<i>N</i>-Hydroxyphthalimide
Miao, F.-M.; Wang, J.-L.; Miao, X.-S.; Acta Crystallographica Section C 51 (1995) 712–713; doi:10.1107/S0108270194007638

data_2003306
_publ_section_title
;
 <i>N</i>-Hydroxyphthalimide
;
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              712
_journal_page_last               713
_journal_paper_doi               10.1107/S0108270194007638
_journal_volume                  51
_journal_year                    1995
_chemical_compound_source        'from water solution'
_chemical_formula_moiety         'C8 H5 N1 O3'
_chemical_formula_sum            'C8 H5 N O3'
_chemical_formula_weight         163.13
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.00(3)
_cell_angle_beta                 104.94(3)
_cell_angle_gamma                90.00(2)
_cell_formula_units_Z            4
_cell_length_a                   11.549(3)
_cell_length_b                   3.756(1)
_cell_length_c                   16.442(8)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    298
_cell_measurement_theta_max      9.50
_cell_measurement_theta_min      5.42
_cell_volume                     689.1(4)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.032
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       4
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            1309
_diffrn_reflns_theta_max         24
_diffrn_standards_decay_%        -0.5
_diffrn_standards_interval_time  150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.1151
_exptl_absorpt_correction_T_max  0.9992
_exptl_absorpt_correction_T_min  0.8358
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.572
_exptl_crystal_density_meas      1.58
_exptl_crystal_description       prism
_exptl_crystal_size_max          0.5
_exptl_crystal_size_mid          0.4
_exptl_crystal_size_min          0.25
_refine_diff_density_max         0.169
_refine_diff_density_min         -0.189
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   0.685
_refine_ls_hydrogen_treatment    refxyz
_refine_ls_number_parameters     125
_refine_ls_number_reflns         535
_refine_ls_R_factor_obs          0.041
_refine_ls_shift/esd_max         0.01
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme
; If F < 61 then w = 1, if F >= 61 then w = (61/F)^2^, if F^2^ < 3\sF^2^
then w = 0
;
_refine_ls_wR_factor_obs         0.045
_reflns_number_observed          536
_reflns_number_total             1262
_reflns_observed_criterion       F~o~>3\sF~o~
_cod_data_source_file            as1104.cif
_cod_data_source_block           as1104a
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C8 H5 N1 O3'
_cod_database_code               2003306