Ag~2~[Pd(NH~3~)~2~(SO~3~)~2~] powder
Solovyov, Leonid A.; Blokhin, Alexander I.; Mulagaleev, Ruslan F.; Kirik, Sergei D.; Acta Crystallographica Section C 55 (1999) 293–296; doi:10.1107/S0108270198012724

data_2008199
_publ_contact_author
; Dr Sergei Kirik
  Institute of Chemistry & Chemical Technology,
  660049, Krasnoyarsk,
  Russia
;
_publ_section_title
;
 Ag~2~[Pd(NH~3~)~2~(SO~3~)~2~] powder
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              293
_journal_page_last               296
_journal_paper_doi               10.1107/S0108270198012724
_journal_volume                  55
_journal_year                    1999
_chemical_formula_analytical     'Ag2.01 (Pd1.01 (N H3)1.95 (S O3)1.98)'
_chemical_formula_iupac          'Ag2 [Pd (N H3)2 (SO3)2]'
_chemical_formula_structural     'Ag2 (Pd (N H3)2 (S O3)2)'
_chemical_formula_sum            'Ag2 H6 N2 O6 Pd S2'
_chemical_formula_weight         516.33
_chemical_name_common            'silver(I) diammino-disulfito-palladat(II)'
_chemical_name_systematic
;
disilver(I) diamminedisulfitopalladium(II)
;
_chemical_temperature_decomposition 448.15
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 108.2200(10)
_cell_angle_gamma                90.0
_cell_formula_units_Z            2
_cell_length_a                   7.05180(10)
_cell_length_b                   5.85100(10)
_cell_length_c                   10.3799(2)
_cell_measurement_temperature    293
_cell_volume                     406.803(12)
_computing_cell_refinement
'DBWM [local modification of DBWS-9006PC (Wiles & Young, 1981)]'
_computing_data_collection       'DRON-4 data collection software'
_computing_data_reduction        'XDIG (Solovyov, 1998)'
_computing_molecular_graphics    'XP (Siemens, 199?)'
_computing_structure_refinement  DBWM
_computing_structure_solution
'Patterson & Fourier syntheses (local programs)'
_diffrn_ambient_temperature      293
_diffrn_measurement_device       'DRON-4 powder diffractometer'
_diffrn_measurement_method       '\q/2\q scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'conventional sealed tube'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.5418
_diffrn_reflns_av_R_equivalents  0
_diffrn_reflns_number            330
_diffrn_reflns_theta_max         45
_diffrn_reflns_theta_min         6
_exptl_absorpt_process_details   none
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   1.66
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_constraints    5
_refine_ls_number_parameters     41
_refine_ls_number_restraints     0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_scheme      sigma
_cod_data_source_file            av1026.cif
_cod_data_source_block           agpdnso3
_cod_depositor_comments
;
The following automatic conversions were performed:

'_chemical_melting_point' tag was changed to
'_chemical_temperature_decomposition' since the value had been given
as 'decomposes at 175\%C'. The value 'decomposes at 175\%C' was
changed to '448.15' - it was converted from degrees Celsius(C) to
Kelvins(K).

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 

The following automatic conversions were performed:

'_chemical_melting_point' tag was changed to
'_chemical_temperature_decomposition' since the value had been given
as 'decomposes at 175\%C'. The value 'decomposes at 175\%C' was
changed to '448.15' - it was converted from degrees Celsius(C) to
Kelvins(K).

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        406.80(3)
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               2008199