The solid state conformation of oxo stabilised ylides: X-ray structures of four new polyoxo phosphorus ylides
Aitken, R. Alan; Karodia, Nazira; Lightfoot, Philip; Journal of the Chemical Society, Perkin Transactions 2  (2000) 333–; doi:10.1039/a905747a

data_7203875
_publ_section_title
;
 The solid state conformation of oxo stabilised ylides: X-ray
 structures of four new polyoxo phosphorus ylides
;
_journal_issue                   2
_journal_name_full
'Journal of the Chemical Society, Perkin Transactions 2'
_journal_page_first              333
_journal_paper_doi               10.1039/a905747a
_journal_year                    2000
_chemical_formula_sum            'C48 H38 Cl6 O8 P2'
_chemical_formula_weight         1017.49
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
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_audit_creation_date             'Tue Sep 28 13:07:41 1999'
_audit_creation_method           'from TEXRAY.INF file'
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_cell_angle_gamma                76.20(7)
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_cell_length_b                   14.23(2)
_cell_length_c                   17.18(1)
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_cell_measurement_temperature    200
_cell_measurement_theta_max      10.0
_cell_measurement_theta_min      5.1
_cell_volume                     2364(4)
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_computing_publication_material  teXsan
_computing_structure_refinement  teXsan
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_diffrn_orient_matrix_UB_12      0.02720
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_diffrn_radiation_monochromator  graphite
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_diffrn_reflns_limit_k_min       -13
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_diffrn_reflns_limit_l_min       -16
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_refine_ls_structure_factor_coef F
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_cod_data_source_file            a905747a.txt
_cod_data_source_block           Aitken_No.9
_cod_depositor_comments
;
The following automatic conversions were performed:

'_atom_site_thermal_displace_type' tag value 'Uij' was replaced with
'Uani' value 102 times.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_sg_symbol_H-M      'P -1       '
_cod_original_formula_sum        'C48 H38 Cl6 O8 P2 '
_cod_database_code               7203875