Two Quasi-Stable Lead(II) Hydrides at Ambient Temperature
Queen, Joshua Douglas; Fettinger, James C.; Power, Philip P.; Chemical Communications  (2019) –; doi:10.1039/C9CC05106F

data_7123944
_publ_section_title
;
 Two Quasi-Stable Lead(II) Hydrides at Ambient Temperature
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/C9CC05106F
_journal_year                    2019
_chemical_formula_moiety         'C60 H76 Pb2, 4(C7 H8)'
_chemical_formula_sum            'C88 H108 Pb2'
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Air-sensitive,Moisture-sensitive,Heat-sensitive,Light-sensitive
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_audit_update_record
;
2019-05-12 deposited with the CCDC.    2019-08-02 downloaded from the CCDC.
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_diffrn_reflns_limit_l_min       -19
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0131P)^2^+0.6821P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0338
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_reflns_number_gt                10955
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 
;
_cod_database_code               7123944
_shelx_shelxl_version_number     2018/3
_shelx_estimated_absorpt_t_min   0.232
_shelx_estimated_absorpt_t_max   0.519
_shelx_res_checksum              27152