Coinage metal coordination chemistry of stable primary, secondary and tertiary ferrocenylethyl-based phosphines.
Azizpoor Fard, M.; Rabiee Kenaree, A.; Boyle, P. D.; Ragogna, P. J.; Gilroy, J. B.; Corrigan, J. F.; Dalton transactions (Cambridge, England : 2003) 45 (2016) 2868–2880; doi:10.1039/c5dt03962b

data_7038093
_publ_section_title
;
 Coinage metal coordination chemistry of stable primary, secondary and
 tertiary ferrocenylethyl-based phosphines.
;
_journal_issue                   7
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2868
_journal_page_last               2880
_journal_paper_doi               10.1039/c5dt03962b
_journal_volume                  45
_journal_year                    2016
_chemical_formula_sum            'C48 H60 Ag2 Cl2 Fe4 P4'
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_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
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_atom_sites_solution_secondary   difmap
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_audit_update_record
;
2015-10-06 deposited with the CCDC.
2016-01-06 downloaded from the CCDC.
;
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_diffrn_detector                 'CCD plate'
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_diffrn_measurement_device       '\k-geometry diffractometer'
_diffrn_measurement_device_type  'Bruker Kappa Axis Apex2'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
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_refine_ls_R_factor_all          0.0931
_refine_ls_R_factor_gt           0.0438
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0158P)^2^+9.6992P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.0912
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_reflns_number_gt                4015
_reflns_number_total             6180
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c5dt03962b2.cif
_cod_data_source_block           b15188
_cod_depositor_comments
'Adding full bibliography for 7038091--7038098.cif.'
_cod_database_code               7038093
_shelx_shelxl_version_number     2014/7
_shelx_estimated_absorpt_t_min   0.518
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