NHC-ligated indenyl- and fluorenyl-substituted Alanes and Gallanes: synthons towards indenyl- and fluorenyl-bridged (AlC)<sub><i>n</i></sub>-heterocycles (<i>n</i> = 2,3).
Werner, Luis; Hagn, Julika; Gerstner, Alexander; Radius, Udo; Dalton transactions (Cambridge, England : 2003) 53 (2024) 5932–5946; doi:10.1039/d4dt00244j

data_7715398
_publ_section_title
;
 NHC-ligated indenyl- and fluorenyl-substituted Alanes and Gallanes:
 synthons towards indenyl- and fluorenyl-bridged
 (AlC)<sub><i>n</i></sub>-heterocycles (<i>n</i> = 2,3).
;
_journal_issue                   13
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'Dalton transactions (Cambridge, England : 2003)'
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_journal_paper_doi               10.1039/d4dt00244j
_journal_volume                  53
_journal_year                    2024
_chemical_formula_moiety         'C22 H27 Ga N2'
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;
2024-01-25 deposited with the CCDC.	2024-03-04 downloaded from the CCDC.
;
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;
CrysAlisPro 1.171.41.73a (Rigaku Oxford Diffraction, 2020)
Numerical absorption correction based on gaussian integration over
a multifaceted crystal model
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0306P)^2^+0.7077P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0674
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_reflns_number_total             5348
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           compound_11
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'Adding full bibliography for 7715387--7715402.cif.'
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_shelx_shelxl_version_number     2018/3
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_shelx_res_checksum              63112