Latent chemical behavior revealed in the crystalline state: novel photochemistry of a cis-9-decalyl aryl ketone
Cheung, Eugene; Kang, Ting; Scheffer, John R.; Trotter, James; Chemical Communications  (2000) 2309–; doi:10.1039/b007398i

data_7111130
_publ_section_title
;
 Latent chemical behavior revealed in the crystalline state: novel
 photochemistry of a cis-9-decalyl aryl ketone
;
_journal_issue                   23
_journal_name_full               'Chemical Communications'
_journal_page_first              2309
_journal_paper_doi               10.1039/b007398i
_journal_year                    2000
_chemical_formula_moiety         'C19 H22 O3 '
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_audit_update_record
;
?
;
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_cell_angle_gamma                90
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_cell_length_b                   10.149(1)
_cell_length_c                   7.5641(8)
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_cell_measurement_temperature    294.2
_cell_measurement_theta_max      42.6
_cell_measurement_theta_min      37.6
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_computing_data_reduction        'teXsan (MSC, 1992-1997)'
_computing_publication_material  'teXsan (MSC, 1992-1997)'
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;
SIR97 (Altomare, et. al. 1998)
;
_diffrn_ambient_temperature      294.2
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_diffrn_reflns_limit_k_min       -12
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;
\y scans (North,Phillips & Matthews, 1968)
;
_exptl_crystal_colour            colorless
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_refine_ls_extinction_expression 'equ(3) Acta Cryst.(1968) A24, p213.'
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_refine_ls_goodness_of_fit_all   2.554
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_refine_ls_shift/su_max          0.0000
_refine_ls_shift/su_mean         0.0000
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo) + 0.00000|Fo|^2^]'
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_all         0.0464
_refine_ls_wR_factor_ref         0.0444
_reflns_number_gt                1465
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_reflns_threshold_expression     I>3.00\s(I)
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_cod_data_source_block           eugkt10ax98
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        810.5(2)
_cod_original_sg_symbol_H-M      'P 21       '
_cod_original_formula_sum        'C19 H22 O3 '
_cod_database_code               7111130