Volatility Enhancement in Calcium, Strontium, and Barium Complexes Containing β-Diketiminate Ligands with Dimethylamino Groups on the Ligand Core Nitrogen Atoms
Sedai, Baburam; Heeg, Mary Jane; Winter, Charles H.; Organometallics 28 (2009) 1032–; doi:10.1021/om8006739

data_4068302
_publ_section_title
;
 Volatility Enhancement in Calcium, Strontium, and Barium Complexes
 Containing \b-Diketiminate Ligands with Dimethylamino Groups on the
 Ligand Core Nitrogen Atoms
;
_journal_issue                   4
_journal_name_full               Organometallics
_journal_page_first              1032
_journal_paper_doi               10.1021/om8006739
_journal_volume                  28
_journal_year                    2009
_chemical_formula_sum            'C36 H76 Ba2 N16'
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_cell_angle_beta                 69.361(2)
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_computing_publication_material  SHELXL-97
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_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
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_diffrn_measurement_method       'Bruker APEX2'
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_exptl_crystal_colour            'pale yellow'
_exptl_crystal_density_diffrn    1.412
_exptl_crystal_density_method    'not measured'
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'calc w=1/[\s^2^(Fo^2^)+(0.0203P)^2^+0.2777P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_gt                7965
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_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om8006739_si_003.cif
_cod_data_source_block           gban
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        1185.28(12)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4068302