s-Block metal ions induce structural transformations between figure-eight and double trefoil knots
Dang, Li-Long; Gao, Xiang; Lin, Yue-Jian; Jin, Guo-Xin; Chemical Science 11 (2020) 1226–1232; doi:10.1039/C9SC05796J

data_1557440
_publ_section_title
;
 s-Block metal ions induce structural transformations between figure-eight
 and double trefoil knots
;
_journal_issue                   5
_journal_name_full               'Chemical Science'
_journal_page_first              1226
_journal_page_last               1232
_journal_paper_doi               10.1039/C9SC05796J
_journal_volume                  11
_journal_year                    2020
_chemical_formula_sum            'C173 H189 F24 N24 O37.5 Rh6 S8 Sr'
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_audit_update_record
;
2019-11-08 deposited with the CCDC.	2020-01-07 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       '\f and \w scans'
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_diffrn_reflns_limit_h_min       -25
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; 
 Refined as an inversion twin. 
;
_refine_ls_abs_structure_Flack   0.22(4)
_refine_ls_extinction_method     none
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1953P)^2^+120.0435P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                10667
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_cod_data_source_file            c9sc05796j2.cif
_cod_data_source_block           3b
_cod_depositor_comments
'Adding full bibliography for 1557437--1557441.cif.'
_cod_original_cell_volume        8984(3)
_cod_original_formula_sum        'C173 H189 F24 N24 O37.50 Rh6 S8 Sr'
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_shelx_res_checksum              30206
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