Sn~8.7~(Ni~0.5~,Zn~0.4~,Cu~0.1~)~10.4~, a new tin-based alloy from a complex metallic mixture
Larsson, A-K.; Lidin, S.; Jacob, M.; Acta Crystallographica Section C 50 (1994) 9–12; doi:10.1107/S0108270193006481

data_2009419
_publ_section_title
;
 Sn~8.7~(Ni~0.5~,Zn~0.4~,Cu~0.1~)~10.4~, a new tin-based alloy from a
 complex metallic mixture
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              9
_journal_page_last               12
_journal_paper_doi               10.1107/S0108270193006481
_journal_volume                  50
_journal_year                    1994
_chemical_formula_moiety         Sn8.7(Ni0.5Zn0.4Cu0.1)10.4
_chemical_formula_sum            'Cu Ni5 Sn9 Zn5'
_chemical_formula_weight         1676.0(10)
_symmetry_cell_setting           cubic
_symmetry_space_group_name_Hall  'P -4 2 3'
_symmetry_space_group_name_H-M   'P -4 3 m'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.
_cell_angle_beta                 90.
_cell_angle_gamma                90.
_cell_formula_units_Z            2
_cell_length_a                   8.854(7)
_cell_length_b                   8.854(7)
_cell_length_c                   8.854(7)
_cell_measurement_reflns_used    17
_cell_measurement_temperature    293
_cell_measurement_theta_max      23.3
_cell_measurement_theta_min      6.9
_cell_volume                     694.1(10)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.05142
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            2591
_diffrn_reflns_theta_max         40
_diffrn_standards_decay_%        3
_diffrn_standards_interval_time  120
_diffrn_standards_number         2
_exptl_absorpt_coefficient_mu    31.0
_exptl_absorpt_correction_T_max  0.2245
_exptl_absorpt_correction_T_min  0.0184
_exptl_absorpt_correction_type   integration
_exptl_crystal_colour            'Grey metallic'
_exptl_crystal_density_diffrn    8.02
_exptl_crystal_description       Rod
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.06
_refine_diff_density_max         4.7
_refine_diff_density_min         -3.9
_refine_ls_goodness_of_fit_obs   1.01
_refine_ls_number_parameters     35
_refine_ls_number_reflns         355
_refine_ls_R_factor_obs          0.0535
_refine_ls_shift/esd_max         0.002
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w=1/(\s^2^ + 0.07F~o~)^2^'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.0752
_reflns_number_observed          355
_reflns_number_total             487
_reflns_observed_criterion       F~o~^2^<3\s(F~o~^2^)
_cod_data_source_file            sh1035.cif
_cod_data_source_block           sh1035_structure_1_of_1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'w=1/(\s^2^ + 0.07F~o~)^2^' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to 'w=1/(\s^2^ +
0.07F~o~)^2^'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        694(2)
_cod_original_formula_sum        'Cu1 Ni5 Sn9 Zn5'
_cod_database_code               2009419