Thiohydrazide complexes of molybdenum and their relevance to reduction of dinitrogen to ammonia.
Sengupta, Dolan; Gangopadhyay, Snigdha; Drew, Michael G. B.; Gangopadhyay, Pijush Kanti; Dalton transactions (Cambridge, England : 2003) 44 (2015) 1323–1331; doi:10.1039/c4dt01945h

data_7033215
_publ_section_title
;
 Thiohydrazide complexes of molybdenum and their relevance to reduction of
 dinitrogen to ammonia.
;
_journal_issue                   3
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1323
_journal_page_last               1331
_journal_paper_doi               10.1039/c4dt01945h
_journal_volume                  44
_journal_year                    2015
_chemical_formula_sum            'C39 H36 Mo N6 O3 S3'
_chemical_formula_weight         828.86
_chemical_name_systematic
; 
 ? 
;
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_symmetry_space_group_name_Hall  '-P 3'
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_atom_sites_solution_primary     direct
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_cell_angle_beta                 90.00
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_cell_length_c                   11.9425(3)
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_computing_data_reduction        'Crysalis, Oxford Diffraction'
_computing_molecular_graphics    PLATON(Spek,2004)
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_diffrn_ambient_temperature      150(2)
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_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device       'Oxford Diffaction X-Calibur System'
_diffrn_measurement_method       '321 frames, counting time 10 s.'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
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_diffrn_reflns_limit_l_min       -16
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_refine_ls_shift/su_mean         0.000
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;
_refine_ls_weighting_details 
  w=1/[\s^2^(Fo^2^)+(0.0365P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3 
;
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_cod_depositor_comments
'Adding full bibliography for 7033215--7033217.cif.'
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_cod_database_code               7033215