<i>catena</i>-Poly[[aqua(2,2'-bipyridine-<i>N</i>,<i>N</i>')cadmium(II)-μ-cyclohexane-1,4-dicarboxylato-κ^4^<i>O</i>,<i>O</i>':<i>O</i>'',<i>O</i>'''] 2.5-hydrate]
Li, Na; Wang, Yan-Qin; Weng, Jia-Bao; Acta Crystallographica Section E 63 (2007) m1862–m1863; doi:10.1107/S160053680702020X

data_2214267
_publ_section_title
;<i>catena</i>-Poly[[aqua(2,2'-bipyridine-<i>N</i>,<i>N</i>')cadmium(II)-\m-cyclohexane-1,4-dicarboxylato-\k^4^<i>O</i>,<i>O</i>':<i>O</i>'',<i>O</i>''']
 2.5-hydrate]
;
_journal_coeditor_code           HY2051
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1862
_journal_page_last               m1863
_journal_paper_doi               10.1107/S160053680702020X
_journal_volume                  63
_journal_year                    2007
_chemical_formula_iupac          '[Cd (C8 H10 O4) (C10 H8 N2) (H2 O)], 2.5H2O'
_chemical_formula_moiety         'C18 H20 Cd N2 O5, 2.5(H2 O)'
_chemical_formula_sum            'C18 H25 Cd N2 O7.5'
_chemical_formula_weight         501.81
_chemical_name_systematic
;
catena-Poly[[aqua(2,2'-bipyridine-N,N')cadmium(II)-\m-
cyclohexane-1,4-dicarboxylato-\k^4^O,O':O'',O'''] 2.5-hydrate]
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 111.129(7)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   15.657(2)
_cell_length_b                   13.140(2)
_cell_length_c                   21.287(3)
_cell_measurement_reflns_used    5652
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.4835
_cell_measurement_theta_min      2.0508
_cell_volume                     4085.0(10)
_computing_cell_refinement       CrystalClear
_computing_data_collection       'CrystalClear (Rigaku, 2000)'
_computing_data_reduction        CrystalClear
_computing_molecular_graphics    'SHELXTL (Siemens, 1994)'
_computing_publication_material  SHELXTL
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 14.6306
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Rigaku Mercury70 CCD'
_diffrn_measurement_method       \w
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0130
_diffrn_reflns_av_sigmaI/netI    0.0397
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            16648
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         2.08
_exptl_absorpt_coefficient_mu    1.113
_exptl_absorpt_correction_T_max  0.893
_exptl_absorpt_correction_T_min  0.789
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Sheldrick, 1996)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.632
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1020
_exptl_crystal_size_max          0.35
_exptl_crystal_size_mid          0.25
_exptl_crystal_size_min          0.15
_refine_diff_density_max         0.604
_refine_diff_density_min         -0.422
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.065
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     258
_refine_ls_number_reflns         4681
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.065
_refine_ls_R_factor_all          0.0246
_refine_ls_R_factor_gt           0.0225
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0247P)^2^+3.851P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0529
_refine_ls_wR_factor_ref         0.0542
_reflns_number_gt                4397
_reflns_number_total             4681
_reflns_threshold_expression     I>2\s(I)
_cod_data_source_file            hy2051.cif
_cod_data_source_block           I
_cod_original_cell_volume        4085.2(11)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               2214267
_cod_database_fobs_code          2214267