Magnetic on-off switching in redox non-innocent ligand bridged binuclear cobalt complexes.
Wang, Yichen; Li, Jing; Zhang, Li; Chen, Chao; Feng, Rui; Zhao, Yue; Zhang, Yi-Quan; Tan, Gengwen; Song, You; Wang, Xinping; Dalton transactions (Cambridge, England : 2003) 47 (2018) 17211–17215; doi:10.1039/c8dt04157a

data_7048117
_publ_section_title
;
 Magnetic on-off switching in redox non-innocent ligand bridged binuclear
 cobalt complexes.
;
_journal_issue                   48
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              17211
_journal_page_last               17215
_journal_paper_doi               10.1039/c8dt04157a
_journal_volume                  47
_journal_year                    2018
_chemical_formula_sum            'C94 H116 B Co2 N8 O'
_chemical_formula_weight         1502.61
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2018-08-17 deposited with the CCDC.
2018-11-13 downloaded from the CCDC.
;
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_computing_structure_solution    'SHELXT 2014/4 (Sheldrick, 2014)'
_diffrn_ambient_temperature      123(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
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_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0538P)^2^+1.4702P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.1111
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_reflns_number_gt                12850
_reflns_number_total             16458
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c8dt04157a2.cif
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_cod_depositor_comments
'Adding full bibliography for 7048116--7048117.cif.'
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