Preparation of seven-coordinated hypervalent tin(IV)-fused azobenzene and applications for stimuli-responsive π-conjugated polymer films.
Gon, Masayuki; Morisaki, Yusuke; Tanimura, Kazuya; Tanaka, Kazuo; Dalton transactions (Cambridge, England : 2003) 53 (2024) 11858–11866; doi:10.1039/d4dt01738b

data_7716480
_publ_section_title
;
 Preparation of seven-coordinated hypervalent tin(IV)-fused azobenzene and
 applications for stimuli-responsive &#x3c0;-conjugated polymer films.
;
_journal_issue                   28
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
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_journal_paper_doi               10.1039/d4dt01738b
_journal_volume                  53
_journal_year                    2024
_chemical_formula_sum            'C24 H16 Br2 N2 O2 Sn'
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;
2024-04-19 deposited with the CCDC.	2024-06-27 downloaded from the CCDC.
;
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Rigaku Saturn724+ (4x4 bin mode)
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_exptl_crystal_colour            'deep red'
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0231P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0674
_refine_ls_wR_factor_ref         0.0729
_reflns_Friedel_coverage         0.000
_reflns_number_gt                4079
_reflns_number_total             5091
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d4dt01738b2.cif
_cod_data_source_block           TAz
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'Multi-scan' was
changed to 'multi-scan' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas 

 Adding full bibliography for 7716480--7716481.cif.
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7716480
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_shelx_hkl_checksum              48489