Low valent lead and tin hydrides in reactions with heteroallenes.
Weiß, Sebastian; Widemann, Max; Eichele, Klaus; Schubert, Hartmut; Wesemann, Lars; Dalton transactions (Cambridge, England : 2003) 50 (2021) 4952–4958; doi:10.1039/d1dt00542a

data_7706809
_publ_section_title
;
 Low valent lead and tin hydrides in reactions with heteroallenes.
;
_journal_issue                   14
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              4952
_journal_page_last               4958
_journal_paper_doi               10.1039/d1dt00542a
_journal_volume                  50
_journal_year                    2021
_chemical_formula_moiety         'C73 H100 S2 Sn2'
_chemical_formula_sum            'C73 H100 S2 Sn2'
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_audit_update_record
;
2021-03-08 deposited with the CCDC.	2021-03-09 downloaded from the CCDC.
;
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_diffrn_measurement_method       '\f and \w scans'
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_exptl_crystal_description       prism
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;
 Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack   0.459(13)
_refine_ls_extinction_method     none
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_refine_ls_R_factor_gt           0.0373
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0183P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                28061
_reflns_number_total             33864
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d1dt00542a2.cif
_cod_data_source_block           MW113_0m_a
_cod_depositor_comments
'Adding full bibliography for 7706807--7706812.cif.'
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_shelx_res_checksum              40651
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