Incorporation of Three or Two Distal Double Bonds at the Methylene Bridges of the Calix[4]arene Scaffold.
Shalev, Ori; Biali, Silvio E.; The Journal of organic chemistry 79 (2014) 8584–8591; doi:10.1021/jo501177g

data_4029902
_publ_section_title
;
 Incorporation of Three or Two Distal Double Bonds at the Methylene
 Bridges of the Calix[4]arene Scaffold.
;
_journal_issue                   18
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              8584
_journal_page_last               8591
_journal_paper_doi               10.1021/jo501177g
_journal_volume                  79
_journal_year                    2014
_chemical_formula_moiety         'C48 H60 O6, 0.5 (C H3 O H), 0.5 (H2 O)'
_chemical_formula_sum            'C48.5 H60 O7'
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_chemical_name_systematic
; 
 ? 
;
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_exptl_crystal_colour            colorless
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.1086P)^2^+2.6847P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_data_source_file            jo501177g_si_002.cif
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_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to
/home/saulius/struct/COD-crude-data--automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 

 Adding full bibliography for 4029900--4029902.cif.
;
_cod_original_cell_volume        2233.1(2)
_cod_original_sg_symbol_Hall     '-P 1 '
_cod_original_sg_symbol_H-M      P-1
_cod_original_formula_sum        'C48.50 H60 O7'
_cod_database_code               4029902