Part 1. Solubility effect on the formation of coordination polymer networks between AgNO<small><sub>3</sub></small> and <strong>L</strong> (<strong>L</strong> = ethanediyl bis(isonicotinate) as a function of solvent
Adeline Y. Robin; Jorge L. Sagué; Katharina M. Fromm; CrystEngComm 8 (2006) 403–; doi:10.1039/b517191a

data_7203240
_publ_section_title
;
 Part 1. Solubility effect on the formation of coordination polymer
 networks between AgNO<small><sub>3</sub></small> and
 <strong>L</strong>                (<strong>L</strong>                = ethanediyl
 bis(isonicotinate) as a function of solvent
;
_journal_issue                   5
_journal_name_full               CrystEngComm
_journal_page_first              403
_journal_paper_doi               10.1039/b517191a
_journal_volume                  8
_journal_year                    2006
_chemical_formula_moiety         '[Ag(C14H12N2O4)NO3]'
_chemical_formula_sum            'C14 H12 Ag N3 O7'
_chemical_formula_weight         442.14
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                93.15(2)
_cell_angle_beta                 99.898(16)
_cell_angle_gamma                91.43(2)
_cell_formula_units_Z            2
_cell_length_a                   6.1591(13)
_cell_length_b                   8.895(3)
_cell_length_c                   14.439(3)
_cell_measurement_temperature    293(2)
_cell_volume                     777.6(4)
_computing_cell_refinement       Xred
_computing_data_collection       Stoe
_computing_data_reduction        Xred
_computing_molecular_graphics    Schakal
_computing_publication_material  Word
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.439
_diffrn_measured_fraction_theta_max 0.439
_diffrn_measurement_device_type  'Stoe IPDS'
_diffrn_measurement_method       'Omega scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0213
_diffrn_reflns_av_sigmaI/netI    0.0216
_diffrn_reflns_limit_h_max       7
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       1
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            1565
_diffrn_reflns_theta_full        27.01
_diffrn_reflns_theta_max         27.01
_diffrn_reflns_theta_min         2.87
_exptl_absorpt_coefficient_mu    1.341
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.888
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             440
_refine_diff_density_max         0.189
_refine_diff_density_min         -0.216
_refine_diff_density_rms         0.040
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.070
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     226
_refine_ls_number_reflns         1494
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.070
_refine_ls_R_factor_all          0.0408
_refine_ls_R_factor_gt           0.0312
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0334P)^2^+0.7275P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0686
_refine_ls_wR_factor_ref         0.0732
_reflns_number_gt                1291
_reflns_number_total             1494
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b517191a.txt
_cod_data_source_block           '[AgLNO3]'
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7203240