<i>catena</i>-Poly[[(benzoato-κ^2^<i>O</i>,<i>O</i>')(2,2'-bipyridine-κ^2^<i>N</i>,<i>N</i>')lead(II)]-μ~3~-nitrato-κ^4^<i>O</i>:<i>O</i>,<i>O</i>':<i>O</i>'']
Yang, Juan; Dai, Jun; Wang, Xiaohan; Acta Crystallographica Section E 66 (2010) m1686–; doi:10.1107/S160053681004907X

data_2228327
_publ_section_title
;
 <i>catena</i>-Poly[[(benzoato-\k^2^<i>O</i>,<i>O</i>')(2,2'-bipyridine-\k^2^<i>N</i>,<i>N</i>')lead(II)]-\m~3~-nitrato-\k^4^<i>O</i>:<i>O</i>,<i>O</i>':<i>O</i>'']
;
_journal_coeditor_code           GK2325
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1686
_journal_paper_doi               10.1107/S160053681004907X
_journal_volume                  66
_journal_year                    2010
_chemical_formula_iupac
;
[Pb (C7 H5 O2) (N O3) (C10 H8 N2)]
;
_chemical_formula_moiety         'C17 H13 N3 O5 Pb'
_chemical_formula_sum            'C17 H13 N3 O5 Pb'
_chemical_formula_weight         546.49
_chemical_name_systematic
;
<i>catena</i>-Poly[[(benzoato-\k^2^<i>O</i>,<i>O</i>')(2,2'-bipyridine-
\k^2^<i>N</i>,<i>N</i>')lead(II)]-\m~3~-nitrato-
\k^4^<i>O</i>:<i>O</i>,<i>O</i>':<i>O</i>'']
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                84.566(3)
_cell_angle_beta                 86.593(3)
_cell_angle_gamma                83.729(2)
_cell_formula_units_Z            2
_cell_length_a                   6.5389(11)
_cell_length_b                   8.5052(14)
_cell_length_c                   15.548(3)
_cell_measurement_reflns_used    3772
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      28.18
_cell_measurement_theta_min      2.63
_cell_volume                     854.6(3)
_computing_cell_refinement       'SAINT (Bruker, 2007)'
_computing_data_collection       'APEX2 (Bruker, 2007)'
_computing_data_reduction        'SAINT (Bruker, 2007)'
_computing_molecular_graphics    'SHELXTL (Sheldrick, 2008)'
_computing_publication_material  'SHELXTL (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measurement_device_type  'Bruker APEXII CCD area-detector'
_diffrn_measurement_method       '\f and \w'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0297
_diffrn_reflns_av_sigmaI/netI    0.0575
_diffrn_reflns_limit_h_max       7
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -9
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            4385
_diffrn_reflns_theta_full        25.01
_diffrn_reflns_theta_max         25.01
_diffrn_reflns_theta_min         2.65
_diffrn_standards_decay_%        0
_exptl_absorpt_coefficient_mu    9.905
_exptl_absorpt_correction_T_max  0.226
_exptl_absorpt_correction_T_min  0.118
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Bruker, 2007)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.124
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       column
_exptl_crystal_F_000             516
_exptl_crystal_size_max          0.23
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.15
_refine_diff_density_max         2.695
_refine_diff_density_min         -2.786
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.024
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     235
_refine_ls_number_reflns         2981
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.024
_refine_ls_R_factor_all          0.0395
_refine_ls_R_factor_gt           0.0370
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0675P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0971
_refine_ls_wR_factor_ref         0.0988
_reflns_number_gt                2769
_reflns_number_total             2981
_reflns_threshold_expression     I>2sigma(I)
_cod_data_source_file            gk2325.cif
_cod_data_source_block           I
_cod_database_code               2228327
_cod_database_fobs_code          2228327