LMucko/crystallography-open-database huggingface dataset:
Crystal structure of di-[<i>S</i>-(2-aminoethyl)thiouronium] tribromocuprate dibromide, [C~3~H~11~N~3~S]~2~[CuBr~3~][Br]~2~
Blachnik, Roger; Wiest, Thomas; Eickmeier, Henning; Dülmer, Ansgar; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 245–246; doi:

data_8101236
_publ_section_title
;
Crystal structure of di-[<i>S</i>-(2-aminoethyl)thiouronium] tribromocuprate 
dibromide, [C~3~H~11~N~3~S]~2~[CuBr~3~][Br]~2~
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              245
_journal_page_last               246
_journal_volume                  215
_journal_year                    2000
_chemical_formula_structural     '[C3H11N3S]2[CuBr3][Br]2'
_chemical_formula_sum            'C6 H22 Br5 Cu N6 S2'
_chemical_formula_weight         705.51
_chemical_name_common
;
Di-[S-(2-aminoethyl)thiouronium]tribromocuprate dibromide
;
_space_group_IT_number           62
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   8.5897(17)
_cell_length_b                   20.792(4)
_cell_length_c                   11.280(2)
_cell_measurement_temperature    293(2)
_cell_volume                     2014.6(7)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    2.326
_cod_database_code               8101236
Crystal structure of bis[tetraethyl-μ-hydroxyperfluorophenylacetato μ~3~-oxoditin], [(F~5~C~6~CH~2~CO~2~)Et~2~Sn(OH)OSnEt~2~]~2~
Gielen, M.; Tiekink, E. R. T.; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 255–256; doi:

data_8101237
_publ_section_title
;
Crystal structure of bis[tetraethyl-\m-hydroxyperfluorophenylacetato 
\m~3~-oxoditin], [(F~5~C~6~CH~2~CO~2~)Et~2~Sn(OH)OSnEt~2~]~2~
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              255
_journal_page_last               256
_journal_volume                  215
_journal_year                    2000
_chemical_formula_moiety         'C32 H46 F10 O8 Sn4 '
_chemical_formula_structural     '[(F5 C6 C H2 C O2)Et2 Sn(O H)O Sn Et2]2'
_chemical_formula_sum            'C32 H46 F10 O8 Sn4'
_chemical_formula_weight         1223.45
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 98.10(3)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   10.100(10)
_cell_length_b                   12.296(4)
_cell_length_c                   18.225(2)
_cell_measurement_temperature    293
_cell_volume                     2240.9(17)
_diffrn_ambient_temperature      293
_exptl_crystal_density_diffrn    1.813
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C32 H46 F10 O8 Sn4 '
_cod_database_code               8101237
Crystal structure of (3<i>R</i>*,3a<i>R</i>*,4<i>S</i>*,7<i>S</i>*, 7a<i>R</i>*)-4-(<i>tert</i>-butyldimethyl silyloxy)-4,7-epoxy-3-methoxy- 7-methyloctahydro-1<i>H</i>-inden-1-one, C~17~H~30~O~4~Si
Tinant, Bernard; Trembleau, Laurent; Ghosez, Leon; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 261–262; doi:

data_8101238
_publ_section_title
;
Crystal structure of (3<i>R</i>*,3a<i>R</i>*,4<i>S</i>*,7<i>S</i>*,
7a<i>R</i>*)-4-(<i>tert</i>-butyldimethyl silyloxy)-4,7-epoxy-3-methoxy-
7-methyloctahydro-1<i>H</i>-inden-1-one, C~17~H~30~O~4~Si
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              261
_journal_page_last               262
_journal_volume                  215
_journal_year                    2000
_chemical_formula_sum            'C17 H30 O4 Si'
_chemical_formula_weight         326.50
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 106.37(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   13.700(4)
_cell_length_b                   7.681(2)
_cell_length_c                   18.889(6)
_cell_measurement_temperature    293(2)
_cell_volume                     1907.1(10)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.137
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               8101238
Crystal structure of the low temperature modification of tris(ethyldimethylphenylammonium) nanoiododiantimonate(III), [EtMe~2~PhN]~3~[Sb~2~I~9~]
Ahmed, Ibrahim Abdelhalim; Blachnik, Roger; Reuter, Hans; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 253–254; doi:

