Ground-State Singlet L3Fe-(μ-N)-FeL3 and L3Fe(NR) Complexes Featuring Pseudotetrahedral Fe(II) Centers
Steven D. Brown; Jonas C. Peters; Journal of the American Chemical Society 127 (2005) 1913–1923; doi:10.1021/ja0453073

data_4111466
_publ_section_title
;
 Ground-State Singlet L3Fe-(\m-N)-FeL3 and L3Fe(NR) Complexes Featuring
 Pseudotetrahedral Fe(II) Centers
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              1913
_journal_page_last               1923
_journal_paper_doi               10.1021/ja0453073
_journal_volume                  127
_journal_year                    2005
_chemical_formula_sum            'C114 H130 B2 Fe2 N Na O6 P6'
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_chemical_name_systematic
; 
 ? 
;
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_computing_cell_refinement       'Bruker SMART'
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_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
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_diffrn_measured_fraction_theta_max 0.734
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
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_exptl_crystal_colour            dark
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0000P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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