Structure of μ-[bis(chloroacetato-<i>O</i>)-mercury(II)-κ^2^<i>Hg</i>]-μ-[1,8-naphthalenediamino-κ^2^<i>NN</i>':κ^2^<i>NN</i>']-bis[<i>cis</i>-dicarbonyl(triisopropylphosphine-<i>P</i>)ruthenium(I)](<i>Ru</i>‒<i>Ru</i>)
García-Granda, S.; Van der Maelen Uría, J. F.; Cabeza, J. A.; Fernández-Colinas, J. M.; Riera, V.; Acta Crystallographica Section C 49 (1993) 1483–1485; doi:10.1107/S010827019300160X

data_2001447
_publ_section_title
;Structure of
 \m-[bis(chloroacetato-<i>O</i>)-mercury(II)-\k^2^<i>Hg</i>]-\m-[1,8-naphthalenediamino-\k^2^<i>NN</i>':\k^2^<i>NN</i>']-bis[<i>cis</i>-dicarbonyl(triisopropylphosphine-<i>P</i>)ruthenium(I)](<i>Ru</i>--<i>Ru</i>)
;
_journal_issue                   8
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1483
_journal_page_last               1485
_journal_paper_doi               10.1107/S010827019300160X
_journal_volume                  49
_journal_year                    1993
_chemical_formula_sum            'C36 H54 Cl2 Hg N2 O8 P2 Ru2'
_chemical_formula_weight         1178.42
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.0
_cell_angle_beta                 93.83(3)
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   23.586(8)
_cell_length_b                   12.584(2)
_cell_length_c                   14.540(5)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293
_cell_measurement_theta_max      17
_cell_measurement_theta_min      15
_cell_volume                     4306(2)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.027
_diffrn_reflns_limit_h_max       27
_diffrn_reflns_limit_h_min       -27
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            4099
_diffrn_reflns_theta_max         25
_diffrn_standards_decay_%        5
_diffrn_standards_interval_time  60
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    4.482
_exptl_absorpt_correction_T_max  1.34
_exptl_absorpt_correction_T_min  0.77
_exptl_crystal_colour            Yellow
_exptl_crystal_density_diffrn    1.818
_exptl_crystal_description       Prismatic
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.33
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.90
_refine_diff_density_min         -0.75
_refine_ls_hydrogen_treatment    refall
_refine_ls_number_parameters     306
_refine_ls_number_reflns         2626
_refine_ls_R_factor_obs          0.033
_refine_ls_shift/esd_max         0.04
_refine_ls_weighting_details     'w = 1/[\s^2^(F)+0.0004F^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.034
_reflns_number_observed          2626
_reflns_number_total             2756
_reflns_observed_criterion       F>3\s(F)
_cod_data_source_file            hu1035.cif
_cod_data_source_block           hu1035a
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value '1/[\s^2^(F)+0.0004F^2^]' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to 'w =
1/[\s^2^(F)+0.0004F^2^]'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        4306.0(2)
_cod_database_code               2001447