A new antibacterial silver(I) complex incorporating 2,5-dimethylpyrazine and the anti-inflammatory diclofenac
Hamamci Alisir, Sevim; Dege, Necmi; Acta Crystallographica Section C 72 (2016) 947–951; doi:10.1107/S2053229616017009

data_2020655
_publ_contact_author
;
Hamamci Alisir, Sevim
Ondokuz May\?is University
Faculty of Engineering
Department of Materials Science and Engineering
55139-Samsun
Turkey
;
_publ_section_title
;
 A new antibacterial silver(I) complex incorporating 2,5-dimethylpyrazine
 and the anti-inflammatory diclofenac
;
_journal_coeditor_code           LF3042
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              947
_journal_page_last               951
_journal_paper_doi               10.1107/S2053229616017009
_journal_volume                  72
_journal_year                    2016
_chemical_formula_iupac          '[Ag2 (C14 H10 Cl2 N O2)2 (C6 H8 N2)]'
_chemical_formula_moiety         'C34 H28 Ag2 Cl4 N4 O4'
_chemical_formula_sum            'C34 H28 Ag2 Cl4 N4 O4'
_chemical_formula_weight         914.14
_chemical_name_systematic
Bis{\m-2-[2-(2,6-dichloroanilino)phenyl]acetato-\k^3^<i>O</i>,<i>O</i>':<i>O</i>}bis(\m-2,5-dimethylpyrazine-\k^2^<i>N</i>:<i>N</i>')silver(I)
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_space_group_name_Hall  '-C 2yc'
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_computing_cell_refinement
;
<i>X-AREA</i> (Stoe & Cie, 2001)
;
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;
<i>X-AREA</i> (Stoe & Cie, 2001)
;
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;
<i>X-AREA</i> (Stoe & Cie, 2001)
;
_computing_molecular_graphics    '<b>[Program(s) for molecular graphics?]</b>'
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SHELXTL (Sheldrick, 2008)
;
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SHELXL2014 (Sheldrick, 2015)
;
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WinGX (Farrugia, 2012)
;
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_diffrn_reflns_limit_h_max       47
_diffrn_reflns_limit_h_min       -47
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_exptl_crystal_description       needle
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_exptl_crystal_size_mid          0.210
_exptl_crystal_size_min          0.080
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_refine_ls_number_restraints     0
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_refine_ls_R_factor_all          0.0475
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_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0399P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_refine_ls_wR_factor_ref         0.0817
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments          'Adding full bibliography for 2020655.cif.'
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