Copper(ii) complexes with benzhydrazone-related ligands: synthesis, structural studies and cytotoxicity assay
Cindrić, Marina; Bjelopetrović, Alen; Pavlović, Gordana; Damjanović, Vladimir; Lovrić, Jasna; Matković-Čalogović, Dubravka; Vrdoljak, Višnja; New J. Chem. 41 (2017) 2425–; doi:10.1039/C6NJ03827A

data_7056006
_publ_section_title
;
 Copper(ii) complexes with benzhydrazone-related ligands: synthesis,
 structural studies and cytotoxicity assay
;
_journal_issue                   6
_journal_name_full               'New J. Chem.'
_journal_page_first              2425
_journal_paper_doi               10.1039/C6NJ03827A
_journal_volume                  41
_journal_year                    2017
_chemical_formula_moiety         'C26 H18 Cu N4 O2'
_chemical_formula_sum            'C26 H18 Cu N4 O2'
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2016-12-05 deposited with the CCDC.
2017-02-10 downloaded from the CCDC.
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.35 
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.35 (
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.35 
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_diffrn_source                   'Enhance (Mo) X-ray Source'
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET)
(compiled Aug 13 2014,18:06:01)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
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_exptl_crystal_colour            'dark green'
_exptl_crystal_density_diffrn    1.501
_exptl_crystal_description       prism
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_refine_ls_abs_structure_details
;
 Refined as an inversion twin.
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_refine_ls_abs_structure_Flack   0.44(4)
_refine_ls_extinction_method     none
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_refine_ls_R_factor_all          0.0894
_refine_ls_R_factor_gt           0.0633
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0465P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1051
_refine_ls_wR_factor_ref         0.1139
_reflns_Friedel_coverage         0.998
_reflns_Friedel_fraction_full    0.995
_reflns_Friedel_fraction_max     0.996
_reflns_number_gt                2296
_reflns_number_total             2969
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c6nj03827a2.cif
_cod_data_source_block           1phen
_cod_depositor_comments
'Adding full bibliography for 7056006--7056012.cif.'
_cod_database_code               7056006
_shelx_shelxl_version_number     2014/7
_shelx_res_checksum              9099