Polymeric [<i>p</i>-(2-Hydroxy-5-methylphenylazo)benzoato]trimethyltin
Basu Baul, T. S.; Tiekink, E. R. T.; Acta Crystallographica Section C 52 (1996) 1428–1430; doi:10.1107/S0108270196001990

data_2005066
_publ_section_title
;
 Polymeric [<i>p</i>-(2-Hydroxy-5-methylphenylazo)benzoato]trimethyltin
;
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1428
_journal_page_last               1430
_journal_paper_doi               10.1107/S0108270196001990
_journal_volume                  52
_journal_year                    1996
_chemical_formula_iupac          '[Sn (C14 H11 N2 O3) (C1 H3)3]n'
_chemical_formula_moiety         'C17 H20 N2 O3 Sn'
_chemical_formula_sum            'C17 H20 N2 O3 Sn'
_chemical_formula_weight         419.05
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.
_cell_angle_beta                 98.27(1)
_cell_angle_gamma                90.
_cell_formula_units_Z            8
_cell_length_a                   13.165(3)
_cell_length_b                   9.530(5)
_cell_length_c                   28.924(2)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293
_cell_measurement_theta_max      23.9
_cell_measurement_theta_min      21.6
_cell_volume                     3591(2)
_computing_cell_refinement       'MSC/AFC Diffractometer Control Software'
_computing_data_collection
;
MSC/AFC Diffractometer Control Software
(Molecular Structure Corporation, 1988)
;
_computing_data_reduction
'TEXSAN (Molecular Structure Corporation, 1992)'
_computing_publication_material  TEXSAN
_computing_structure_refinement  'TEXSAN; all reflection data used'
_diffrn_ambient_temperature      293
_diffrn_measurement_device       'Rigaku AFC6R'
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Rigaku rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.0356
_diffrn_reflns_av_sigmaI/netI    13.9
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       37
_diffrn_reflns_limit_l_min       -37
_diffrn_reflns_number            4605
_diffrn_reflns_theta_max         27.5
_diffrn_reflns_theta_min         3.0
_diffrn_standards_decay_%        0.58
_diffrn_standards_interval_count 400
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    1.438
_exptl_absorpt_correction_T_max  0.825
_exptl_absorpt_correction_T_min  0.627
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details   'Tompa analytical'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.550
_exptl_crystal_description       block
_exptl_crystal_F_000             1680.00
_exptl_crystal_size_max          0.39
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.14
_refine_diff_density_max         0.95
_refine_diff_density_min         -0.64
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   1.572
_refine_ls_goodness_of_fit_obs   1.572
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_parameters     208
_refine_ls_number_reflns         4160
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0639
_refine_ls_R_factor_obs          0.0639
_refine_ls_shift/esd_max         0.0007
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_all         0.0848
_refine_ls_wR_factor_obs         0.0848
_reflns_number_observed          4160
_reflns_number_total             4160
_cod_data_source_file            ta1087.cif
_cod_data_source_block           me3snd2
_cod_original_cell_volume        3591.0(10)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               2005066