data_5000359
_chemical_formula_moiety         ?
_chemical_formula_sum            'C58 H70 B F24 N O3 Os P2'
_chemical_formula_weight         1548.15
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 97.412(4)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   15.183(2)
_cell_length_b                   17.785(3)
_cell_length_c                   24.578(4)
_cell_measurement_reflns_used    ?
_cell_measurement_temperature    113
_cell_measurement_theta_max      ?
_cell_measurement_theta_min      ?
_cell_volume                     6581.5(19)
_diffrn_ambient_temperature      113
_diffrn_detector                 'Smart 6000 CCD'
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 1
_diffrn_measured_fraction_theta_max 1
_diffrn_measurement_device_type  'Bruker AXS Smart6000'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  3959
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -31
_diffrn_reflns_number            3
_diffrn_reflns_theta_full        27.6665
_diffrn_reflns_theta_max         27.6665
_diffrn_reflns_theta_min         2.02578
_diffrn_standards_decay_%        ?
_diffrn_standards_interval_count ?
_diffrn_standards_number         ?
_exptl_absorpt_coefficient_mu    2.0948
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_type   none
_exptl_absorpt_process_details   none
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.562
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       'small fragment'
_exptl_crystal_F_000             3104
_exptl_crystal_size_max          .23
_exptl_crystal_size_mid          .20
_exptl_crystal_size_min          .11
_refine_diff_density_max         2.22
_refine_diff_density_min         -1.53
_refine_ls_abs_structure_details none
_refine_ls_abs_structure_Flack   ?
_refine_ls_extinction_coef       -0.000000003(10)
_refine_ls_extinction_expression
;
Larson, A. C. (1967).  Acta Cryst. 23, p. 664.  Eq. (3)
;
_refine_ls_extinction_method     Zachariasen
_refine_ls_goodness_of_fit_ref   1.0819
_refine_ls_hydrogen_treatment    ?
_refine_ls_matrix_type           full
_refine_ls_number_parameters     782
_refine_ls_number_reflns         3959
_refine_ls_R_factor_gt           0.0627
_refine_ls_shift/su_max          0.3486
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w^-1^=\s^2^(F)+(.07F)^2^
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.0552
_reflns_number_gt                3959
_reflns_number_total             15093
_reflns_threshold_expression     'Fo^2^> 2.33\s(Fo^2^)'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C58 H70 B1 F24 N1 O3 Os1 P2'
_cod_database_code               5000359