Copper-catalyzed synthesis of enantioenriched tetraarylethanes.
Jen, Wendy S.; Truppo, Matthew D.; Amos, Deborah; Devine, Paul; McNevin, Michael; Biba, Mirlinda; Campos, Kevin R.; Organic letters 10 (2008) 741–744; doi:10.1021/ol7027543

data_1504504
_publ_section_title
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 Copper-catalyzed synthesis of enantioenriched tetraarylethanes.
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_journal_issue                   5
_journal_name_full               'Organic letters'
_journal_page_first              741
_journal_page_last               744
_journal_paper_doi               10.1021/ol7027543
_journal_volume                  10
_journal_year                    2008
_chemical_absolute_configuration ad
_chemical_formula_moiety         'C12 H10 Br N O'
_chemical_formula_sum            'C12 H10 Br N O'
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_chemical_name_common            compound_12
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_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
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_cell_length_a                   8.7335(6)
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_cell_volume                     1076.99(13)
_diffrn_ambient_temperature      100
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device       '\k-geometry diffractometer'
_diffrn_radiation_type           'Mo K\a'
_diffrn_reflns_av_R_equivalents  0.0231
_diffrn_reflns_av_sigmaI/netI    0.0276
_diffrn_reflns_limit_h_max       11
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_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            11423
_diffrn_reflns_theta_full        26.73
_diffrn_reflns_theta_max         26.73
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_exptl_absorpt_correction_T_min  0.280
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            clear
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_exptl_crystal_F_000             528
_exptl_crystal_size_max          0.455
_exptl_crystal_size_mid          0.431
_exptl_crystal_size_min          0.356
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   -0.001(8)
_refine_ls_goodness_of_fit_ref   1.072
_refine_ls_number_parameters     138
_refine_ls_number_reflns         2235
_refine_ls_R_factor_gt           0.0235
_refine_ls_wR_factor_ref         0.0552
_reflns_number_gt                2208
_reflns_number_total             2235
_cod_data_source_file            ol7027543-file003.cif
_cod_data_source_block           MDC098
_cod_depositor_comments
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The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Orthorhombic' changed to
'orthorhombic' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
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_cod_original_cell_volume        1076.98(13)
_cod_database_code               1504504