Dissecting the Gold(I)-Catalyzed Carboaminations of N-Allyl Tetrahydro-β-carbolines to Allenes.
Gobé, Valérian; Dousset, Maxime; Retailleau, Pascal; Gandon, Vincent; Guinchard, Xavier; The Journal of organic chemistry 83 (2018) 898–912; doi:10.1021/acs.joc.7b02900

data_4033334
_publ_section_title
;
 Dissecting the Gold(I)-Catalyzed Carboaminations of N-Allyl
 Tetrahydro-\b-carbolines to Allenes.
;
_journal_issue                   2
_journal_name_full               'The Journal of organic chemistry'
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_journal_paper_doi               10.1021/acs.joc.7b02900
_journal_volume                  83
_journal_year                    2018
_chemical_formula_moiety         'C25 H28 N2'
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;
CrystalClear-SM Expert 2.0 r16 (Rigaku, 2014)
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CrystalClear-SM Expert 2.0 r16 (Rigaku, 2014)
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CrystalClear-SM Expert 2.0 r16 (Rigaku, 2014)
;
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Crystal Goniometer
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Rigaku RAXIS conversion
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0724P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.1471
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_cod_data_source_file            jo7b02900_si_002.cif
_cod_data_source_block           xg-1323_cmpd_11l
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 

 Adding full bibliography for 4033334--4033336.cif.
;
_cod_database_code               4033334
_shelx_shelxl_version_number     2014/7
_shelx_res_checksum              50086
_shelx_hkl_checksum              60962