Redetermination of tetraphenyllead
Preut, H.; Huber, F.; Acta Crystallographica Section C 49 (1993) 1372–1373; doi:10.1107/S0108270193001878

data_2001543
_publ_contact_author
;
       Dr. Hans Preut
       Anorganische Chemie II Universit\"at Dortmund
       Postfach 500500
       Otto-Hahn-Strasse 6
       D-4600 Dortmund 50
       Germany
;
_publ_section_title
;
 Redetermination of tetraphenyllead
;
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1372
_journal_page_last               1373
_journal_paper_doi               10.1107/S0108270193001878
_journal_volume                  49
_journal_year                    1993
_chemical_formula_moiety         'C24 H20 Pb'
_chemical_formula_sum            'C24 H20 Pb'
_chemical_formula_weight         515.62
_chemical_name_systematic
;
Tetraphenyllead
;
_space_group_IT_number           114
_symmetry_cell_setting           tetragonal
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;
text program Nroffd under UNIX
;
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PARST (Nardelli, 1983); PLATON (Spek, 1982);
MISSYM (Le Page, 1987)
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_diffrn_reflns_reduction_process
; Lorentz-polarization and absorption correction via \y-scans,
data averaged
;
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;
The absolute structure was confirmed by refinement of  \h=0.91(9)
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;
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;
refl observed if F> 3.0\s(F)
;
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The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(F)+0.000673F^2^]' was changed to 'calc'. New tag
'_refine_ls_weighting_details' was created. The value of the new tag
was set to 'w=1/[\s^2^(F)+0.000673F^2^]'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        966.4(3)
_cod_original_sg_symbol_H-M      'P-4 21 c'
_cod_database_code               2001543