Access to 2-pyridinones comprising enaminonitriles <i>via</i> AgOAc promoted cascade reactions of thioesters with aminomethylene malononitriles.
Zhu, Chen; Zhou, Jubao; Li, Tianxing; Yang, Jiaxin; Jin, Hui; Zhang, Lixin; Organic & biomolecular chemistry 21 (2023) 6881–6885; doi:10.1039/d3ob00915g

data_7159481
_publ_section_title
;
 Access to 2-pyridinones comprising enaminonitriles <i>via</i> AgOAc
 promoted cascade reactions of thioesters with aminomethylene
 malononitriles.
;
_journal_issue                   34
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              6881
_journal_page_last               6885
_journal_paper_doi               10.1039/d3ob00915g
_journal_volume                  21
_journal_year                    2023
_chemical_formula_sum            'C12 H8 Cl N3 O'
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_space_group_crystal_system      orthorhombic
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_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2023-05-31 deposited with the CCDC.	2023-07-17 downloaded from the CCDC.
;
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_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
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_exptl_crystal_colour            colorless
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0538P)^2^+0.9908P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.1385
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_reflns_number_gt                1166
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d3ob00915g2.cif
_cod_data_source_block           1_a
_cod_depositor_comments          'Adding full bibliography for 7159481.cif.'
_cod_database_code               7159481
_shelx_shelxl_version_number     2014/7
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