[<i>SP</i>-4-2]-Dinitratobis(trimethylphosphine)platinum(II)
Suzuki, Y.; Miyamoto, T. K.; Ichida, H.; Acta Crystallographica Section C 49 (1993) 1318–1320; doi:10.1107/S0108270192013507

data_2001519
_publ_contact_author
;
    Dr. Miyamoto, T. Ken
    Department of Chemistry
    Faculty of Science
    The University of Tokyo
    Tokyo  113
    Japan
;
_publ_section_title
;
 [<i>SP</i>-4-2]-Dinitratobis(trimethylphosphine)platinum(II)
;
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1318
_journal_page_last               1320
_journal_paper_doi               10.1107/S0108270192013507
_journal_volume                  49
_journal_year                    1993
_chemical_formula_structural     '[Pt (N O3)2 (C3 H9 P)2]'
_chemical_formula_sum            'C6 H18 N2 O6 P2 Pt'
_chemical_formula_weight         471.26
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90
_cell_angle_beta                 98.790(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.5140(10)
_cell_length_b                   14.7600(10)
_cell_length_c                   11.360(2)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    296
_cell_measurement_theta_max      17.2
_cell_measurement_theta_min      15.9
_cell_volume                     1410.8(3)
_computing_molecular_graphics    'ORTEPII (Johnson, 1976)'
_diffrn_measurement_device       'Rigaku AFC-5R diffractometer'
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         '12kW rotating anode generator'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     .71069
_diffrn_reflns_av_R_equivalents  .037
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            5557
_diffrn_reflns_theta_max         32.6
_diffrn_standards_decay_%        14.90
_diffrn_standards_interval_count 147
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    10.286
_exptl_absorpt_correction_T_max  1.00
_exptl_absorpt_correction_T_min  .43
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.218
_exptl_crystal_density_meas      2.22
_exptl_crystal_description       prism
_exptl_crystal_F_000             896
_exptl_crystal_size_max          .25
_exptl_crystal_size_mid          .18
_exptl_crystal_size_min          .12
_refine_diff_density_max         2.31
_refine_diff_density_min         -2.16
_refine_ls_goodness_of_fit_obs   1.38
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_parameters     154
_refine_ls_number_reflns         2548
_refine_ls_R_factor_obs          .044
_refine_ls_shift/esd_max         .02
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/\s^2^(F~o~)'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         .045
_reflns_number_observed          2548
_reflns_number_total             5268
_reflns_observed_criterion       F>3.0\s(F)
_cod_data_source_file            as1039.cif
_cod_data_source_block           default
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'w = 1/\s^2^(F~o~)' was changed
to 'calc'. New tag '_refine_ls_weighting_details' was created. The
value of the new tag was set to 'w = 1/\s^2^(F~o~)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C6 H18 N2 O6 P2 Pt1'
_cod_database_code               2001519