Self-assembly patterns of non-metalloid silver thiolates: structural, HR-ESI-MS and stability studies
Chupina, Anastasia; Abramov, Pavel A.; Yanshole, Vadim V.; Sulyaeva, Veronica S.; Kokovkin, Vasily; Sokolov, Maksim Nailyevich; Dalton Transactions  (2021) –; doi:10.1039/D1DT02398E

data_7708912
_publ_section_title
;
 Self-assembly patterns of non-metalloid silver thiolates: structural,
 HR-ESI-MS and stability studies
;
_journal_name_full               'Dalton Transactions'
_journal_paper_doi               10.1039/D1DT02398E
_journal_year                    2021
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_atom_sites_solution_secondary   difmap
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_audit_update_record
;
2021-10-12 deposited with the CCDC.	2021-10-26 downloaded from the CCDC.
;
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_computing_molecular_graphics    'ShelXle (H\"ubschle, 2011)'
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_computing_structure_solution    'SHELXS-2014 (Sheldrick, 2014)'
_diffrn_ambient_temperature      140(2)
_diffrn_detector                 'CCD plate'
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_diffrn_measurement_device       'four-circle diffractometer'
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_diffrn_measurement_method       '\w scans'
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_diffrn_radiation_probe          x-ray
_diffrn_radiation_source         'fine-focus sealed tube'
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_exptl_absorpt_process_details
;
CrysAlisPro 1.171.38.41 (Rigaku Oxford Diffraction, 2015)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colorless
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_exptl_crystal_description       block
_exptl_crystal_F_000             6102
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_exptl_crystal_size_mid          0.100
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_refine_diff_density_max         3.208
_refine_diff_density_min         -1.376
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_refine_ls_extinction_method     none
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0838P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     >2\s(I)
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_cod_data_source_block           1_a
_cod_original_formula_sum        'C226.50 H459 Ag58 N46.40 O94.20 S30'
_cod_database_code               7708912
_shelx_shelxl_version_number     2017/1
_shelx_estimated_absorpt_t_min   0.571
_shelx_estimated_absorpt_t_max   0.743
_shelx_res_checksum              72132
_shelx_hkl_checksum              6924