Azamacrocycles and the azaoxacryptand 4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane as structure-directing agents in the synthesis of microporous metalloaluminophosphates
Maple, Martin J.; Philp, Eilidh F.; Slawin, Alexandra M. Z.; Lightfoot, Philip; Cox, Paul A.; Wright, Paul A.; Journal of Materials Chemistry 11 (2001) 98–104; doi:10.1039/b003430o

data_7203985
_publ_section_title
;
 Azamacrocycles and the azaoxacryptand
 4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane as
 structure-directing agents in the synthesis of microporous
 metalloaluminophosphates
;
_journal_coden_ASTM              JMACEP
_journal_issue                   1
_journal_name_full               'Journal of Materials Chemistry'
_journal_page_first              98
_journal_page_last               104
_journal_paper_doi               10.1039/b003430o
_journal_volume                  11
_journal_year                    2001
_chemical_formula_moiety         'C1.50 Al0.80 N0.17 O4.50 P Zn0.20 '
_chemical_formula_sum            'C1.5 Al0.8 N0.17 O4.5 P Zn0.2'
_chemical_formula_weight         158.03
_space_group_IT_number           226
_symmetry_cell_setting           cubic
_symmetry_Int_Tables_number      226
_symmetry_space_group_name_Hall  '-F 4a 2 3'
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_audit_creation_date             'Wed Apr 27 09:21:29 2000'
_audit_creation_method           'from TEXRAY.INF file'
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_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            96
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_cell_length_b                   23.990(8)
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_cell_measurement_theta_max      0.0
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_computing_publication_material  teXsan
_computing_structure_refinement  teXsan
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_diffrn_orient_matrix_UB_13      0.00000
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_diffrn_orient_matrix_UB_22      0.00000
_diffrn_orient_matrix_UB_23      0.00000
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_diffrn_radiation_source         'Daresbury Synchrotron'
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_diffrn_radiation_wavelength     0.6942
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_diffrn_reflns_limit_h_min       -33
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_diffrn_reflns_limit_k_min       -32
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -9
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_diffrn_standards_number         0
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_exptl_crystal_description       cube
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_refine_ls_structure_factor_coef F
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_reflns_number_observed          312
_reflns_number_total             1007
_reflns_observed_criterion       3.00
_cod_data_source_file            b003430o.txt
_cod_data_source_block           A_TEXRAY.INF_file_is_not_p
_cod_depositor_comments
;
The following automatic conversions were performed:

'_atom_site_thermal_displace_type' tag value 'Uij' was replaced with
'Uani' value 32 times.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_cell_volume        13806(6)
_cod_original_sg_symbol_H-M      'F m -3 c   '
_cod_original_formula_sum        'C1.50 Al0.80 N0.17 O4.50 P Zn0.20 '
_cod_database_code               7203985