Copper(i) diselenocarbamate clusters: synthesis, structures and single-source precursors for Cu and Se composite materials.
Dhayal, Rajendra S.; Liao, Jian-Hong; Hou, Hsing-Nan; Ervilita, Ria; Liao, Ping-Kuei; Liu, C. W.; Dalton transactions (Cambridge, England : 2003) 44 (2015) 5898–5908; doi:10.1039/c4dt03810j

data_7033912
_publ_section_title
;
 Copper(i) diselenocarbamate clusters: synthesis, structures and
 single-source precursors for Cu and Se composite materials.
;
_journal_issue                   12
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              5898
_journal_page_last               5908
_journal_paper_doi               10.1039/c4dt03810j
_journal_volume                  44
_journal_year                    2015
_chemical_formula_sum            'C36 H73 Cu8 F6 N6 O2 P Se12'
_chemical_formula_weight         2222.81
_chemical_properties_physical    'Air-sensitive, Heat-sensitive'
_space_group_crystal_system      tetragonal
_space_group_IT_number           85
_space_group_name_Hall           '-P 4a'
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_symmetry_space_group_name_Hall  '-P 4a'
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_atom_sites_solution_hydrogens   mixed
_audit_block_doi                 10.5517/cc13tk7q
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_audit_update_record
;
2015-01-21 deposited with the CCDC.
2015-02-05 downloaded from the CCDC.
;
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_computing_cell_refinement       'Bruker SAINT (Bruker APEX2 v2014.11-0)'
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       '\f and \w scans'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0342P)^2^+11.4423P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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'Adding full bibliography for 7033910--7033914.cif.'
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