LMucko/crystallography-open-database huggingface dataset:
Novel Chiral and Achiral NCN Pincer Complexes Based on 1,3-Bis(1,2,4-triazol- 1-ylmethyl)benzene
Díez-Barra, E.; Guerra, J.; López-Solera, Isabel; Merino, S.; Rodríguez-López, J.; Sánchez-Verdú, P.; Tejeda, J.; Organometallics  (2003) –; doi:

data_4060723
_publ_section_title
;
Novel Chiral and Achiral NCN Pincer Complexes Based on 1,3-Bis(1,2,4-triazol-
1-ylmethyl)benzene
;
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C52 H80 N8 O6 Sm2'
_chemical_formula_weight         1213.94
_space_group_IT_number           19
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   11.1930(10)
_cell_length_b                   17.9546(17)
_cell_length_c                   26.580(2)
_cell_measurement_temperature    203(2)
_cell_volume                     5341.6(8)
_diffrn_ambient_temperature      203(2)
_exptl_crystal_density_diffrn    1.510
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4060723
Alexandr Shafir; John Arnold; Organometallics  (2003) –; doi:

data_4060724
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_analytical     'C54 H46 B F15 Fe N2 Si2 Zr '
_chemical_formula_moiety         'C54 H46 B F15 Fe N2 Si2 Zr '
_chemical_formula_structural     'C54 H46 B F15 Fe N2 Si2 Zr '
_chemical_formula_sum            'C54 H46 B F15 Fe N2 Si2 Zr'
_chemical_formula_weight         1221.99
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                80.143(1)
_cell_angle_beta                 79.695(1)
_cell_angle_gamma                62.849(1)
_cell_formula_units_Z            2
_cell_length_a                   13.1328(3)
_cell_length_b                   13.7959(3)
_cell_length_c                   16.6316(4)
_cell_measurement_temperature    142.2
_cell_volume                     2624.2(1)
_diffrn_ambient_temperature      142.2
_exptl_crystal_density_diffrn    1.546
_cod_depositor_comments
;
The following automatic conversions were performed:

'_atom_site_thermal_displace_type' tag value 'Uij' was replaced with
'Uani' value 122 times.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_formula_sum        'C54 H46 B F15 Fe N2 Si2 Zr '
_cod_database_code               4060724
; Organometallics  (2003) –; doi:

data_4060725
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_moiety         'C17 H28 Cl4 Fe N2 Si2 Zr '
_chemical_formula_sum            'C17 H28 Cl4 Fe N2 Si2 Zr'
_chemical_formula_weight         605.47
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                112.123(1)
_cell_angle_beta                 101.207(1)
_cell_angle_gamma                105.035(1)
_cell_formula_units_Z            2
_cell_length_a                   10.8988(3)
_cell_length_b                   10.9214(4)
_cell_length_c                   12.2609(4)
_cell_measurement_temperature    113.2
_cell_volume                     1234.16(7)
_diffrn_ambient_temperature      113.2
_exptl_crystal_density_diffrn    1.629
_cod_depositor_comments
;
The following automatic conversions were performed:

'_atom_site_thermal_displace_type' tag value 'Uij' was replaced with
'Uani' value 55 times.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_formula_sum        'C17 H28 Cl4 Fe N2 Si2 Zr '
_cod_database_code               4060725
Reactivity of Trimethylaluminium with Lanthanide Aryloxides: Adduct and Tetramethylaluminate Formation
Fischbach, A.; Herdtweck, E.; Anwander, R.; Eickerling, G.; Scherer, W.; Organometallics  (2003) –; doi:

data_4060726
_publ_section_title
;
 Reactivity of Trimethylaluminium with Lanthanide Aryloxides:
 Adduct and Tetramethylaluminate Formation
;
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_absolute_configuration ad
_chemical_formula_moiety         'C42 H69 Al2 O3 Y'
_chemical_formula_sum            'C42 H69 Al2 O3 Y'
_chemical_formula_weight         764.84
_space_group_IT_number           19
_space_group_name_Hall           'P 2ac 2ab'
_space_group_name_H-M_alt        'P 21 21 21'
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   11.7263(1)
_cell_length_b                   18.1264(1)
_cell_length_c                   20.7998(1)
_cell_measurement_temperature    123(1)
_cell_volume                     4421.11(5)
_diffrn_ambient_temperature      123(1)
_exptl_crystal_density_diffrn    1.149
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4060726
Reactivity of Trimethylaluminium with Lanthanide Aryloxides: Adduct and Tetramethylaluminate Formation
Fischbach, A.; Herdtweck, E.; Anwander, R.; Eickerling, G.; Scherer, W.; Organometallics  (2003) –; doi:

