Iron complexes of a bidentate picolyl-NHC ligand: synthesis, structure and reactivity.
Liang, Qiuming; Janes, Trevor; Gjergji, Xhoana; Song, Datong; Dalton transactions (Cambridge, England : 2003) 45 (2016) 13872–13880; doi:10.1039/c6dt02792j

data_7040145
_publ_section_title
;
 Iron complexes of a bidentate picolyl-NHC ligand: synthesis, structure
 and reactivity.
;
_journal_issue                   35
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              13872
_journal_page_last               13880
_journal_paper_doi               10.1039/c6dt02792j
_journal_volume                  45
_journal_year                    2016
_chemical_formula_sum            'C44 H54 Br2 Fe N6 O2'
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_space_group_name_Hall           '-P 2yn'
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_symmetry_space_group_name_Hall  '-P 2yn'
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_audit_update_record
;
2016-07-14 deposited with the CCDC.
2016-08-04 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'Bruker Kappa Apex II'
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_exptl_crystal_description       plate
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0980P)^2^+15.6741P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1657
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_reflns_number_gt                5883
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_reflns_threshold_expression     'I > 2\s(I)'
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'Adding full bibliography for 7040145--7040152.cif.'
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