Novel ferrocenyl functionalised phosphinecarboxamides: synthesis, characterisation and coordination.
Navrátil, Michal; Faria, Erica N.; Panahy, Geve; Císařová, Ivana; Goicoechea, Jose M.; Štěpnička, Petr; Dalton transactions (Cambridge, England : 2003) 49 (2020) 8645–8651; doi:10.1039/d0dt01908a

data_7704652
_publ_section_title
;
 Novel ferrocenyl functionalised phosphinecarboxamides: synthesis,
 characterisation and coordination.
;
_journal_issue                   25
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              8645
_journal_page_last               8651
_journal_paper_doi               10.1039/d0dt01908a
_journal_volume                  49
_journal_year                    2020
_chemical_formula_moiety         'C11 H12 Fe N O P'
_chemical_formula_sum            'C11 H12 Fe N O P'
_chemical_formula_weight         261.04
_chemical_name_systematic
;
 PH2C(O)NH[Fe]
;
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2ybc'
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_atom_sites_solution_hydrogens   mixed
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_audit_update_record
;
2020-05-26 deposited with the CCDC.	2020-06-10 downloaded from the CCDC.
;
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_computing_cell_refinement
;
'CrysAlisPro 1.171.38.43b (Rigaku OD, 2015)'
;
_computing_data_collection
;
'CrysAlisPro 1.171.38.43b (Rigaku OD, 2015)'
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'CrysAlisPro 1.171.38.43b (Rigaku OD, 2015)'
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_computing_molecular_graphics    'WinGX (Farrugia, 2005)'
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_exptl_absorpt_process_details
;
CrysAlisPro 1.171.38.43b (Rigaku Oxford Diffraction, 2015)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            orange
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_exptl_crystal_description       plate
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0484P)^2^+1.2725P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1016
_refine_ls_wR_factor_ref         0.1134
_reflns_Friedel_coverage         0.000
_reflns_number_gt                3553
_reflns_number_total             4582
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7704652--7704657.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7704652
_shelx_estimated_absorpt_t_min   0.380
_shelx_estimated_absorpt_t_max   0.715
_shelxl_version_number           2013-4
_shelx_res_checksum              6843