Additive-free regio- and diastereoselective construction of fully-substituted isoxazolidines employing diazo compounds
Gupta, Ekta; Zaheer, Mohd Khalid; Kant, Ruchir; Mohanan, Kishor; Organic Chemistry Frontiers 6 (2019) 1109–; doi:10.1039/C8QO01421C

data_1554586
_publ_section_title
;
 Additive-free regio- and diastereoselective construction of
 fully-substituted isoxazolidines employing diazo compounds
;
_journal_issue                   8
_journal_name_full               'Organic Chemistry Frontiers'
_journal_page_first              1109
_journal_paper_doi               10.1039/C8QO01421C
_journal_volume                  6
_journal_year                    2019
_chemical_compound_source        'see text'
_chemical_formula_moiety         'C17 H20 F3 N O3'
_chemical_formula_sum            'C17 H20 F3 N O3'
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_symmetry_space_group_name_Hall  '-P 2ybc'
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_audit_update_record
;
2018-07-20 deposited with the CCDC.	2019-02-20 downloaded from the CCDC.
;
_cell_angle_alpha                90
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CrystalClear-SM Expert 2.1 b24 (Rigaku, 2012)
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_computing_data_collection
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CrystalClear-SM Expert 2.1 b24 (Rigaku, 2012)
;
_computing_data_reduction
;
CrystalClear-SM Expert 2.1 b24 (Rigaku, 2012)
;
_computing_molecular_graphics    'SHELXTL (Bruker, 1997)'
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_diffrn_ambient_temperature      293(2)
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AFC12 (Right): Kappa 3 circle
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_diffrn_measurement_device_type
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Rigaku Saturn724+ (4x4 bin mode)
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_diffrn_measurement_method       'profile data from \w-scans'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0973P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_data_source_file            c8qo01421c2.cif
_cod_data_source_block           xxx
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'Multi-scan' was
changed to 'multi-scan' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/RSC/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

data item '_refine_ls_hydrogen_treatment' value 'Constr' was changed
to 'constr' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/RSC/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

data item '_symmetry_cell_setting' value 'Monoclinic' was changed to
'monoclinic' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/RSC/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               1554586