Direct synthesis of enone-hydrazones under solvent free and additive free conditions.
He, Kun; Zeng, Weikun; Yu, Xianglin; Zhou, Jun; Jin, Yi; Organic & biomolecular chemistry 23 (2025) 377–382; doi:10.1039/d4ob01578a

data_7160207
_publ_section_title
;
 Direct synthesis of enone-hydrazones under solvent free and additive free
 conditions.
;
_journal_issue                   2
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              377
_journal_page_last               382
_journal_paper_doi               10.1039/d4ob01578a
_journal_volume                  23
_journal_year                    2025
_chemical_formula_moiety         'C16 H14 N2 O'
_chemical_formula_sum            'C16 H14 N2 O'
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Olex2 1.2
(compiled 2014.09.19 svn.r3010 for OlexSys, GUI svn.r4874)
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2022-07-15 deposited with the CCDC.	2024-11-06 downloaded from the CCDC.
;
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_cell_angle_gamma                90
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_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0454
_diffrn_reflns_av_unetI/netI     0.0390
_diffrn_reflns_Laue_measured_fraction_full 1.000
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'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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'Adding full bibliography for 7160207--7160208.cif.'
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;
1. Others
 Fixed Uiso: H1(0.077) H2(0.082) H3(0.082) H4(0.083) H5(0.073) H7(0.073)
 H8(0.073) H9(0.067) H12(0.069) H13(0.081) H14(0.082) H15(0.081) H16(0.068)
 Fixed X: H1(0.460441) H2(0.47295) H3(0.616813) H4(0.751396) H5(0.741792)
 H7(0.532487) H8(0.767917) H9(0.756744) H12(0.741944) H13(0.726713)
 H14(0.593925) H15(0.47425) H16(0.486607)
 Fixed Y: H1(0.529382) H2(0.433259) H3(0.245857) H4(0.153518) H5(0.246205)
 H7(0.539227) H8(0.34213) H9(0.429292) H12(0.485979) H13(0.560105)
 H14(0.765065) H15(0.895451) H16(0.819186)
 Fixed Z: H1(0.220005) H2(0.147966) H3(0.127167) H4(0.177526) H5(0.249324)
 H7(0.295282) H8(0.383772) H9(0.453202) H12(0.518816) H13(0.591888)
 H14(0.614053) H15(0.563422) H16(0.490306)
;
_shelx_res_checksum              20491
_shelx_shelxl_version_number     2016/6
_olex2_submission_special_instructions 'No special instructions were received'