Reappraising the formation of Jaff�'s base: studies of the treatment of imidazolidine-2-thione with mild oxidising agents
Thanyasirikul, Yupa; Pakawatchai, Chaveng; Cole, Marcus L.; Junk, Peter C.; Skelton, Brian W.; White, Allan H.; Organic & Biomolecular Chemistry 1 (2003) 3217–; doi:10.1039/b306647a

data_7151501
_publ_section_title
;
 Reappraising the formation of Jaff&#xFFFD;'s base: studies of the
 treatment of imidazolidine-2-thione with mild oxidising agents
;
_journal_issue                   18
_journal_name_full               'Organic &amp;  Biomolecular Chemistry'
_journal_page_first              3217
_journal_paper_doi               10.1039/b306647a
_journal_volume                  1
_journal_year                    2003
_chemical_formula_sum            'C6 H11 Br N4 S'
_chemical_formula_weight         251.15
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_audit_creation_date             02-05-08
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_cell_angle_alpha                90.00000
_cell_angle_beta                 90.00000
_cell_angle_gamma                90.00000
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_cell_length_b                   6.895(7)
_cell_length_c                   9.063(2)
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_cell_measurement_temperature    293
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_cell_measurement_theta_min      24.3
_cell_volume                     955.8(10)
_computing_cell_refinement       'Enraf Nonius software'
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_diffrn_measurement_device_type
;
CAD4 diffractometer
;
_diffrn_measurement_method       '2\q-\w scans'
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_diffrn_radiation_source         'sealed tube'
_diffrn_radiation_type           'Mo K\a'
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_exptl_absorpt_correction_T_max  .36
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_exptl_absorpt_process_details
;
XTAl absorb
;
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         .049
_reflns_d_resolution_high        .663
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_reflns_Friedel_coverage         0
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_reflns_limit_h_min              0
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_reflns_number_gt                1056
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_reflns_threshold_expression     'I    > 3.00 sig(I   )'
_cod_data_source_file            b306647a.txt
_cod_data_source_block           etucub
_cod_original_sg_symbol_Hall     -p_2ac_2n
_cod_original_sg_symbol_H-M      P_n_m_a
_cod_original_formula_sum        'C6 H11 Br1 N4 S1'
_cod_database_code               7151501