(η^6^-Fluorene)(η^6^-1-isopropyl-4-methylbenzene)ruthenium(II) bis(tetrafluoroborate), [Ru(C~10~H~14~)(C~13~H~10~)](BF~4~)~2~
Suravajjala, S.; Cervantes-Lee, F.; Porter, L.C.; Acta Crystallographica Section C 50 (1994) 1678–1681; doi:10.1107/S010827019400051X

data_2010156
_publ_section_title
;
 (\h^6^-Fluorene)(\h^6^-1-isopropyl-4-methylbenzene)ruthenium(II)
 bis(tetrafluoroborate), [Ru(C~10~H~14~)(C~13~H~10~)](BF~4~)~2~
;
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1678
_journal_page_last               1681
_journal_paper_doi               10.1107/S010827019400051X
_journal_volume                  50
_journal_year                    1994
_chemical_formula_moiety         'C23 H24 Ru,2(B F4)'
_chemical_formula_sum            'C23 H24 B2 F8 Ru'
_chemical_formula_weight         575.1
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.445(2)
_cell_length_b                   16.345(5)
_cell_length_c                   16.413(5)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    295
_cell_measurement_theta_max      15.0
_cell_measurement_theta_min      7.5
_cell_volume                     2265.5(11)
_diffrn_measurement_device       'Siemens R3m/V'
_diffrn_measurement_method       \w
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1972
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       0
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       2
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            2001
_diffrn_reflns_theta_max         22.50
_diffrn_standards_decay_%        <2
_diffrn_standards_interval_count 97
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.751
_exptl_absorpt_correction_T_max  0.4648
_exptl_absorpt_correction_T_min  0.4485
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            amber
_exptl_crystal_density_diffrn    1.686
_exptl_crystal_description       'Regularly-shaped fragment'
_exptl_crystal_size_max          0.44
_exptl_crystal_size_mid          0.36
_exptl_crystal_size_min          0.28
_refine_diff_density_max         0.49
_refine_diff_density_min         -0.33
_refine_ls_goodness_of_fit_obs   2.18
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     307
_refine_ls_number_reflns         1948
_refine_ls_R_factor_obs          0.0275
_refine_ls_shift/esd_max         0.001
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w=1/\s^2^(F)
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.0231
_reflns_number_observed          1948
_reflns_number_total             1948
_reflns_observed_criterion       I>\s(I)
_cod_data_source_file            cd1066.cif
_cod_data_source_block           cd1066_structure_1_of_1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'w=1/\s^2^(F)' was changed to
'calc'. New tag '_refine_ls_weighting_details' was created. The value
of the new tag was set to 'w=1/\s^2^(F)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_formula_sum        'C23 H24 B2 F8 Ru1'
_cod_database_code               2010156