Fabrication of blue organic light-emitting diodes from novel uranium complexes: synthesis, characterization, and electroluminescence studies of uranium anthracene-9-carboxylate complexes.
Darzinezhad, Khodabakhsh; Amini, Mostafa M.; Mohajerani, Ezeddin; Armaghan, Mahsa; Knedel, Tim Oliver; Abareghi, Afshin; Janiak, Christoph; Dalton transactions (Cambridge, England : 2003) 48 (2019) 3695–3703; doi:10.1039/c8dt04981e

data_7049024
_publ_section_title
;
 Fabrication of blue organic light-emitting diodes from novel uranium
 complexes: synthesis, characterization, and electroluminescence studies
 of uranium anthracene-9-carboxylate complexes.
;
_journal_issue                   11
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              3695
_journal_page_last               3703
_journal_paper_doi               10.1039/c8dt04981e
_journal_volume                  48
_journal_year                    2019
_chemical_formula_moiety         ' C34 H30 O8 U, 2(C2 H6 O)'
_chemical_formula_sum            'C38 H42 O10 U'
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_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2017/1
_audit_update_record
;
2018-08-13 deposited with the CCDC.    2019-02-14 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_computing_structure_refinement  'SHELXL-2017/1 (Sheldrick, 2017)'
_diffrn_ambient_temperature      140(2)
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_diffrn_measurement_device_type  'CCD area detector'
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_diffrn_reflns_Laue_measured_fraction_full 1.000
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_diffrn_reflns_point_group_measured_fraction_full 1.000
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_diffrn_reflns_theta_max         26.372
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_exptl_absorpt_coefficient_mu    4.439
_exptl_absorpt_correction_type   multi-scan
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_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.609
_exptl_crystal_description       cubic
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_exptl_crystal_size_max          0.679
_exptl_crystal_size_mid          0.346
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0180P)^2^+5.2527P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.0468
_reflns_Friedel_coverage         0.000
_reflns_number_gt                7144
_reflns_number_total             7574
_reflns_threshold_expression     'I > 2\s(I)'
_publcif_datablock.id            {9ef112b7-5cdf-4471-948b-a6ef1e810108}
_cod_data_source_file            c8dt04981e2.cif
_cod_data_source_block           q
_cod_depositor_comments
'Adding full bibliography for 7049024--7049026.cif.'
_cod_original_cell_volume        3702.9(6)
_cod_original_formula_sum        '	C38 H42 O10 U'
_cod_database_code               7049024
_shelx_shelxl_version_number     2017/1
_shelx_res_checksum              42216