Synthesis and characterization of bis(amidate) rare-earth metal amides and their application in catalytic addition of amines to carbodiimides
Cheng, Hao; Xiao, Yang; Lu, Chengrong; Zhao, Bei; Wang, Yaorong; Yao, Yingming; New J. Chem. 39 (2015) 7667–; doi:10.1039/C5NJ00506J

data_7054948
_publ_section_title
;
 Synthesis and characterization of bis(amidate) rare-earth metal amides
 and their application in catalytic addition of amines to carbodiimides
;
_journal_issue                   10
_journal_name_full               'New J. Chem.'
_journal_page_first              7667
_journal_paper_doi               10.1039/C5NJ00506J
_journal_volume                  39
_journal_year                    2015
_chemical_formula_moiety         'C76 H124 N6 O6 Si4 Yb2, 3(C4 H8 O)'
_chemical_formula_sum            'C88 H148 N6 O9 Si4 Yb2'
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_space_group_crystal_system      triclinic
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_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
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_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2015-05-06 deposited with the CCDC.
2015-06-18 downloaded from the CCDC.
;
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_diffrn_ambient_temperature      293(2)
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_diffrn_measurement_device_type  'Rigaku Saturn'
_diffrn_measurement_method       \w
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_diffrn_reflns_number            23938
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0532P)^2^+1.9688P] where P=(Fo^2^+2Fc^2^)/3'
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'Adding full bibliography for 7054947--7054948.cif.'
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