Doubly N-Confused Porphyrin: A New Complexing Agent Capable of Stabilizing Higher Oxidation States
Hiroyuki Furuta; Hiromitsu Maeda; Atsuhiro Osuka; Journal of the American Chemical Society 122 (2000) 803–807; doi:10.1021/ja992679g

data_4115911
_publ_contact_author_address
;
    Department of Chemistry, graduate School of Science, Kyoto University,
Kyoto-606-8502, Japan
;
_publ_contact_author_email       ' hfuruta@kuchem.kyoto-u.ac.jp '
_publ_contact_author_fax         ' 81-75-753-3970 '
_publ_contact_author_name        ' Hiroyuki Furuta'
_publ_contact_author_phone       ' 81-75-753-4010 '
_publ_section_title
;
 Doubly N-Confused Porphyrin: A New Complexing Agent Capable of
 Stabilizing Higher Oxidation States
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              803
_journal_page_last               807
_journal_paper_doi               10.1021/ja992679g
_journal_volume                  122
_journal_year                    2000
_chemical_formula_moiety         'C46 H14 F20 N4 O '
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_cell_angle_beta                 107
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_cell_measurement_temperature    296.2
_cell_measurement_theta_max      12.5
_cell_measurement_theta_min      11.0
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_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
_computing_data_reduction        'teXsan for Windows (MSC, 1997)'
_computing_publication_material  'teXsan for Windows (MSC, 1997)'
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_computing_structure_solution
;
SIR97 (Altomare, et. al. 1997)
;
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_diffrn_radiation_detector       'scintillation counter'
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_refine_ls_extinction_method     none
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_refine_ls_goodness_of_fit_ref   1.830
_refine_ls_hydrogen_treatment    noref
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_refine_ls_number_constraints    0
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_refine_ls_number_reflns         2771
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0620
_refine_ls_R_factor_gt           0.0620
_refine_ls_shift/su_max          0.0000
_refine_ls_shift/su_mean         0.0003
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo) + 0.00000|Fo|^2^]'
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_reflns_threshold_expression     I>2.00\s(I)
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_cod_data_source_block           '_master_file_afc7*.xtl____'
_cod_original_cell_volume        4246(2)
_cod_original_sg_symbol_H-M      'P 21/n '
_cod_original_formula_sum        'C46 H14 F20 N4 O '
_cod_database_code               4115911