Dinuclear ytterbium(III) benzamidinate complexes with bridging S<sub>3</sub><sup>2-</sup>, Se<sub>2</sub><sup>2-</sup> and Te<sub>2</sub><sup>2-</sup> ligands: synthesis, structure and magnetic properties.
Ma, Ying-Zhao; Yu, Lian; Zhou, Qi; Fu, Wensheng; Dalton transactions (Cambridge, England : 2003) 53 (2024) 8118–8123; doi:10.1039/d4dt00724g

data_7715862
_publ_section_title
;
 Dinuclear ytterbium(III) benzamidinate complexes with bridging
 S<sub>3</sub><sup>2-</sup>, Se<sub>2</sub><sup>2-</sup> and
 Te<sub>2</sub><sup>2-</sup> ligands: synthesis, structure and magnetic
 properties.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              8118
_journal_page_last               8123
_journal_paper_doi               10.1039/d4dt00724g
_journal_volume                  53
_journal_year                    2024
_chemical_formula_moiety         'C56 H100 N8 O S3 Si8 Yb2'
_chemical_formula_sum            'C56 H100 N8 O S3 Si8 Yb2'
_chemical_formula_weight         1568.41
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_audit_creation_date             2023-11-07
_audit_creation_method
;
Olex2 1.5
(compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817)
;
_audit_update_record
;
2024-03-03 deposited with the CCDC.	2024-04-26 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 101.055(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   16.9080(7)
_cell_length_b                   14.7978(6)
_cell_length_c                   30.2287(12)
_cell_measurement_reflns_used    9802
_cell_measurement_temperature    100.00
_cell_measurement_theta_max      29.90
_cell_measurement_theta_min      2.48
_cell_volume                     7422.9(5)
_computing_cell_refinement       'SAINT V8.38A (Bruker, 2018)'
_computing_data_reduction        'SAINT V8.38A (Bruker, 2018)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_diffrn_ambient_temperature      100.00
_diffrn_detector                 'CCD area detector'
_diffrn_detector_area_resol_mean 7.9
_diffrn_detector_type            'Bruker SMART CCD 1K area detector'
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.989
_diffrn_measurement_device       'three-circle diffractometer'
_diffrn_measurement_device_type  'Bruker SMART APEX2 area detector'
_diffrn_measurement_method       '\w and \f scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0684
_diffrn_reflns_av_unetI/netI     0.0788
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.989
_diffrn_reflns_limit_h_max       24
_diffrn_reflns_limit_h_min       -24
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       43
_diffrn_reflns_limit_l_min       -43
_diffrn_reflns_number            78334
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.989
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.653
_diffrn_reflns_theta_min         2.436
_diffrn_source                   'sealed X-ray tube'
_diffrn_source_current           1.4
_diffrn_source_power             0.07
_diffrn_source_target            Mo
_diffrn_source_type              'Incoatec I\ms'
_diffrn_source_voltage           50.0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    2.758
_exptl_absorpt_correction_T_max  0.0998
_exptl_absorpt_correction_T_min  0.0531
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1407 before and 0.0681 after correction.
The Ratio of minimum to maximum transmission is 0.5321.
The \l/2 correction factor is Not present.
;
_exptl_crystal_colour            'clear dark orange'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   dark
_exptl_crystal_colour_primary    orange
_exptl_crystal_density_diffrn    1.403
_exptl_crystal_description       prism
_exptl_crystal_F_000             3200
_exptl_crystal_size_max          0.03
_exptl_crystal_size_mid          0.02
_exptl_crystal_size_min          0.01
_refine_diff_density_max         2.355
_refine_diff_density_min         -2.960
_refine_diff_density_rms         0.211
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.123
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1166
_refine_ls_number_reflns         22696
_refine_ls_number_restraints     1914
_refine_ls_restrained_S_all      2.423
_refine_ls_R_factor_all          0.1228
_refine_ls_R_factor_gt           0.0918
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0001P)^2^+144.0181P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1794
_refine_ls_wR_factor_ref         0.1924
_reflns_Friedel_coverage         0.000
_reflns_number_gt                16494
_reflns_number_total             22696
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d4dt00724g2.cif
_cod_data_source_block           1
_cod_depositor_comments
'Adding full bibliography for 7715860--7715862.cif.'
