Increased carrier mobility in end-functionalized oligosilanes
Surampudi, S.; Yeh, M.-L.; Siegler, M. A.; Hardigree, J. F. Martinez; Kasl, T. A.; Katz, H. E.; Klausen, R. S.; Chem. Sci. 6 (2015) 1905–; doi:10.1039/C4SC03274H

data_1518528
_publ_section_title
;
 Increased carrier mobility in end-functionalized oligosilanes
;
_journal_issue                   3
_journal_name_full               'Chem. Sci.'
_journal_page_first              1905
_journal_paper_doi               10.1039/C4SC03274H
_journal_volume                  6
_journal_year                    2015
_chemical_formula_moiety         'C30 H40 N2 O4 Si4'
_chemical_formula_sum            'C30 H40 N2 O4 Si4'
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_space_group_name_Hall           '-P 1'
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2014-10-24 deposited with the CCDC.
2015-01-05 downloaded from the CCDC.
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET)
(compiled Jan 14 2014,18:38:05)
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET)
(compiled Jan 14 2014,18:38:05)
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET)
(compiled Jan 14 2014,18:38:05)
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_diffrn_ambient_temperature      110(2)
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_diffrn_radiation_wavelength     1.54178
_diffrn_reflns_av_R_equivalents  0.0506
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_diffrn_reflns_point_group_measured_fraction_full 0.988
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET)
(compiled Jan 14 2014,18:38:05)
Analytical numeric absorption correction using a multifaceted crystal
            model based on expressions derived by R.C. Clark & J.S. Reid.
(Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            'pale yellow'
_exptl_crystal_density_diffrn    1.181
_exptl_crystal_description       needle
_exptl_crystal_F_000             644
_exptl_crystal_size_max          0.41
_exptl_crystal_size_mid          0.05
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_refine_diff_density_rms         0.077
_refine_ls_extinction_method     none
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_refine_ls_number_restraints     0
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_refine_ls_R_factor_all          0.0889
_refine_ls_R_factor_gt           0.0629
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
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 w=1/[\s^2^(Fo^2^)+(0.1067P)^2^+0.7535P]
 where P=(Fo^2^+2Fc^2^)/3
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_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1706
_refine_ls_wR_factor_ref         0.1941
_reflns_Friedel_coverage         0.000
_reflns_number_gt                4730
_reflns_number_total             6566
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c4sc03274h2.cif
_cod_data_source_block           Si4C1
_cod_depositor_comments
'Adding full bibliography for 1518526--1518529.cif.'
_cod_database_code               1518528
_shelxl_version_number           2013-2
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