data_8101239
_publ_section_title
;
Crystal structure of the low temperature modification of 
tris(ethyldimethylphenylammonium) nanoiododiantimonate(III), 
[EtMe~2~PhN]~3~[Sb~2~I~9~]
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              253
_journal_page_last               254
_journal_volume                  215
_journal_year                    2000
_chemical_formula_structural     '[Et Me2 Ph N]3 [Sb2 I9]'
_chemical_formula_sum            'C30 H48 I9 N3 Sb2'
_chemical_formula_weight         1836.31
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 92.425(19)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   19.052(4)
_cell_length_b                   13.764(3)
_cell_length_c                   18.952(4)
_cell_measurement_temperature    293(2)
_cell_volume                     4965.3(17)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    2.456
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               8101239
Crystal structure of pyrene—5,10,15,20-tetraphenyl-21<i>H</i>,23 <i>H</i>-porphyrin (1/1), C~60~H~40~N~4~
Blömker, Jens; Frey, Wolfgang; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 263–264; doi:

data_8101240
_publ_section_title
;
Crystal structure of pyrene---5,10,15,20-tetraphenyl-21<i>H</i>,23
<i>H</i>-porphyrin (1/1), C~60~H~40~N~4~
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              263
_journal_page_last               264
_journal_volume                  215
_journal_year                    2000
_chemical_formula_sum            'C60 H40 N4'
_chemical_formula_weight         816.96
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                106.30(2)
_cell_angle_beta                 104.11(2)
_cell_angle_gamma                104.43(2)
_cell_formula_units_Z            1
_cell_length_a                   9.727(3)
_cell_length_b                   10.854(3)
_cell_length_c                   11.620(3)
_cell_measurement_temperature    293(2)
_cell_volume                     1073.4(5)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.264
_refine_ls_R_factor_obs          0.0608
_refine_ls_wR_factor_obs         0.1424
_cod_database_code               8101240
Crystal structure of phenanthrene—5,10,15,20-tetraphenyl-21<i>H </i>,23<i>H</i>-porphyrin (1/1), C~58~H~40~N~4~
Blömker, Jens; Frey, Wolfgang; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 265–266; doi:

data_8101241
_publ_section_title
;
Crystal structure of phenanthrene---5,10,15,20-tetraphenyl-21<i>H
</i>,23<i>H</i>-porphyrin (1/1), C~58~H~40~N~4~
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              265
_journal_page_last               266
_journal_volume                  215
_journal_year                    2000
_chemical_formula_sum            'C58 H40 N4'
_chemical_formula_weight         792.94
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                106.182(10)
_cell_angle_beta                 102.811(11)
_cell_angle_gamma                104.213(11)
_cell_formula_units_Z            1
_cell_length_a                   9.4576(14)
_cell_length_b                   10.7860(13)
_cell_length_c                   11.6798(14)
_cell_measurement_temperature    293(2)
_cell_volume                     1054.0(2)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.249
_refine_ls_R_factor_obs          0.0715
_refine_ls_wR_factor_obs         0.1365
_cod_database_code               8101241
Crystal structure of anthracene—5,10,15,20-tetraphenyl-21<i>H</i>, 23<i>H</i>-porphyrin (1/1), C~58~H~40~N~4~
Blömker, Jens; Frey, Wolfgang; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 267–268; doi:

data_8101242
_publ_section_title
;
Crystal structure of anthracene---5,10,15,20-tetraphenyl-21<i>H</i>,
23<i>H</i>-porphyrin (1/1), C~58~H~40~N~4~
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              267
_journal_page_last               268
_journal_volume                  215
_journal_year                    2000
_chemical_formula_sum            'C58 H40 N4'
_chemical_formula_weight         792.94
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                106.393(8)
_cell_angle_beta                 101.822(9)
_cell_angle_gamma                105.468(9)
_cell_formula_units_Z            1
_cell_length_a                   9.3524(11)
_cell_length_b                   10.9001(12)
_cell_length_c                   11.7806(11)
_cell_measurement_temperature    293(2)
_cell_volume                     1058.2(2)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.244
_refine_ls_R_factor_obs          0.0620
_refine_ls_wR_factor_obs         0.1259
_cod_database_code               8101242
Crystal structure of 1,2-vinylenbis(triphenylphosphonium) tetrabromoplumbate (II), [Ph~3~P‒CH=CH‒PPh~3~][PbBr~4~]
Blachnik, Roger; Reuter, Hans; Wiest, Thomas; Eickmeier, Henning; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 247–248; doi:

