A new route to medium and large heterocyclic compounds
Ventrice, Tina; Campi, Eva M.; Roy Jackson, W.; Patti, Antonio F.; Chemical Communications  (1999) 1463–; doi:10.1039/a904168k

data_7110602
_publ_section_title
;
 A new route to medium and large heterocyclic compounds
;
_journal_issue                   16
_journal_name_full               'Chemical Communications'
_journal_page_first              1463
_journal_paper_doi               10.1039/a904168k
_journal_year                    1999
_chemical_formula_moiety         'C25 H33 N O2 '
_chemical_formula_sum            'C25 H33 N O2'
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_audit_creation_method           'by teXsan v1.8'
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_cell_measurement_temperature    123(2)
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_diffrn_ambient_temperature      123(2)
_diffrn_measurement_device_type  'Nonius Kappa CCD'
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_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_type           'Mo K\a'
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_diffrn_reflns_limit_l_min       -12
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_diffrn_reflns_reduction_process 'Lp corrections applied'
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_diffrn_reflns_theta_min         3.26
_exptl_absorpt_coefficient_mu    0.073
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.167
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_refine_ls_R_factor_gt           0.0368
_refine_ls_shift/su_max          0.0004
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo)]'
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_cod_depositor_comments
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The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
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_cod_original_cell_volume        2159.46(6)
_cod_original_sg_symbol_H-M      'P 21/n     '
_cod_original_formula_sum        'C25 H33 N O2 '
_cod_database_code               7110602