Nucleophilic borylation of fluorobenzenes with reduced arylboranes
Budy, Hendrik; Prey, Sven E.; Buch, Christoph D.; Bolte, Michael; Lerner, Hans-Wolfram; Wagner, Matthias; Chemical Communications  (2021) –; doi:10.1039/D1CC06225E

data_7129377
_publ_section_title
;
 Nucleophilic borylation of fluorobenzenes with reduced arylboranes
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/D1CC06225E
_journal_year                    2021
_chemical_formula_moiety         'C46 H48 B2 F5, C16 H34 Na O5, C4 H8 O'
_chemical_formula_sum            'C66 H90 B2 F5 Na O6'
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_atom_sites_solution_primary     direct
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_audit_update_record
;
2021-11-02 deposited with the CCDC.	2021-11-29 downloaded from the CCDC.
;
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_diffrn_measured_fraction_theta_max 0.996
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1800P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d1cc06225e2.cif
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_cod_original_cell_volume        3286.7(5)
_cod_database_code               7129377
_shelx_shelxl_version_number     2018/3
_platon_squeeze_void_probe_radius 1.20
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_shelx_fab_checksum              28965