Diamondoid-Type Copper Coordination Polymers Containing Soft Cyclodiphosphazane Ligands.
Siddiqui, Mujahuddin M.; Mague, Joel T.; Balakrishna, Maravanji S.; Inorganic chemistry 54 (2015) 6063–6065; doi:10.1021/acs.inorgchem.5b00525

data_4343364
_publ_section_title
;
 Diamondoid-Type Copper Coordination Polymers Containing Soft
 Cyclodiphosphazane Ligands.
;
_journal_issue                   13
_journal_name_full               'Inorganic chemistry'
_journal_page_first              6063
_journal_page_last               6065
_journal_paper_doi               10.1021/acs.inorgchem.5b00525
_journal_volume                  54
_journal_year                    2015
_chemical_formula_moiety         'C28 H34 Cu4 I4 N4 P2'
_chemical_formula_sum            'C28 H34 Cu4 I4 N4 P2'
_chemical_formula_weight         1250.29
_chemical_name_systematic
;
 ?
;
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_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_primary     direct
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_cell_angle_beta                 96.485(3)
_cell_angle_gamma                90.109(3)
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_cell_length_b                   18.495(4)
_cell_length_c                   21.830(5)
_cell_measurement_reflns_used    9916
_cell_measurement_temperature    200(2)
_cell_measurement_theta_max      27.212
_cell_measurement_theta_min      2.358
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_computing_cell_refinement       '<i>SAINT</i> (Bruker AXS, 2009)'
_computing_data_collection       '<i>APEX2</i> (Bruker AXS, 2010)'
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_diffrn_measurement_device_type  'Bruker Smart APEX CCD'
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_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       slab
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_exptl_crystal_size_max          0.193
_exptl_crystal_size_mid          0.125
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_refine_ls_extinction_method     none
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+244.8000P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_gt                20638
_reflns_number_total             24879
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 4343363--4343365.cif.'
_cod_original_cell_volume        3849.2(15)
_cod_database_code               4343364
_shelx_estimated_absorpt_t_min   0.417
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_shelxl_version_number           2013-3
_shelx_res_checksum              8265
_shelx_hkl_checksum              12783