Colorimetric and luminescent sensing of DMF by crystalline non-porous pyrene-based coordination compounds
Sangrador-Pérez, Jorge; Jiménez-Hernández, Patricia; Hernández, Mar García; Sañudo, E. Carolina; Costa, Jose Sanchez; Resines-Urien, Esther; CrystEngComm 27 (2025) 5286–5291; doi:10.1039/D5CE00600G

data_7250701
_publ_section_title
;
 Colorimetric and luminescent sensing of DMF by crystalline non-porous
 pyrene-based coordination compounds
;
_journal_issue                   31
_journal_name_full               CrystEngComm
_journal_page_first              5286
_journal_page_last               5291
_journal_paper_doi               10.1039/D5CE00600G
_journal_volume                  27
_journal_year                    2025
_chemical_formula_sum            'C203 H135 Co4 N48 O5 S8'
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_space_group_name_Hall           '-P 1'
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_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2025-06-10 deposited with the CCDC.	2025-07-17 downloaded from the CCDC.
;
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_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_diffrn_ambient_temperature      100(2)
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_diffrn_measured_fraction_theta_max 0.505
_diffrn_measurement_device_type  'MD2M (Arinax)'
_diffrn_measurement_method       'Phi scan'
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_exptl_crystal_colour            orange
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1256P)^2^+4.9247P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2016
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d5ce00600g2.cif
_cod_data_source_block           005_ERU647_a
_cod_depositor_comments          'Adding full bibliography for 7250701.cif.'
_cod_original_cell_volume        4398.3(17)
_cod_database_code               7250701
_shelx_shelxl_version_number     2018/3
_exptl_absorpt_special_details   XSCALE
_shelx_res_checksum              35368