Palladium-Catalyzed anti-Michael Reductive Heck Reaction of α,β-Unsaturated Esters
Guo, Tao; Ding, Yalan; Zhou, Lili; Xu, Haiyan; Loh, Teck-Peng; Wu, Xiaojin; ACS Catalysis 10 (2020) 7262–7268; doi:10.1021/acscatal.0c02414

data_4517779
_publ_section_title
;
 Palladium-Catalyzed anti-Michael Reductive Heck Reaction of
 \a,\b-Unsaturated Esters
;
_journal_issue                   13
_journal_name_full               'ACS Catalysis'
_journal_page_first              7262
_journal_page_last               7268
_journal_paper_doi               10.1021/acscatal.0c02414
_journal_volume                  10
_journal_year                    2020
_chemical_formula_sum            'C29 H29 N2 O3'
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_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
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_diffrn_reflns_theta_min         1.633
_exptl_absorpt_coefficient_mu    0.069
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+2.5000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2003
_refine_ls_wR_factor_ref         0.2382
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2640
_reflns_number_total             6991
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            cs0c02414_si_003.cif
_cod_data_source_block           20190313zh_ngd_0m_sq
_cod_depositor_comments
;Adding full bibliography for 4517779.cif.

 Adding full bibliography for 4517779.cif.
;
_cod_database_code               4517779
_shelx_shelxl_version_number     2018/3
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