Configurational Stability and Stereochemistry of P-Stereogenic Nickel POCOP-Pincer Complexes
Adhikary, Anubendu; Krause, Jeanette A.; Guan, Hairong; Organometallics 34 (2015) 3603–; doi:10.1021/acs.organomet.5b00402

data_4086061
_publ_section_title
;
 Configurational Stability and Stereochemistry of P-Stereogenic Nickel
 POCOP-Pincer Complexes
;
_journal_issue                   14
_journal_name_full               Organometallics
_journal_page_first              3603
_journal_paper_doi               10.1021/acs.organomet.5b00402
_journal_volume                  34
_journal_year                    2015
_chemical_formula_moiety         'C26 H31 Cl Ni O2 P2'
_chemical_formula_sum            'C26 H31 Cl Ni O2 P2'
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_space_group_IT_number           61
_space_group_name_Hall           '-P 2ac 2ab'
_space_group_name_H-M_alt        'P b c a'
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
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_cell_measurement_theta_max      67/71
_cell_measurement_theta_min      4.59
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_diffrn_measured_fraction_theta_max 0.995
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_diffrn_radiation_monochromator  graphite
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_diffrn_radiation_type           CuK\a
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_diffrn_reflns_point_group_measured_fraction_full 0.999
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_exptl_crystal_description       'rectangular plate'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0499P)^2^+2.6318P] where P=(Fo^2^+2Fc^2^)/3'
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