Silver(I) <i>N</i>-Phthaloylglycinate
Jaber, F.; Charbonnier, F.; Faure, R.; Acta Crystallographica Section C 51 (1995) 1765–1767; doi:10.1107/S0108270195002447

data_2003939
_publ_section_title
;
 Silver(I) <i>N</i>-Phthaloylglycinate
;
_journal_issue                   9
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1765
_journal_page_last               1767
_journal_paper_doi               10.1107/S0108270195002447
_journal_volume                  51
_journal_year                    1995
_chemical_compound_source        'aqueous solution'
_chemical_formula_moiety         'C10 H6 Ag1 N1 O4'
_chemical_formula_sum            'C10 H6 Ag N O4'
_chemical_formula_weight         312.0
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_type_scat_source
'International Tables for X-ray Crystallography (1974)'
_cell_angle_alpha                90
_cell_angle_beta                 127.630(10)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   27.571(4)
_cell_length_b                   5.0620(10)
_cell_length_c                   17.284(3)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    291
_cell_measurement_theta_max      23.1
_cell_measurement_theta_min      11.6
_cell_volume                     1910.4(6)
_diffrn_measurement_device       'Enraf-Nonius CAD4'
_diffrn_measurement_method       \w--4/3\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     .7107
_diffrn_reflns_av_R_equivalents  .028
_diffrn_reflns_limit_h_max       38
_diffrn_reflns_limit_h_min       -038
_diffrn_reflns_limit_k_max       7
_diffrn_reflns_limit_k_min       -07
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            4721
_diffrn_reflns_theta_max         30
_diffrn_standards_decay_%        .5
_diffrn_standards_interval_time  60
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    2.08
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  .852
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    2.17
_exptl_crystal_description       needle
_exptl_crystal_size_max          .5
_exptl_crystal_size_mid          .1
_exptl_crystal_size_min          .05
_refine_diff_density_max         .42
_refine_diff_density_min         -0.52
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   1.48
_refine_ls_hydrogen_treatment    refxyz
_refine_ls_number_parameters     164
_refine_ls_number_reflns         1839
_refine_ls_R_factor_obs          .017
_refine_ls_shift/esd_max         .01
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/\s^2^(F~o~)'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         .019
_reflns_number_observed          1839
_reflns_number_total             2401
_reflns_observed_criterion       >3\s(I)
_cod_data_source_file            pa1128.cif
_cod_data_source_block           pa1128a
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value '1/\s^2^(F~o~)' was changed to
'calc'. New tag '_refine_ls_weighting_details' was created. The value
of the new tag was set to 'w = 1/\s^2^(F~o~)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        1910.0(10)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_original_formula_sum        'C10 H6 Ag1 N1 O4'
_cod_database_code               2003939