Metal ion-driven formation of 2<i>H</i>-silolides and -germolides.
Liu, Chenghuan; Schmidtmann, Marc; Müller, Thomas; Chemical communications (Cambridge, England) 60 (2024) 11295–11298; doi:10.1039/d4cc03984j

data_7133645
_publ_section_title
;
 Metal ion-driven formation of 2<i>H</i>-silolides and -germolides.
;
_journal_issue                   80
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              11295
_journal_page_last               11298
_journal_paper_doi               10.1039/d4cc03984j
_journal_volume                  60
_journal_year                    2024
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;
2024-07-05 deposited with the CCDC.	2024-08-30 downloaded from the CCDC.
;
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_diffrn_source                   'I\mS microfocus'
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_refine_ls_extinction_method     none
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_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0500P)^2^+0.9000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                12038
_reflns_number_total             14466
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d4cc03984j3.cif
_cod_data_source_block           lch0826ge
_cod_depositor_comments
'Adding full bibliography for 7133645--7133649.cif.'
_cod_database_code               7133645
_shelx_shelxl_version_number     2018/3
_shelx_estimated_absorpt_t_min   0.828
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_shelx_res_checksum              94364