Anisole-diphenoxide ligands and their zirconium dichloride and dialkyl complexes.
Matsuo, Tsukasa; Kawaguchi, Hiroyuki; Inorganic chemistry 46 (2007) 8426–8434; doi:10.1021/ic7011167

data_4339460
_publ_section_title
;
 Anisole-diphenoxide ligands and their zirconium dichloride and dialkyl
 complexes.
;
_journal_issue                   20
_journal_name_full               'Inorganic chemistry'
_journal_page_first              8426
_journal_page_last               8434
_journal_paper_doi               10.1021/ic7011167
_journal_volume                  46
_journal_year                    2007
_chemical_formula_moiety         'C43 H56 Cl2 O4 Zr '
_chemical_formula_sum            'C43 H56 Cl2 O4 Zr'
_chemical_formula_weight         799.04
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_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      4
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90.0000
_cell_angle_beta                 90.257(10)
_cell_angle_gamma                90.0000
_cell_formula_units_Z            2
_cell_length_a                   12.018(7)
_cell_length_b                   11.985(7)
_cell_length_c                   14.529(9)
_cell_measurement_reflns_used    7342
_cell_measurement_temperature    173.1
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      3.3
_cell_volume                     2093(2)
_computing_cell_refinement       CrystalClear
_computing_data_collection       CrystalClear
_computing_data_reduction        CrystalStructure
_computing_publication_material  'CrystalStructure 3.8'
_computing_structure_refinement  CRYSTALS
_computing_structure_solution    SIR97
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_diffrn_measured_fraction_theta_full 0.989
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'Rigaku Saturn'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71070
_diffrn_reflns_limit_h_max       15
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_diffrn_reflns_limit_l_min       -18
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_exptl_crystal_colour            colorless
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_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
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_exptl_crystal_size_mid          0.20
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_refine_ls_structure_factor_coef Fsqd
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_cod_data_source_block           '__[MeO2O]ZrCl2(thf)'
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_cod_database_code               4339460