<i>M~m~</i>H~<i>n~</i>(<i>X</i>O~4~)~(<i>m~+{ıt n</i>)/2} crystals: structure, phase transitions, hydrogen bonds, conductivity. I. K~9~H~7~(SO~4~)~8~·H~2~O crystals ‒ a new representative of the family of solid acid conductors
Makarova, Irina; Grebenev, Vadim; Dmitricheva, Elena; Dolbinina, Valentina; Chernyshov, Dmitry; Acta Crystallographica Section B 70 (2014) 218–226; doi:10.1107/S2052520613029892

data_2105793
_publ_section_title
;
 <i>M~m~</i>H~<i>n~</i>(<i>X</i>O~4~)~(<i>m~+{\?it n</i>)/2} crystals:
 structure, phase transitions, hydrogen bonds, conductivity. I.
 K~9~H~7~(SO~4~)~8~&#x00B7;H~2~O crystals -- a new representative of the
 family of solid acid conductors
;
_journal_coeditor_code           BP5061
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_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              218
_journal_page_last               226
_journal_paper_doi               10.1107/S2052520613029892
_journal_volume                  70
_journal_year                    2014
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_symmetry_space_group_name_H-M   'P c a n'
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_cell_angle_beta                 90
_cell_angle_gamma                90
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'B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)'
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w=1/(\s^2^(F)+0.000025F^2^)
_refine_ls_weighting_scheme      sigma
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_refine_ls_wR_factor_ref         0.0480
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_reflns_threshold_expression     I>3\s(I)
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_cod_original_sg_symbol_Hall     '-P -2xc;-2yab;-2zabc'
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