Ca-, Sr-, and Ba-Coordination polymers based on anthranilic acid via mechanochemistry.
Al-Terkawi, Abdal-Azim; Scholz, Gudrun; Prinz, Carsten; Emmerling, Franziska; Kemnitz, Erhard; Dalton transactions (Cambridge, England : 2003) 48 (2019) 6513–6521; doi:10.1039/c9dt00991d

data_1550862
_publ_section_title
;
 Ca-, Sr-, and Ba-Coordination polymers based on anthranilic acid via
 mechanochemistry.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              6513
_journal_page_last               6521
_journal_paper_doi               10.1039/c9dt00991d
_journal_volume                  48
_journal_year                    2019
_chemical_compound_source        'Mechanochemical synthesis'
_chemical_formula_moiety         'C14 H18 Ca N2 O7'
_chemical_formula_structural     'Ca-Anthranilate trihydrate'
_chemical_formula_sum            'C14 H18 Ca N2 O7'
_chemical_formula_weight         366.38
_chemical_name_common            'Ca-Anthranilate trihydrate'
_chemical_name_mineral           'Ca-Anthranilate trihydrate'
_space_group_IT_number           60
_space_group_name_Hall           '-P 2n 2ab'
_space_group_name_H-M_alt        'P b c n'
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      60
_symmetry_space_group_name_Hall  '-P 2n 2ab'
_symmetry_space_group_name_H-M   'P b c n'
_audit_update_record
;
2019-03-06 deposited with the CCDC.    2019-04-08 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   28.4326(6)
_cell_length_b                   7.33162(12)
_cell_length_c                   7.92571(13)
_cell_measurement_temperature    293
_cell_volume                     1652.17(5)
_computing_cell_refinement       'TOPAS Academic (Coelho, 2007)'
_computing_data_reduction        'DASH (David <i>et al.</i>, 2006)'
_computing_molecular_graphics    'Diamond (Crystal Impact GbR,2014)'
_computing_publication_material  'publCIF (Westrip, 2010)'
_computing_structure_refinement  'TOPAS Academic (Coelho, 2007)'
_computing_structure_solution    'DASH (David <i>et al.</i>, 2006)'
_diffrn_ambient_temperature      293(2)
_diffrn_measurement_device_type  'D8 Discover Bruker'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_source         'X-ray tube'
_exptl_absorpt_coefficient_mu    3.642
_exptl_crystal_colour            white
_exptl_crystal_density_diffrn    1.473
_exptl_crystal_density_method    'Not Measured'
_exptl_crystal_description       powder
_exptl_crystal_F_000             768
_pd_meas_2theta_range_max        66
_pd_meas_2theta_range_min        5.4
_pd_proc_2theta_range_inc        0.009
_pd_proc_info_excluded_regions   none
_pd_proc_ls_prof_wR_factor       2.69
_pd_spec_mounting                '0.5 mm glass capillary'
_pd_spec_mount_mode              transmission
_refine_ls_goodness_of_fit_all   2.31
_refine_ls_R_I_factor            2.213
_cod_data_source_file            c9dt00991d2.cif
_cod_data_source_block           CaIobPbcn
_cod_depositor_comments
'Adding full bibliography for 1550862--1550864.cif.'
_cod_database_code               1550862