Structures of three alicyclic α-dioximes with a ring size of six to eight
Streltsova, N. R.; Bel'sky, V. K.; Voloshin, Y. Z.; Acta Crystallographica Section C 49 (1993) 635–639; doi:10.1107/S0108270192011144

data_2001926
_publ_section_title
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 Structures of three alicyclic \a-dioximes with a ring size of six to
 eight
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_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              635
_journal_page_last               639
_journal_paper_doi               10.1107/S0108270192011144
_journal_volume                  49
_journal_year                    1993
_chemical_formula_sum            'C6 H10 N2 O2'
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_cell_angle_beta                 90.
_cell_angle_gamma                90.
_cell_formula_units_Z            4
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_cell_length_c                   7.474(2)
_cell_measurement_reflns_used    16
_cell_measurement_temperature    298
_cell_measurement_theta_max      28
_cell_measurement_theta_min      23
_cell_volume                     709.2(3)
_diffrn_measurement_device       'Syntex P-1'
_diffrn_measurement_method       \q/2\q
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_limit_h_min       0
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_diffrn_standards_decay_%        .0
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_exptl_absorpt_coefficient_mu    0.0948
_exptl_absorpt_correction_type   none
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_refine_ls_hydrogen_treatment    refall
_refine_ls_number_parameters     131
_refine_ls_number_reflns         603
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_refine_ls_shift/esd_max         0.382
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     'w = 1/[\s^2^(F)+0.00066F^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.027
_reflns_number_observed          603
_reflns_number_total             726
_reflns_observed_criterion       I>=3\s(I)
_cod_data_source_file            vs0102.cif
_cod_data_source_block           vs0102_structure_1_of_3
_cod_depositor_comments
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The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value '1/[\s^2^(F)+0.00066F^2^]' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to 'w =
1/[\s^2^(F)+0.00066F^2^]'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
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_cod_database_code               2001926