Protonation of cyclen-based chelating agents containing fluorescent moieties
Bartoli, Francesco; Conti, Luca; Romano, Giammarco Maria; Massai, Lara; Paoli, Paola; Rossi, Patrizia; Pietraperzia, Giangaetano; Gellini, Cristina; Bencini, Andrea; New Journal of Chemistry 45 (2021) 16926–16938; doi:10.1039/D1NJ03539H

data_7060896
_publ_section_title
;
 Protonation of cyclen-based chelating agents containing fluorescent
 moieties
;
_journal_issue                   36
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              16926
_journal_page_last               16938
_journal_paper_doi               10.1039/D1NJ03539H
_journal_volume                  45
_journal_year                    2021
_chemical_formula_sum            'C28 H46 Cl4 N6 O20'
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2021-07-16 deposited with the CCDC.	2021-08-11 downloaded from the CCDC.
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
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CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
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Empirical absorption correction using spherical harmonics,
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_exptl_crystal_colour            colourless
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0234P)^2^+15.2015P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1695
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_reflns_number_gt                5646
_reflns_number_total             8976
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d1nj03539h2.cif
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_cod_depositor_comments          'Adding full bibliography for 7060896.cif.'
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               7060896
_shelxl_version_number           2014-1
_shelx_res_checksum              55711