Exploration of metal sulfide syntheses and the dissolution process of antimony sulfide in phosphonium-based ionic liquids.
Grasser, Matthias A.; Pietsch, Tobias; Brunner, Eike; Ruck, Michael; Dalton transactions (Cambridge, England : 2003) 51 (2022) 4079–4086; doi:10.1039/d1dt04165g

data_7709478
_publ_section_title
;
 Exploration of metal sulfide syntheses and the dissolution process of
 antimony sulfide in phosphonium-based ionic liquids.
;
_journal_issue                   10
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              4079
_journal_page_last               4086
_journal_paper_doi               10.1039/d1dt04165g
_journal_volume                  51
_journal_year                    2022
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Air-sensitive,Moisture-sensitive,Oxygen-sensitive
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_audit_update_record
;
2021-12-01 deposited with the CCDC.	2022-02-03 downloaded from the CCDC.
;
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_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     'w=1/[\s^2^(Fo^2^)] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0265
_refine_ls_wR_factor_ref         0.0273
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_reflns_number_gt                17999
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d1dt04165g1.cif
_cod_data_source_block           (Sb13S16Cl2)[AlCl4]5
_cod_depositor_comments          'Adding full bibliography for 7709478.cif.'
_cod_database_code               7709478
_shelx_shelxl_version_number     2014/7
_shelx_res_checksum              89256