(Dimethyl sulfoxide-κ<i>O</i>)[3-hydroxy-2-hydroxymethyl-2-(3-methoxy-2-oxidobenzylideneamino-κ^2^<i>O</i>^2^,<i>N</i>)propanolato-κ<i>O</i>]dioxomolybdenum(VI). Corrigendum
Sui, Yan; Fang, Xiao-Niu; Luo, Qiu-Yan; Chen, Hong-Mei; Zhou, Meng-Qiang; Acta Crystallographica Section E 66 (2010) e23–; doi:10.1107/S1600536810007476

data_2225941
_publ_section_title
;
 (Dimethyl
 sulfoxide-\k<i>O</i>)[3-hydroxy-2-hydroxymethyl-2-(3-methoxy-2-oxidobenzylideneamino-\k^2^<i>O</i>^2^,<i>N</i>)propanolato-\k<i>O</i>]dioxomolybdenum(VI).
 Corrigendum
;
_journal_coeditor_code           NG9064
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              e23
_journal_paper_doi               10.1107/S1600536810007476
_journal_volume                  66
_journal_year                    2010
_chemical_formula_iupac          '[Mo (C12 H15 N O5) O2 (C2 H6 O S)]'
_chemical_formula_moiety         'C14 H21 Mo N O8 S'
_chemical_formula_sum            'C14 H21 Mo N O8 S'
_chemical_formula_weight         459.32
_chemical_melting_point_gt       454
_chemical_melting_point_lt       456
_chemical_name_systematic
;
(Dimethyl sulfoxide-\kO)[3-hydroxy-2-hydroxymethyl-2-(3-methoxy-2-
oxidobenzylideneamino-\k^2^O^2^,N)propanolato-\kO]dioxomolybdenum(VI)
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 115.3240(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.3130(7)
_cell_length_b                   9.2596(5)
_cell_length_c                   14.8563(7)
_cell_measurement_reflns_used    11097
_cell_measurement_temperature    295(2)
_cell_measurement_theta_max      26.00
_cell_measurement_theta_min      2.61
_cell_volume                     1779.74(16)
_computing_cell_refinement       'APEX2 (Bruker, 2004)'
_computing_data_collection       'APEX2 (Bruker, 2004)'
_computing_data_reduction        'APEX2 (Bruker, 2004)'
_computing_molecular_graphics    'SHELXL97 (Sheldrick, 2008)'
_computing_publication_material  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      295(2)
_diffrn_measured_fraction_theta_full 0.989
_diffrn_measured_fraction_theta_max 0.989
_diffrn_measurement_device_type  'Bruker APEXII area-detector'
_diffrn_measurement_method       '\f and \w scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0241
_diffrn_reflns_av_sigmaI/netI    0.0176
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            10668
_diffrn_reflns_theta_full        25.49
_diffrn_reflns_theta_max         25.49
_diffrn_reflns_theta_min         2.61
_exptl_absorpt_coefficient_mu    0.896
_exptl_absorpt_correction_T_max  0.7457
_exptl_absorpt_correction_T_min  0.6315
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Bruker, 2004)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.714
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             936
_exptl_crystal_size_max          0.56
_exptl_crystal_size_mid          0.39
_exptl_crystal_size_min          0.35
_refine_diff_density_max         0.356
_refine_diff_density_min         -0.442
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.069
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     259
_refine_ls_number_reflns         3278
_refine_ls_number_restraints     40
_refine_ls_restrained_S_all      1.096
_refine_ls_R_factor_all          0.0238
_refine_ls_R_factor_gt           0.0222
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0347P)^2^+0.9103P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0630
_refine_ls_wR_factor_ref         0.0636
_reflns_number_gt                3056
_reflns_number_total             3278
_reflns_threshold_expression     I>2\s(I)
_cod_data_source_file            ng9064.cif
_cod_data_source_block           I
_cod_original_cell_volume        1779.74(15)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2225941
_cod_database_fobs_code          2225941