Structure of δ~1~-CoZn~7.8~, an example of a phason pinning‒unpinning transformation?
Lind, Hanna; Boström, Magnus; Petříček, Vaclav; Lidin, Sven; Acta Crystallographica Section B 59 (2003) 720–729; doi:10.1107/S0108768103019694

data_2104016
_publ_section_title
;
 Structure of \d~1~-CoZn~7.8~, an example of a phason
 pinning--unpinning transformation?
;
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              720
_journal_page_last               729
_journal_paper_doi               10.1107/S0108768103019694
_journal_volume                  59
_journal_year                    2003
_chemical_formula_sum            'Co Zn7.8'
_chemical_formula_weight         568.90
_symmetry_cell_setting           monoclinic
_audit_creation_method           'Jana2000 Version : 16/05/2003'
_cell_angle_alpha                90
_cell_angle_beta                 89.90(3)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   9.030(2)
_cell_length_b                   4.3380(10)
_cell_length_c                   12.511(3)
_cell_measurement_reflns_used    2026
_cell_measurement_temperature    293
_cell_measurement_theta_max      48.4
_cell_measurement_theta_min      2.9
_cell_volume                     490.1(2)
_computing_data_reduction
'XRED: Data Reduction Program, Stoe and Cie, (1996)'
_computing_publication_material  '(Jana2000; Petricek and Dusek, 2000)'
_computing_structure_refinement  '(Jana2000; Petricek and Dusek, 2000)'
_diffrn_ambient_temperature      293
_diffrn_measurement_device_type  'STOE IPDS'
_diffrn_measurement_method       \q-2\q
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0750
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       5
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            8488
_diffrn_reflns_theta_max         48.4
_diffrn_reflns_theta_min         2.9
_exptl_absorpt_coefficient_mu    20.290
_exptl_absorpt_correction_T_max  0.7244
_exptl_absorpt_correction_T_min  0.2627
_exptl_absorpt_correction_type   'Numerical from crystal shape'
_exptl_crystal_colour            metallic
_exptl_crystal_density_diffrn    3.8539(15)
_exptl_crystal_description       tabular
_exptl_crystal_F_000             1006
_exptl_crystal_size_max          0.082
_exptl_crystal_size_mid          0.045
_exptl_crystal_size_min          0.015
_refine_diff_density_max         4.98
_refine_diff_density_min         -4.53
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   2.92
_refine_ls_number_parameters     104
_refine_ls_number_reflns         2026
_refine_ls_R_factor_all          0.1140
_refine_ls_R_factor_gt           0.0624
_refine_ls_shift/su_max          0.0002
_refine_ls_shift/su_mean         0.0000
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w=1/(\s^2^(F)+0.0001F^2^)
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.0668
_refine_ls_wR_factor_ref         0.0687
_reflns_number_gt                1095
_reflns_number_total             2026
_reflns_threshold_expression     I>3\s(I)
_cod_data_source_file            sn5001.cif
_cod_data_source_block           global
_cod_database_code               2104016