New crystalline 1D/2D/3D indium selenides directed by piperidine and auxiliary solvents.
Xue, Chaozhuang; Lin, Jian; Zhang, Yifan; Liu, Zhiyang; Li, Rui; Gong, Shuwen; Qu, Konggang; Dalton transactions (Cambridge, England : 2003) 51 (2022) 3248–3253; doi:10.1039/d2dt00174h

data_7709444
_publ_section_title
;
 New crystalline 1D/2D/3D indium selenides directed by piperidine and
 auxiliary solvents.
;
_journal_issue                   8
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              3248
_journal_page_last               3253
_journal_paper_doi               10.1039/d2dt00174h
_journal_volume                  51
_journal_year                    2022
_chemical_formula_sum            'C5 H0 In N Se3'
_chemical_formula_weight         425.76
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2ybc'
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_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2022-01-18 deposited with the CCDC.	2022-01-25 downloaded from the CCDC.
;
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_cell_volume                     1077.3(2)
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      298(2)
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_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_theta_min         1.985
_exptl_absorpt_coefficient_mu    12.266
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    2.625
_exptl_crystal_description       block
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_exptl_crystal_size_max          0.11
_exptl_crystal_size_mid          0.10
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_exptl_transmission_factor_min   0.270
_refine_diff_density_max         2.911
_refine_diff_density_min         -5.111
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_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.055
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1496P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2261
_refine_ls_wR_factor_ref         0.2482
_reflns_Friedel_coverage         0.000
_reflns_number_gt                1811
_reflns_number_total             2586
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d2dt00174h2.cif
_cod_data_source_block           ISP-2
_cod_depositor_comments
'Adding full bibliography for 7709442--7709445.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7709444
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