Antimony(III) and bismuth(III) amides containing pendant N-donor groups‒a combined experimental and theoretical study.
Vránová, Iva; Jambor, Roman; Růžička, Aleš; Hoffmann, Alexander; Herres-Pawlis, Sonja; Dostál, Libor; Dalton transactions (Cambridge, England : 2003) 44 (2015) 395–400; doi:10.1039/c4dt02692f

data_7032942
_publ_section_title
;
 Antimony(III) and bismuth(III) amides containing pendant N-donor
 groups--a combined experimental and theoretical study.
;
_journal_issue                   1
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              395
_journal_page_last               400
_journal_paper_doi               10.1039/c4dt02692f
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety         'C17 H21 Cl2 N2 Sb'
_chemical_formula_sum            'C17 H21 Cl2 N2 Sb'
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_chemical_name_systematic
; 
 ? 
;
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_cell_angle_beta                 119.731(4)
_cell_angle_gamma                90
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_cell_length_b                   10.8550(5)
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_computing_cell_refinement       'COLLECT and DENZO'
_computing_data_collection
'COLLECT (Hooft, 1998) and DENZO (Otwinowski & Minor, 1997)'
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_computing_molecular_graphics    'PLATON (Spek, 2003)'
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_diffrn_ambient_temperature      150(1)
_diffrn_detector_area_resol_mean 9.091
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Bruker Nonius KappaCCD area detector'
_diffrn_measurement_method       '\f and \w scans to fill the Ewald sphere'
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_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -24
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;
Gaussian integration (Coppens, 1970)
;
_exptl_crystal_colour            'light yellow'
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_refine_ls_R_factor_all          0.0295
_refine_ls_R_factor_gt           0.0214
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'calc w=1/[\s^2^(Fo^2^)+(0.0138P)^2^+1.8064P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_data_source_file            c4dt02692f1.cif
_cod_data_source_block           shelxl
_cod_depositor_comments
'Adding full bibliography for 7032942--7032945.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7032942