data_8101243
_publ_section_title
;
Crystal structure of 1,2-vinylenbis(triphenylphosphonium) tetrabromoplumbate
(II), [Ph~3~P--CH=CH--PPh~3~][PbBr~4~]
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              247
_journal_page_last               248
_journal_volume                  215
_journal_year                    2000
_chemical_formula_structural     '[Ph3 P-C H=C H-P Ph3][Pb Br4]'
_chemical_formula_sum            'C38 H32 Br4 P2 Pb'
_chemical_formula_weight         1077.41
_chemical_name_common            1,2-Vinylen-bis(triphenylphosphonium)tetrabrom
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 99.97(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.913(2)
_cell_length_b                   17.618(4)
_cell_length_c                   19.848(4)
_cell_measurement_temperature    293(2)
_cell_volume                     3758.5(13)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.904
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               8101243
Crystal structure of 1,2-vinylenbis(triphenylphosphonium) tetrabromocuprate(II), [Ph~3~P‒CH=CH‒PPh~3~][CuBr~4~]
Blachnik, Roger; Reuter, Hans; Wiest, Thomas; Eickmeier, Henning; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 249–250; doi:

data_8101244
_publ_section_title
;
Crystal structure of 1,2-vinylenbis(triphenylphosphonium) 
tetrabromocuprate(II), [Ph~3~P--CH=CH--PPh~3~][CuBr~4~]
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              249
_journal_page_last               250
_journal_volume                  215
_journal_year                    2000
_chemical_formula_structural     '[Ph3P-CH=CH-PPh3][CuBr4]'
_chemical_formula_sum            'C38 H32 Br4 Cu P2'
_chemical_formula_weight         933.76
_chemical_name_common
;
1,2-Vinylen-bis(triphenylphosphonium)tetrabromocuprate(II)
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 100.35(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.191(3)
_cell_length_b                   18.205(4)
_cell_length_c                   19.884(3)
_cell_measurement_temperature    293(2)
_cell_volume                     3629.0(15)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.709
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               8101244
Crystal structure of 1,2-vinylenbis(triphenylphosphonium) dibromide dihydrate, [Ph~3~P–CH=CH–PPh~3~][Br]~2~ · 2H~2~O
Blachnik, Roger; Reuter, Hans; Wiest, Thomas; Eickmeier, Henning; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 251–252; doi:

data_8101245
_publ_section_title
;
Crystal structure of 1,2-vinylenbis(triphenylphosphonium) dibromide 
dihydrate, [Ph~3~P--CH=CH--PPh~3~][Br]~2~ &#x00B7; 2H~2~O
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              251
_journal_page_last               252
_journal_volume                  215
_journal_year                    2000
_chemical_formula_structural     '[Ph3P-CH=CH-PPh3][Br]2*2H2O'
_chemical_formula_sum            'C19 H18 Br O P'
_chemical_formula_weight         373.21
_chemical_name_common
;
1,2-Vinylen-bis(triphenylphosphonium)dibromide-dihydrate
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 115.39(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   11.716(3)
_cell_length_b                   14.145(4)
_cell_length_c                   11.250(3)
_cell_measurement_temperature    293(2)
_cell_volume                     1684.2(8)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.472
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               8101245
Crystal structure of 5,2'-dihydroxyflavone, C~15~H~10~O~4~
Shoja, M.; Kirkava, A.; Kabbani, R.; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 269–270; doi:

data_8101246
_publ_section_title
;
Crystal structure of 5,2'-dihydroxyflavone, C~15~H~10~O~4~
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              269
_journal_page_last               270
_journal_volume                  215
_journal_year                    2000
_chemical_formula_sum            'C15 H10 O4'
_chemical_formula_weight         254.24
_chemical_melting_point          541.5(5)
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00000
_cell_angle_beta                 95.62(3)
_cell_angle_gamma                90.00000
_cell_formula_units_Z            4
_cell_length_a                   5.331(4)
_cell_length_b                   9.179(2)
_cell_length_c                   23.057(4)
_cell_measurement_temperature    293
_cell_volume                     1122.8(9)
_diffrn_ambient_temperature      293
_exptl_crystal_density_diffrn    1.504
_refine_ls_R_factor_obs          .044
_refine_ls_wR_factor_obs         .045
_cod_depositor_comments
;
The following automatic conversions were performed:

'_chemical_melting_point' value '541-542' was changed to '541.5(5)' -
the average value was taken and precision was estimated.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_sg_symbol_Hall     -p_2ybc
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               8101246
Crystal structure of 8-hydroxy-7-methoxyflavone, C~16~H~12~O~4~
Shoja, M.; Krikava, A; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 271–272; doi:

