Bench-stable frustrated Lewis pair chemistry: fluoroborate salts as precatalysts for the C-H borylation of heteroarenes.
Légaré, Marc-André; Rochette, Étienne; Légaré Lavergne, Julien; Bouchard, Nicolas; Fontaine, Frédéric-Georges; Chemical communications (Cambridge, England) 52 (2016) 5387–5390; doi:10.1039/c6cc01267a

data_7124592
_publ_section_title
;
 Bench-stable frustrated Lewis pair chemistry: fluoroborate salts as
 precatalysts for the C-H borylation of heteroarenes.
;
_journal_issue                   31
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              5387
_journal_page_last               5390
_journal_paper_doi               10.1039/c6cc01267a
_journal_volume                  52
_journal_year                    2016
_chemical_formula_sum            'C15 H24 B N O2'
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_audit_creation_method           SHELXL-2014/6
_audit_update_record
;
2015-12-04 deposited with the CCDC.
2016-03-14 downloaded from the CCDC.
;
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_diffrn_ambient_temperature      150(2)
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_diffrn_measured_fraction_theta_max 0.954
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_diffrn_reflns_Laue_measured_fraction_full 1.000
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_exptl_crystal_recrystallization_method 'Re-crystallisation from solvent: '
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0696P)^2^+0.2503P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_data_source_file            c6cc01267a2.cif
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_shelx_res_checksum              1316