Dichloro(propane-1,3-diamine-κ^2^<i>N</i>,<i>N</i>')platinum(II), dichloro(propane-1,3-diamine-κ^2^<i>N</i>,<i>N</i>')palladium(II) and μ-4,9-diazadodecane-1,12-diamine-κ^2^<i>N</i>^1^,<i>N</i>^4^:κ^2^<i>N</i>^9^,<i>N</i>^12^-bis[dichloroplatinum(II)]
Odoko, Mamiko; Okabe, Nobuo; Acta Crystallographica Section C 62 (2006) m136–m139; doi:10.1107/S010827010600610X

data_2015266
_publ_section_title
;Dichloro(propane-1,3-diamine-\k^2^<i>N</i>,<i>N</i>')platinum(II),
 dichloro(propane-1,3-diamine-\k^2^<i>N</i>,<i>N</i>')palladium(II) and
 \m-4,9-diazadodecane-1,12-diamine-\k^2^<i>N</i>^1^,<i>N</i>^4^:\k^2^<i>N</i>^9^,<i>N</i>^12^-bis[dichloroplatinum(II)]
;
_journal_coeditor_code           OB1247
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m136
_journal_page_last               m139
_journal_paper_doi               10.1107/S010827010600610X
_journal_volume                  62
_journal_year                    2006
_chemical_formula_iupac          '[Pt2 Cl4 (C10 H26 N4)]'
_chemical_formula_moiety         'C10 H26 Cl4 N4 Pt2'
_chemical_formula_sum            'C10 H26 Cl4 N4 Pt2'
_chemical_formula_weight         734.31
_chemical_name_systematic
;
\m-4,9-diazadodecane-1,12-diamine-\k^2^N^1^,N^4^;\k^2^N^9^,N^12^-
bis[dichlorodiplatinum(II)]
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 92.09(4)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   8.860(10)
_cell_length_b                   8.018(6)
_cell_length_c                   12.930(10)
_cell_measurement_reflns_used    8101
_cell_measurement_temperature    123
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      3.1
_cell_volume                     917.9(14)
_computing_cell_refinement       RAPID-AUTO
_computing_data_collection       'RAPID-AUTO (Rigaku Corporation, 1998)'
_computing_data_reduction
'CrystalStructure (Rigaku/MSC, 2005) and CRYSTALS (Watkin <i>et al.</i>, 1996)'
_computing_molecular_graphics    'ORTEPII (Johnson, 1976)'
_computing_publication_material  CrystalStructure
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 1997)'
_diffrn_detector_area_resol_mean 10.00
_diffrn_measured_fraction_theta_full 0.9960
_diffrn_measured_fraction_theta_max 0.9960
_diffrn_measurement_device_type  'Rigaku R-AXIS RAPID'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.040
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            9030
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    15.802
_exptl_absorpt_correction_T_max  0.455
_exptl_absorpt_correction_T_min  0.089
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(ABSCOR; Higashi, 1995)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.657
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       platelet
_exptl_crystal_F_000             676.00
_exptl_crystal_size_max          0.10
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.05
_refine_diff_density_max         2.61
_refine_diff_density_min         -2.71
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.050
_refine_ls_hydrogen_treatment    constr
_refine_ls_number_parameters     92
_refine_ls_number_reflns         2105
_refine_ls_R_factor_gt           0.0290
_refine_ls_shift/su_max          0.0010
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^)+(0.0438P)^2^+0.3492P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.0760
_reflns_number_gt                1725
_reflns_number_total             2105
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
_cod_data_source_file            ob1247.cif
_cod_data_source_block           III
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2015266
_cod_database_fobs_code          2015266