Copper(II) and Gallium(III) Complexes of trans-Bis(2-hydroxybenzyl) Cyclen Derivatives: Absence of a Cross-Bridge Proves Surprisingly More Favorable.
Esteves, Catarina V.; Madureira, Joana; Lima, Luís M P; Mateus, Pedro; Bento, Isabel; Delgado, Rita; Inorganic chemistry 53 (2014) 4371–4386; doi:10.1021/ic403156h

data_4338190
_publ_section_title
;
 Copper(II) and Gallium(III) Complexes of trans-Bis(2-hydroxybenzyl)
 Cyclen Derivatives: Absence of a Cross-Bridge Proves Surprisingly More
 Favorable.
;
_journal_issue                   9
_journal_name_full               'Inorganic chemistry'
_journal_page_first              4371
_journal_page_last               4386
_journal_paper_doi               10.1021/ic403156h
_journal_volume                  53
_journal_year                    2014
_chemical_formula_sum            'C22 H31 Cl Cu N4 O7'
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_chemical_name_systematic
; 
 ? 
;
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_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      150(2)
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_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Bruker AXS-KAPPA APEX II diffractometer'
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_exptl_crystal_colour            blue
_exptl_crystal_density_diffrn    1.548
_exptl_crystal_density_method    'not measured'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'calc w=1/[\s^2^(Fo^2^)+(0.0348P)^2^+27.0295P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_data_source_file            ic403156h_si_002.cif
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_cod_depositor_comments
'Adding full bibliography for 4338190--4338192.cif.'
_cod_database_code               4338190