Structures and Photochemistry of Inclusion Compounds of 9,10-Dihydro-9,10-ethenoanthracene-11,12-bis(diphenylphosphine Oxide)
Fu, T. Y.; Liu, Z.; Olovsson, G.; Scheffer, J. R.; Trotter, J.; Acta Crystallographica Section B 53 (1997) 293–299; doi:10.1107/S0108768196013602

data_2101813
_publ_contact_author
;
Professor James Trotter
Department of Chemistry
University of British Columbia
Vancouver, B.C., Canada V6T 1Z1
;
_publ_section_title
;
 Structures and Photochemistry of Inclusion Compounds of
 9,10-Dihydro-9,10-ethenoanthracene-11,12-bis(diphenylphosphine Oxide)
;
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              293
_journal_page_last               299
_journal_paper_doi               10.1107/S0108768196013602
_journal_volume                  53
_journal_year                    1997
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_cell_angle_beta                 90
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_cell_length_b                   20.748(2)
_cell_length_c                   9.436(2)
_cell_measurement_reflns_used    24
_cell_measurement_temperature    294
_cell_measurement_theta_max      40.3
_cell_measurement_theta_min      27.6
_cell_volume                     3561.4(9)
_computing_cell_refinement       'MSC/AFC (MSC, 1988)'
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;
SIR92 (Altomare et. al. 1993)
;
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_exptl_absorpt_correction_type
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\y scans (North,Phillips & Matthews, 1968)
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_exptl_crystal_colour            colorless
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/\s^2^(Fo)'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_obs         0.0390
_reflns_number_observed          2907
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_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'w = 1/\s^2^(Fo)' was changed to
'calc'. New tag '_refine_ls_weighting_details' was created. The value
of the new tag was set to 'w = 1/\s^2^(Fo)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        3561.5(6)
_cod_original_formula_sum        'C43 H38 O3 P2 '
_cod_database_code               2101813
_cod_database_fobs_code          2101813