A germanimidoyl chloride: synthesis, characterization and reactivity.
Li, Tong; Zhang, Li; He, Yuhao; Chen, Yizhen; Wang, Dongmin; Liu, Jingjing; Tan, Gengwen; Chemical communications (Cambridge, England) 59 (2023) 1533–1536; doi:10.1039/d2cc05970c

data_7131186
_publ_section_title
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 A germanimidoyl chloride: synthesis, characterization and reactivity.
;
_journal_issue                   11
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              1533
_journal_page_last               1536
_journal_paper_doi               10.1039/d2cc05970c
_journal_volume                  59
_journal_year                    2023
_chemical_formula_sum            'C79 H97 Ge N'
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_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2022-11-04 deposited with the CCDC.	2023-01-17 downloaded from the CCDC.
;
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_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      135(2)
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_diffrn_measurement_device_type  'Bruker D8 Venture'
_diffrn_measurement_method       '\f and \w scans'
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_diffrn_reflns_point_group_measured_fraction_full 0.996
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_diffrn_reflns_theta_max         54.008
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_exptl_absorpt_coefficient_mu    0.606
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_exptl_crystal_description       block
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0856P)^2^+2.5624P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_gt                9592
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d2cc05970c2.cif
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_cod_depositor_comments
'Adding full bibliography for 7131185--7131189.cif.'
_cod_original_cell_volume        3340.9(5)
_cod_database_code               7131186
_shelx_shelxl_version_number     2014/7
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_shelx_res_checksum              8064
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