Tautomerization of 2,6-lutidines in the presence of B(C6F5)3 using catecholborane as a precatalyst.
Zheng, Junhao; Fan, Xiaoting; Zhou, Benyu; Li, Zhen Hua; Wang, Huadong; Chemical communications (Cambridge, England) 52 (2016) 4655–4658; doi:10.1039/c6cc00347h

data_7118849
_publ_section_title
;
 Tautomerization of 2,6-lutidines in the presence of B(C6F5)3 using
 catecholborane as a precatalyst.
;
_journal_issue                   25
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              4655
_journal_page_last               4658
_journal_paper_doi               10.1039/c6cc00347h
_journal_volume                  52
_journal_year                    2016
_chemical_formula_sum            'C32 H14 B2 Cl2 F15 N O2'
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_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2016-01-05 deposited with the CCDC.
2016-03-07 downloaded from the CCDC.
;
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_refine_ls_structure_factor_coef Fsqd
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; 
 w=1/[\s^2^(Fo^2^)+(0.2000P)^2^] 
 where P=(Fo^2^+2Fc^2^)/3 
;
_refine_ls_weighting_scheme      calc
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'Adding full bibliography for 7118849--7118850.cif.'
_cod_original_cell_volume        1635.8(6)
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