A novel pyridine-templated open framework gallophosphate
Wragg, David S.; Bull, Ivor; Hix, Gary B.; Morris, Russell E.; Chemical Communications  (1999) 2037–; doi:10.1039/a906544j

data_7115223
_publ_section_title
;
 A novel pyridine-templated open framework gallophosphate
;
_journal_issue                   20
_journal_name_full               'Chemical Communications'
_journal_page_first              2037
_journal_paper_doi               10.1039/a906544j
_journal_year                    1999
_chemical_formula_sum            'C10 H12 F2 Ga6 N2 O25 P6'
_chemical_formula_weight         1202.36
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
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_audit_conform_dict_name         cif_core.dic
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_audit_creation_date             1999-08-06T10:42:30-00:00
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                71.04(3)
_cell_angle_beta                 68.39(2)
_cell_angle_gamma                66.88(2)
_cell_formula_units_Z            2
_cell_length_a                   11.391(4)
_cell_length_b                   12.414(3)
_cell_length_c                   12.846(4)
_cell_measurement_temperature    150(2)
_cell_volume                     1518.3(9)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.833
_diffrn_measured_fraction_theta_max 0.833
_diffrn_radiation_monochromator  silicon
_diffrn_radiation_wavelength     0.6849
_diffrn_reflns_av_R_equivalents  0.029
_diffrn_reflns_av_sigmaI/netI    0.025
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            14097
_diffrn_reflns_theta_full        29.25
_diffrn_reflns_theta_max         29.25
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_exptl_absorpt_coefficient_mu    5.682
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_exptl_absorpt_correction_T_min  0.3961
_exptl_crystal_density_diffrn    2.63
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1160
_exptl_crystal_size_max          0.02
_exptl_crystal_size_mid          0.02
_exptl_crystal_size_min          0.008
_refine_diff_density_max         1.766
_refine_diff_density_min         -1.364
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_refine_ls_extinction_method     none
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_refine_ls_number_restraints     0
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_refine_ls_R_factor_all          0.0481
_refine_ls_R_factor_gt           0.0454
_refine_ls_shift/su_max          0.024
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_refine_ls_structure_factor_coef Fsqd
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