_cod_database_code               7715862
_shelx_shelxl_version_number     2018/3
_shelx_estimated_absorpt_t_max   0.973
_shelx_estimated_absorpt_t_min   0.922
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 Si2-C11
 1.86 with sigma of 0.02
 Si2-C13
 1.86 with sigma of 0.02
 Si2-C12
 1.86 with sigma of 0.02
 N1-C4 \\sim N1A-C4A \\sim N2-C4 \\sim N2A-C4A
 with sigma of 0.02
 C4A-C5A \\sim C5-C4
 with sigma of 0.02
 C10-C5 \\sim C9-C8 \\sim C5A-C10A \\sim C6A-C6
 with sigma of 0.02
 C10-C5 \\sim C9-C8 \\sim C6A-C6 \\sim C9A-C7
 with sigma of 0.02
 C23-C21 \\sim C23A-C22A \\sim C21A-C22A \\sim C23-C22
 with sigma of 0.02
 C18A-C19A \\sim C20A-C22 \\sim C21-C23 \\sim C23A-C22A \\sim C21A-C18 \\sim
C19-C20
 with sigma of 0.02
 C18A-C19A \\sim C20A-C21A \\sim C22A-C23A \\sim C22-C21 \\sim C23-C18 \\sim
C19-C20
 with sigma of 0.02
 C18-C17 \\sim C17-C18A
 with sigma of 0.02
 Si6-C38 \\sim Si6A-C39A \\sim Si6-C37 \\sim Si6A-C38A \\sim Si6-C39 \\sim
Si6A-C37A
 with sigma of 0.02
 C31-C34 \\sim C36-C35 \\sim C32-C33 \\sim C36A-C34A \\sim C33A-C32A \\sim
C35A-C31A
 with sigma of 0.02
 C31-C36 \\sim C35-C34 \\sim C33-C32 \\sim C31A-C36A \\sim C35A-C34A \\sim
C33A-C32A
 with sigma of 0.02
 Si7A-N7A \\sim Si7-N7A
 with sigma of 0.02
 Si7A-C42A \\sim Si7A-C40A \\sim Si7-C40 \\sim Si7A-C41A \\sim Si7-C41 \\sim
Si7-C42
 with sigma of 0.02
 N7-C43 \\sim N7A-C43A \\sim N8-C43A
 with sigma of 0.02
 Yb2-N8 \\sim Yb2-N7A \\sim Yb2-N7
 with sigma of 0.02
 C44-C43 \\sim C44A-C43A
 with sigma of 0.02
 C45A-C44A \\sim C45-C44 \\sim C46A-C45A \\sim C46-C45 \\sim C47-C46 \\sim
C47A-C46A \\sim C48A-C47A ~
 C48-C47 \\sim C49A-C48A \\sim C49-C48 \\sim C49A-C44A \\sim C49-C44
 with sigma of 0.02
3. Rigid bond restraints
 Si6, Si6A
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
 C11, C11A, C12, C12A, C13, C13A
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01
4. Uiso/Uaniso restraints and constraints
C5 \\sim C5A \\sim C6 \\sim C6A \\sim C7 \\sim C7A \\sim C8 \\sim C8A \\sim C9
\\sim C9A \\sim C10 \\sim C10A: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02 within 2A
N1 \\sim N1A \\sim N2 \\sim N2A \\sim C4 \\sim C4A: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
Si1 \\sim Si1A \\sim Si2 \\sim Si2A: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02 within 2A
C11 \\sim C11A \\sim C12A \\sim C13: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02 within 2A
C1 \\sim C1A \\sim C2A \\sim C3 \\sim C3A: within 2A with sigma of 0.01 and
sigma for terminal atoms of 0.02 within 2A
C1 \\sim C1A \\sim C3 \\sim C3A: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02 within 2A
