A facile solution-phase synthetic approach for constructing phenol-based porous organic cages and covalent organic frameworks
Zhang, Lei; Liang, Rongran; Hang, Cheng; Wang, Haiying; Sun, Lin; Xu, Lei; Liu, Dairong; Zhang, Zhenyi; Zhang, Xingmin; Chang, Feifan; Zhao, Shengyu; Huang, Wei; Green Chemistry 22 (2020) 2498–2504; doi:10.1039/C9GC04033A

data_7240128
_publ_section_title
;
 A facile solution-phase synthetic approach for constructing phenol-based
 porous organic cages and covalent organic frameworks
;
_journal_issue                   8
_journal_name_full               'Green Chemistry'
_journal_page_first              2498
_journal_page_last               2504
_journal_paper_doi               10.1039/C9GC04033A
_journal_volume                  22
_journal_year                    2020
_chemical_absolute_configuration rm
_chemical_formula_moiety         'C58 H64 N8 O4, 2(C2 H6 O), 2(H2 O)'
_chemical_formula_sum            'C62 H80 N8 O8'
_chemical_formula_weight         1065.34
_space_group_crystal_system      tetragonal
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_space_group_name_Hall           'P 4nw 2abw'
_space_group_name_H-M_alt        'P 43 21 2'
_atom_sites_solution_hydrogens   mixed
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_audit_update_record
;
2017-09-11 deposited with the CCDC.	2020-03-12 downloaded from the CCDC.
;
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_computing_cell_refinement       SMART
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_diffrn_measurement_device_type  'PHOTON100 CMOS detector'
_diffrn_measurement_method       '\f and \w scans'
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;
 Refined as an inversion twin.
;
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0605P)^2^+1.7310P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c9gc04033a2.cif
_cod_data_source_block           NC2-R
_cod_depositor_comments
;Adding full bibliography for 7240126--7240128.cif.

 Adding full bibliography for 7240126--7240128.cif.
;
_cod_original_cell_volume        5966.6(5)
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_shelx_estimated_absorpt_t_max   0.992
_shelx_res_checksum              7762