Transition-metal-free synthesis of vicinal triborated compounds and selective functionalisation of the internal C-B bond.
Davenport, Elliot; Fernandez, Elena; Chemical communications (Cambridge, England) 54 (2018) 10104–10107; doi:10.1039/c8cc06153j

data_7122140
_publ_section_title
;
 Transition-metal-free synthesis of vicinal triborated compounds and
 selective functionalisation of the internal C-B bond.
;
_journal_issue                   72
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              10104
_journal_page_last               10107
_journal_paper_doi               10.1039/c8cc06153j
_journal_volume                  54
_journal_year                    2018
_chemical_formula_sum            'C30 H44 B2 O5'
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_audit_update_record
;
2018-07-05 deposited with the CCDC.
2018-08-10 downloaded from the CCDC.
;
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;
 Fullsphere data collection, phi and omega scans
;
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; 
 SADABS Version 2008/1 Bruker-Nonius
 Blessing, Acta Cryst. (1995) A51 33-38
;
_exptl_crystal_colour            yellow
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0684P)^2^+4.0543P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c8cc06153j2.cif
_cod_data_source_block           mo_ED134_0m
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 

 Adding full bibliography for 7122140.cif.
;
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_database_code               7122140
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