<i>catena</i>-[[(nitrato-κ<i>O</i>)silver(I)]-μ-1,10-phenanthroline-5,6-dione-κ^4^<i>O</i>,<i>O</i>':<i>N</i>,<i>N</i>']
Jing, Xiao; Zhu, Yu-Lan; Ma, Kui-Rong; Cao, Li; Shao, Shuai; Acta Crystallographica Section E 67 (2011) m957–m958; doi:10.1107/S1600536811020939

data_2230714
_publ_section_title
;
 <i>catena</i>-[[(nitrato-\k<i>O</i>)silver(I)]-\m-1,10-phenanthroline-5,6-dione-\k^4^<i>O</i>,<i>O</i>':<i>N</i>,<i>N</i>']
;
_journal_coeditor_code           IM2282
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m957
_journal_page_last               m958
_journal_paper_doi               10.1107/S1600536811020939
_journal_volume                  67
_journal_year                    2011
_chemical_formula_iupac          '[Ag (N O3) (C12 H6 N2 O2)]'
_chemical_formula_moiety         'C12 H6 Ag N3 O5'
_chemical_formula_sum            'C12 H6 Ag N3 O5'
_chemical_formula_weight         380.07
_chemical_name_systematic
;
<i>catena</i>-[[(nitrato-\k<i>O</i>)silver(I)]-\m-1,10-phenanthroline-
5,6-dione-\k^4^<i>O</i>,<i>O</i>':<i>N</i>,<i>N</i>']
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 99.766(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   9.5058(14)
_cell_length_b                   10.4647(15)
_cell_length_c                   12.1615(17)
_cell_measurement_reflns_used    1252
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      22.59
_cell_measurement_theta_min      2.58
_cell_volume                     1192.2(3)
_computing_cell_refinement       'SAINT (Bruker, 2004)'
_computing_data_collection       'APEX2 (Bruker, 2004)'
_computing_data_reduction        'SAINT (Bruker, 2004)'
_computing_molecular_graphics    'ORTEP-3 for Windows (Farrugia, 1997)'
_computing_publication_material
'SHELXL97 (Sheldrick, 2008) and PLATON (Spek, 2009)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      296(2)
_diffrn_detector_area_resol_mean 0
_diffrn_measured_fraction_theta_full 0.983
_diffrn_measured_fraction_theta_max 0.983
_diffrn_measurement_device_type  'Bruker APEXII CCD area-detector'
_diffrn_measurement_method       '\f and \w'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0405
_diffrn_reflns_av_sigmaI/netI    0.0494
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       7
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            6626
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         26.00
_diffrn_reflns_theta_min         2.58
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    1.719
_exptl_absorpt_correction_T_max  0.84
_exptl_absorpt_correction_T_min  0.66
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Bruker 2000)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.117
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             744
_exptl_crystal_size_max          0.3
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.1
_refine_diff_density_max         0.843
_refine_diff_density_min         -1.050
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.001
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     190
_refine_ls_number_reflns         2307
_refine_ls_number_restraints     32
_refine_ls_restrained_S_all      1.104
_refine_ls_R_factor_all          0.0948
_refine_ls_R_factor_gt           0.0524
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0445P)^2^+3.5057P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1110
_refine_ls_wR_factor_ref         0.1237
_reflns_number_gt                1374
_reflns_number_total             2307
_reflns_threshold_expression     I>2\s(I)
_cod_data_source_file            im2282.cif
_cod_data_source_block           I
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2230714
_cod_database_fobs_code          2230714