(<i>E</i>)-1-Ethoxycarbonyl-2-[(2-hydroxy-1-naphthyl)(phenyl)methyliminio]propan-1-ide
Jing-Hua Li; Chui-Pan Lin; Acta Crystallographica Section E 62 (2006) o942–o944; doi:10.1107/S1600536806003771

data_2208237
_publ_section_title
(<i>E</i>)-1-Ethoxycarbonyl-2-[(2-hydroxy-1-naphthyl)(phenyl)methyliminio]propan-1-ide
_journal_coeditor_code           AT6079
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o942
_journal_page_last               o944
_journal_paper_doi               10.1107/S1600536806003771
_journal_volume                  62
_journal_year                    2006
_chemical_formula_iupac          'C23 H23 N O3'
_chemical_formula_moiety         'C23 H23 N O3'
_chemical_formula_sum            'C23 H23 N O3'
_chemical_formula_weight         361.44
_chemical_name_systematic
(E)-1-Ethoxycarbonyl-3-[(2-hydroxynaphthalen-1-ylmethyl)phenyliminio]butan-2-ide
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                100.775(19)
_cell_angle_beta                 109.714(14)
_cell_angle_gamma                93.722(18)
_cell_formula_units_Z            2
_cell_length_a                   9.602(4)
_cell_length_b                   9.962(5)
_cell_length_c                   10.899(5)
_cell_measurement_reflns_used    7862
_cell_measurement_temperature    298.0(10)
_cell_measurement_theta_max      27.6
_cell_measurement_theta_min      3.1
_cell_volume                     954.9(8)
_computing_cell_refinement       PROCESS-AUTO
_computing_data_collection       'PROCESS-AUTO (Rigaku, 1998)'
_computing_data_reduction        'CrystalStructure (Rigaku/MSC, 2004)'
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_computing_publication_material  CrystalStructure
_computing_structure_refinement  'CRYSTALS (Betteridge <i>et al.</i>,  2003)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 1997)'
_diffrn_detector_area_resol_mean 10.00
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'Rigaku R-AXIS RAPID'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71075
_diffrn_reflns_av_R_equivalents  0.023
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_diffrn_reflns_theta_full        27.49
_diffrn_reflns_theta_max         27.49
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.083
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
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_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Chunk
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_exptl_crystal_size_max          0.30
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_refine_diff_density_min         -0.23
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