Highly sensitive phototransistor with crystalline microribbons from new p-extended pyrene derivative via solution-phase self-assembly
Youn Sun Kim; Suk Young Bae; Kyung Hwan Kim; Tae Wan Lee; Jung A Hur; Mai Ha Hoang; Min Ju Cho; Sung-Jin Kim; Youngmee Kim; Minsik Kim; Kwangyeol Lee; Suk Joong Lee; Dong Hoon Choi; Chem.Commun. 47 (2011) 8907–; doi:10.1039/c1cc11589h

data_7106718
_publ_section_title
;
 Highly sensitive phototransistor with crystalline microribbons from new
 p-extended pyrene derivative via solution-phase self-assembly
;
_journal_name_full               Chem.Commun.
_journal_page_first              8907
_journal_paper_doi               10.1039/c1cc11589h
_journal_volume                  47
_journal_year                    2011
_chemical_formula_sum            'C72 H53'
_chemical_formula_weight         918.14
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.01(3)
_cell_angle_beta                 90.28(3)
_cell_angle_gamma                90.04(3)
_cell_formula_units_Z            4
_cell_length_a                   8.9660(18)
_cell_length_b                   15.540(3)
_cell_length_c                   40.712(8)
_cell_measurement_reflns_used    4365
_cell_measurement_temperature    170(2)
_cell_measurement_theta_max      26.65
_cell_measurement_theta_min      2.33
_cell_volume                     5672.4(19)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      170(2)
_diffrn_measured_fraction_theta_full 0.969
_diffrn_measured_fraction_theta_max 0.969
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.2075
_diffrn_reflns_av_sigmaI/netI    0.7773
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       50
_diffrn_reflns_limit_l_min       -47
_diffrn_reflns_number            31412
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         26.00
_diffrn_reflns_theta_min         2.27
_exptl_absorpt_coefficient_mu    0.061
_exptl_absorpt_correction_T_max  0.999
_exptl_absorpt_correction_T_min  0.988
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Bruker, 1997)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.075
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             1940
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.02
_refine_diff_density_max         0.240
_refine_diff_density_min         -0.261
_refine_diff_density_rms         0.054
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.841
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1290
_refine_ls_number_reflns         21548
_refine_ls_number_restraints     74
_refine_ls_restrained_S_all      0.840
_refine_ls_R_factor_all          0.4805
_refine_ls_R_factor_gt           0.1151
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0000P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2078
_refine_ls_wR_factor_ref         0.3586
_reflns_number_gt                7484
_reflns_number_total             21548
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c1cc11589h.txt
_cod_data_source_block           ym561sadp-1
_cod_original_cell_volume        5672(2)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7106718