Incorporation of cu(2+) ions into nanotubular uranyl diphosphonates.
Adelani, Pius O.; Cook, Nathaniel D.; Babo, Jean-Marie; Burns, Peter C.; Inorganic chemistry 53 (2014) 4169–4176; doi:10.1021/ic500220d

data_4338062
_publ_section_title
;
 Incorporation of cu(2+) ions into nanotubular uranyl diphosphonates.
;
_journal_issue                   8
_journal_name_full               'Inorganic chemistry'
_journal_page_first              4169
_journal_page_last               4176
_journal_paper_doi               10.1021/ic500220d
_journal_volume                  53
_journal_year                    2014
_chemical_formula_moiety         'C20 H14 Cu N4 O9 P2 U'
_chemical_formula_sum            'C20 H14 Cu N4 O9 P2 U'
_chemical_formula_weight         817.86
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
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_cell_angle_beta                 74.852(3)
_cell_angle_gamma                68.034(3)
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_cell_length_b                   10.786(3)
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_cell_measurement_temperature    100(2)
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_cell_volume                     1182.3(6)
_computing_cell_refinement       'Bruker SAINT'
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_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.982
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
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_diffrn_reflns_limit_h_max       11
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_diffrn_standards_number         0
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_exptl_absorpt_correction_T_min  0.6124
_exptl_absorpt_correction_type   empirical
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_exptl_crystal_colour            green
_exptl_crystal_density_diffrn    2.297
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle-like
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_refine_ls_R_factor_all          0.0596
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_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0435P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1096
_refine_ls_wR_factor_ref         0.1155
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_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic500220d_si_002.cif
_cod_data_source_block           p-1
_cod_depositor_comments
'Adding full bibliography for 4338061--4338063.cif.'
_cod_database_code               4338062