Crystal structures of three <i>ortho</i>-substituted <i>N</i>-acyl-hydrazone derivatives.
Purandara, H.; Foro, Sabine; Thimme Gowda, B.; Acta crystallographica. Section E, Crystallographic communications 73 (2017) 1946–1951; doi:10.1107/S2056989017016814

data_2311551
_publ_section_title
;
 Crystal structures of three <i>ortho</i>-substituted
 <i>N</i>-acyl-hydrazone derivatives.
;
_journal_coeditor_code           RZ5225
_journal_issue                   'Pt 12'
_journal_name_full
'Acta crystallographica. Section E, Crystallographic communications'
_journal_page_first              1946
_journal_page_last               1951
_journal_paper_doi               10.1107/S2056989017016814
_journal_volume                  73
_journal_year                    2017
_chemical_formula_iupac          'C16 H16 N4 O5 S'
_chemical_formula_moiety         'C16 H16 N4 O5 S'
_chemical_formula_sum            'C16 H16 N4 O5 S'
_chemical_formula_weight         376.39
_chemical_name_systematic
(<i>E</i>)-<i>N</i>-{2-[2-(2-Nitrobenzylidene)hydrazinyl]-2-oxoethyl}-4-methylbenzenesulfonamide
_space_group_crystal_system      triclinic
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_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   mixed
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_cell_length_c                   11.181(2)
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_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.86
_cell_measurement_theta_min      2.67
_cell_volume                     864.5(2)
_computing_cell_refinement
;
CrysAlis RED (Oxford Diffraction, 2009)
;
_computing_data_collection
;
CrysAlis CCD (Oxford Diffraction, 2009)
;
_computing_data_reduction
;
CrysAlis RED (Oxford Diffraction, 2009)
;
_computing_molecular_graphics
;
PLATON (Spek, 2009)
;
_computing_publication_material
;
SHELXL2014 (Sheldrick, 2015)
;
_computing_structure_refinement
;
SHELXL2014 (Sheldrick, 2015)
;
_computing_structure_solution
;
SHELXS2013 (Sheldrick, 2008)
;
_diffrn_ambient_temperature      293(2)
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_diffrn_measured_fraction_theta_max 0.998
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;
Oxford Diffraction Xcalibur diffractometer
with Sapphire CCD detector
;
_diffrn_measurement_method
;
Rotation method data acquisition using omega scans
;
_diffrn_radiation_type           MoK\a
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_exptl_absorpt_coefficient_mu    0.224
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_exptl_absorpt_process_details
;
CrysAlis RED (Oxford Diffraction, 2009)
;
_exptl_crystal_colour            'light yellow'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0346P)^2^+0.6348P] where P=(Fo^2^+2Fc^2^)/3'
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