Construction of Azaspirocyclic Ketones through α-Hydroxyiminium Ion or α-Siloxy Epoxide Semipinacol Rearrangements
Fenster, Michaël D. B.; Patrick, Brian O.; Dake, Gregory R.; Organic Letters 3 (2001) 2109–; doi:10.1021/ol0160708

data_1507518
_publ_section_title
;
 Construction of Azaspirocyclic Ketones through \a-Hydroxyiminium Ion or
 \a-Siloxy Epoxide Semipinacol Rearrangements
;
_journal_issue                   13
_journal_name_full               'Organic Letters'
_journal_page_first              2109
_journal_paper_doi               10.1021/ol0160708
_journal_volume                  3
_journal_year                    2001
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_audit_update_record
;
?
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SIR97 (Altomare, et. al. 1998)
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_reflns_threshold_expression     I>3.00\s(I)
_cod_data_source_file            ol0160708_s2.cif
_cod_data_source_block           gd002/MF-H-19-A
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        6968.8(4)
_cod_original_sg_symbol_H-M      'P 21/n     '
_cod_original_formula_sum        'C24 H26 N2 O7 S '
_cod_database_code               1507518