Si- and C-Functional Organosilicon Building Blocks for Synthesis Based on 4-Silacyclohexan-1-ones Containing the Silicon Protecting Groups MOP (4-Methoxyphenyl), DMOP (2,6-Dimethoxyphenyl), or TMOP (2,4,6-Trimethoxyphenyl).
Geyer, Marcel; Karlsson, Olle; Baus, Johannes A.; Wellner, Eric; Tacke, Reinhold; The Journal of organic chemistry 80 (2015) 5804–5811; doi:10.1021/acs.joc.5b00774

data_4031005
_publ_section_title
;
 Si- and C-Functional Organosilicon Building Blocks for Synthesis Based on
 4-Silacyclohexan-1-ones Containing the Silicon Protecting Groups MOP
 (4-Methoxyphenyl), DMOP (2,6-Dimethoxyphenyl), or TMOP
 (2,4,6-Trimethoxyphenyl).
;
_journal_issue                   11
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              5804
_journal_page_last               5811
_journal_paper_doi               10.1021/acs.joc.5b00774
_journal_volume                  80
_journal_year                    2015
_chemical_formula_moiety         'C16 H25 N O3 Si'
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_monochromator  graphite
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0382P)^2^+3.6685P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 4031004--4031005.cif.'
_cod_original_cell_volume        3294.3(14)
_cod_database_code               4031005
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_shelx_hkl_checksum              61769