Synthesis, Chemistry, and Electronic Structures of Group 9 Metallaboranes.
Borthakur, Rosmita; Kar, Sourav; Barik, Subrat Kumar; Bhattacharya, Somnath; Kundu, Gargi; Varghese, Babu; Ghosh, Sundargopal; Inorganic chemistry 56 (2017) 1524–1533; doi:10.1021/acs.inorgchem.6b02626

data_1545105
_publ_section_title
;
 Synthesis, Chemistry, and Electronic Structures of Group 9
 Metallaboranes.
;
_journal_issue                   3
_journal_name_full               'Inorganic chemistry'
_journal_page_first              1524
_journal_page_last               1533
_journal_paper_doi               10.1021/acs.inorgchem.6b02626
_journal_volume                  56
_journal_year                    2017
_chemical_formula_sum            'C30 H49 B5 Cl Ir3'
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_space_group_name_Hall           '-P 2n 2ab'
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_symmetry_space_group_name_Hall  '-P 2n 2ab'
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_cell_volume                     6740.9(4)
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'ORTEP3 (Farrugia, 1997) and Mercury (Bruno et al., 2002)'
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_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker axs kappa apex2 CCD Diffractometer'
_diffrn_measurement_method       '\w and \f scan'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0384P)^2^+137.9307P] where P=(Fo^2^+2Fc^2^)/3'
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'Adding full bibliography for 1545104--1545108.cif.'
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