Bis(μ-benzoato-κ<i>O</i>:κ<i>O</i>')-bis[(benzoato-κ^2^<i>O</i>,<i>O</i>')(<i>N</i>,<i>N</i>-dimethylformamide-κ<i>O</i>)dioxouranium(VI)]
Navaza, A.; Iroulart, M. G.; Nierlich, M.; Lance, M.; Vigner, J.; Acta Crystallographica Section C 49 (1993) 1767–1770; doi:10.1107/S0108270193003518

data_2001301
_publ_section_title
Bis(\m-benzoato-\k<i>O</i>:\k<i>O</i>')-bis[(benzoato-\k^2^<i>O</i>,<i>O</i>')(<i>N</i>,<i>N</i>-dimethylformamide-\k<i>O</i>)dioxouranium(VI)]
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1767
_journal_page_last               1770
_journal_paper_doi               10.1107/S0108270193003518
_journal_volume                  49
_journal_year                    1993
_chemical_formula_moiety         'U1 (C7 H5 O2 )2 , O2 , C3 H7 N1 O1'
_chemical_formula_sum            'C34 H34 N2 O14 U2'
_chemical_formula_weight         1170.70
_space_group_IT_number           2
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_type_scat_source           'IntTabIV Tables 2.2B and 2.3.1'
_cell_angle_alpha                90
_cell_angle_beta                 92.63(4)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   9.387(5)
_cell_length_b                   9.507(5)
_cell_length_c                   21.279(8)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    295
_cell_measurement_theta_max      12
_cell_measurement_theta_min      8
_cell_volume                     1897.0(16)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.016
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -25
_diffrn_reflns_number            3778
_diffrn_reflns_theta_max         25
_diffrn_standards_decay_%        0.8
_diffrn_standards_interval_time  60
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    8.15
_exptl_absorpt_correction_T_max  1.215
_exptl_absorpt_correction_T_min  0.824
_exptl_absorpt_correction_type   analytical
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.05
_exptl_crystal_description       prismatic
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.9
_refine_diff_density_min         -1.1
_refine_ls_goodness_of_fit_obs   2.4
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     235
_refine_ls_number_reflns         2191
_refine_ls_R_factor_obs          0.025
_refine_ls_shift/esd_max         0.01
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      unit
_refine_ls_wR_factor_obs         0.028
_reflns_number_observed          2191
_reflns_number_total             3318
_reflns_observed_criterion       I~net~>3\s(I~net~)
_cod_data_source_file            pa1039.cif
_cod_data_source_block           pa1039_structure_1_of_1
_cod_original_cell_volume        1897(3)
_cod_original_sg_symbol_Hall     '-P 2ybc'
_cod_original_sg_symbol_H-M      'P 1 21/c 1'
_cod_database_code               2001301