Rhodium-catalyzed divergent dehydroxylation/alkenylation of hydroxyisoindolinones with vinylene carbonate
Nan, Jiang; Liang, Lu; Chemical Communications  (2023) –; doi:10.1039/D3CC03760F

data_7132301
_publ_section_title
;
 Rhodium-catalyzed divergent dehydroxylation/alkenylation of
 hydroxyisoindolinones with vinylene carbonate
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/D3CC03760F
_journal_year                    2023
_chemical_formula_sum            'C17 H13 N O2'
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_audit_update_record
;
2023-08-02 deposited with the CCDC.	2023-11-02 downloaded from the CCDC.
;
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_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
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_diffrn_reflns_limit_h_max       9
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_diffrn_reflns_point_group_measured_fraction_full 0.997
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_diffrn_reflns_theta_full        25.242
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_exptl_absorpt_coefficient_mu    0.085
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_refine_ls_extinction_method     none
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_refine_ls_number_reflns         2654
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1561P)^2^+3.9949P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_total             2654
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d3cc03760f2.cif
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_cod_original_cell_volume        677.2(2)
_cod_database_code               7132301
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