Photo-activation of d(0) niobium imido azides: en route to nitrido complexes.
Camp, Clément; Grant, Lauren N.; Bergman, Robert G.; Arnold, John; Chemical communications (Cambridge, England) 52 (2016) 5538–5541; doi:10.1039/c6cc02081j

data_7124622
_publ_section_title
;
 Photo-activation of d(0) niobium imido azides: en route to nitrido
 complexes.
;
_journal_issue                   32
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              5538
_journal_page_last               5541
_journal_paper_doi               10.1039/c6cc02081j
_journal_volume                  52
_journal_year                    2016
_chemical_formula_sum            'C38 H49 N3 Nb'
_chemical_formula_weight         640.71
_space_group_crystal_system      orthorhombic
_space_group_IT_number           58
_space_group_name_Hall           '-P 2 2n'
_space_group_name_H-M_alt        'P n n m'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2016-03-08 deposited with the CCDC.
2016-03-23 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'phi and omega scans'
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0335P)^2^+6.8797P] where P=(Fo^2^+2Fc^2^)/3'
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