1,4-Bis[(2,2':6',2''-terpyridin-4'-yl)oxy]butane
Akerman, Matthew P.; Grimmer, Craig D.; Nikolayenko, Varvara I.; Reddy, Desigan; Acta Crystallographica Section E 67 (2011) o3478–o3479; doi:10.1107/S1600536811050343

data_2232859
_publ_section_title
;
 1,4-Bis[(2,2':6',2''-terpyridin-4'-yl)oxy]butane
;
_journal_coeditor_code           LR2036
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o3478
_journal_page_last               o3479
_journal_paper_doi               10.1107/S1600536811050343
_journal_volume                  67
_journal_year                    2011
_chemical_formula_iupac          'C34 H28 N6 O2'
_chemical_formula_moiety         'C34 H28 N6 O2'
_chemical_formula_sum            'C34 H28 N6 O2'
_chemical_formula_weight         552.62
_chemical_name_systematic
;
1,4-Bis[(2,2':6',2''-terpyridin-4'-yl)oxy]butane
;
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_atom_sites_solution_secondary   difmap
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_cell_volume                     673.64(4)
_computing_cell_refinement
'<i>CrysAlis CCD</i> (Oxford Diffraction, 2008)'
_computing_data_collection
'<i>CrysAlis CCD</i> (Oxford Diffraction, 2008)'
_computing_data_reduction
'<i>CrysAlis RED</i> (Oxford Diffraction, 2008)'
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_computing_publication_material  'WinGX (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
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_diffrn_measured_fraction_theta_max 0.825
_diffrn_measurement_device_type  'Oxford Diffraction Xcalibur 2 CCD'
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_diffrn_reflns_theta_max         34.20
_diffrn_reflns_theta_min         3.21
_diffrn_standards_decay_%        0
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_diffrn_standards_interval_time  0
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_exptl_absorpt_correction_type   multi-scan
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_exptl_crystal_colour            colourless
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_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       triangular
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_refine_ls_R_factor_all          0.0630
_refine_ls_R_factor_gt           0.0527
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.1033P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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