<i>cis</i>-Dichloro(dimethyl sulfoxide-<i>S</i>)(2-methoxypyridine-<i>N</i>)platinum(II)
Georgia M. Arvanitis; Charles E. Holmes; Diana G. Johnson; Michael Berardini; Acta Crystallographica Section C 56 (2000) 1332–1333; doi:10.1107/S0108270100010465

data_2011496
_publ_section_title
;
 <i>cis</i>-Dichloro(dimethyl
 sulfoxide-<i>S</i>)(2-methoxypyridine-<i>N</i>)platinum(II)
;
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1332
_journal_page_last               1333
_journal_paper_doi               10.1107/S0108270100010465
_journal_volume                  56
_journal_year                    2000
_chemical_formula_structural     '[Pt Cl2 (C6 H7 N O) (C2 H6 S O)]'
_chemical_formula_sum            'C8 H13 Cl2 N O2 Pt S'
_chemical_formula_weight         453.25
_chemical_name_systematic
;
cis-dichloro(dimethyl sulfoxide-S)(2-methoxypyridine-N)platinum(II)
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.
_cell_angle_beta                 96.62(2)
_cell_angle_gamma                90.
_cell_formula_units_Z            4
_cell_length_a                   8.749(2)
_cell_length_b                   8.486(2)
_cell_length_c                   17.325(3)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    193
_cell_measurement_theta_max      17.5
_cell_measurement_theta_min      12.5
_cell_volume                     1277.7(5)
_computing_cell_refinement       'MSC/AFC Diffractometer Control Software'
_computing_data_collection
;MSC/AFC Diffractometer Control Software (Molecular Structure Corporation,
 1993)
;
_computing_data_reduction        'MSC/AFC Diffractometer Control Software'
_computing_molecular_graphics    TEXSAN
_computing_publication_material  TEXSAN
_computing_structure_refinement
'TEXSAN (Molecular Structure Corporation, 1995)'
_computing_structure_solution    'SIR88 (Burla et al., 1989)'
_diffrn_measurement_device_type  'Rigaku AFC-6S'
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     .71073
_diffrn_reflns_av_R_equivalents  .033
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            2078
_diffrn_reflns_theta_max         25
_diffrn_reflns_theta_min         1
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 100
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    11.499
_exptl_absorpt_correction_T_max  .080
_exptl_absorpt_correction_T_min  .032
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   'via \y scan (North et al., 1968)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.356
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             848.00
_exptl_crystal_size_max          .46
_exptl_crystal_size_mid          .26
_exptl_crystal_size_min          .22
_refine_diff_density_max         1.82
_refine_diff_density_min         -1.72
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.42
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_parameters     137
_refine_ls_number_reflns         1388
_refine_ls_restrained_S_obs      1.42
_refine_ls_R_factor_gt           .029
_refine_ls_shift/su_max          <0.001
_refine_ls_shift/su_mean         .00
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(F) + 0.01F^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         .036
_reflns_number_gt                1388
_reflns_number_total             1936
_reflns_threshold_expression     I>3\s(I)
_cod_data_source_file            da1145.cif
_cod_data_source_block           I
_cod_original_cell_volume        1277.7(4)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2011496