Supramolecular Structure of a Cadmium‒Silver Complex Forming a Two-Dimensional Network Embracing One-Dimensional Chains in a Layered Crystal Structure
Soma, T.; Iwamoto, T.; Acta Crystallographica Section C 52 (1996) 1200–1203; doi:10.1107/S0108270195016118

data_2004824
_publ_contact_author
;
   Prof. Dr. Toschitake Iwamoto
   Department of Chemistry,
   College of Arts and Sciences,
   The University of Tokyo,
   Komaba, Meguro, Tokyo 153,
   Japan
;
_publ_section_title
;
 Supramolecular Structure of a Cadmium--Silver Complex Forming a
 Two-Dimensional Network Embracing One-Dimensional Chains in a Layered
 Crystal Structure
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1200
_journal_page_last               1203
_journal_paper_doi               10.1107/S0108270195016118
_journal_volume                  52
_journal_year                    1996
_chemical_formula_iupac
'[Ag2 Cd(C N)4(C5 H6 N2)2] , 2[Ag2 Cd (C N)4(C5 H6 N2) (C2 H7 N O)]'
_chemical_formula_moiety
'0.5(C14 H12 Ag2 Cd N8),(C11 H13 Ag2 Cd N7 O)'
_chemical_formula_sum            'C18 H19 Ag3 Cd1.5 N11 O'
_chemical_formula_weight         897.64
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
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_cell_angle_beta                 104.95(2)
_cell_angle_gamma                68.68(2)
_cell_formula_units_Z            1
_cell_length_a                   10.882(3)
_cell_length_b                   13.295(4)
_cell_length_c                   10.824(2)
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_cell_measurement_temperature    293
_cell_measurement_theta_max      19.51
_cell_measurement_theta_min      17.38
_cell_volume                     1386.1(7)
_computing_cell_refinement
;      MSC/AFC Diffractometer Control Software
       (Molecular Structure Corporation, 1988)
;
_computing_data_collection
;      MSC/AFC Diffractometer Control Software
       (Molecular Structure Corporation, 1988)
;
_computing_data_reduction        'SHELX76 (Sheldrick, 1976)'
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_diffrn_measurement_device       'RIGAKU AFC5S diffractometer'
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71069
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_diffrn_reflns_limit_h_max       15
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_diffrn_reflns_theta_max         19.51
_diffrn_reflns_theta_min         17.38
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
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_exptl_absorpt_correction_T_max  0.999
_exptl_absorpt_correction_T_min  0.608
_exptl_absorpt_correction_type
'empirical via \y-scans (North, Phillips & Mathews, 1968)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    2.15
_exptl_crystal_density_meas      2.150(10)
_exptl_crystal_density_method    'flotation in mesitylene--bromoform'
_exptl_crystal_description       needle
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_refine_ls_weighting_details     'w = 1/[\s^2^(Fo)+0.0001Fo^2^]'
_refine_ls_weighting_scheme      calc
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_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc w =
1/[\s^2^(Fo)+0.0001Fo^2^]' was changed to 'calc'. New tag
'_refine_ls_weighting_details' was created. The value of the new tag
was set to 'w = 1/[\s^2^(Fo)+0.0001Fo^2^]'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        1386.2(6)
_cod_database_code               2004824