Structural Consequences of an Extreme Difference between theTransInfluence of the Donor Atoms in a Palladacycle
Koller, Stephan G.; Martín-Romo, Raquel; Melero, José S.; Colquhoun, Victoria P.; Schildbach, Daniel; Strohmann, Carsten; Villafañe, Fernando; Organometallics 33 (2014) 7329–; doi:10.1021/om501100y

data_4084991
_publ_section_title
;
 Structural Consequences of an Extreme Difference between
 theTransInfluence of the Donor Atoms in a Palladacycle
;
_journal_issue                   24
_journal_name_full               Organometallics
_journal_page_first              7329
_journal_paper_doi               10.1021/om501100y
_journal_volume                  33
_journal_year                    2014
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;
CrysAlis RED, Oxford Diffraction Ltd.,
Version 1.171.32.37 (release 24-10-2008 CrysAlis171 .NET)
(compiled Oct 24 2008,09:44:38)'
;
_computing_data_collection
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CrysAlis CCD, Oxford Diffraction Ltd.,
Version 1.171.32.37 (release 24-10-2008 CrysAlis171 .NET)
(compiled Oct 24 2008,09:44:38)
;
_computing_data_reduction
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CrysAlis RED, Oxford Diffraction Ltd.,
Version 1.171.32.37 (release 24-10-2008 CrysAlis171 .NET)
(compiled Oct 24 2008,09:44:38)
;
_computing_molecular_graphics
;
Ortep-3 (Farrugia, 1997) and Schakal 92 (Keller 1992)
;
_computing_publication_material  'wingx (Farrugia, 1999)'
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_diffrn_radiation_monochromator  graphite
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_diffrn_reflns_number            58301
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_diffrn_reflns_theta_min         2.41
_exptl_absorpt_coefficient_mu    0.855
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;
        CrysAlisPro, Agilent Technologies,
        Version 1.171.36.24 (release 03-12-2012 CrysAlis171 .NET)
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        Empirical absorption correction using spherical harmonics,
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;
_exptl_crystal_density_diffrn    1.327
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;
;
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_refine_ls_abs_structure_Flack   0.01(2)
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_refine_ls_R_factor_all          0.0247
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0360P)^2^+2.0099P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                5407
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_cod_depositor_comments
'Adding full bibliography for 4084989--4084991.cif.'
_cod_original_cell_volume        4664.91(18)
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