Iodine(III)-promoted oxidative carbotrifluoromethylation of maleimides with imidazopyridines and Langlois' reagent.
Lai, Dipti; Bhattacharjee, Suvam; Mandal, Saurodeep; Ghosh, Sumit; Sahoo, Prithidipa; Sinha, Subrata; Hajra, Alakananda; Chemical communications (Cambridge, England) 60 (2024) 2232–2235; doi:10.1039/d3cc05889a

data_7132663
_publ_section_title
;
 Iodine(III)-promoted oxidative carbotrifluoromethylation of maleimides
 with imidazopyridines and Langlois' reagent.
;
_journal_issue                   16
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              2232
_journal_page_last               2235
_journal_paper_doi               10.1039/d3cc05889a
_journal_volume                  60
_journal_year                    2024
_chemical_formula_sum            'C25 H16 F3 N3 O2'
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_audit_update_record
;
2022-12-22 deposited with the CCDC.	2024-01-30 downloaded from the CCDC.
;
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_cell_angle_gamma                90
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
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_diffrn_radiation_type           MoK\a
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0548P)^2^+0.5980P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1038
_refine_ls_wR_factor_ref         0.1205
_reflns_Friedel_coverage         0.000
_reflns_number_gt                3100
_reflns_number_total             3681
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d3cc05889a2.cif
_cod_data_source_block           BM2_0ma_a
_cod_depositor_comments          'Adding full bibliography for 7132663.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7132663
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