(<i>E</i>)-1,1-Diphenyl-2-(thiophen-2-ylmethylidene)hydrazine
Cabrera-Vivas, Blanca M.; Flores-Alamo, Marcos; Meléndrez-Luévano, Ruth; Meléndez-Balbuena, Lidia; Ramirez, Juan C.; Acta Crystallographica Section E 70 (2014) o80–; doi:10.1107/S1600536813033874

data_2239101
_publ_section_title
;
 (<i>E</i>)-1,1-Diphenyl-2-(thiophen-2-ylmethylidene)hydrazine
;
_journal_coeditor_code           IS5326
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o80
_journal_paper_doi               10.1107/S1600536813033874
_journal_volume                  70
_journal_year                    2014
_chemical_formula_iupac          'C17 H14 N2 S'
_chemical_formula_moiety         'C17 H14 N2 S'
_chemical_formula_sum            'C17 H14 N2 S'
_chemical_formula_weight         278.36
_chemical_name_systematic
;
(<i>E</i>)-1,1-Diphenyl-2-(thiophen-2-ylmethylidene)hydrazine
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                100.290(6)
_cell_angle_beta                 101.696(7)
_cell_angle_gamma                109.129(9)
_cell_formula_units_Z            4
_cell_length_a                   9.8336(11)
_cell_length_b                   9.8665(9)
_cell_length_c                   16.6357(8)
_cell_measurement_reflns_used    6444
_cell_measurement_temperature    144(2)
_cell_measurement_theta_max      25.9999
_cell_measurement_theta_min      3.5597
_cell_volume                     1439.9(3)
_computing_cell_refinement
;
<i>CrysAlis PRO</i> (Agilent, 2012)
;
_computing_data_collection
;
<i>CrysAlis PRO</i> (Agilent, 2012)
;
_computing_data_reduction
;
<i>CrysAlis RED</i> (Agilent, 2012)
;
_computing_molecular_graphics    'Mercury (Macrae <i>et al.</i>, 2006)'
_computing_publication_material  'WinGX (Farrugia, 2012)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      144(2)
_diffrn_detector_area_resol_mean 10.4685
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Agilent Xcalibur (Atlas, Gemini)'
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0197
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            10771
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         26.065
_diffrn_reflns_theta_min         3.568
_exptl_absorpt_coefficient_mu    0.215
_exptl_absorpt_correction_T_max  0.939
_exptl_absorpt_correction_T_min  0.916
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(<i>CrysAlis RED</i>; Agilent, 2012)
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.284
_exptl_crystal_description       prism
_exptl_crystal_F_000             584
_exptl_crystal_size_max          0.579
_exptl_crystal_size_mid          0.511
_exptl_crystal_size_min          0.362
_refine_diff_density_max         0.225
_refine_diff_density_min         -0.331
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.074
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     361
_refine_ls_number_reflns         5672
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.074
_refine_ls_R_factor_all          0.0486
_refine_ls_R_factor_gt           0.0394
_refine_ls_shift/su_max          0
_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0382P)^2^+0.4189P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0916
_refine_ls_wR_factor_ref         0.0987
_reflns_number_gt                4856
_reflns_number_total             5672
_reflns_threshold_expression     I>2\s(I)
_cod_data_source_file            is5326sup1.cif
_cod_data_source_block           I
_cod_original_cell_volume        1439.9(2)
_cod_database_code               2239101
_cod_database_fobs_code          2239101