Two structural types of 1,3-alternate tetrapropoxycalix[4]arene derivatives in the solid state.
Sýkora, Jan; Budka, Jan; Lhoták, Pavel; Stibor, Ivan; Císarová, Ivana; Organic & biomolecular chemistry 3 (2005) 2572–2578; doi:10.1039/b505454k

data_7150190
_publ_section_title
;
 Two structural types of 1,3-alternate tetrapropoxycalix[4]arene
 derivatives in the solid state.
;
_journal_issue                   14
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              2572
_journal_page_last               2578
_journal_paper_doi               10.1039/b505454k
_journal_volume                  3
_journal_year                    2005
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;
?
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;
?
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_atom_sites_solution_primary     direct
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_computing_cell_refinement
;
SPARE
;
_computing_data_collection
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DATA COLLECTION
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_computing_data_reduction
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SPARE
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_computing_molecular_graphics
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CAMERON (Watkin et al 1996)
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_computing_publication_material
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CRYSTALS (Watkin et al 2001)
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CRYSTALS (Watkin et al 2001)
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SHELXS 86 (Sheldrick, 1986)
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;
Unknown
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_diffrn_measurement_method       \w/2\q
_diffrn_radiation_monochromator  graphite
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_diffrn_reflns_limit_l_min       -24
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;
Method= Tukey and Prince
W = [weight] * [1-(deltaF/6*sigmaF)^2]^2

1.62 1.45 1.00
;
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_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic ' changed to 'monoclinic'
according to '/home/adriana/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1555 2011-01-17 13:19:09Z saulius 

The following automatic conversions were performed:

'_chemical_melting_point' value 'not measured' was changed to '?' -
the value is undefined or not given.

Automatic conversion script
Id: cif_fix_values 1569 2011-02-09 13:29:24Z adriana 
;
_cod_original_cell_volume        3370.7(1)
_cod_original_sg_symbol_H-M      'C 1 2/c 1 '
_cod_original_formula_sum        ' C20 H24 O2 '
_cod_database_code               7150190