Palladium-catalyzed synthesis of endocyclic allenes and their application in stereoselective [2 + 2]cycloaddition with ketenes.
Ogasawara, Masamichi; Okada, Atsushi; Nakajima, Kiyohiko; Takahashi, Tamotsu; Organic letters 11 (2009) 177–180; doi:10.1021/ol802280c

data_1503714
_publ_section_title
;
 Palladium-catalyzed synthesis of endocyclic allenes and their application
 in stereoselective [2 + 2]cycloaddition with ketenes.
;
_journal_issue                   1
_journal_name_full               'Organic letters'
_journal_page_first              177
_journal_page_last               180
_journal_paper_doi               10.1021/ol802280c
_journal_volume                  11
_journal_year                    2009
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_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
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_cell_angle_beta                 114.059(8)
_cell_angle_gamma                71.183(8)
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_cell_length_a                   11.1848(11)
_cell_length_b                   15.5317(17)
_cell_length_c                   9.8946(12)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    298.1
_cell_measurement_theta_max      30.0
_cell_measurement_theta_min      25.3
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'Larson (1970) Crystallographic Computing eq. 22'
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_refine_ls_structure_factor_coef F
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'w = 1/[0.0030Fo^2^ + 1.0000\s(Fo^2^) + 0.5000]'
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