Supramolecular cooperative interaction-induced assembly of phosphotungstate polyanions and sulfur-containing pyridine-based cations
Tian, Xuerui; Xin, Xing; Gao, Yuanzhe; Han, Zhangang; CrystEngComm 20 (2018) 1588–; doi:10.1039/C8CE00026C

data_7230087
_publ_section_title
;
 Supramolecular cooperative interaction-induced assembly of
 phosphotungstate polyanions and sulfur-containing pyridine-based cations
;
_journal_issue                   11
_journal_name_full               CrystEngComm
_journal_page_first              1588
_journal_paper_doi               10.1039/C8CE00026C
_journal_volume                  20
_journal_year                    2018
_chemical_formula_sum            'C20 H48 Ag12 N4 O137 P4 S4 W36'
_chemical_formula_weight         10701.46
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2017-12-26 deposited with the CCDC.
2018-02-07 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_cell_measurement_theta_max      26.80
_cell_measurement_theta_min      2.51
_cell_volume                     6892.5(13)
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_diffrn_ambient_temperature      296(2)
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_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0669P)^2^+27.0255P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7230085--7230087.cif.'
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