Temperature-dependent characteristics of n-channel transistors based on 5,5′-bithiazolidinylidene-2,4,2′,4′-tetrathiones
Ryo, Suho; Yoo, Dongho; Iijima, Kodai; Sato, Ryonosuke; Le Gal, Yann; Lorcy, Dominique; Mori, Takehiko; New Journal of Chemistry 43 (2019) 11865–; doi:10.1039/C9NJ02731A

data_7058547
_publ_section_title
;
 Temperature-dependent characteristics of n-channel transistors based on
 5,5&#x2032;-bithiazolidinylidene-2,4,2&#x2032;,4&#x2032;-tetrathiones
;
_journal_issue                   30
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              11865
_journal_paper_doi               10.1039/C9NJ02731A
_journal_volume                  43
_journal_year                    2019
_chemical_formula_moiety         'C18 H26 N2 S6'
_chemical_formula_sum            'C18 H26 N2 S6'
_chemical_formula_weight         462.78
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_update_record
;
2019-04-29 deposited with the CCDC.    2019-06-27 downloaded from the CCDC.
;
_cell_angle_alpha                90.0000
_cell_angle_beta                 90.05(4)
_cell_angle_gamma                90.0000
_cell_formula_units_Z            2
_cell_length_a                   14.970(8)
_cell_length_b                   5.028(4)
_cell_length_c                   15.075(6)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    298
_cell_measurement_theta_max      17.38
_cell_measurement_theta_min      15.12
_cell_volume                     1134.7(12)
_computing_cell_refinement       WinAFC
_computing_data_collection       WinAFC
_computing_data_reduction        WinAFC
_computing_molecular_graphics    'CrystalStructure 4.3'
_computing_publication_material  'CrystalStructure 4.3 (Rigaku, 2018)'
_computing_structure_refinement  'SHELXL Version 2018/1 (Sheldrick, 2008)'
_computing_structure_solution    'Il Milione (Burla, et al., 2007)'
_diffrn_ambient_temperature      298
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Rigaku AFC7R'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0673
_diffrn_reflns_av_unetI/netI     0.1362
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       6
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            2984
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_theta_full        25.240
_diffrn_reflns_theta_max         26.998
_diffrn_reflns_theta_min         2.702
_diffrn_standards_decay_%        -1.386
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.609
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.354
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prismatic
_exptl_crystal_F_000             488.00
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.200
_refine_diff_density_max         0.68
_refine_diff_density_min         -0.62
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.985
_refine_ls_hydrogen_treatment    constr
_refine_ls_number_parameters     119
_refine_ls_number_reflns         2472
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.1824
_refine_ls_R_factor_gt           0.0694
_refine_ls_shift/su_max          0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^)+(0.1397P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1802
_refine_ls_wR_factor_ref         0.2494
_reflns_Friedel_coverage         0.000
_reflns_number_gt                1147
_reflns_number_total             2472
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
_cod_data_source_file            c9nj02731a2.cif
_cod_data_source_block           Cytidine_(Rigaku_Master_for_Mo)
_cod_depositor_comments
'Adding full bibliography for 7058546--7058547.cif.'
_cod_original_cell_volume        1134.6(12)
_cod_database_code               7058547
_shelx_res_checksum              95437