Synthesis and Characterization of Copper(I) Amidinates as Precursors for Atomic Layer Deposition (ALD) of Copper Metal
Zhengwen Li; Seán T. Barry; Roy G. Gordon; Inorganic Chemistry 44 (2005) 1728–1735; doi:10.1021/ic048492u

data_4300853
_publ_section_title
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Synthesis and Characterization of Copper(I) Amidinates as Precursors for

Atomic Layer Deposition (ALD) of Copper Metal

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_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1728
_journal_page_last               1735
_journal_paper_doi               10.1021/ic048492u
_journal_volume                  44
_journal_year                    2005
_chemical_formula_moiety         'C20 H42 Cu2 N4'
_chemical_formula_sum            'C20 H42 Cu2 N4'
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_cell_measurement_temperature    193(2)
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_computing_cell_refinement       'SMART (BRUKER, V5.625, 2001)'
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_diffrn_ambient_temperature      193(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker CCD'
_diffrn_measurement_method       '\w, 0.3 deg'
_diffrn_radiation_monochromator  graphite
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_diffrn_reflns_limit_k_min       -13
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_diffrn_reflns_limit_l_min       -17
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_diffrn_reflns_theta_full        28.26
_diffrn_reflns_theta_max         28.26
_diffrn_reflns_theta_min         2.21
_diffrn_source                   'normal-focus sealed tube'
_diffrn_standards_decay_%        <1
_diffrn_standards_interval_count 0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    1.779
_exptl_absorpt_correction_T_max  0.9653
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_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            clear
_exptl_crystal_density_diffrn    1.286
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_exptl_crystal_description       block
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_refine_ls_matrix_type           full
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_refine_ls_number_reflns         2983
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_refine_ls_R_factor_gt           0.0302
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0311P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.0762
_reflns_number_gt                1947
_reflns_number_total             2983
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic048492usi20050114_035217.cif
_cod_data_source_block           rg12
_cod_depositor_comments
;
The following automatic conversions were performed:
'_exptl_absorpt_correction_type' value 'Empirical' changed to 'empirical'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
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_cod_original_cell_volume        2405.1(7)
_cod_database_code               4300853