<i>trans</i>-Dichloro[(2<i>RS</i>,5<i>RS</i>,9<i>SR</i>,12<i>RS</i>)-2,5,9,12-tetraazatridecane]cobalt(III) perchlorate, [CoCl~2~(C~9~H~24~N~4~)]ClO~4~
Lu, T.-H.; Lai, C.-Y.; Chung, C.-S.; Acta Crystallographica Section C 50 (1994) 202–203; doi:10.1107/S0108270193007231

data_2009428
_publ_section_title
;<i>trans</i>-Dichloro[(2<i>RS</i>,5<i>RS</i>,9<i>SR</i>,12<i>RS</i>)-2,5,9,12-tetraazatridecane]cobalt(III)
 perchlorate, [CoCl~2~(C~9~H~24~N~4~)]ClO~4~
;
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              202
_journal_page_last               203
_journal_paper_doi               10.1107/S0108270193007231
_journal_volume                  50
_journal_year                    1994
_chemical_formula_sum            'C9 H24 Cl3 Co N4 O4'
_chemical_formula_weight         417.60
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2c -2b'
_symmetry_space_group_name_H-M   'P b c 21'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   6.366(2)
_cell_length_b                   15.052(2)
_cell_length_c                   17.574(3)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    298
_cell_measurement_theta_max      18.6
_cell_measurement_theta_min      8.7
_cell_volume                     1684.0(6)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \q/2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            2933
_diffrn_reflns_theta_max         29.9
_diffrn_standards_decay_%        +-1
_diffrn_standards_interval_time  60
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    1.51
_exptl_absorpt_correction_T_max  0.9999
_exptl_absorpt_correction_T_min  0.8209
_exptl_absorpt_correction_type   'empirical (North, Phillips & Mathews, 1968)'
_exptl_crystal_colour            Green
_exptl_crystal_density_diffrn    1.647
_exptl_crystal_description       'Rectangular pillar'
_exptl_crystal_size_max          0.34
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.13
_refine_diff_density_max         0.68(5)
_refine_diff_density_min         -0.55(5)
_refine_ls_goodness_of_fit_obs   0.80
_refine_ls_hydrogen_treatment    refU
_refine_ls_number_parameters     209
_refine_ls_number_reflns         1703
_refine_ls_R_factor_obs          0.056
_refine_ls_shift/esd_max         0.250
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      unit
_refine_ls_wR_factor_obs         0.054
_reflns_number_observed          1703
_reflns_number_total             2524
_reflns_observed_criterion       I>2.5\s(I)
_cod_data_source_file            as1032.cif
_cod_data_source_block           as1032_structure_1_of_1
_cod_original_cell_volume        1683.9(6)
_cod_database_code               2009428