Synthesis and characterization of bis(imino)pyridine complexes of divalent Mg and Zn.
Myers, Thomas W.; Sherbow, Tobias J.; Fettinger, James C.; Berben, Louise A.; Dalton transactions (Cambridge, England : 2003) 45 (2016) 5989–5998; doi:10.1039/c5dt01541c

data_7035601
_publ_section_title
;
 Synthesis and characterization of bis(imino)pyridine complexes of
 divalent Mg and Zn.
;
_journal_issue                   14
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              5989
_journal_page_last               5998
_journal_paper_doi               10.1039/c5dt01541c
_journal_volume                  45
_journal_year                    2016
_chemical_formula_moiety         'C43 H47 Al Cl2 N3, 2(C4 H8 O)'
_chemical_formula_sum            'C51 H63 Al Cl2 N3 O2'
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_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
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_audit_update_record
;
2015-04-15 deposited with the CCDC.
2015-06-22 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
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_diffrn_reflns_limit_l_min       -26
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_exptl_crystal_colour            Purple
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_refine_ls_number_restraints     38
_refine_ls_restrained_S_all      1.055
_refine_ls_R_factor_all          0.0551
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0921P)^2^+1.2336P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1433
_refine_ls_wR_factor_ref         0.1475
_reflns_Friedel_coverage         0.000
_reflns_number_gt                7324
_reflns_number_total             8006
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c5dt01541c1.cif
_cod_data_source_block           TWM126FMI
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3271 2015-04-21 07:52:19Z andrius 

 Adding full bibliography for 7035598--7035603.cif.
;
_cod_database_code               7035601
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_shelx_res_checksum              80891