Iron-Catalyzed Oxidative C-H Functionalization of Internal Olefins for the Synthesis of Tetrasubstituted Furans.
Lou, Jiang; Wang, Quannan; Wu, Kaikai; Wu, Ping; Yu, Zhengkun; Organic letters 19 (2017) 3287–3290; doi:10.1021/acs.orglett.7b01431

data_1546468
_publ_section_title
;
 Iron-Catalyzed Oxidative C-H Functionalization of Internal Olefins for
 the Synthesis of Tetrasubstituted Furans.
;
_journal_issue                   12
_journal_name_full               'Organic letters'
_journal_page_first              3287
_journal_page_last               3290
_journal_paper_doi               10.1021/acs.orglett.7b01431
_journal_volume                  19
_journal_year                    2017
_chemical_formula_sum            'C21 H18 O4 S'
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_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     SHELXL
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_refine_ls_number_reflns         3686
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.028
_refine_ls_R_factor_all          0.0683
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0477P)^2^+0.2279P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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