Current-induced metallic state in an organic (EDT-TSF)2GaCl4 conductor.
Endo, Hisataka; Kawamoto, Tadashi; Mori, Takehiko; Terasaki, Ichiro; Kakiuchi, Toru; Sawa, Hiroshi; Kodani, Mie; Takimiya, Kazuo; Otsubo, Tetsuo; Journal of the American Chemical Society 128 (2006) 9006–9007; doi:10.1021/ja062277q

data_4101315
_publ_section_title
;
 Current-induced metallic state in an organic (EDT-TSF)2GaCl4
 conductor.
;
_journal_issue                   28
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              9006
_journal_page_last               9007
_journal_paper_doi               10.1021/ja062277q
_journal_volume                  128
_journal_year                    2006
_chemical_formula_moiety         '2(C8 H6 S2 Se4), Cl4 Fe '
_chemical_formula_sum            'C16 H12 Cl4 Fe S4 Se8'
_chemical_formula_weight         1161.85
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      11
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 100.42(4)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   7.290(5)
_cell_length_b                   30.655(4)
_cell_length_c                   6.696(2)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293.2
_cell_measurement_theta_max      14.4
_cell_measurement_theta_min      12.6
_cell_volume                     1471(1)
_computing_cell_refinement       WinAFC
_computing_data_collection       WinAFC
_computing_data_reduction        'teXsan Ver. 1.10'
_computing_publication_material  'teXsan Ver. 1.10'
_computing_structure_refinement  'teXsan Ver. 1.10'
_computing_structure_solution    SIR92
_diffrn_measured_fraction_theta_full 0.9993
_diffrn_measured_fraction_theta_max 0.9993
_diffrn_measurement_device_type  'Rigaku AFC7R'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.030
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       43
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       9
_diffrn_reflns_limit_l_min       -9
_diffrn_reflns_number            5223
_diffrn_reflns_theta_full        30.00
_diffrn_reflns_theta_max         30.00
_diffrn_standards_decay_%        0.52
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    11.063
_exptl_absorpt_correction_T_max  0.179
_exptl_absorpt_correction_T_min  0.058
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details   Tompa_analytical
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    2.622
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_size_max          0.540
_exptl_crystal_size_mid          0.280
_exptl_crystal_size_min          0.170
_refine_diff_density_max         0.61
_refine_diff_density_min         -0.70
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.372
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     154
_refine_ls_number_reflns         4369
_refine_ls_R_factor_gt           0.0378
_refine_ls_shift/su_max          0.0011
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^) + (0.05000(Max(Fo^2^,0) + 2Fc^2^)/3)^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1188
_reflns_number_gt                3089
_reflns_number_total             4369
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
_cod_data_source_file            ja062277qsi20060607_125053.cif
_cod_data_source_block           Cytidine_(Rigaku_Master_fo
_cod_original_formula_sum        'C16 H12 Cl4 Fe S4 Se8 '
_cod_database_code               4101315