Vanadoantimonates: from discrete clusters to high dimensional aggregates
Guo, Hai-Yang; Zhang, Xiao; Cui, Xiao-Bing; Huo, Qi-Sheng; Xu, Ji-Qing; CrystEngComm 18 (2016) 5130–; doi:10.1039/C6CE00616G

data_7225237
_publ_section_title
;
 Vanadoantimonates: from discrete clusters to high dimensional aggregates
;
_journal_issue                   27
_journal_name_full               CrystEngComm
_journal_page_first              5130
_journal_paper_doi               10.1039/C6CE00616G
_journal_volume                  18
_journal_year                    2016
_chemical_formula_sum            'C12 H62 Co2 N12 O48 Sb6 V15'
_chemical_formula_weight         2755.19
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_space_group_name_Hall           'R 3'
_space_group_name_H-M_alt        'R 3 :H'
_symmetry_space_group_name_Hall  'R 3'
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_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2016-05-11 deposited with the CCDC.
2016-05-13 downloaded from the CCDC.
;
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_computing_cell_refinement       'Bruker XSCANS'
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_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      293(2)
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_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
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_refine_ls_abs_structure_details
;
 Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack   0.44(7)
_refine_ls_extinction_method     none
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0870P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_cod_data_source_file            c6ce00616g2.cif
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_cod_depositor_comments
'Adding full bibliography for 7225235--7225239.cif.'
_cod_original_cell_volume        5361.9(19)
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