Orthogonal non-covalent binding forces in solid state supramolecular herringbone-shaped “interlocked dimers”. Pseudopolymorphism in [(ppy)Pd(μ-pz)]2 (ppy = 2-(2-pyridyl)phenyl, pz = pyrazol-1-yl) complex
Pérez, José; Espinosa, Arturo; Galiana, J. Miguel; Pérez, Eduardo; Serrano, J. Luis; Aranda, Miguel A. G.; Insausti, Maite; Dalton Transactions  (2009) 9625–9636; doi:10.1039/b910502f

data_7002723
_publ_section_title
;
 Orthogonal non-covalent binding forces in solid state supramolecular
 herringbone-shaped &#x201C;interlocked dimers&#x201D;.
 Pseudopolymorphism in [(ppy)Pd(\m-pz)]2 (ppy = 2-(2-pyridyl)phenyl, pz
 = pyrazol-1-yl) complex
;
_journal_issue                   43
_journal_name_full               'Dalton Transactions'
_journal_page_first              9625
_journal_page_last               9636
_journal_paper_doi               10.1039/b910502f
_journal_year                    2009
_chemical_formula_sum            'C28 H22 N6 Pd2'
_chemical_formula_weight         655.3
_chemical_name_common
bis(mu2-pyrazol-1-yl)-(2-pyridininphenyl)-C,N)palladium
_chemical_name_systematic
' bis(mu2-pyrazol-1-yl)-(2-pyridininphenyl)-C,N)palladium'
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                81.548(2)
_cell_angle_beta                 83.5446(20)
_cell_angle_gamma                65.502(2)
_cell_formula_units_Z            4
_cell_length_a                   12.2500(5)
_cell_length_b                   12.4596(5)
_cell_length_c                   18.0792(7)
_cell_measurement_temperature    298
_cell_volume                     2479.68(18)
_computing_structure_refinement  FULLPROF
_diffrn_ambient_temperature      298(2)
_diffrn_detector_type            X'Celerator
_diffrn_measurement_device_type  Diffractometer
_diffrn_measurement_method       Bragg-Brentano
_diffrn_radiation_monochromator  'Ge 111'
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.5406
_diffrn_source                   'sealed X-ray tube'
_diffrn_source_target            Cu
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.755
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.016711
_pd_meas_2theta_range_max        99.97301
_pd_meas_2theta_range_min        5.02110
_pd_meas_number_of_points        5683
_pd_meas_scan_method             cont
_pd_proc_2theta_range_inc        0.016711
_pd_proc_2theta_range_max        99.9730
_pd_proc_2theta_range_min        5.0211
_pd_proc_ls_pref_orient_corr     ' ?'
_pd_proc_ls_prof_R_factor        8.1028
_pd_proc_ls_prof_wR_expected     3.3499
_pd_proc_ls_prof_wR_factor       10.9910
_pd_proc_wavelength              1.540590
_pd_spec_mounting                ' ?'
_refine_ls_hydrogen_treatment    constr
_refine_ls_number_parameters     89
_refine_ls_number_reflns         5639
_refine_ls_number_restraints     19
_refine_ls_R_I_factor            8.5991
_cod_data_source_file            b910502f.txt
_cod_data_source_block           complex1
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        2479.67(17)
_cod_database_code               7002723