A series of Ln-p-chlorobenzoic acid‒terpyridine complexes: lanthanide contraction effects, supramolecular interactions and luminescent behavior
Carter, Korey P.; Pope, Simon J. A.; Cahill, Christopher L.; CrystEngComm 16 (2014) 1873–; doi:10.1039/c3ce42267d

data_7213691
_publ_section_title
;
 A series of Ln-p-chlorobenzoic acid--terpyridine complexes: lanthanide
 contraction effects, supramolecular interactions and luminescent behavior
;
_journal_issue                   10
_journal_name_full               CrystEngComm
_journal_page_first              1873
_journal_paper_doi               10.1039/c3ce42267d
_journal_volume                  16
_journal_year                    2014
_chemical_formula_sum            'C36 H25 Cl3 Er N3 O7'
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_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
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_diffrn_ambient_temperature      100(2)
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_diffrn_radiation_type           MoK\a
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_diffrn_reflns_point_group_measured_fraction_full 1.000
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_diffrn_source                   'fine-focus sealed tube'
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_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    1.798
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_refine_ls_matrix_type           full
_refine_ls_number_parameters     451
_refine_ls_number_reflns         7461
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_refine_ls_restrained_S_all      0.986
_refine_ls_R_factor_all          0.0785
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0509P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_total             7461
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c3ce42267d.txt
_cod_data_source_block           Compound_9
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_cod_database_code               7213691
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