Synthesis of pyrrolidine-fused [34]- and [36]octaphyrins via 1,3-dipolar cycloaddition.
Hata, Hiroshi; Kamimura, Yiho; Shinokubo, Hiroshi; Osuka, Atsuhiro; Organic letters 8 (2006) 1169–1172; doi:10.1021/ol060067c

data_1516751
_publ_section_title
;
 Synthesis of pyrrolidine-fused [34]- and [36]octaphyrins via 1,3-dipolar
 cycloaddition.
;
_journal_issue                   6
_journal_name_full               'Organic letters'
_journal_page_first              1169
_journal_page_last               1172
_journal_paper_doi               10.1021/ol060067c
_journal_volume                  8
_journal_year                    2006
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_chemical_formula_weight         2376.36
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_symmetry_cell_setting           triclinic
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_symmetry_space_group_name_H-M   'P -1'
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_cell_angle_beta                 87.14(6)
_cell_angle_gamma                66.80(5)
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_cell_length_b                   18.91(1)
_cell_length_c                   19.84(1)
_cell_measurement_reflns_used    39468
_cell_measurement_temperature    123.1
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      3.0
_cell_volume                     5126(5)
_computing_cell_refinement       PROCESS-AUTO
_computing_data_collection       PROCESS-AUTO
_computing_data_reduction        CrystalStructure
_computing_publication_material  'CrystalStructure 3.6.0'
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_computing_structure_solution    DirectMethod
_diffrn_detector_area_resol_mean 10.00
_diffrn_measured_fraction_theta_full 0.8870
_diffrn_measured_fraction_theta_max 0.8870
_diffrn_measurement_device_type  'Rigaku RAXIS-RAPID'
_diffrn_measurement_method       \w
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_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -19
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_exptl_crystal_colour            green
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_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
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_exptl_crystal_size_max          0.40
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_refine_ls_R_factor_gt           0.0980
_refine_ls_shift/su_max          0.0000
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details
'w = 1/[0.0080Fo^2^ + 3.0000\s(Fo^2^) + 0.5000]'
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_cod_original_formula_sum        'C107 H47 Cl4 F40 N9 O '
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