Co(II)-Doped Cd-MOF as an Efficient Water Oxidation Catalyst: Doubly Interpenetrated Boron Nitride Network with the Encapsulation of Free Ligand Containing Pyridine Moieties.
Maity, Kartik; Bhunia, Kousik; Pradhan, Debabrata; Biradha, Kumar; ACS applied materials & interfaces 9 (2017) 37548–37553; doi:10.1021/acsami.7b12926

data_4514256
_publ_section_title
;
 Co(II)-Doped Cd-MOF as an Efficient Water Oxidation Catalyst: Doubly
 Interpenetrated Boron Nitride Network with the Encapsulation of Free
 Ligand Containing Pyridine Moieties.
;
_journal_issue                   43
_journal_name_full               'ACS applied materials &amp; interfaces'
_journal_page_first              37548
_journal_page_last               37553
_journal_paper_doi               10.1021/acsami.7b12926
_journal_volume                  9
_journal_year                    2017
_chemical_formula_sum            'C44 H38 Cd N8 O9'
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_cell_measurement_theta_min      2.049
_cell_volume                     1994.4(3)
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.986
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_diffrn_measurement_device_type  'Bruker APEX-2 CCD'
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_diffrn_reflns_Laue_measured_fraction_full 0.986
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_diffrn_reflns_theta_max         26.000
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_exptl_absorpt_coefficient_mu    0.618
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colourless
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_exptl_crystal_description       rectangular
_exptl_crystal_F_000             956
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.26
_exptl_crystal_size_min          0.22
_refine_diff_density_max         0.733
_refine_diff_density_min         -0.603
_refine_diff_density_rms         0.072
_refine_ls_extinction_method     none
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0100P)^2^+0.5078P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0693
_refine_ls_wR_factor_ref         0.0716
_reflns_Friedel_coverage         0.000
_reflns_number_gt                6240
_reflns_number_total             7662
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            am7b12926_si_002.cif
_cod_data_source_block           Cd-BNN
_cod_database_code               4514256
_shelx_shelxl_version_number     2014/7
_exptl_absorpt_special_details   SADABS
_shelx_res_checksum              50060
_shelx_hkl_checksum              99710