Regioselective electrosynthesis of tetra- and hexa-functionalized [60]fullerene derivatives with unprecedented addition patterns.
Liu, Kai-Qing; Wang, Jun-Jie; Yan, Xing-Xing; Niu, Chuang; Wang, Guan-Wu; Chemical science 11 (2020) 384–388; doi:10.1039/c9sc02131k

data_1552951
_publ_section_title
;
 Regioselective electrosynthesis of tetra- and hexa-functionalized
 [60]fullerene derivatives with unprecedented addition patterns.
;
_journal_issue                   2
_journal_name_full               'Chemical science'
_journal_page_first              384
_journal_page_last               388
_journal_paper_doi               10.1039/c9sc02131k
_journal_volume                  11
_journal_year                    2020
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_audit_update_record
;
2019-04-24 deposited with the CCDC.	2019-11-11 downloaded from the CCDC.
;
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;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.21 (release 14-08-2012 CrysAlis171 .NET)
(compiled Sep 14 2012,17:21:16)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            black
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_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0929P)^2^+4.3224P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_Friedel_coverage         0.000
_reflns_number_gt                4941
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_cod_depositor_comments
;Adding full bibliography for 1552951.cif.

 Adding full bibliography for 1552951.cif.
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               1552951
_shelx_estimated_absorpt_t_min   0.634
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_shelx_res_checksum              34099
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