Synthesis and Characterization of Alkali-Metal Salts of 2,2'- and 2,4'-Bipyridyl Radicals and Dianions
Edward Gore-Randall; Mark Irwin; Mark S. Denning; Jose M. Goicoechea; Inorganic Chemistry 48 (2009) 8304–8316; doi:10.1021/ic9009459

data_4303038
_publ_contact_author
;
 Dr. J. M. Goicoechea           
 Chemistry Research Laboratory
 University of Oxford
 Mansfield Road
 Oxford
 OX1 3TA
 UK
;
_publ_contact_author_email       jose.goicoechea@chem.ox.ac.uk
_publ_contact_author_fax         '+44 1865 272690'
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_publ_section_title
;
Synthesis and Characterization of Alkali-Metal Salts of 2,2'- and
2,4'-Bipyridyl Radicals and Dianions
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              8304
_journal_page_last               8316
_journal_paper_doi               10.1021/ic9009459
_journal_volume                  48
_journal_year                    2009
_chemical_formula_moiety         'K4, 2(N2C10H8), 3.5(N2C2H8)'
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; 
K4(N2C10H8)2(N2C2H8)3.5
;
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KappaCCD software "DENZO" (Otwinowski & Minor, 1996)
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KappaCCD software "Collect" (Nonius, 2000)
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KappaCCD software "DENZO" (Otwinowski & Minor, 1996)
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_exptl_absorpt_process_details   'DENZO/SCALEPACK (Otwinowski & Minor, 1997)'
_exptl_crystal_colour            purple
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_exptl_crystal_density_meas      ?
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_refine_ls_structure_factor_coef Fsqd
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'calc w=1/[\s^2^(Fo^2^)+(0.0493P)^2^+1.3650P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:
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Automatic conversion script
Id: cif_correct_tags 4998 2017-03-02 13:24:31Z antanas 
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_cod_original_cell_volume        3289.86(7)
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