2,3-Ethylene-bridged dihomooxacalix[4]arenes: synthesis, X-ray crystal structures and highly selective binding properties with anions
An, Lin; Wang, Jia-wei; Wang, Chan; Zhou, Shan-shan; Sun, Jing; Yan, Chao-Guo; New Journal of Chemistry 42 (2018) 10689–; doi:10.1039/C8NJ01284A

data_7057406
_publ_section_title
;
 2,3-Ethylene-bridged dihomooxacalix[4]arenes: synthesis, X-ray crystal
 structures and highly selective binding properties with anions
;
_journal_issue                   13
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              10689
_journal_paper_doi               10.1039/C8NJ01284A
_journal_volume                  42
_journal_year                    2018
_chemical_formula_moiety         'C47 H60 O5'
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_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-I 2ya'
_space_group_name_H-M_alt        'I 1 2/a 1'
_symmetry_space_group_name_Hall  '-I 2ya'
_symmetry_space_group_name_H-M   'I 1 2/a 1'
_atom_sites_solution_hydrogens   mixed
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_audit_update_record
;
2017-08-06 deposited with the CCDC.
2018-05-09 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.54
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_cell_volume                     8463.2(16)
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_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      293(2)
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_diffrn_measured_fraction_theta_max 0.981
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_source         'fine-focus sealed tube'
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'w=1/[\s^2^(Fo^2^)+(0.0152P)^2^+344.0247P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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'Adding full bibliography for 7057406--7057408.cif.'
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