Lead tartrate from X-ray powder diffraction data
De Ridder, Dirk J. A.; Goubitz, Kees; Sonneveld, Ed J.; Molleman, Wim; Schenk, Henk; Acta Crystallographica Section C 58 (2002) m596–m598; doi:10.1107/S0108270102019637

data_2013056
_publ_section_title
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 Lead tartrate from X-ray powder diffraction data
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_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m596
_journal_page_last               m598
_journal_paper_doi               10.1107/S0108270102019637
_journal_volume                  58
_journal_year                    2002
_chemical_formula_iupac          '[Pb (C4 H4 O6)]'
_chemical_formula_moiety         'Pb^2+^ , C4 H4 O6^2-^'
_chemical_formula_sum            'C4 H4 O6 Pb'
_chemical_formula_weight         355.27
_chemical_name_common            'Lead tartrate'
_chemical_name_systematic
;
Lead tartrate
;
_space_group_IT_number           19
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   7.99482(3)
_cell_length_b                   8.84525(4)
_cell_length_c                   8.35318(4)
_cell_measurement_temperature    295
_cell_volume                     590.705(4)
_computing_data_collection       'Please provide missing information'
_computing_data_reduction        'Please provide missing information'
_computing_molecular_graphics    'Please provide missing information'
_computing_publication_material  'Please provide missing information'
_computing_structure_refinement  'GSAS (Larson & Von Dreele, 1994)'
_computing_structure_solution    'Please provide missing information'
_diffrn_ambient_temperature      295
_diffrn_measurement_device_type  'XPERT PRO Alpha-1'
_diffrn_radiation_monochromator  Johannson
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.54056
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       7
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       7
_diffrn_reflns_limit_l_min       0
_exptl_absorpt_coefficient_mu    55.348
_exptl_absorpt_correction_T_max  0.913
_exptl_absorpt_correction_T_min  0.532
_exptl_absorpt_process_details
;
GSAS absorption/surface roughness correction: function number 3
Surface roughness absorption correction (Suortti)
Terms =     0.38408        0.27990
Correction is not refined.
;
_exptl_crystal_density_diffrn    3.983
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             632
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   1.69
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     43
_refine_ls_number_restraints     31
_refine_ls_shift/su_max          0.13
_refine_ls_shift/su_mean         0.04
_refine_ls_weighting_scheme      sigma
_reflns_number_observed          200
_cod_data_source_file            av1119.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:
'_geom_bond_publ_flag' value 'N' changed to 'n' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29 (39 times).

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_geom_bond_publ_flag' value 'N' changed to 'n' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29 (39
times).

'_geom_angle_publ_flag' value 'N' changed to 'n' according
to /home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary
named 'cif_core.dic' version 2.4.1 from 2010-06-29 (27 times).

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_sg_symbol_Hall     p_2ac_2ab
_cod_database_code               2013056
_cod_database_fobs_code          2013056