data_8101247
_publ_section_title
;
Crystal structure of 8-hydroxy-7-methoxyflavone, C~16~H~12~O~4~
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              271
_journal_page_last               272
_journal_volume                  215
_journal_year                    2000
_chemical_formula_sum            'C16 H12 O4'
_chemical_formula_weight         268.27
_space_group_crystal_system      orthorhombic
_space_group_IT_number           61
_space_group_name_Hall           '-P 2ac 2ab'
_space_group_name_H-M_alt        'P b c a'
_cell_angle_alpha                90.00000
_cell_angle_beta                 90.00000
_cell_angle_gamma                90.00000
_cell_formula_units_Z            8
_cell_length_a                   10.615(5)
_cell_length_b                   14.257(2)
_cell_length_c                   16.509(2)
_cell_measurement_temperature    293
_cell_volume                     2498.4(13)
_diffrn_ambient_temperature      293
_exptl_crystal_density_diffrn    1.426
_refine_ls_R_factor_obs          .091
_refine_ls_wR_factor_obs         .097
_cod_database_code               8101247
Crystal structure of bis(7-nitro-8-quinolinolato)copper(II), CuC~18~H~10~O~6~N~4~
Shoja, M.; Gershon, H.; Clarke, D. D.; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 273–274; doi:

data_8101248
_publ_section_title
;
Crystal structure of bis(7-nitro-8-quinolinolato)copper(II), 
CuC~18~H~10~O~6~N~4~
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              273
_journal_page_last               274
_journal_volume                  215
_journal_year                    2000
_chemical_formula_sum            'C18 H10 Cu N4 O6'
_chemical_melting_point          623
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00000
_cell_angle_beta                 100.00(10)
_cell_angle_gamma                90.00000
_cell_formula_units_Z            2
_cell_length_a                   4.567(9)
_cell_length_b                   10.723(8)
_cell_length_c                   17.095(6)
_cell_measurement_temperature    293
_cell_volume                     824.5(18)
_diffrn_ambient_temperature      293
_exptl_crystal_density_diffrn    1.474
_refine_ls_R_factor_obs          .043
_refine_ls_wR_factor_obs         .067
_cod_original_sg_symbol_Hall     -p_2ybc
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'Cu C18 H10 O6 N4'
_cod_database_code               8101248
Crystal structure of bis(diethyloxy-<i>O</i>-dilithium) hexakis(μ~2~- dimethylamido)zirconate, C~20~H~56~Li~2~N~6~O~2~Zr
Kempe, Rhett; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 275–276; doi:

data_8101249
_publ_section_title
;
Crystal structure of bis(diethyloxy-<i>O</i>-dilithium) hexakis(\m~2~-
dimethylamido)zirconate, C~20~H~56~Li~2~N~6~O~2~Zr
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              275
_journal_page_last               276
_journal_volume                  215
_journal_year                    2000
_chemical_formula_sum            'C20 H56 Li2 N6 O2 Zr'
_chemical_formula_weight         517.81
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                94.42(2)
_cell_angle_beta                 111.02(2)
_cell_angle_gamma                93.12(2)
_cell_formula_units_Z            2
_cell_length_a                   10.051(2)
_cell_length_b                   12.187(2)
_cell_length_c                   13.152(2)
_cell_measurement_temperature    200(2)
_cell_volume                     1493.5(4)
_diffrn_ambient_temperature      200(2)
_exptl_crystal_density_diffrn    1.151
_refine_ls_R_factor_obs          0.0335
_refine_ls_wR_factor_obs         0.0492
_cod_database_code               8101249
Crystal structure of 1,1,5,5-tetrakis[bis(trimethylsilyl)amido]-4, 8-diphenyl-2,6-dioxa-1,5-distannacyclooctane—cyclohexane (1/0.75), C~49~H~108~N~4~O~2~Si~8~Sn~2~
Kempe, Rhett; Zeitschrift für Kristallographie - New Crystal Structures 215 (2000) 277–278; doi:

data_8101250
_publ_section_title
;
Crystal structure of 1,1,5,5-tetrakis[bis(trimethylsilyl)amido]-4,
8-diphenyl-2,6-dioxa-1,5-distannacyclooctane---cyclohexane (1/0.75), 
C~49~H~108~N~4~O~2~Si~8~Sn~2~
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              277
_journal_page_last               278
_journal_volume                  215
_journal_year                    2000
_chemical_formula_sum            'C49 H108 N4 O2 Si8 Sn2'
_chemical_formula_weight         1247.49
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                110.570(14)
_cell_angle_beta                 97.570(14)
_cell_angle_gamma                91.280(14)
_cell_formula_units_Z            1
_cell_length_a                   10.5940(13)
_cell_length_b                   12.548(2)
_cell_length_c                   12.948(2)
_cell_measurement_temperature    473(2)
_cell_volume                     1593.1(4)
_diffrn_ambient_temperature      473(2)
_exptl_crystal_density_diffrn    1.300
_refine_ls_R_factor_obs          0.0407
_refine_ls_wR_factor_obs         0.1174
_cod_database_code               8101250