data_4060727
_publ_section_title
;
 Reactivity of Trimethylaluminium with Lanthanide Aryloxides:
 Adduct and Tetramethylaluminate Formation
;
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_moiety         'C32 H54 Al O2 Y'
_chemical_formula_sum            'C32 H54 Al O2 Y'
_chemical_formula_weight         586.64
_space_group_IT_number           61
_space_group_name_Hall           '-P 2ac 2ab'
_space_group_name_H-M_alt        'P b c a'
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   19.6670(1)
_cell_length_b                   14.4580(2)
_cell_length_c                   23.3750(3)
_cell_measurement_temperature    183
_cell_volume                     6646.58(13)
_diffrn_ambient_temperature      183
_exptl_crystal_density_diffrn    1.173
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4060727
Reactivity of Trimethylaluminium with Lanthanide Aryloxides: Adduct and Tetramethylaluminate Formation
Fischbach, A.; Herdtweck, E.; Anwander, R.; Eickerling, G.; Scherer, W.; Organometallics  (2003) –; doi:

data_4060728
_publ_section_title
;
 Reactivity of Trimethylaluminium with Lanthanide Aryloxides:
 Adduct and Tetramethylaluminate Formation
;
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_moiety         'C32 H54 Al Lu O2'
_chemical_formula_sum            'C32 H54 Al Lu O2'
_chemical_formula_weight         672.70
_space_group_IT_number           61
_space_group_name_Hall           '-P 2ac 2ab'
_space_group_name_H-M_alt        'P b c a'
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   19.6660(1)
_cell_length_b                   14.4500(2)
_cell_length_c                   23.2530(2)
_cell_measurement_temperature    183
_cell_volume                     6607.89(11)
_diffrn_ambient_temperature      183
_exptl_crystal_density_diffrn    1.352
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4060728
Practical synthesis of aminoethyl-o-carboranes
; Organometallics  (2003) –; doi:

data_4060729
_publ_section_title
;
Practical synthesis of aminoethyl-o-carboranes
;
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C18 H29 B10 N'
_chemical_formula_weight         367.52
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 98.818(6)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.2077(6)
_cell_length_b                   15.2630(9)
_cell_length_c                   14.7009(12)
_cell_measurement_temperature    293(2)
_cell_volume                     2263.3(3)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.079
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4060729
Practical synthesis of aminoethyl-o-carboranes
; Organometallics  (2003) –; doi:

data_4060730
_publ_section_title
;
Practical synthesis of aminoethyl-o-carboranes
;
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C11 H24 B10 Cl N'
_chemical_formula_weight         313.86
_space_group_IT_number           19
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   6.8687(7)
_cell_length_b                   11.6255(8)
_cell_length_c                   23.1877(13)
_cell_measurement_temperature    293(2)
_cell_volume                     1851.6(3)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.126
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4060730
; Organometallics  (2003) –; doi:

data_4060731
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_moiety         'C36 H48 Cl2 S2 Ru2 '
_chemical_formula_sum            'C36 H48 Cl2 Ru2 S2'
_chemical_formula_weight         817.94
_space_group_IT_number           19
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      19
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   16.321(3)
_cell_length_b                   29.390(9)
_cell_length_c                   8.862(3)
_cell_measurement_temperature    296.1
_cell_volume                     4251.0(2)
_exptl_crystal_density_diffrn    1.278
_cod_original_formula_sum        'C36 H48 Cl2 S2 Ru2 '
_cod_database_code               4060731
; Organometallics  (2003) –; doi:

data_4060732
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_moiety         'C37 H50 Cl F3 O4 S3 Ru2 '
_chemical_formula_sum            'C37 H50 Cl F3 O4 Ru2 S3'
_chemical_formula_weight         949.57
_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90
_cell_angle_beta                 118.15(5)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   11.80(1)
_cell_length_b                   16.030(8)
_cell_length_c                   12.07(1)
_cell_measurement_temperature    296.1
_cell_volume                     2012.5(3)
_exptl_crystal_density_diffrn    1.567
_cod_original_sg_symbol_H-M      'P 21'
_cod_original_formula_sum        'C37 H50 Cl F3 O4 S3 Ru2 '
_cod_database_code               4060732
; Organometallics  (2003) –; doi:

