Expected and unexpected products of reactions of 2-hydrazinylbenzothiazole with 3-nitrobenzenesulfonyl chloride in different solvents
Morscher, Alexandra; de Souza, Marcus V. N.; Wardell, James L.; Harrison, William T. A.; Acta Crystallographica Section E 74 (2018) 673–677; doi:10.1107/S2056989018005595

data_2242455
_publ_section_title
;
 Expected and unexpected products of reactions of
 2-hydrazinylbenzothiazole with 3-nitrobenzenesulfonyl chloride in
 different solvents
;
_journal_coeditor_code           SJ5555
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              673
_journal_page_last               677
_journal_paper_doi               10.1107/S2056989018005595
_journal_volume                  74
_journal_year                    2018
_chemical_formula_iupac          'C10 H12 N3 S +, C6 H4 NO5 S -'
_chemical_formula_moiety         'C10 H12 N3 S +, C6 H4 NO5 S -'
_chemical_formula_sum            'C16 H16 N4 O5 S2'
_chemical_formula_weight         408.45
_chemical_name_systematic
;
2-[2-(Propan-2-ylidene)hydrazinyl]-1,3-benzothiazol-3-ium
3-nitrobenzenesulfonate
;
_space_group_crystal_system      triclinic
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;
CrystalClear (Rigaku, 2012)
;
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CrystalClear (Rigaku, 2012)
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CrystalClear (Rigaku, 2012)
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ORTEP-3 for Windows (Farrugia, 2012)
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publCIF (Westrip, 2010)
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SHELXL2014 (Sheldrick, 2015)
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SHELXS97 (Sheldrick, 2008)
;
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;
(<i>FS_ABSCOR</i>; Rigaku, 2013)
;
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.1206P)^2^+0.8477P] where P=(Fo^2^+2Fc^2^)/3'
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