Few-layered titanium trisulfide (TiS3) field-effect transistors.
Lipatov, Alexey; Wilson, Peter M.; Shekhirev, Mikhail; Teeter, Jacob D.; Netusil, Ross; Sinitskii, Alexander; Nanoscale 7 (2015) 12291–12296; doi:10.1039/c5nr01895a

data_1520546
_publ_section_title
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 Few-layered titanium trisulfide (TiS3) field-effect transistors.
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_journal_issue                   29
_journal_name_full               Nanoscale
_journal_page_first              12291
_journal_page_last               12296
_journal_paper_doi               10.1039/c5nr01895a
_journal_volume                  7
_journal_year                    2015
_chemical_formula_sum            'S3 Ti'
_chemical_formula_weight         144.1
_chemical_name_systematic        ' ?'
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      11
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 97.617
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   4.9476
_cell_length_b                   3.3787
_cell_length_c                   8.7479
_cell_measurement_temperature    293
_cell_volume                     144.944
_diffrn_ambient_temperature      293
_diffrn_measured_fraction_theta_full 0.83
_diffrn_measured_fraction_theta_max 0.78
_diffrn_radiation_probe          x-ray
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_unetI/netI     0.1389
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_k_max       4
_diffrn_reflns_limit_k_min       -4
_diffrn_reflns_limit_l_max       11
_diffrn_reflns_limit_l_min       -11
_diffrn_reflns_number            702
_diffrn_reflns_theta_full        11.82
_diffrn_reflns_theta_max         27.46
_diffrn_reflns_theta_min         2.35
_exptl_absorpt_coefficient_mu    4.769
_exptl_crystal_density_diffrn    3.3008
_exptl_crystal_F_000             140
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_gt    2.56
_refine_ls_goodness_of_fit_ref   2.13
_refine_ls_number_constraints    0
_refine_ls_number_parameters     21
_refine_ls_number_reflns         702
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.1771
_refine_ls_R_factor_gt           0.1252
_refine_ls_shift/su_max          0.0148
_refine_ls_shift/su_mean         0.0042
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w=1/(\s^2^(F)+0.0001F^2^)
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.1463
_refine_ls_wR_factor_ref         0.1545
_reflns_number_gt                435
_reflns_number_total             702
_reflns_threshold_expression     I>3\s(I)
_cod_data_source_file            c5nr01895a2.cif
_cod_data_source_block           I
_cod_depositor_comments
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The following automatic conversions were performed:

'_diffrn_radiation_probe' value 'X-ray' changed to 'x-ray' according
to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3271 2015-04-21 07:52:19Z andrius 

 Adding full bibliography for 1520546.cif.
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_cod_original_cell_volume        144.9436
_cod_original_formula_sum        'S3 Ti1'
_cod_database_code               1520546