data_4060733
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C25 H10 Al F15 O'
_chemical_formula_weight         638.31
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 100.902(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.318(3)
_cell_length_b                   16.319(5)
_cell_length_c                   14.527(4)
_cell_measurement_temperature    173(2)
_cell_volume                     2402.1(12)
_diffrn_ambient_temperature      173(2)
_exptl_crystal_density_diffrn    1.765
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4060733
; Organometallics  (2003) –; doi:

data_4060734
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C19 H4 Al F15 O'
_chemical_formula_weight         560.20
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 114.830(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.8362(19)
_cell_length_b                   12.6834(19)
_cell_length_c                   13.464(2)
_cell_measurement_temperature    173(2)
_cell_volume                     1989.4(5)
_diffrn_ambient_temperature      173(2)
_exptl_crystal_density_diffrn    1.870
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4060734
; Organometallics  (2003) –; doi:

data_4060735
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_moiety         'C44 H32 Cl2 O P2 Pd'
_chemical_formula_sum            'C44 H32 Cl2 O P2 Pd'
_chemical_formula_weight         815.94
_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90.0000(1)
_cell_angle_beta                 108.33(1)
_cell_angle_gamma                90.0000(1)
_cell_formula_units_Z            2
_cell_length_a                   11.940(3)
_cell_length_b                   11.711(3)
_cell_length_c                   13.548(3)
_cell_measurement_temperature    293(2)
_cell_volume                     1798.4(7)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.507
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21'
_cod_database_code               4060735
; Organometallics  (2003) –; doi:

data_4060736
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_moiety         'C88 H64 O2 P4 Pd'
_chemical_formula_sum            'C88 H64 O2 P4 Pd'
_chemical_formula_weight         1383.67
_space_group_IT_number           1
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  'P 1'
_symmetry_space_group_name_H-M   'P 1'
_cell_angle_alpha                63.11(1)
_cell_angle_beta                 78.27(1)
_cell_angle_gamma                68.29(1)
_cell_formula_units_Z            1
_cell_length_a                   11.956(1)
_cell_length_b                   12.809(1)
_cell_length_c                   13.422(1)
_cell_measurement_temperature    293(2)
_cell_volume                     1701.5(3)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.350
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4060736
; Organometallics  (2003) –; doi:

data_4060737
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_moiety         'C56 H51 I O P2 Pd'
_chemical_formula_sum            'C56 H51 I O P2 Pd'
_chemical_formula_weight         1035.21
_space_group_IT_number           170
_symmetry_cell_setting           hexagonal
_symmetry_space_group_name_Hall  'P 65'
_symmetry_space_group_name_H-M   'P 65'
_cell_angle_alpha                90.0000(10)
_cell_angle_beta                 90.0000(10)
_cell_angle_gamma                120.0000(10)
_cell_formula_units_Z            6
_cell_length_a                   29.934(6)
_cell_length_b                   29.934(6)
_cell_length_c                   11.858(5)
_cell_measurement_temperature    293(2)
_cell_volume                     9202(5)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.121
_exptl_crystal_density_meas      multirun
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Hexagonal' changed to 'hexagonal'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4060737
; Organometallics  (2003) –; doi:

data_4060738
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C24 H42 Si2 Zr'
_chemical_formula_weight         477.98
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 91.0090(12)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   9.0450(2)
_cell_length_b                   19.9540(5)
_cell_length_c                   13.9200(3)
_cell_measurement_temperature    293(2)
_cell_volume                     2511.95(10)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.264
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4060738
; Organometallics  (2003) –; doi:

data_4060739
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C24 H42 Mg Si2 Zr'
_chemical_formula_weight         502.29
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 93.60(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   8.8317(17)
_cell_length_b                   15.7234(15)
_cell_length_c                   19.580(6)
_cell_measurement_temperature    293(2)
_cell_volume                     2713.5(10)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.229
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4060739
; Organometallics  (2003) –; doi:

data_4060740
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C32 H60 Si4 Zr'
_chemical_formula_weight         648.38
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 106.8030(9)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   9.75200(10)
_cell_length_b                   38.3120(7)
_cell_length_c                   10.2510(2)
_cell_measurement_temperature    293(2)
_cell_volume                     3666.44(10)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.175
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4060740
; Organometallics  (2003) –; doi:

data_4060741
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C24 H40 Si2 Zr'
_chemical_formula_weight         475.96
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                83.608(2)
_cell_angle_beta                 74.265(2)
_cell_angle_gamma                67.520(2)
_cell_formula_units_Z            2
_cell_length_a                   8.5260(2)
_cell_length_b                   10.3590(4)
_cell_length_c                   15.5410(7)
_cell_measurement_temperature    293(2)
_cell_volume                     1220.72(8)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.295
_cod_database_code               4060741