Heterobimetallic Complexes with Phenylcyclopentadienyl Ligand: Syntheses and Structures of Tricarbonylchromium-η6,η5-Phenylcyclopentadienyl-Transition Metal Complexes1
Changtao Qian; Jianhua Guo; Jie Sun; Jian Chen; Peiju Zheng; Inorganic Chemistry 36 (1997) 1286–1295; doi:10.1021/ic951630i

data_4323356
_publ_contact_author
;
    Changtao Qian
 354 Fenglin Ru, Sahnghai, China; zip code  200032
;
_publ_contact_author_email       ' sunjie@pub.sioc.ac.cn '
_publ_contact_author_fax         ' 64166128'
_publ_contact_author_phone       ' 86 - 21 - 64163300 - 3301 '
_publ_section_title
;
 Heterobimetallic Complexes with Phenylcyclopentadienyl Ligand: Syntheses
 and Structures of
 Tricarbonylchromium-\h6,\h5-Phenylcyclopentadienyl-Transition Metal
 Complexes1
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1286
_journal_page_last               1295
_journal_paper_doi               10.1021/ic951630i
_journal_volume                  36
_journal_year                    1997
_chemical_formula_sum            'C28 H20 Cr2 O6'
_space_group_IT_number           61
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      61
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
_audit_creation_date             'Tue May 14 13:06:32 1996'
_audit_creation_method           'from TEXRAY.INF file'
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_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8.00
_cell_length_a                   29.616(8)
_cell_length_b                   12.861(5)
_cell_length_c                   12.397(7)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    20.0
_cell_measurement_theta_max      17.20
_cell_measurement_theta_min      9.01
_cell_volume                     4722(3)
_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
_computing_data_reduction        'teXsan: PROCESS (MSC)'
_computing_publication_material  'teXsan: FINISH (MSC)'
_computing_structure_refinement  'teXsan: LS (MSC)'
_diffrn_ambient_temperature      20.0
_diffrn_measurement_device       AFC7R
_diffrn_measurement_method       'omega/2-theta scans'
_diffrn_orient_matrix_UB_11      -0.00229
_diffrn_orient_matrix_UB_12      -0.07717
_diffrn_orient_matrix_UB_13      -0.00820
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_diffrn_orient_matrix_UB_33      0.07975
_diffrn_radiation_monochromator  graphite
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_exptl_absorpt_correction_type   psi-scan
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      sigma
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_cod_data_source_file            ic951630i_5.cif
_cod_data_source_block           master_file_afc7*.xtl
_cod_original_cell_volume        4721(6)
_cod_original_sg_symbol_H-M      'P b c a '
_cod_original_formula_sum        'C28 H20 O6 Cr2'
_cod_database_code               4323356