Synthesis, structure, and magnetic and electrochemical properties of quasi-linear and linear iron(i), cobalt(i), and nickel(i) amido complexes.
Lin, Chun-Yi; Fettinger, James C.; Grandjean, Fernande; Long, Gary J.; Power, Philip P.; Inorganic chemistry 53 (2014) 9400–9406; doi:10.1021/ic501534f

data_4340773
_publ_section_title
;
 Synthesis, structure, and magnetic and electrochemical properties of
 quasi-linear and linear iron(i), cobalt(i), and nickel(i) amido
 complexes.
;
_journal_issue                   17
_journal_name_full               'Inorganic chemistry'
_journal_page_first              9400
_journal_page_last               9406
_journal_paper_doi               10.1021/ic501534f
_journal_volume                  53
_journal_year                    2014
_chemical_formula_moiety         'C30 H52 Fe N2 Si2, C20 H44 K O8'
_chemical_formula_sum            'C50 H96 Fe K N2 O8 Si2'
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_chemical_name_systematic
; 
 ? 
;
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_space_group_name_Hall           '-C 2yc'
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_symmetry_space_group_name_Hall  '-C 2yc'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0457P)^2^+17.8642P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1041
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_reflns_number_gt                11334
_reflns_number_total             13514
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            ic501534f_si_002.cif
_cod_data_source_block           cyl079fmi
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 

 Adding full bibliography for 4340770--4340773.cif.
;
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_shelx_hkl_checksum              92714