Simple fabrication of a carbaldehyde based fluorescent “turn-on” probe for the selective and sole detection of Pd2+: application as test strips
Manna, Chandan Kumar; Gharami, Saswati; Aich, Krishnendu; Patra, Lakshman; Mondal, Tapan K.; New Journal of Chemistry 43 (2019) 16915–; doi:10.1039/C9NJ04313F

data_7058843
_publ_section_title
;
 Simple fabrication of a carbaldehyde based fluorescent
 &#x201C;turn-on&#x201D; probe for the selective and sole detection of
 Pd2+: application as test strips
;
_journal_issue                   43
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              16915
_journal_paper_doi               10.1039/C9NJ04313F
_journal_volume                  43
_journal_year                    2019
_chemical_formula_sum            'C21 H22 N2 O3'
_chemical_formula_weight         350.40
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_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2016/6
_audit_update_record
;
2019-07-09 deposited with the CCDC.    2019-09-27 downloaded from the CCDC.
;
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_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
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_diffrn_measurement_device_type  'Bruker D8 - QUEST'
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_diffrn_reflns_limit_l_min       -18
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_diffrn_reflns_theta_min         2.236
_diffrn_source                   'fine-focuse sealed tube'
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_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   Sadabs
_exptl_crystal_colour            yellow
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_exptl_crystal_description       block
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0721P)^2^+0.2205P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1363
_refine_ls_wR_factor_ref         0.1586
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2751
_reflns_number_total             3853
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c9nj04313f2.cif
_cod_data_source_block           shelx
_cod_depositor_comments          'Adding full bibliography for 7058843.cif.'
_cod_database_code               7058843
_shelx_shelxl_version_number     2016/6
_shelx_res_checksum              4691