Intramolecular C−H and N−H Transfer by Ruthenium(II) Amidophosphine Complexes
Fryzuk, Michael D.; Petrella, Michael J.; Patrick, Brian O.; Organometallics 24 (2005) 5440–; doi:10.1021/om050574i

data_4076085
_publ_section_title
;
 Intramolecular C&#x2212;H and N&#x2212;H Transfer by Ruthenium(II)
 Amidophosphine Complexes
;
_journal_issue                   22
_journal_name_full               Organometallics
_journal_page_first              5440
_journal_paper_doi               10.1021/om050574i
_journal_volume                  24
_journal_year                    2005
_chemical_formula_moiety         'C32 H43 N2 P Ru Si2 '
_chemical_formula_sum            'C32 H43 N2 P Ru Si2'
_chemical_formula_weight         643.92
_space_group_IT_number           148
_symmetry_cell_setting           trigonal
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_symmetry_space_group_name_Hall  '-R 3'
_symmetry_space_group_name_H-M   'R -3 :H'
_audit_creation_date             2005-06-13
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_audit_update_record
;
?
;
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_computing_publication_material  'teXsan (MSC, 1992-1997)'
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SIR97 (Altomare, et. al. 1998)
;
_diffrn_ambient_temperature      173.2
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo^2^)]'
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_reflns_threshold_expression     I>3.00\s(I)
_cod_data_source_file            om050574isi20050708_045639.cif
_cod_data_source_block           mf428/NPNRuCOD
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        13930.4(4)
_cod_original_sg_symbol_H-M      'R -3       '
_cod_original_formula_sum        'C32 H43 N2 P Ru Si2 '
_cod_database_code               4076085