_computing_molecular_graphics    'Bruker SHELXTL'
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_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.980
_diffrn_measured_fraction_theta_max 0.980
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1070
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_exptl_crystal_colour            colorless
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_exptl_crystal_description       block
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.1580P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2684
_refine_ls_wR_factor_ref         0.2841
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2144
_reflns_number_total             3154
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c9ce01045a2.cif
_cod_data_source_block           1_CCDC1
_cod_depositor_comments
'Adding full bibliography for 7233294--7233295.cif.'
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