5-N-Arylaminothiazoles with pyridyl groups and their first-row transition metal complexes: synthesis, photophysical properties, and Zn sensing
Puji Pamungkas, Khurnia Krisna; Maruyama, Toshifumi; Murai, Toshiaki; RSC Advances 12 (2022) 14698–14706; doi:10.1039/D2RA01694J

data_7244943
_publ_section_title
;
 5-N-Arylaminothiazoles with pyridyl groups and their first-row transition
 metal complexes: synthesis, photophysical properties, and Zn sensing
;
_journal_issue                   23
_journal_name_full               'RSC Advances'
_journal_page_first              14698
_journal_page_last               14706
_journal_paper_doi               10.1039/D2RA01694J
_journal_volume                  12
_journal_year                    2022
_chemical_formula_moiety         'C28 H24 N4 S'
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_audit_update_record
;
2022-03-01 deposited with the CCDC.	2022-05-09 downloaded from the CCDC.
;
_cell_angle_alpha                115.971(4)
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'CrystalClear-SM Expert 2.0 r16 (Rigaku, 2014)'
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'CrystalClear-SM Expert 2.0 r16 (Rigaku, 2014)'
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'CrystalClear-SM Expert 2.0 r16 (Rigaku, 2014)'
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_diffrn_measurement_device_type  'Rigaku Mercury CCD (2x2 bin mode)'
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_diffrn_radiation_type           MoK\a
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_exptl_absorpt_correction_type   numerical
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_exptl_crystal_description       Block
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0786P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1271
_refine_ls_wR_factor_ref         0.1347
_reflns_Friedel_coverage         0.000
_reflns_number_gt                3854
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d2ra01694j2.cif
_cod_data_source_block           0507
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'Numerical' was
changed to 'numerical' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas 
;
_cod_database_code               7244943
_shelx_shelxl_version_number     2014/7
_shelx_estimated_absorpt_t_min   0.934
_shelx_estimated_absorpt_t_max   0.948
_shelx_res_checksum              72595