Sr~11~Sb~10~
Rehr, A.; Kauzlarich, S.M.; Acta Crystallographica Section C 50 (1994) 1859–1861; doi:10.1107/S0108270194003951

data_2010259
_publ_section_title
;
 Sr~11~Sb~10~
;
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1859
_journal_page_last               1861
_journal_paper_doi               10.1107/S0108270194003951
_journal_volume                  50
_journal_year                    1994
_chemical_formula_sum            'Sb10 Sr11'
_chemical_formula_weight         2181.3
_space_group_IT_number           139
_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_Hall  '-I 4 2'
_symmetry_space_group_name_H-M   'I 4/m m m'
_atom_type_scat_source           IntTabC
_cell_angle_alpha                90.
_cell_angle_beta                 90.
_cell_angle_gamma                90.
_cell_formula_units_Z            4
_cell_length_a                   12.454(10)
_cell_length_b                   12.454(10)
_cell_length_c                   18.066(11)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    130
_cell_measurement_theta_max      20
_cell_measurement_theta_min      6.5
_cell_volume                     2802(4)
_diffrn_measurement_device       'Syntex P2~1~'
_diffrn_measurement_method       \w
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0942
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            1403
_diffrn_reflns_theta_max         55.0
_diffrn_standards_decay_%        +-2.0%,random
_diffrn_standards_interval_count 198
_diffrn_standards_number         2
_exptl_absorpt_coefficient_mu    30.178
_exptl_absorpt_correction_T_max  0.2658
_exptl_absorpt_correction_T_min  0.2305
_exptl_absorpt_correction_type   XABS
_exptl_crystal_colour            metallic
_exptl_crystal_density_diffrn    5.171
_exptl_crystal_description       cuboid
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.175
_exptl_crystal_size_min          0.15
_refine_diff_density_max         8.46
_refine_diff_density_min         -7.34
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   1.31
_refine_ls_number_parameters     39
_refine_ls_number_reflns         471
_refine_ls_R_factor_obs          0.0799
_refine_ls_shift/esd_max         0.001
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(F)+0.0044F^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.0886
_reflns_number_observed          471
_reflns_number_total             897
_reflns_observed_criterion       F>6.0\s(F)
_cod_data_source_file            br1073.cif
_cod_data_source_block           br1073a
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value '1/[\s^2^(F)+0.0044F^2^]' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to 'w =
1/[\s^2^(F)+0.0044F^2^]'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        2801(4)
_cod_database_code               2010259