Three Guest-Including Coordination Solids from a Single Crystallization: A Discrete Cage and Open-Channel Networks from 1-D Ladders and 1-D Ribbons
Amir H. Mahmoudkhani; George K. H. Shimizu; Inorganic Chemistry 46 (2007) 1593–1602; doi:10.1021/ic0615123

data_4307011
_publ_contact_author_address
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Department of Chemistry, University of Calgary, Calgary, AB, Canada
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_publ_contact_author_email       gshimizu@ucalgary.ca
_publ_contact_author_fax         +1-403-3912350
_publ_contact_author_name        'George K. H. Shimizu'
_publ_contact_author_phone       +1-403-2205344
_publ_section_title
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Three Guest-Including Coordination Solids from a Single Crystallization:
A Discrete Cage and Open-Channel Networks from 1-D Ladders and 1-D Ribbons
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_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1593
_journal_page_last               1602
_journal_paper_doi               10.1021/ic0615123
_journal_volume                  46
_journal_year                    2007
_chemical_formula_sum            'C44 H35 Cu N4 O11.25 S3'
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_chemical_name_systematic
;
 ?
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_cell_angle_gamma                102.6550(10)
_cell_formula_units_Z            4
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_cell_measurement_temperature    173(2)
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_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      173(2)
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_diffrn_radiation_source         'fine-focus sealed tube'
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_diffrn_reflns_limit_k_min       -25
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_exptl_absorpt_coefficient_mu    0.438
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_exptl_absorpt_correction_T_min  0.8705
_exptl_absorpt_process_details   psi-scan
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_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1976
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.2000P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_data_source_file            ic0615123si20060814_082822_4.cif
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_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
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_cod_original_cell_volume        7072.39(18)
_cod_database_code               4307011