Blue LED induced solvent-free multicomponent reactions among aryl diazoacetates, pyridine derivatives and maleimides: direct eco-friendly synthesis of densely functionalized itaconimides
Maiti, Debajit; Das, Ranajit; Prabakar, Tejas; Sen, Subhabrata; Green Chemistry 24 (2022) 3001–3008; doi:10.1039/D1GC03546K

data_7244523
_publ_section_title
;
 Blue LED induced solvent-free multicomponent reactions among aryl
 diazoacetates, pyridine derivatives and maleimides: direct eco-friendly
 synthesis of densely functionalized itaconimides
;
_journal_issue                   7
_journal_name_full               'Green Chemistry'
_journal_page_first              3001
_journal_page_last               3008
_journal_paper_doi               10.1039/D1GC03546K
_journal_volume                  24
_journal_year                    2022
_chemical_formula_moiety         'C26 H25 N3 O6'
_chemical_formula_sum            'C26 H25 N3 O6'
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_space_group_name_H-M_alt        'P b c a'
_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2021-09-17 deposited with the CCDC.	2022-02-24 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_computing_cell_refinement       'Bruker SAINT'
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_diffrn_measurement_device_type  'Bruker PHOTON100 CMOS'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_point_group_measured_fraction_max 0.997
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_diffrn_source                   X-ray
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_refine_ls_extinction_coef       0.0034(16)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2017/1 (Sheldrick 2017)'
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_refine_ls_hydrogen_treatment    constr
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_refine_ls_number_reflns         4921
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.068
_refine_ls_R_factor_all          0.1499
_refine_ls_R_factor_gt           0.1071
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1491P)^2^+12.4193P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2880
_refine_ls_wR_factor_ref         0.3348
_reflns_Friedel_coverage         0.000
_reflns_number_gt                3233
_reflns_number_total             4921
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d1gc03546k2.cif
_cod_data_source_block           mo_MAL_TOL_1_0m_a
_cod_depositor_comments
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The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'Multi-Scan' was
changed to 'multi-scan' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas 

 Adding full bibliography for 7244523.cif.
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_cod_database_code               7244523
_shelx_shelxl_version_number     2017/1
_shelx_res_checksum              23631