2-Oxo Driven Unconventional reactions: Microwave Assisted Approaches to Tetrahydrofuro[3,2-d]oxazoles and Furanones.
Battini, Narsaiah; Battula, Satyanarayana; Kumar, Raju Ranjith; Ahmed, Qazi Naveed; Organic letters 17 (2015) 2992–2995; doi:10.1021/acs.orglett.5b01271

data_1520388
_publ_section_title
;
 2-Oxo Driven Unconventional reactions: Microwave Assisted Approaches to
 Tetrahydrofuro[3,2-d]oxazoles and Furanones.
;
_journal_issue                   12
_journal_name_full               'Organic letters'
_journal_page_first              2992
_journal_page_last               2995
_journal_paper_doi               10.1021/acs.orglett.5b01271
_journal_volume                  17
_journal_year                    2015
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_computing_cell_refinement       'SAINT (Bruker, 2004)'
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;
 Flack x determined using 498 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack   -0.4(10)
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_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     SHELXL
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0528P)^2^+0.0363P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                1956
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments          'Adding full bibliography for 1520388.cif.'
_cod_database_code               1520388
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