Effects of solvents and metal ions on the synthesis, structural diversity and magnetic properties of the 5′-nitro-[1,1′:3′,1′′-terphenyl]-3,3′′,5,5′′-tetracarboxylic acid ligand and a highly sensitive sensor for Fe3+
Yang, Yuan-Yu; Xue, Jian-Hua; Yang, Dong-Dong; Zhang, Li-Yang; Ma, Qi; Zhao, Xuan; CrystEngComm 26 (2024) 170–179; doi:10.1039/D3CE01076G

data_7247797
_publ_section_title
;
 Effects of solvents and metal ions on the synthesis, structural diversity
 and magnetic properties of the
 5&#x2032;-nitro-[1,1&#x2032;:3&#x2032;,1&#x2032;&#x2032;-terphenyl]-3,3&#x2032;&#x2032;,5,5&#x2032;&#x2032;-tetracarboxylic
 acid ligand and a highly sensitive sensor for Fe3+
;
_journal_issue                   2
_journal_name_full               CrystEngComm
_journal_page_first              170
_journal_page_last               179
_journal_paper_doi               10.1039/D3CE01076G
_journal_volume                  26
_journal_year                    2024
_chemical_formula_sum            'C32 H27 N3 O15 Zn2'
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_space_group_name_Hall           '-C 2yc'
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_audit_update_record
;
2020-07-25 deposited with the CCDC.	2023-11-27 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
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_diffrn_reflns_Laue_measured_fraction_full 0.998
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0655P)^2^+22.2209P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.1633
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_reflns_number_gt                2923
_reflns_number_total             4114
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           complex4
_cod_depositor_comments
'Adding full bibliography for 7247796--7247799.cif.'
_cod_original_cell_volume        3304.4(12)
_cod_original_sg_symbol_H-M      'C 2/c'
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