Organosoluble tetravalent actinide di- and trifluorides.
Gotthelf, Garret; Stuber, Matthew A.; Kornienko, Anna Y.; Emge, Thomas J.; Brennan, John G.; Chemical communications (Cambridge, England) 54 (2018) 12018–12020; doi:10.1039/c8cc05501g

data_7122427
_publ_section_title
;
 Organosoluble tetravalent actinide di- and trifluorides.
;
_journal_issue                   85
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              12018
_journal_page_last               12020
_journal_paper_doi               10.1039/c8cc05501g
_journal_volume                  54
_journal_year                    2018
_chemical_formula_moiety
; 
 C20 H20 F2 I2 N4 U, 2(C5 H5 N) 
;
_chemical_formula_sum            'C30 H30 F2 I2 N6 U'
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_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
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;
2018-07-08 deposited with the CCDC.
2018-10-02 downloaded from the CCDC.
;
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_diffrn_ambient_temperature      120(2)
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_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type  'Bruker APEX'
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_diffrn_radiation_type           MoK\a
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_diffrn_reflns_av_unetI/netI     0.0421
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_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2016/6 (Sheldrick 2016)'
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+98.0000P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_Friedel_coverage         0.000
_reflns_number_gt                6783
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_cod_data_source_file            c8cc05501g2.cif
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_cod_depositor_comments
'Adding full bibliography for 7122426--7122427.cif.'
_cod_original_cell_volume        3277.5(13)
_cod_database_code               7122427
_shelx_shelxl_version_number     2016/6
_shelx_estimated_absorpt_t_min   0.340
_shelx_estimated_absorpt_t_max   0.683
_exptl_absorpt_special_details
; 
 C20 H20 F2 I2 N4 U, 2(C5 H5 N) 
;
_shelx_res_checksum              42454