Unlocking the potential of organopalladium complexes for high-grade serous ovarian cancer therapy.
Scattolin, Thomas; Cavarzerani, Enrico; Alessi, Dario; Mauceri, Matteo; Botter, Eleonora; Tonon, Giovanni; Caligiuri, Isabella; Repetto, Ombretta; Kamensek, Urska; Brezar, Simona Kranjc; Dalla Pozza, Maria; Palazzolo, Stefano; Cemazar, Maja; Canzonieri, Vincenzo; Demitri, Nicola; Nolan, Steven P.; Gasser, Gilles; Visentin, Fabiano; Rizzolio, Flavio; Dalton transactions (Cambridge, England : 2003) 54 (2025) 4685–4696; doi:10.1039/d5dt00194c

data_7718059
_publ_section_title
;
 Unlocking the potential of organopalladium complexes for high-grade
 serous ovarian cancer therapy.
;
_journal_issue                   11
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              4685
_journal_page_last               4696
_journal_paper_doi               10.1039/d5dt00194c
_journal_volume                  54
_journal_year                    2025
_chemical_formula_moiety         'C27 H27 Cl N2 O8 Pd'
_chemical_formula_sum            'C27 H27 Cl N2 O8 Pd'
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_space_group_name_Hall           '-P 1'
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_atom_sites_solution_secondary   difmap
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_audit_update_record
;
2024-03-27 deposited with the CCDC.	2025-02-14 downloaded from the CCDC.
;
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_cell_measurement_theta_min      1.516
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_computing_data_collection       'Elettra XRD2 Data Collection SW'
_computing_data_reduction        'XDS (Kabsch, 2010)'
_computing_molecular_graphics    'Ortep3 for Windows - Coot'
_computing_publication_material  'enCIFer - publCIF'
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;
'Arinax MD2s Goniometer, Pilatus 6M detector'
;
_diffrn_measurement_method       'Rotating crystal'
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_diffrn_source                   'Elettra Synchrotron - XRD2 BL'
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_exptl_crystal_description       'Thin rods'
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_exptl_crystal_size_max          0.100
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_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
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_refine_ls_matrix_type           full
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_refine_ls_restrained_S_all      1.050
_refine_ls_R_factor_all          0.0326
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_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0367P)^2^+0.9306P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0831
_refine_ls_wR_factor_ref         0.0834
_reflns_Friedel_coverage         0.000
_reflns_number_gt                11366
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7718057--7718061.cif.'
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_shelx_estimated_absorpt_t_min   0.944
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_shelx_res_checksum              45937