High-Performance Organic Field-Effect Transistors Based on π-Extended Tetrathiafulvalene Derivatives
Naraso; Jun-ichi Nishida; Shinji Ando; Jun Yamaguchi; Kenji Itaka; Hideomi Koinuma; Hirokazu Tada; Shizuo Tokito; Yoshiro Yamashita; Journal of the American Chemical Society 127 (2005) 10142–10143; doi:10.1021/ja051755e

data_4111799
_publ_contact_author
;
Dr. Yoshiro Yamashita
Department of Electronic Chemistry
Interdisciplinary Graduate School of Science and Engineering
Tokyo Institute of Technology
Nagatsuta, Midori-ku, Yokohama 226-8502, Japan
;
_publ_contact_author_email       yoshiro@echem.titech.ac.jp
_publ_contact_author_fax         +81-45-924-5489
_publ_contact_author_phone       +81-45-924-5571
_publ_section_title
;
 High-Performance Organic Field-Effect Transistors Based on \p-Extended
 Tetrathiafulvalene Derivatives
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              10142
_journal_page_last               10143
_journal_paper_doi               10.1021/ja051755e
_journal_volume                  127
_journal_year                    2005
_chemical_formula_sum            'C16 H8 N4 S4'
_chemical_formula_weight         384.51
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                94.01(9)
_cell_angle_beta                 90.78(8)
_cell_angle_gamma                105.03(9)
_cell_formula_units_Z            2
_cell_length_a                   4.88(1)
_cell_length_b                   5.75(1)
_cell_length_c                   29.07(5)
_cell_measurement_reflns_used    7263
_cell_measurement_temperature    93.2
_cell_measurement_theta_max      27.7
_cell_measurement_theta_min      3.5
_cell_volume                     785(3)
_computing_cell_refinement       PROCESS-AUTO
_computing_data_collection       PROCESS-AUTO
_computing_data_reduction        'teXsan Ver. 1.11'
_computing_publication_material  'teXsan Ver. 1.11'
_computing_structure_refinement  'teXsan Ver. 1.10'
_computing_structure_solution    SIR97
_diffrn_detector_area_resol_mean 10.00
_diffrn_measured_fraction_theta_full 0.9994
_diffrn_measured_fraction_theta_max 0.9994
_diffrn_measurement_device_type  'Rigaku RAXIS-RAPID Imaging Plate'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.085
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_k_max       7
_diffrn_reflns_limit_k_min       -7
_diffrn_reflns_limit_l_max       37
_diffrn_reflns_limit_l_min       -36
_diffrn_reflns_number            7365
_diffrn_reflns_theta_full        27.49
_diffrn_reflns_theta_max         27.49
_exptl_absorpt_coefficient_mu    0.610
_exptl_absorpt_correction_T_max  0.958
_exptl_absorpt_correction_T_min  0.335
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(Higashi, 1995)'
_exptl_crystal_colour            palered
_exptl_crystal_density_diffrn    1.625
_exptl_crystal_description       platelet
_exptl_crystal_size_max          0.350
_exptl_crystal_size_mid          0.300
_exptl_crystal_size_min          0.070
_refine_diff_density_max         1.22
_refine_diff_density_min         -1.49
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.810
_refine_ls_hydrogen_treatment    noref
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_refine_ls_R_factor_gt           0.0949
_refine_ls_shift/su_max          0.0026
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^) + (0.05000(Max(Fo^2^,0) + 2Fc^2^)/3)^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.2139
_reflns_number_gt                1234
_reflns_number_total             3580
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
_cod_data_source_file            ja051755esi20050318_020547_1.cif
_cod_data_source_block           4
_cod_original_cell_volume        785(10)
_cod_original_sg_symbol_H-M      'P -1         '
_cod_original_formula_sum        'C16 H8 N4 S4 '
_cod_database_code               4111799