Coordination of bis(pyrazol-1-yl)amine to palladium(II): influence of the co-ligands and counter-ions on the molecular and crystal structures
Mendoza, María de los Angeles; Bernès, Sylvain; Mendoza-Díaz, Guillermo; Acta Crystallographica Section E 71 (2015) 22–27; doi:10.1107/S205698901402595X

data_2240284
_publ_section_title
;
 Coordination of bis(pyrazol-1-yl)amine to palladium(II): influence of the
 co-ligands and counter-ions on the molecular and crystal structures
;
_journal_coeditor_code           WM5076
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              22
_journal_page_last               27
_journal_paper_doi               10.1107/S205698901402595X
_journal_volume                  71
_journal_year                    2015
_chemical_formula_iupac          '[Pd (N3) (C14 H23 N5)] N3, H2 O'
_chemical_formula_moiety         'C14 H23 N8 Pd +, N3 -, H2 O'
_chemical_formula_sum            'C14 H25 N11 O Pd'
_chemical_formula_weight         469.85
_chemical_name_systematic
;
Azido{bis[2-(3,5-dimethylpyrazol-1-yl-\k<i>N</i>^2^)ethyl]amine-\
\k<i>N</i>}palladium azide monohydrate
;
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2ybc'
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;
XSCANS (Siemens, 1996)
;
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XSCANS (Siemens, 1996)
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XSCANS (Siemens, 1996)
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SHELXTL (Sheldrick, 2008)
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SHELXTL (Sheldrick, 2008)
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SHELXL2014 (Sheldrick, 2008)
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SHELXS2014 (Sheldrick, 2008)
;
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;
(XSCANS; Siemens, 1996)
;
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0346P)^2^+1.7119P] where P=(Fo^2^+2Fc^2^)/3'
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