High Mobility Organic Field-Effect Transistor Based on Hexamethylenetetrathiafulvalene with Organic Metal Electrodes
Takahashi, Yukihiro; Hasegawa, Tatsuo; Horiuchi, Sachio; Kumai, Reiji; Tokura, Yoshinori; Saito, Gunji; Chemistry of Materials 19 (2007) 6382–; doi:10.1021/cm702690w

data_4001473
_publ_section_title
;
 High Mobility Organic Field-Effect Transistor Based on
 Hexamethylenetetrathiafulvalene with Organic Metal Electrodes
;
_journal_issue                   26
_journal_name_full               'Chemistry of Materials'
_journal_page_first              6382
_journal_paper_doi               10.1021/cm702690w
_journal_volume                  19
_journal_year                    2007
_chemical_formula_moiety         'C12 H12 S4 '
_chemical_formula_sum            'C12 H12 S4'
_chemical_formula_weight         284.47
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.0000
_cell_angle_beta                 94.683(11)
_cell_angle_gamma                90.0000
_cell_formula_units_Z            4
_cell_length_a                   6.377(3)
_cell_length_b                   14.534(7)
_cell_length_c                   12.919(7)
_cell_measurement_reflns_used    5474
_cell_measurement_temperature    296.1
_cell_measurement_theta_max      31.4
_cell_measurement_theta_min      2.0
_cell_volume                     1193.4(10)
_computing_cell_refinement       PROCESS-AUTO
_computing_data_collection       PROCESS-AUTO
_computing_data_reduction        CrystalStructure
_computing_publication_material  'CrystalStructure 3.8.0'
_computing_structure_refinement  CRYSTALS
_computing_structure_solution    SIR2002
_diffrn_measured_fraction_theta_full 0.974
_diffrn_measured_fraction_theta_max 0.974
_diffrn_measurement_device_type  IPDSC
_diffrn_radiation_type           synchrotron
_diffrn_radiation_wavelength     0.688
_diffrn_reflns_av_R_equivalents  0.037
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            12023
_diffrn_reflns_theta_full        32.56
_diffrn_reflns_theta_max         32.56
_exptl_absorpt_coefficient_mu    0.762
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.583
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             592.00
_exptl_crystal_size_max          0.10
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.10
_refine_diff_density_max         1.32
_refine_diff_density_min         -0.38
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.999
_refine_ls_hydrogen_treatment    refall
_refine_ls_number_parameters     157
_refine_ls_number_reflns         1517
_refine_ls_R_factor_gt           0.0571
_refine_ls_shift/su_max          0.0000
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details
;
    Chebychev polynomial with 3 parameters (Carruthers & Watkin, 1979)
    7.4220    3.8277    5.1727
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.0687
_reflns_number_gt                1501
_reflns_number_total             4236
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
_cod_data_source_file            cm702690w-file003.cif
_cod_data_source_block           '_061201HMTTF'
_cod_original_cell_volume        1193.2(11)
_cod_original_formula_sum        'C12 H12 S4 '
_cod_database_code               4001473