Expedient iron-catalyzed stereospecific synthesis of triazines via cycloaddition of aziridines with diaziridines.
Sarkar, Tanumay; Talukdar, Kangkan; Roy, Subhasish; Punniyamurthy, Tharmalingam; Chemical communications (Cambridge, England) 56 (2020) 3381–3384; doi:10.1039/c9cc10089j

data_7126015
_publ_section_title
;
 Expedient iron-catalyzed stereospecific synthesis of triazines via
 cycloaddition of aziridines with diaziridines.
;
_journal_issue                   23
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              3381
_journal_page_last               3384
_journal_paper_doi               10.1039/c9cc10089j
_journal_volume                  56
_journal_year                    2020
_chemical_formula_moiety         'C28 H33 N3 O2'
_chemical_formula_sum            'C28 H33 N3 O2'
_chemical_formula_weight         443.57
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_audit_creation_method           SHELXL-2016/6
_audit_update_record
;
2019-12-16 deposited with the CCDC.	2020-02-14 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
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_diffrn_reflns_Laue_measured_fraction_full 0.997
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_exptl_absorpt_process_details   SADABS
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+0.2219P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1608
_refine_ls_wR_factor_ref         0.2092
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2297
_reflns_number_total             3951
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c9cc10089j2.cif
_cod_data_source_block           TS-PR5-2
_cod_depositor_comments
'Adding full bibliography for 7126014--7126015.cif.'
_cod_original_cell_volume        1226.4(3)
_cod_database_code               7126015
_shelx_shelxl_version_number     2016/6
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