Two [Ln<sub>4</sub>] molecular rings folded as compact tetrahedra.
Salinas-Uber, Jorge; Barrios, Leoní A; Roubeau, Olivier; Aromí, Guillem; Dalton transactions (Cambridge, England : 2003) 49 (2020) 7182–7188; doi:10.1039/d0dt01259a

data_7704328
_publ_section_title
;
 Two [Ln<sub>4</sub>] molecular rings folded as compact tetrahedra.
;
_journal_issue                   21
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7182
_journal_page_last               7188
_journal_paper_doi               10.1039/d0dt01259a
_journal_volume                  49
_journal_year                    2020
_chemical_formula_moiety
'C116 H104 Cl4 N24 O12 S8 Tb4, 12(C5 H5 N), 2(C H4 O), H2 O'
_chemical_formula_sum            'C178 H174 Cl4 N36 O15 S8 Tb4'
_chemical_formula_weight         4091.48
_space_group_crystal_system      tetragonal
_space_group_IT_number           88
_space_group_name_Hall           '-I 4ad'
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_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2020-05-05 deposited with the CCDC.	2020-05-07 downloaded from the CCDC.
;
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0916P)^2^+392.9011P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1849
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d0dt01259a2.cif
_cod_data_source_block           JSU-S2-Tb
_cod_depositor_comments
'Adding full bibliography for 7704327--7704328.cif.'
_cod_original_cell_volume        20116.7(18)
_cod_original_sg_symbol_H-M      'I 41/a'
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_shelx_res_checksum              9498
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