Development of highly productive nickel‒sodium phenoxyphosphine ethylene polymerization catalysts and their reaction temperature profiles
Tran, Thi V.; Nguyen, Yennie H.; Do, Loi H.; Polymer Chemistry 10 (2019) 3718–; doi:10.1039/C9PY00610A

data_1551200
_publ_section_title
;
 Development of highly productive nickel--sodium phenoxyphosphine ethylene
 polymerization catalysts and their reaction temperature profiles
;
_journal_issue                   27
_journal_name_full               'Polymer Chemistry'
_journal_page_first              3718
_journal_paper_doi               10.1039/C9PY00610A
_journal_volume                  10
_journal_year                    2019
_chemical_formula_sum            'C39 H54 Ni O3 P2'
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_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2019-04-25 deposited with the CCDC.    2019-06-03 downloaded from the CCDC.
;
_cell_angle_alpha                72.2620(10)
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_cell_measurement_temperature    123(2)
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_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_diffrn_ambient_temperature      123(2)
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_diffrn_measured_fraction_theta_max 0.973
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
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_diffrn_reflns_theta_full        25.027
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_exptl_absorpt_correction_type   empirical
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_exptl_crystal_colour            yellow
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_refine_ls_R_factor_gt           0.0466
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1539P)^2^+2.0173P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                6126
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c9py00610a2.cif
_cod_data_source_block           Ni10
_cod_depositor_comments
'Adding full bibliography for 1551200--1551201.cif.'
_cod_database_code               1551200
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