Synthesis and characterisation of boranediyl- and diboranediyl-bridged diplatinum A-frame complexes.
Brunecker, Carina; Arrowsmith, Merle; Müssig, Jonas H; Böhnke, Julian; Stoy, Andreas; Heß, Merlin; Hofmann, Alexander; Lenczyk, Carsten; Lichtenberg, Crispin; Ramler, Jacqueline; Rempel, Anna; Braunschweig, Holger; Dalton transactions (Cambridge, England : 2003) 50 (2021) 3506–3515; doi:10.1039/d0dt03855e

data_7706360
_publ_section_title
;
 Synthesis and characterisation of boranediyl- and diboranediyl-bridged
 diplatinum A-frame complexes.
;
_journal_issue                   10
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              3506
_journal_page_last               3515
_journal_paper_doi               10.1039/d0dt03855e
_journal_volume                  50
_journal_year                    2021
_chemical_formula_moiety         'C14 H40 B2 Cl2 N2 P4 Pt2'
_chemical_formula_sum            'C14 H40 B2 Cl2 N2 P4 Pt2'
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'Air-sensitive,Moisture-sensitive,Heat-sensitive,rapidly decomposes in solution'
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_audit_update_record
;
2020-11-06 deposited with the CCDC.	2021-01-08 downloaded from the CCDC.
;
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'Re-crystallisation from solvent: CH2Cl2/pentane'
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0206P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_gt                4321
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d0dt03855e2.cif
_cod_data_source_block           JoMu222_CaBr_a
_cod_depositor_comments
'Adding full bibliography for 7706356--7706368.cif.'
_cod_original_cell_volume        10885(5)
_cod_original_sg_symbol_H-M      'I 41/a'
_cod_database_code               7706360
_shelx_shelxl_version_number     2014/7
_shelx_estimated_absorpt_t_min   0.481
_shelx_estimated_absorpt_t_max   0.674
_shelx_res_checksum              76176