A Bench-Stable, Single-Component Precatalyst for Silyl-Heck Reactions.
Krause, Sarah B.; McAtee, Jesse R.; Yap, Glenn P. A.; Watson, Donald A.; Organic letters 19 (2017) 5641–5644; doi:10.1021/acs.orglett.7b02807

data_1547490
_publ_section_title
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 A Bench-Stable, Single-Component Precatalyst for Silyl-Heck Reactions.
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_journal_issue                   20
_journal_name_full               'Organic letters'
_journal_page_first              5641
_journal_page_last               5644
_journal_paper_doi               10.1021/acs.orglett.7b02807
_journal_volume                  19
_journal_year                    2017
_chemical_formula_moiety         'C64 H102 I4 P4 Pd2, 5(C2 H4 Cl2)'
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_diffrn_measurement_device_type  'Bruker AXS APEX diffractometer'
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_refine_ls_number_restraints     0
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_refine_ls_R_factor_all          0.0442
_refine_ls_R_factor_gt           0.0309
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0266P)^2^+3.1387P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           donw052_sq
_cod_depositor_comments
'Adding full bibliography for 1547490--1547491.cif.'
_cod_database_code               1547490
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