Fluorine-decoupled carbon spectroscopy for the determination of configuration at fully substituted, trifluoromethyl- and perfluoroalkyl-bearing carbons: comparison with (19)f-(1)h heteronuclear overhauser effect spectroscopy.
Mandhapati, Appi Reddy; Kato, Takayuki; Matsushita, Takahiko; Ksebati, Bashar; Vasella, Andrea; Böttger, Erik C; Crich, David; The Journal of organic chemistry 80 (2015) 1754–1763; doi:10.1021/jo502677a

data_4030566
_publ_section_title
;
 Fluorine-decoupled carbon spectroscopy for the determination of
 configuration at fully substituted, trifluoromethyl- and
 perfluoroalkyl-bearing carbons: comparison with (19)f-(1)h heteronuclear
 overhauser effect spectroscopy.
;
_journal_issue                   3
_journal_name_full               'The Journal of organic chemistry'
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_journal_page_last               1763
_journal_paper_doi               10.1021/jo502677a
_journal_volume                  80
_journal_year                    2015
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;
 ?
;
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_symmetry_space_group_name_Hall  '-P 1'
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_diffrn_reflns_Laue_measured_fraction_full 0.921
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
 w=1/[\s^2^(Fo^2^)+(0.0817P)^2^+3.2419P]
 where P=(Fo^2^+2Fc^2^)/3
;
_refine_ls_weighting_scheme      calc
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_cod_depositor_comments          'Adding full bibliography for 4030566.cif.'
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