K5Eu(MoO4)4 red phosphor for solid state lighting applications, prepared by different techniques
Posokhova, Svetlana M.; Morozov, Vladimir A.; Deyneko, Dina V.; Redkin, Boris S.; Spassky, Dmitry A.; Nagirnyi, Vitali; Belik, Alexei A.; Hadermann, Joke; Pavlova, Erzhena T.; Lazoryak, Bogdan I.; CrystEngComm 25 (2023) 835–847; doi:10.1039/D2CE01107G

data_7246099
_publ_section_title
;
 K5Eu(MoO4)4 red phosphor for solid state lighting applications, prepared
 by different techniques
;
_journal_issue                   5
_journal_name_full               CrystEngComm
_journal_page_first              835
_journal_page_last               847
_journal_paper_doi               10.1039/D2CE01107G
_journal_volume                  25
_journal_year                    2023
_chemical_formula_analytical     K5Eu(MoO4)4
_chemical_formula_iupac          K5Eu(MoO4)4
_chemical_formula_moiety         'Eu1 K5 Mo4 O16'
_chemical_formula_structural     K5Eu(MoO4)4
_chemical_formula_sum            'Eu K5 Mo4 O16'
_chemical_formula_weight         987.2
_chemical_name_common            K5Eu(MoO4)4
_chemical_name_systematic        K5Eu(MoO4)4
_space_group_IT_number           12
_space_group_name_Hall           '-C 2y'
_space_group_name_H-M_alt        'C 1 2/m 1'
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      12
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_audit_update_record
;
2021-10-07 deposited with the CCDC.	2023-01-04 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 116.5836(5)
_cell_angle_gamma                90
_cell_formula_units_Z            1
_cell_length_a                   10.37099(5)
_cell_length_b                   5.98542(3)
_cell_length_c                   7.72496(4)
_cell_measurement_temperature    293
_cell_volume                     428.831(4)
_computing_cell_refinement       '(Jana2000; Petricek and Dusek, 2000)'
_computing_publication_material  '(Jana2000; Petricek and Dusek, 2000)'
_computing_structure_refinement  '(Jana2000; Petricek and Dusek, 2000)'
_diffrn_ambient_temperature      293(1)
_diffrn_measurement_device_type  'BL15XU beamline of SPring-8'
_diffrn_radiation_monochromator  Si(111)
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           synchrotron
_diffrn_radiation_wavelength     0.65297
_diffrn_source                   synchrotron
_diffrn_source_type              synchrotron
_exptl_absorpt_coefficient_mu    6.082
_exptl_absorpt_process_details   '(Jana2000; Petricek, Dusek & Palatinus, 2000)'
_exptl_crystal_density_diffrn    3.8227
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             454
_exptl_crystal_preparation       Luminescent
_pd_calc_method                  'Rietveld Refinement'
_pd_char_colour                  white
_pd_instr_location               ' ?'
_pd_meas_2theta_range_max        61.831
_pd_meas_2theta_range_min        2.041
_pd_meas_number_of_points        19916
_pd_meas_scan_method             step
_pd_proc_2theta_range_max        47.208
_pd_proc_2theta_range_min        4.23
_pd_proc_ls_background_function  '15 Legendre polynoms'
_pd_proc_ls_pref_orient_corr     none
_pd_proc_ls_profile_function     Pseudo-Voigt
_pd_proc_ls_prof_R_factor        0.0330
_pd_proc_ls_prof_wR_expected     0.0114
_pd_proc_ls_prof_wR_factor       0.0608
_refine_diff_density_max         3.09
_refine_diff_density_min         -2.65
_refine_ls_goodness_of_fit_all   5.32
_refine_ls_number_constraints    1
_refine_ls_number_parameters     39
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0983
_refine_ls_R_factor_gt           0.0927
_refine_ls_shift/su_max          0.0439
_refine_ls_shift/su_mean         0.0058
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_all         0.1293
_refine_ls_wR_factor_gt          0.1284
_cod_data_source_file            d2ce01107g10.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_diffrn_radiation_probe' value 'X-ray' was changed to
'x-ray' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas 

 Adding full bibliography for 7246099.cif.
;
_cod_original_formula_sum        'Eu1 K5 Mo4 O16'
_cod_database_code               7246099