Trimethylammonium Trichlorostannate(II)
Halfpenny, J.; Acta Crystallographica Section C 52 (1996) 340–342; doi:10.1107/S0108270195009668

data_2004475
_publ_section_title
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 Trimethylammonium Trichlorostannate(II)
;
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              340
_journal_page_last               342
_journal_paper_doi               10.1107/S0108270195009668
_journal_volume                  52
_journal_year                    1996
_chemical_formula_moiety         '[N H (C H3)3]+, (Cl3 Sn)-'
_chemical_formula_sum            'C3 H10 Cl3 N Sn'
_chemical_formula_weight         285.17
_chemical_name_systematic
;
trimethylammonium trichlorostannate(IV)
;
_space_group_crystal_system      orthorhombic
_space_group_IT_number           36
_space_group_name_Hall           'C 2c -2'
_space_group_name_H-M_alt        'C m c 21'
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   9.53(1)
_cell_length_b                   8.31(1)
_cell_length_c                   12.39(1)
_cell_measurement_reflns_used    15
_cell_measurement_temperature    286
_cell_measurement_theta_max      25
_cell_measurement_theta_min      5
_cell_volume                     981.2(18)
_computing_data_collection       'Stoe  STADI-2'
_computing_data_reduction        'DATR (Small, 1977)'
_computing_molecular_graphics    'SNOOPI (Davies, 1983)'
_computing_structure_refinement  SHELX76
_computing_structure_solution    'SHELX76 (Sheldrick, 1976), Patterson'
_diffrn_ambient_temperature      288
_diffrn_measurement_device       'Stoe STADI-2 two-circle diffractometer'
_diffrn_measurement_method       'variable \w scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine focus X-ray tube'
_diffrn_radiation_type           'Mo  K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.017
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            583
_diffrn_reflns_reduction_process SHELX76
_diffrn_reflns_theta_max         30.0
_diffrn_reflns_theta_min         3.0
_diffrn_standards_decay_%        '<=5, corrected by interpolation'
_diffrn_standards_interval_count 20
_diffrn_standards_number         'one per layer'
_exptl_absorpt_coefficient_mu    3.11
_exptl_absorpt_correction_T_max  .886
_exptl_absorpt_correction_T_min  .330
_exptl_absorpt_correction_type   'integration (SHELX76)'
_exptl_crystal_colour            'pale yellow'
_exptl_crystal_density_diffrn    1.930
_exptl_crystal_density_meas      1.921
_exptl_crystal_density_method    flotation
_exptl_crystal_description       'thin plates, tabular on (010)'
_exptl_crystal_F_000             544
_exptl_crystal_size_max          0.56
_exptl_crystal_size_mid          0.44
_exptl_crystal_size_min          0.039
_refine_diff_density_max         0.65
_refine_diff_density_min         -0.45
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   0.906
_refine_ls_hydrogen_treatment    'H-atom treatment: see text'
_refine_ls_matrix_type           full
_refine_ls_number_constraints    3
_refine_ls_number_parameters     50
_refine_ls_number_reflns         552
_refine_ls_R_factor_obs          0.031
_refine_ls_shift/esd_max         <0.001
_refine_ls_shift/esd_mean        0.0
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      unit
_refine_ls_wR_factor_obs         0.031
_reflns_number_observed          552
_reflns_number_total             580
_reflns_observed_criterion       >3\s(I)
_cod_data_source_file            bm1018.cif
_cod_data_source_block           sna
_cod_depositor_comments
;
 Changing the space group from 'P 2c -2' to 'C 2c -2' after consulting
 the original publication. All related space group information was changed
 accordingly.

 Antanas Vaitkus,
 2017-07-06
;
_cod_original_cell_volume        981(3)
_cod_original_formula_sum        'C3 H10 Cl3 N1 Sn1'
_cod_database_code               2004475