Synthesis and crystal structures of 5,5'-(propane-2,2-diyl)bis(2-hydroxybenzaldehyde) and 5,5'-(propane-2,2-diyl)bis(2-hydroxyisophthalaldehyde)
Sausa, Rosario C.; Lastovickova, Dominika N.; La Scala, John J.; Acta Crystallographica Section E 74 (2018) 1872–1877; doi:10.1107/S2056989018016316

data_2242748
_publ_section_title
;
 Synthesis and crystal structures of
 5,5'-(propane-2,2-diyl)bis(2-hydroxybenzaldehyde) and
 5,5'-(propane-2,2-diyl)bis(2-hydroxyisophthalaldehyde)
;
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              1872
_journal_page_last               1877
_journal_paper_doi               10.1107/S2056989018016316
_journal_volume                  74
_journal_year                    2018
_chemical_formula_iupac          'C19 H16 O6'
_chemical_formula_moiety         'C19 H16 O6'
_chemical_formula_sum            'C19 H16 O6'
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_chemical_name_systematic
;
5,5'-(propane-2,2-diyl)bis(2-hydroxyisophthalaldehyde)
;
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
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;
Olex2 1.2
(compiled 2016.09.09 svn.r3337 for OlexSys, GUI svn.r5227)
;
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;
CrysAlisPro (Rigaku OD, 2015)
;
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;
CrysAlisPro (Rigaku OD, 2015)
;
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CrysAlisPro (Rigaku OD, 2015)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>,  2009)
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Mercury (Macrae <i>et al.</i>,  2008)
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ShelXL (Sheldrick, 2015b)
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_computing_structure_solution
;
ShelXT (Sheldrick, 2015a)
;
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'Rigaku Oxford Diffraction SuperNova, Dualflex, EosS2'
_diffrn_measurement_method       '\w scans'
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;
(CrysAlisPro; Bourhis <i>et al.</i>,  2015)
;
_exptl_crystal_colour            Yellow
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_exptl_crystal_description       Irregular
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_exptl_crystal_size_min          0.28
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_refine_diff_density_min         -0.273
_refine_ls_extinction_method     none
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_refine_ls_number_restraints     0
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0850P)^2^+0.5400P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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