Organometallic electrodes: modification of electrode surfaces through cathodic reduction of cyclopentadienyldiazonium complexes of cobalt and manganese.
Laws, Derek R.; Sheats, John; Rheingold, Arnold L.; Geiger, William E.; Langmuir : the ACS journal of surfaces and colloids 26 (2010) 15010–15021; doi:10.1021/la102579t

data_4502731
_publ_section_title
;
 Organometallic electrodes: modification of electrode surfaces through
 cathodic reduction of cyclopentadienyldiazonium complexes of cobalt and
 manganese.
;
_journal_issue                   18
_journal_name_full
'Langmuir : the ACS journal of surfaces and colloids'
_journal_page_first              15010
_journal_page_last               15021
_journal_paper_doi               10.1021/la102579t
_journal_volume                  26
_journal_year                    2010
_chemical_formula_sum            'C11 H12 Co F12 N3 O2 P2'
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_chemical_name_systematic
; 
 ? 
;
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_atom_sites_solution_primary     direct
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_cell_length_a                   7.8867(11)
_cell_length_b                   10.0100(14)
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_cell_measurement_temperature    100(2)
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_cell_volume                     918.6(2)
_computing_cell_refinement       'Bruker SMART'
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_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
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_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.950
_diffrn_measured_fraction_theta_max 0.950
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_diffrn_radiation_monochromator  graphite
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_diffrn_reflns_theta_min         2.39
_exptl_absorpt_coefficient_mu    1.242
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_exptl_absorpt_correction_T_min  0.7069
_exptl_absorpt_correction_type   empirical
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_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.050
_exptl_crystal_density_meas      0
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_exptl_crystal_description       plate
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_refine_ls_shift/su_mean         0.007
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0600P)^2^+0.6000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0926
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_cod_data_source_file            la102579t_si_003.cif
_cod_data_source_block           geiger1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4502731