<i>cis</i>-Bis(2,2'-bipyridine-κ^2^<i>N</i>,<i>N</i>')dichloridoiron(III) perchlorate
Zhang, Zhi-Fang; Acta Crystallographica Section E 67 (2011) m677–; doi:10.1107/S1600536811016035

data_2230553
_publ_section_title
;
 <i>cis</i>-Bis(2,2'-bipyridine-\k^2^<i>N</i>,<i>N</i>')dichloridoiron(III)
 perchlorate
;
_journal_coeditor_code           ZQ2098
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m677
_journal_paper_doi               10.1107/S1600536811016035
_journal_volume                  67
_journal_year                    2011
_chemical_formula_iupac          '[Fe Cl2 (C10 H8 N2)2] Cl O4'
_chemical_formula_moiety         'C20 H16 Cl2 Fe N4 +, Cl O4 -'
_chemical_formula_sum            'C20 H16 Cl3 Fe N4 O4'
_chemical_formula_weight         538.57
_chemical_name_systematic
;
<i>cis</i>-Bis(2,2'-bipyridine-\k^2^<i>N</i>,<i>N</i>')dichloridoiron(III)
perchlorate
;
_space_group_IT_number           19
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_symmetry_space_group_name_H-M   'P 21 21 21'
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_cell_measurement_temperature    295(2)
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_computing_structure_solution    'SHELXTL (Sheldrick, 2008)'
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_diffrn_measurement_method       '\f and \w'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0430P)^2^+0.4377P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     I>2sigma(I)
_cod_data_source_file            zq2098.cif
_cod_data_source_block           I
_cod_original_cell_volume        2132.1(7)
_cod_database_code               2230553
_cod_database_fobs_code          2230553