Giant phototransistor response in dithienyltetrathiafulvalene derivatives
Tomoyuki Kakinuma; Hirotaka Kojima; Tadashi Kawamoto; Takehiko Mori; Journal of Materials Chemistry C 1 (2013) 2900–2905; doi:10.1039/C3TC30089G

data_7233204
_publ_section_title
;
 Giant phototransistor response in dithienyltetrathiafulvalene derivatives
;
_journal_name_full               'Journal of Materials Chemistry C'
_journal_page_first              2900
_journal_page_last               2905
_journal_paper_doi               10.1039/C3TC30089G
_journal_volume                  1
_journal_year                    2013
_chemical_formula_moiety         'C22 H24 S6 '
_chemical_formula_sum            'C22 H24 S6'
_chemical_formula_weight         480.79
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.0000
_cell_angle_beta                 100.39(3)
_cell_angle_gamma                90.0000
_cell_formula_units_Z            2
_cell_length_a                   17.710(6)
_cell_length_b                   6.1607(12)
_cell_length_c                   10.744(4)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293.1
_cell_measurement_theta_max      14.9
_cell_measurement_theta_min      12.7
_cell_volume                     1153.0(6)
_computing_cell_refinement       WinAFC
_computing_data_collection       WinAFC
_computing_data_reduction        CrystalStructure
_computing_publication_material  'CrystalStructure 3.8'
_computing_structure_refinement  CRYSTALS
_computing_structure_solution    SIR92
_diffrn_ambient_temperature      293.1
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Rigaku AFC7R'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.096
_diffrn_reflns_limit_h_max       24
_diffrn_reflns_limit_h_min       -24
_diffrn_reflns_limit_k_max       8
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            6780
_diffrn_reflns_theta_full        30.02
_diffrn_reflns_theta_max         30.02
_diffrn_standards_decay_%        0.00
_diffrn_standards_interval_count 0
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.600
_exptl_absorpt_correction_T_max  0.887
_exptl_absorpt_correction_T_min  0.650
_exptl_absorpt_correction_type   psi-scan
_exptl_absorpt_process_details   '(North, Phillips & Mathews, 1968)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.385
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prismatic
_exptl_crystal_F_000             504.00
_exptl_crystal_size_max          0.60
_exptl_crystal_size_mid          0.50
_exptl_crystal_size_min          0.10
_refine_diff_density_max         1.17
_refine_diff_density_min         -0.99
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.052
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     127
_refine_ls_number_reflns         5146
_refine_ls_R_factor_gt           0.0807
_refine_ls_shift/su_max          0.0000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[0.0010Fo^2^ + 3.0000\s(Fo^2^) + 0.5000]/(4Fo^2^)'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1768
_reflns_number_gt                3158
_reflns_number_total             3373
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
_cod_data_source_file            1000002.cif
_cod_data_source_block           PCOD1000002
_cod_original_formula_sum        'C22 H24 S6 '
_cod_database_code               7233204