Mechanistic studies of the palladium-catalyzed S,O-ligand promoted C–H olefination of aromatic compounds
Naksomboon, Kananat; Gómez-Bengoa, Enrique; Mehara, Jaya; Roithová, Jana; Otten, Edwin; Fernández-Ibáñez, M. Ángeles; Chemical Science 14 (2023) 2943–2953; doi:10.1039/D2SC06840K

data_1568425
_publ_section_title
;
 Mechanistic studies of the palladium-catalyzed S,O-ligand promoted C--H
 olefination of aromatic compounds
;
_journal_issue                   11
_journal_name_full               'Chemical Science'
_journal_page_first              2943
_journal_page_last               2953
_journal_paper_doi               10.1039/D2SC06840K
_journal_volume                  14
_journal_year                    2023
_chemical_formula_sum            'C30 H29 O4 P Pd S'
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_audit_update_record
;
2019-12-03 deposited with the CCDC.	2023-02-16 downloaded from the CCDC.
;
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_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
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_exptl_crystal_description       block
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0082P)^2^+8.6315P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                4609
_reflns_number_total             5489
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d2sc06840k2.cif
_cod_data_source_block           mo_molan472_0ma_a
_cod_depositor_comments
'Adding full bibliography for 1568424--1568427.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               1568425
_shelx_shelxl_version_number     2014/7
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