Isomerism and reactivity of nickel(ii) acetylacetonate bis(thiosemicarbazone) complexes.
Bilyj, Jessica K.; Riley, Mark J.; Bernhardt, Paul V.; Dalton transactions (Cambridge, England : 2003) 47 (2018) 2018–2030; doi:10.1039/c7dt04337f

data_7045276
_publ_section_title
;
 Isomerism and reactivity of nickel(ii) acetylacetonate
 bis(thiosemicarbazone) complexes.
;
_journal_issue                   6
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2018
_journal_page_last               2030
_journal_paper_doi               10.1039/c7dt04337f
_journal_volume                  47
_journal_year                    2018
_chemical_compound_source        'synthesis as described'
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_symmetry_space_group_name_Hall  '-P 2yn'
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;
2017-10-21 deposited with the CCDC.
2018-01-11 downloaded from the CCDC.
;
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        CrysAlisPro, Agilent Technologies,
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        CrysAlisPro, Agilent Technologies,
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        CrysAlisPro, Agilent Technologies,
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        Empirical absorption correction using spherical harmonics,
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_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.26
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
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_refine_ls_R_factor_all          0.0368
_refine_ls_R_factor_gt           0.034
_refine_ls_shift/su_max          0.001
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_refine_ls_structure_factor_coef Fsqd
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'calc w=1/[\s^2^(Fo^2^)+(0.0513P)^2^+0.2481P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0858
_refine_ls_wR_factor_ref         0.0897
_reflns_number_gt                2492
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_cod_depositor_comments
'Adding full bibliography for 7045276--7045277.cif.'
_cod_original_formula_sum        'C13 H22 N6  S2'
_cod_database_code               7045276