Calcium mediated efficient synthesis of N-arylamidines from organic nitriles and amines.
Banerjee, Indrani; Sagar, Shweta; Panda, Tarun K.; Organic & biomolecular chemistry 18 (2020) 4231–4237; doi:10.1039/d0ob00805b

data_7157506
_publ_section_title
;
 Calcium mediated efficient synthesis of N-arylamidines from organic
 nitriles and amines.
;
_journal_issue                   22
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              4231
_journal_page_last               4237
_journal_paper_doi               10.1039/d0ob00805b
_journal_volume                  18
_journal_year                    2020
_chemical_formula_moiety         'C19 H23 Br N2'
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;
2020-04-18 deposited with the CCDC.	2020-05-18 downloaded from the CCDC.
;
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_exptl_absorpt_correction_type   multi-scan
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1012P)^2^+1.6317P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1999
_refine_ls_wR_factor_ref         0.2609
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_reflns_number_gt                3647
_reflns_number_total             8825
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d0ob00805b2.cif
_cod_data_source_block           3d
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'Multi-scan' was
changed to 'multi-scan' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas 

 Adding full bibliography for 7157506--7157509.cif.
;
_cod_original_cell_volume        3717.3(7)
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