Complexation of uranyl ions by polyphenols. Crystal structures of two linear oligomers and one uranyl ion complex
Thuéry, Pierre; Nierlich, Martine; Asfari, Zouhair; Vicens, Jacques; Journal of the Chemical Society, Dalton Transactions  (2000) 1297–; doi:10.1039/b001083i

data_7009442
_publ_section_title
;
 Complexation of uranyl ions by polyphenols. Crystal structures of two
 linear oligomers and one uranyl ion complex
;
_journal_issue                   8
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              1297
_journal_paper_doi               10.1039/b001083i
_journal_year                    2000
_chemical_formula_sum            'C81 H118 N4 O9 U'
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_computing_data_collection       'Kappa-CCD software (Nonius, 1997)'
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_computing_molecular_graphics    'SHELXTL (Sheldrick, 1999)'
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_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.926
_diffrn_measured_fraction_theta_max 0.926
_diffrn_measurement_device_type  'Nonius Kappa-CCD'
_diffrn_measurement_method       'area detector'
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_exptl_crystal_colour            'translucent dark orange'
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_exptl_crystal_density_meas      ?
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_refine_ls_R_factor_all          0.1348
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.1190P)^2^+25.2051P] where P=(Fo^2^+2Fc^2^)/3'
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