A multicomponent approach for the preparation of homoallylic alcohols
Poh, Jian-Siang; Lau, Shing-Hing; Dykes, Iain G.; Tran, Duc N.; Battilocchio, Claudio; Ley, Steven V.; Chem. Sci. 7 (2016) 6803–; doi:10.1039/C6SC02581A

data_1543741
_publ_section_title
;
 A multicomponent approach for the preparation of homoallylic alcohols
;
_journal_issue                   11
_journal_name_full               'Chem. Sci.'
_journal_page_first              6803
_journal_paper_doi               10.1039/C6SC02581A
_journal_volume                  7
_journal_year                    2016
_chemical_formula_moiety         'C18 H22 Cl N O2'
_chemical_formula_sum            'C18 H22 Cl N O2'
_chemical_formula_weight         319.81
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
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_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2016-06-06 deposited with the CCDC.
2016-07-26 downloaded from the CCDC.
;
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_cell_angle_gamma                90.5090(10)
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_cell_volume                     1698.94(5)
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_computing_data_reduction
'HKL Denzo and Scalepack (Otwinowski & Minor, 1997)'
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_diffrn_ambient_temperature      180(2)
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_diffrn_measured_fraction_theta_max 0.958
_diffrn_measurement_device_type  'Nonius KappaCCD'
_diffrn_measurement_method       '\w and \f-scans'
_diffrn_radiation_type           MoK\a
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_refine_ls_R_factor_all          0.0505
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0388P)^2^+0.6583P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c6sc02581a2.cif
_cod_data_source_block           sl_k3_0002
_cod_depositor_comments          'Adding full bibliography for 1543741.cif.'
_cod_database_code               1543741
_cambridge_user_name             'Shing Lau'
_cambridge_user_crsid            shl56
_cambridge_supervisor_name       'Steven Ley'
_cambridge_supervisor_crsid      svl1000
_cambridge_crystallographer_name 'Andrew Bond'
_cambridge_crystallographer_crsid adb29
_cambridge_sample_id             DNT-182
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_shelx_estimated_absorpt_t_min   0.903
_shelx_estimated_absorpt_t_max   0.944
_shelx_res_checksum              41088