Selective ethylene oligomerisation using supported tungsten mono-imido catalysts
Wright, Christopher M. R.; Williams, Thomas J.; Turner, Zoë R.; Buffet, Jean-Charles; O'Hare, Dermot; Inorganic Chemistry Frontiers 4 (2017) 1048–; doi:10.1039/C7QI00128B

data_4349693
_publ_section_title
;
 Selective ethylene oligomerisation using supported tungsten mono-imido
 catalysts
;
_journal_issue                   6
_journal_name_full               'Inorganic Chemistry Frontiers'
_journal_page_first              1048
_journal_paper_doi               10.1039/C7QI00128B
_journal_volume                  4
_journal_year                    2017
_chemical_formula_moiety         'C12 H17 Cl4 N O W'
_chemical_formula_sum            'C12 H17 Cl4 N O W'
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_chemical_properties_physical    ', Air-sensitive,Moisture-sensitive'
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
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_audit_update_record
;
2016-11-23 deposited with the CCDC.
2017-05-10 downloaded from the CCDC.
;
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_computing_data_collection       'Collect (Nonius BV, 1997-2000)'
_computing_data_reduction
'HKL Denzo and Scalepack (Otwinowski & Minor 1997)'
_computing_molecular_graphics
'ORTEP, L. J. Farrugia, J. Appl. Crystallogr., 1997, 30, 565.'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution
'L. Palatinus and G. Chapuis, J. Appl. Crystallogr., 2007, 40, 786-790.'
_diffrn_ambient_temperature      150(2)
_diffrn_detector_area_resol_mean 9
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_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  KappaCCD
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_diffrn_source                   'Enraf Nonius FR590'
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'Re-crystallisation from solvent: hexane'
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0387P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_shelx_estimated_absorpt_t_min   0.306
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_exptl_absorpt_special_details
'HKL Denzo and Scalepack (Otwinowski & Minor 1997)'
_shelxl_version_number           2014-3
_shelx_res_checksum              40201