Total Synthesis of Epoxyeujindole A.
Lu, Zhaohong; Li, Hailong; Bian, Ming; Li, Ang; Journal of the American Chemical Society 137 (2015) 13764–13767; doi:10.1021/jacs.5b09198

data_4129645
_publ_section_title
;
 Total Synthesis of Epoxyeujindole A.
;
_journal_issue                   43
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              13764
_journal_page_last               13767
_journal_paper_doi               10.1021/jacs.5b09198
_journal_volume                  137
_journal_year                    2015
_chemical_formula_sum            'C33 H37 N O4 S'
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_cell_angle_gamma                115.930(9)
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_cell_measurement_theta_min      4.399
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_computing_structure_refinement  'SHELXL-2013 (Sheldrick, 2013)'
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_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_theta_max         25.050
_diffrn_reflns_theta_min         2.112
_exptl_absorpt_coefficient_mu    0.142
_exptl_absorpt_correction_T_max  0.7457
_exptl_absorpt_correction_T_min  0.4741
_exptl_absorpt_correction_type   multi-scan
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_exptl_crystal_colour            clolorless
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_exptl_crystal_description       prismatic
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_platon_squeeze_details
;
;
_refine_diff_density_max         0.328
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_refine_ls_R_factor_all          0.1612
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0855P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                2473
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_reflns_threshold_expression     'I > 2\s(I)'
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