Enantioselective synthesis of isoquinoline alkaloids from simple sugar. I. Structure of an oxaziridine derivative
Czarnocki, Z.; Maurin, J. K.; Acta Crystallographica Section C 49 (1993) 1992–1994; doi:10.1107/S0108270193004433

data_2001244
_publ_section_title
;
 Enantioselective synthesis of isoquinoline alkaloids from simple
 sugar. I. Structure of an oxaziridine derivative
;
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1992
_journal_page_last               1994
_journal_paper_doi               10.1107/S0108270193004433
_journal_volume                  49
_journal_year                    1993
_chemical_formula_moiety         'C23 H29 N1 O11'
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_cell_measurement_temperature    295(2)
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_cell_volume                     2545.9(4)
_computing_molecular_graphics    'ORTEPII (Johnson, 1976)'
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_diffrn_measurement_device       'Kuma Diffraction KM-4'
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_diffrn_reflns_av_R_equivalents  0.014
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_diffrn_reflns_limit_h_min       0
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_refine_ls_hydrogen_treatment
'Only common isotropic displacement parameter for H atoms refined'
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_refine_ls_R_factor_obs          0.0589
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s(F) + 0.0005F^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.0828
_reflns_number_observed          1897
_reflns_number_total             1857
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_cod_data_source_file            ab0308.cif
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_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'w = 1/[\s(F) + 0.0005F^2^]' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to 'w = 1/[\s(F) +
0.0005F^2^]'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_formula_sum        'C23 H29 N1 O11'
_cod_database_code               2001244