Dibenzoacridines: synthesis by alkyne-carbonyl-metathesis and properties.
Ammon, Erich; Heine, Paul; Cordero, Miguel Andre Argüello; Lochbrunner, Stefan; Villinger, Alexander; Ehlers, Peter; Langer, Peter; Organic & biomolecular chemistry 21 (2023) 4504–4517; doi:10.1039/d3ob00407d

data_7159361
_publ_section_title
;
 Dibenzoacridines: synthesis by alkyne-carbonyl-metathesis and properties.
;
_journal_issue                   21
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              4504
_journal_page_last               4517
_journal_paper_doi               10.1039/d3ob00407d
_journal_volume                  21
_journal_year                    2023
_chemical_formula_moiety         'C31 H17 N O2 S2'
_chemical_formula_sum            'C31 H17 N O2 S2'
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_space_group_name_Hall           '-C 2yc'
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_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2022-05-02 deposited with the CCDC.	2023-05-15 downloaded from the CCDC.
;
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_computing_cell_refinement       'Bruker Apex V7.51A'
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_diffrn_ambient_temperature      123(2)
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_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker Apex Kappa-II-CCD-diffractometer'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_av_unetI/netI     0.0505
_diffrn_reflns_Laue_measured_fraction_full 0.998
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_exptl_absorpt_process_details   '(SADABS; Sheldrick, 2004)'
_exptl_crystal_colour            yellow
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0616P)^2^+1.2614P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                2964
_reflns_number_total             3939
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d3ob00407d2.cif
_cod_data_source_block           is_erp126
_cod_depositor_comments
'Adding full bibliography for 7159361--7159362.cif.'
_cod_original_cell_volume        2271.3(11)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               7159361
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_shelx_res_checksum              81384