Synthesis and Characterization of N-Heterocyclic Carbene Complexes of Uranium(III)
Hidetaka Nakai; Xile Hu; Lev N. Zakharov; Arnold L. Rheingold; Karsten Meyer; Inorganic Chemistry 43 (2004) 855–857; doi:10.1021/ic035142j

data_4310570
_publ_section_title
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 Synthesis and Characterization of N-Heterocyclic Carbene Complexes of
 Uranium(III)
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_journal_name_full               'Inorganic Chemistry'
_journal_page_first              855
_journal_page_last               857
_journal_paper_doi               10.1021/ic035142j
_journal_volume                  43
_journal_year                    2004
_chemical_formula_sum            'C76 H108 N5 O3 U'
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_cell_length_a                   11.0692(11)
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_cell_length_c                   25.395(3)
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_computing_cell_refinement       'Bruker SMART'
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_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
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_diffrn_ambient_temperature      100(2)
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_diffrn_measurement_device_type  'CCD area detector'
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0000P)^2^+100.0000P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_data_source_file            ic035142jsi20031110_074828.cif
_cod_data_source_block           hide29
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan' changed
to 'multi-scan' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
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_cod_original_cell_volume        3351.3(6)
_cod_database_code               4310570