A Series of Zinc(II) 3D →3D Interpenetrated Coordination Polymers Based On Thiophene-2,5-dicarboxylate and Bis(Imidazole) Derivative Linkers
Erer, Hakan; Yeşilel, Okan Zafer; Arıcı, Mürsel; Crystal Growth & Design 15 (2015) 3201–; doi:10.1021/acs.cgd.5b00276

data_4513206
_publ_section_title
;
 A Series of Zinc(II) 3D \\rightarrow 3D Interpenetrated Coordination
 Polymers Based On Thiophene-2,5-dicarboxylate and Bis(Imidazole)
 Derivative Linkers
;
_journal_issue                   7
_journal_name_full               'Crystal Growth &amp; Design'
_journal_page_first              3201
_journal_paper_doi               10.1021/acs.cgd.5b00276
_journal_volume                  15
_journal_year                    2015
_chemical_formula_moiety         'C12 H11 N2 O4 S Zn'
_chemical_formula_sum            'C12 H11 N2 O4 S Zn'
_chemical_formula_weight         344.66
_chemical_name_systematic
;
 ?
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             2015-01-22
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Olex2 1.2
(compiled 2014.06.27 svn.r2953 for OlexSys, GUI svn.r4855)
;
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_cell_length_c                   14.2857(5)
_cell_measurement_reflns_used    52914
_cell_measurement_temperature    293(2)
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_cell_measurement_theta_min      2.41
_cell_volume                     1383.39(9)
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_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 6.67
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'STOE IPDS 2'
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_diffrn_reflns_av_unetI/netI     0.0094
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_diffrn_reflns_limit_l_min       -17
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_diffrn_reflns_theta_max         26.49
_diffrn_reflns_theta_min         2.79
_diffrn_source                   'fine-focus sealed tube'
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_exptl_absorpt_coefficient_mu    1.939
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_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.655
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'calc w=1/[\s^2^(Fo^2^)+(0.0353P)^2^+1.2839P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cg5b00276_si_002.cif
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_cod_depositor_comments
'Adding full bibliography for 4513206--4513212.cif.'
_cod_original_cell_volume        1383.39(8)
_cod_database_code               4513206