Crystal structure of hexaprop-2-en-1-yl 4,4',4'',4''',4'''',4'''''-[1,3,5,2λ^5^,4λ^5^,6λ^5^-triazatriphosphinine-2,2,4,4,6,6-hexaylhexakis(oxy)]hexabenzoate
Zhu, Jing; Li, Qian; Zheng, Fu-Wei; He, Juan; Qu, Ling-Bo; Acta Crystallographica Section E 71 (2015) o955–o956; doi:10.1107/S2056989015021301

data_2241327
_publ_section_title
;
 Crystal structure of hexaprop-2-en-1-yl
 4,4',4'',4''',4'''',4'''''-[1,3,5,2\l^5^,4\l^5^,6\l^5^-triazatriphosphinine-2,2,4,4,6,6-hexaylhexakis(oxy)]hexabenzoate
;
_journal_coeditor_code           ZQ2233
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o955
_journal_page_last               o956
_journal_paper_doi               10.1107/S2056989015021301
_journal_volume                  71
_journal_year                    2015
_chemical_formula_iupac          'C60 H54 N3 O18 P3'
_chemical_formula_moiety         'C60 H54 N3 O18 P3'
_chemical_formula_sum            'C60 H54 N3 O18 P3'
_chemical_formula_weight         1197.97
_chemical_name_systematic
;Hexaprop-2-en-1-yl
4,4',4'',4''',4'''',4'''''-[1,3,5,2\l^5^,4\l^5^,6\l^5^-triazatriphosphinine-2,2,4,4,6,6-hexaylhexakis(oxy)]hexabenzoate
;
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
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Olex2 1.2
(compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998)
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CrysAlis PRO  (Agilent, 2011)
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CrysAlis PRO (Agilent, 2011)
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CrysAlis PRO (Agilent, 2011)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>, 2009)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>, 2009)
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SHELXL97 (Sheldrick, 2008)
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SHELXS97 (Sheldrick, 2008)
;
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_diffrn_measurement_device_type  'Agilent Xcalibur Eos Gemini'
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           CuK\a
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;
(CrysAlis PRO; Agilent, 2011)
;
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0780P)^2^+0.6732P] where P=(Fo^2^+2Fc^2^)/3'
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