Preparation of Cyclopropanediol: Novel [2 + 1] Cycloaddition Reaction of Bis(iodozincio)methane with 1,2-Diketones
Katsumi Ukai; Koichiro Oshima; Seijiro Matsubara; Journal of the American Chemical Society 122 (2000) 12047–12048; doi:10.1021/ja003360v

data_4116261
_publ_section_title
;
 Preparation of Cyclopropanediol: Novel [2 + 1] Cycloaddition Reaction of
 Bis(iodozincio)methane with 1,2-Diketones
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              12047
_journal_page_last               12048
_journal_paper_doi               10.1021/ja003360v
_journal_volume                  122
_journal_year                    2000
_chemical_formula_moiety         'C13 H20 O4 '
_chemical_formula_sum            'C13 H20 O4'
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_cell_length_c                   5.619(1)
_cell_measurement_temperature    296.2
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_computing_data_reduction        'teXsan Ver. 1.10'
_computing_publication_material  'teXsan Ver. 1.10'
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_refine_ls_R_factor_gt           0.0544
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo) + 0.00040|Fo|^2^]'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                1164
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_reflns_threshold_expression     F^2^>2.0\s(F^2^)
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