C11 \\sim C11A \\sim C12A \\sim C13 \\sim C13A: within 2A with sigma of 0.01
and sigma for terminal atoms of 0.02 within 2A
C11A \\sim C12A \\sim C13A: within 2A with sigma of 0.01 and sigma for terminal
atoms of 0.02 within 2A
C11 \\sim C12A: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
All non-hydrogen atoms have similar U: within 2A with sigma of 0.04 and sigma
for terminal atoms of 0.08 within 2A
C14 \\sim C14A \\sim C15 \\sim C15A \\sim C16 \\sim C16A: within 2A with sigma
of 0.01 and sigma for terminal atoms of 0.02 within 2A
C1 \\sim C1A \\sim C2 \\sim C2A \\sim C3 \\sim C3A: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
C40 \\sim C40A \\sim C41 \\sim C41A \\sim C42 \\sim C42A: within 2A with sigma
of 0.01 and sigma for terminal atoms of 0.02 within 2A
Si7 \\sim Si7A: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
Si1 \\sim Si1A: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
Si3 \\sim Si3A: within 2A with sigma of 0.005 and sigma for terminal atoms of
0.01 within 2A
C37 \\sim C37A \\sim C38 \\sim C38A \\sim C39 \\sim C39A: within 2A with sigma
of 0.01 and sigma for terminal atoms of 0.02 within 2A
Si6 \\sim Si6A: within 2A with sigma of 0.001 and sigma for terminal atoms of
0.002 within 2A
C11 \\sim C11A \\sim C12 \\sim C12A \\sim C13: within 2A with sigma of 0.01 and
sigma for terminal atoms of 0.02 within 2A
C11 \\sim C11A \\sim C12 \\sim C12A \\sim C13 \\sim C13A: within 2A with sigma
of 0.01 and sigma for terminal atoms of 0.02 within 2A
C18 \\sim C18A \\sim C19 \\sim C19A \\sim C20 \\sim C20A \\sim C21 \\sim C21A
\\sim C22 \\sim C22A \\sim C23 \\sim C23A: within 2A with sigma of 0.01 and
sigma for terminal atoms of 0.02 within 2A
C31 \\sim C31A \\sim C32 \\sim C32A \\sim C33 \\sim C33A \\sim C34 \\sim C34A
\\sim C35 \\sim C35A \\sim C36 \\sim C36A: within 2A with sigma of 0.01 and
sigma for terminal atoms of 0.02 within 2A
N7 \\sim N7A \\sim N8 \\sim C43 \\sim C43A \\sim C44 \\sim C44A \\sim C45 \\sim
C45A \\sim C46 \\sim C46A \\sim C47 \\sim C47A \\sim C48 \\sim C48A \\sim C49
\\sim C49A: within 2A with sigma of 0.05 and sigma for terminal atoms of 0.1
within 2A
N7 \\sim N7A \\sim N8 \\sim C43 \\sim C43A \\sim C44 \\sim C44A \\sim C45 \\sim
C45A \\sim H45A \\sim C46 \\sim C46A \\sim C47 \\sim C47A \\sim C48 \\sim C48A
\\sim C49 \\sim C49A: within 2A with sigma of 0.02 and sigma for terminal atoms
of 0.04 within 2A
N8: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
Uanis(Si6) \\sim Ueq, Uanis(Si6A) \\sim Ueq: with sigma of 0.05 and sigma for
terminal atoms of 0.1
Uanis(Si6) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01
