[(4<i>RS</i>,7<i>SR</i>,11<i>RS</i>)-4,12-Dimethyl-4,7,11-triazatridecylamine-<i>N</i>,<i>N</i>',<i>N</i>'',<i>N</i>''']nickel(II) diperchlorate
Tahirov, T.H.; Lu, T.-H.; Shu, K.; Chung, C.-S.; Acta Crystallographica Section C 50 (1994) 516–518; doi:10.1107/S0108270193009795

data_2009584
_publ_section_title
;[(4<i>RS</i>,7<i>SR</i>,11<i>RS</i>)-4,12-Dimethyl-4,7,11-triazatridecylamine-<i>N</i>,<i>N</i>',<i>N</i>'',<i>N</i>''']nickel(II)
 diperchlorate
;
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              516
_journal_page_last               518
_journal_paper_doi               10.1107/S0108270193009795
_journal_volume                  50
_journal_year                    1994
_chemical_formula_sum            'C12 H30 Cl2 N4 Ni O8'
_chemical_formula_weight         488.0
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.
_cell_angle_beta                 90.
_cell_angle_gamma                90.
_cell_formula_units_Z            4
_cell_length_a                   8.491(4)
_cell_length_b                   14.679(4)
_cell_length_c                   16.827(3)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    298(3)
_cell_measurement_theta_max      16
_cell_measurement_theta_min      6.07
_cell_volume                     2097.3(12)
_diffrn_measurement_device       'Nonius CAD-4'
_diffrn_measurement_method       \q/2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            3430
_diffrn_reflns_theta_max         29.9
_diffrn_standards_decay_%        .0
_diffrn_standards_interval_time  60
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    1.23
_exptl_absorpt_correction_T_max  0.87217
_exptl_absorpt_correction_T_min  0.87147
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.546
_exptl_crystal_description       parallelepiped
_exptl_crystal_size_max          0.31
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.13
_refine_diff_density_max         0.54
_refine_diff_density_min         -0.35
_refine_ls_goodness_of_fit_obs   0.59
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     261
_refine_ls_number_reflns         1924
_refine_ls_R_factor_obs          0.055
_refine_ls_shift/esd_max         0.78
_refine_ls_structure_factor_coef 'F; structure-factor coefficient 2.978(7)'
_refine_ls_weighting_scheme      unit
_refine_ls_wR_factor_obs         0.054
_reflns_number_observed          1924
_reflns_number_total             3430
_reflns_observed_criterion       I>=2.5\s(I)
_cod_data_source_file            as1060.cif
_cod_data_source_block           as1060_structure_1_of_1
_cod_original_cell_volume        2097.0(10)
_cod_original_formula_sum        'C12 H30 Cl2 N4 Ni1 O8'
_cod_database_code               2009584