Synthesis, structures and properties of platinum(II) complexes of oligoacetylenic sulfides
Zhang, Hongkui; Lee, Albert W. M.; Wong, Wai-Yeung; Yuen, Mabel S. M.; Journal of the Chemical Society, Dalton Transactions  (2000) 3675–; doi:10.1039/b004253f

data_7009892
_publ_contact_author
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    ENTER NAME
 ENTER ADDRESS
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_publ_section_title
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 Synthesis, structures and properties of platinum(II) complexes of
 oligoacetylenic sulfides
;
_journal_issue                   20
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              3675
_journal_paper_doi               10.1039/b004253f
_journal_year                    2000
_chemical_formula_moiety         'C38 H54 N2 Pt S2 Si2 '
_chemical_formula_sum            'C38 H54 N2 Pt S2 Si2'
_chemical_formula_weight         854.24
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_audit_creation_date             'Mon Jun  8 20:09:07 1998'
_audit_creation_method           'from TEXRAY.INF file'
_cell_angle_alpha                98.66(1)
_cell_angle_beta                 92.38(1)
_cell_angle_gamma                97.83(1)
_cell_formula_units_Z            2
_cell_length_a                   7.906(1)
_cell_length_b                   14.018(1)
_cell_length_c                   19.069(1)
_cell_measurement_reflns_used    0
_cell_measurement_temperature    298.2
_cell_measurement_theta_max      0.0
_cell_measurement_theta_min      0.0
_cell_volume                     2065.6(3)
_computing_cell_refinement       'MAR research Image plate scanner'
_computing_data_collection       'MAR research Image plate scanner'
_computing_data_reduction        teXsan
_computing_publication_material  teXsan
_computing_structure_refinement  teXsan
_computing_structure_solution    SHELXS86
_diffrn_ambient_temperature      298.2
_diffrn_measurement_device       'MAR research Image plate scanner'
_diffrn_measurement_method       'omega scans with profile analysis'
_diffrn_orient_matrix_UB_11      0.00000
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_diffrn_radiation_monochromator  graphite
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_diffrn_reflns_limit_l_min       -19
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_diffrn_reflns_theta_min         1
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_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    3.568
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_exptl_crystal_description       block
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_obs         0.0601
_reflns_number_observed          2139
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_reflns_observed_criterion       1.50
_cod_data_source_file            b004253f.txt
_cod_data_source_block           wtwong774-wywong070
_cod_depositor_comments
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The following automatic conversions were performed:

'_atom_site_thermal_displace_type' tag value 'Uij' was replaced with
'Uani' value 99 times.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_sg_symbol_H-M      P-1
_cod_original_formula_sum        'C38 H54 N2 Pt S2 Si2 '
_cod_database_code               7009892