Expansion of Thiele's Acid Chemistry in Pursuit of a Suite of Conformationally Constrained Scaffolds.
Chen, Jun; Kilpatrick, Brenden; Oliver, Allen G.; Wulff, Jeremy E.; The Journal of organic chemistry 80 (2015) 8979–8989; doi:10.1021/acs.joc.5b01332

data_4036262
_publ_section_title
;
 Expansion of Thiele's Acid Chemistry in Pursuit of a Suite of
 Conformationally Constrained Scaffolds.
;
_journal_issue                   18
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              8979
_journal_page_last               8989
_journal_paper_doi               10.1021/acs.joc.5b01332
_journal_volume                  80
_journal_year                    2015
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_diffrn_radiation_type           CuK\a
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0475P)^2^+0.5268P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           uvic1404a
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_shelx_estimated_absorpt_t_max   0.948
_diffrn_source_monochromator     'MONTEL Multi-layer'
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_shelx_res_checksum              86157
_shelx_hkl_checksum              70350