A transition metal-gallium cluster formed via insertion of "GaI".
Blundell, Toby J.; Taylor, Laurence J.; Valentine, Andrew J.; Lewis, William; Blake, Alexander J.; McMaster, Jonathan; Kays, Deborah L.; Chemical communications (Cambridge, England) 56 (2020) 8139–8142; doi:10.1039/d0cc03559a

data_7126687
_publ_section_title
;
 A transition metal-gallium cluster formed via insertion of
 &quot;GaI&quot;.
;
_journal_issue                   58
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              8139
_journal_page_last               8142
_journal_paper_doi               10.1039/d0cc03559a
_journal_volume                  56
_journal_year                    2020
_chemical_formula_moiety         'C56 H66 Ga I'
_chemical_formula_sum            'C56 H66 Ga I'
_chemical_formula_weight         935.70
_space_group_crystal_system      monoclinic
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Olex2 1.2
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2020-05-18 deposited with the CCDC.	2020-06-10 downloaded from the CCDC.
;
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
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omega____ theta____ kappa____ phi______ frames
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  3 omega   14.00  114.00   1.0000   40.0000
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  5 omega   99.00  168.00   1.0000  160.0000
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  7 omega   63.00   90.00   1.0000  110.5900
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  8 omega   53.00   80.00   1.0000  110.5900
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  9 omega   46.00  130.00   1.0000  110.5900
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 10 omega  110.00  175.00   1.0000  110.5900
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 11 omega   32.00   91.00   1.0000  110.5900
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 12 omega   92.00  175.00   1.0000  110.5900
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 13 omega   18.00  111.00   1.0000  110.5900
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omega____ theta____ kappa____ phi______ frames
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 15 omega    2.00   84.00   1.0000  110.5900
omega____ theta____ kappa____ phi______ frames
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_diffrn_reflns_Laue_measured_fraction_full 0.998
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CrysAlisPro, Agilent Technologies,
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Numerical absorption correction based on gaussian integration over
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_exptl_crystal_colour            'clear colourless'
_exptl_crystal_colour_lustre     clear
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'w=1/[\s^2^(Fo^2^)+(0.0864P)^2^+1.7908P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_data_source_block           gatblg
_cod_depositor_comments
'Adding full bibliography for 7126685--7126689.cif.'
_cod_original_cell_volume        4614.94(17)
_cod_database_code               7126687
_nottingham_internal_coll_name   GATBLG
_nottingham_internal_coll_number 13617
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_nottingham_internal_coll_type   custom
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_nottingham_internal_coll_frame_width 1.0000
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1. Fixed Uiso
 At 1.2 times of:
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 At 1.5 times of:
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2.a Aromatic/amide H refined with riding coordinates:
 C3(H3), C4(H4), C5(H5), C31(H31), C32(H32), C33(H33)
2.b Idealised Me refined as rotating group:
 C13(H13A,H13B,H13C), C14(H14A,H14B,H14C), C15(H15A,H15B,H15C), C16(H16A,H16B,
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;
_shelx_res_checksum              51638
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_olex2_exptl_crystal_mounting_method 'in fomblin film on a micromount'
_olex2_submission_special_instructions 'No special instructions were received'