Oligomeric pentafluorophenylboron azides
Fraenk, Wolfgang; Klapötke, Thomas M.; Krumm, Burkhard; Nöth, Heinrich; Suter, Max; Warchhold, Marcus; Journal of the Chemical Society, Dalton Transactions  (2000) 4635–; doi:10.1039/b007626k

data_7010277
_publ_contact_author
;
      Heinrich N\"oth
      Institut f\"ur anorganische Chemie
      Universit\"at M\"unchen
      Butenandtstr. 5-13 (Haus D)
      81377 M\"unchen
      Bundesrepublik Deutschland
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_publ_section_title
;
 Oligomeric pentafluorophenylboron azides
;
_journal_issue                   24
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              4635
_journal_paper_doi               10.1039/b007626k
_journal_year                    2000
_chemical_formula_sum            'C11 H5 B F5 N7'
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_chemical_name_systematic
; 
?
;
_space_group_IT_number           19
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_cell_angle_beta                 90.00
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_cell_measurement_temperature    193(2)
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_cell_measurement_theta_min      20.00
_cell_volume                     1324.71(17)
_computing_cell_refinement       'SMART (V4.C50)'
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_computing_molecular_graphics    'XP (SHELXTL-Ver.5)'
_computing_publication_material  'SHELXL (Sheldrick 1997)'
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_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      193(2)
_diffrn_measured_fraction_theta_full 0.812
_diffrn_measured_fraction_theta_max 0.812
_diffrn_measurement_device_type  'Siemens SMART Area-detector'
_diffrn_measurement_method       Hemisphere
_diffrn_radiation_monochromator  graphite
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_exptl_absorpt_correction_T_min  0.980584
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_exptl_crystal_colour            colorless
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_exptl_crystal_description       needle
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_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
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'calc w=1/[\s^2^(Fo^2^)+(0.0597P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_refine_ls_hydrogen_treatment' value 'mixed ' changed to
'mixed' according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_atom_sites_solution_primary' value 'direct methods' was changed to
'direct'.

'_atom_sites_solution_hydrogens' value 'geometrically' was changed to
'geom'.

Automatic conversion script
Id: cif_fix_values 6452 2018-10-05 10:23:21Z andrius 
;
_cod_original_sg_symbol_H-M      P2(1)2(1)2(1)
_cod_database_code               7010277