An alternative route for the synthesis of hydroxylated pillar[5]arene-based amphiphiles.
Al-Azemi, Talal F; Vinodh, Mickey; Alipour, Fatemeh H.; Mohamod, Abdirahman A.; Organic & biomolecular chemistry 16 (2018) 7513–7517; doi:10.1039/c8ob02074d

data_7156448
_publ_section_title
;
 An alternative route for the synthesis of hydroxylated
 pillar[5]arene-based amphiphiles.
;
_journal_issue                   40
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              7513
_journal_page_last               7517
_journal_paper_doi               10.1039/c8ob02074d
_journal_volume                  16
_journal_year                    2018
_chemical_formula_sum            'C109 H98 Cl4 O10'
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_symmetry_space_group_name_Hall  '-P 2yn'
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_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2018-07-25 deposited with the CCDC.
2018-09-26 downloaded from the CCDC.
;
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_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Rigaku R-AXIS RAPID'
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_exptl_crystal_colour            Colorless
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.1593P)^2^+2.4959P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_Friedel_coverage         0.000
_reflns_number_gt                10379
_reflns_number_total             15429
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c8ob02074d2.cif
_cod_data_source_block           shelxl_CCDC1
_cod_depositor_comments
'Adding full bibliography for 7156447--7156448.cif.'
_cod_database_code               7156448
_shelx_shelxl_version_number     2017/1
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