InP nanowires from surfactant-free thermolysis of single molecule precursors.
Banerjee, Chiranjib; Hughes, David L.; Bochmann, Manfred; Nann, Thomas; Dalton transactions (Cambridge, England : 2003) 41 (2012) 7244–7248; doi:10.1039/c2dt30283g

data_7019386
_publ_section_title
;
 InP nanowires from surfactant-free thermolysis of single molecule
 precursors.
;
_journal_issue                   24
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7244
_journal_page_last               7248
_journal_paper_doi               10.1039/c2dt30283g
_journal_volume                  41
_journal_year                    2012
_chemical_formula_moiety         'C40 H64 In2 P2 Si4'
_chemical_formula_structural     '[{Bz2 In P(SiMe3)2}2]'
_chemical_formula_sum            'C40 H64 In2 P2 Si4'
_chemical_formula_weight         948.85
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
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_atom_sites_solution_secondary   difmap
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_cell_angle_alpha                102.721(9)
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_cell_measurement_temperature    140(1)
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_cell_measurement_theta_min      3.5718
_cell_volume                     1132.32(18)
_computing_cell_refinement
;
CrysAlisPro RED, Oxford Diffraction Ltd., Version 1.171.32.24
;
_computing_data_collection
;
CrysAlisPro CCD, Oxford Diffraction Ltd., Version 1.171.32.24
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_computing_data_reduction
;
CrysAlisPro RED, Oxford Diffraction Ltd., Version 1.171.32.24
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_computing_molecular_graphics    'ORTEP (Johnson, 1976 and Farrugia, 1997)'
_computing_publication_material
'SHELXL-97 (Sheldrick, 2008) and WINGX (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      140(1)
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_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Oxford Diffraction Xcalibur 3/CCD'
_diffrn_measurement_method       'Thin slice \f and \w scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Enhance (Mo) X-ray Source'
_diffrn_radiation_type           Mo-K\a
_diffrn_radiation_wavelength     0.71073
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_diffrn_reflns_limit_k_max       15
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_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            23201
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;
CrysAlisPro RED, Oxford Diffraction Ltd., Version 1.171.32.24
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.391
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             488
_exptl_crystal_size_max          0.33
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0304P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0522
_refine_ls_wR_factor_ref         0.0529
_reflns_number_gt                5849
_reflns_number_total             6588
_reflns_threshold_expression     I>2sigma(I)
_cod_data_source_file            c2dt30283g.txt
_cod_data_source_block           chiranb1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_cell_volume        1132.32(15)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7019386