Uanis(C13) \\sim Ueq, Uanis(C11A) \\sim Ueq, Uanis(C11) \\sim Ueq, Uanis(C12)
\\sim Ueq, Uanis(C12A) \\sim Ueq, Uanis(C13A) \\sim Ueq: with sigma of 0.1 and
sigma for terminal atoms of 0.2
Uanis(C39A) \\sim Ueq, Uanis(C38) \\sim Ueq, Uanis(C37A) \\sim Ueq, Uanis(C39)
\\sim Ueq, Uanis(C38A) \\sim Ueq, Uanis(C37) \\sim Ueq: with sigma of 0.01 and
sigma for terminal atoms of 0.02
Uanis(C12A) \\sim Ueq, Uanis(C13) \\sim Ueq, Uanis(C11A) \\sim Ueq, Uanis(C11)
\\sim Ueq, Uanis(C12) \\sim Ueq, Uanis(C13A) \\sim Ueq: with sigma of 0.01 and
sigma for terminal atoms of 0.02
Uanis(Si1A) \\sim Ueq, Uanis(Si1) \\sim Ueq: with sigma of 0.01 and sigma for
terminal atoms of 0.02
Uanis(C12A) \\sim Ueq, Uanis(C13A) \\sim Ueq, Uanis(C11A) \\sim Ueq, Uanis(C13)
\\sim Ueq, Uanis(C12) \\sim Ueq, Uanis(C11) \\sim Ueq: with sigma of 0.01 and
sigma for terminal atoms of 0.02
Uanis(C11) \\sim Ueq, Uanis(C12) \\sim Ueq, Uanis(C13) \\sim Ueq: with sigma of
0.005 and sigma for terminal atoms of 0.01
Uanis(C12A) \\sim Ueq, Uanis(C13A) \\sim Ueq, Uanis(C11A) \\sim Ueq: with sigma
of 0.005 and sigma for terminal atoms of 0.01
Uanis(C43A) \\sim Ueq, Uanis(C45A) \\sim Ueq, Uanis(C46A) \\sim Ueq,
Uanis(C47A) \\sim Ueq, Uanis(C48A) \\sim Ueq, Uanis(C49A) \\sim Ueq,
Uanis(C44A) \\sim Ueq: with sigma of 0.1 and sigma for terminal atoms of 0.2
Uanis(N8) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
5. Others
 Sof(Si1A)=Sof(Si2A)=Sof(N1A)=Sof(N2A)=Sof(C1A)=Sof(H1AA)=Sof(H1AB)=Sof(H1AC)=
 Sof(C2A)=Sof(H2AA)=Sof(H2AB)=Sof(H2AC)=Sof(C3A)=Sof(H3AA)=Sof(H3AB)=Sof(H3AC)=
 Sof(C4A)=Sof(C5A)=Sof(C6A)=Sof(H6A)=Sof(C7A)=Sof(H7A)=Sof(C8A)=Sof(H8A)=
 Sof(C9A)=Sof(H9A)=Sof(C10A)=Sof(H10A)=Sof(C11A)=Sof(H11D)=Sof(H11E)=Sof(H11F)=
 Sof(C12A)=Sof(H12D)=Sof(H12E)=Sof(H12F)=Sof(C13A)=Sof(H13D)=Sof(H13E)=
 Sof(H13F)=1-FVAR(1)
 Sof(Si1)=Sof(Si2)=Sof(N1)=Sof(N2)=Sof(C1)=Sof(H1A)=Sof(H1B)=Sof(H1C)=Sof(C2)=
 Sof(H2A)=Sof(H2B)=Sof(H2C)=Sof(C3)=Sof(H3A)=Sof(H3B)=Sof(H3C)=Sof(C4)=Sof(C5)=
 Sof(C6)=Sof(H6)=Sof(C7)=Sof(H7)=Sof(C8)=Sof(H8)=Sof(C9)=Sof(H9)=Sof(C10)=
 Sof(H10)=Sof(C11)=Sof(H11A)=Sof(H11B)=Sof(H11C)=Sof(C12)=Sof(H12A)=Sof(H12B)=
 Sof(H12C)=Sof(C13)=Sof(H13A)=Sof(H13B)=Sof(H13C)=FVAR(1)
 Sof(Si3A)=Sof(Si4A)=Sof(C14A)=Sof(H14D)=Sof(H14E)=Sof(H14F)=Sof(C15A)=
 Sof(H15D)=Sof(H15E)=Sof(H15F)=Sof(C16A)=Sof(H16D)=Sof(H16E)=Sof(H16F)=
 Sof(C18A)=Sof(C19A)=Sof(H19A)=Sof(C20A)=Sof(H20A)=Sof(C21A)=Sof(H21A)=
 Sof(C22A)=Sof(H22A)=Sof(C23A)=Sof(H23A)=Sof(C24A)=Sof(H24D)=Sof(H24E)=
 Sof(H24F)=Sof(C25A)=Sof(H25D)=Sof(H25E)=Sof(H25F)=Sof(C26A)=Sof(H26D)=
 Sof(H26E)=Sof(H26F)=1-FVAR(2)
 Sof(Si3)=Sof(Si4)=Sof(C14)=Sof(H14A)=Sof(H14B)=Sof(H14C)=Sof(C15)=Sof(H15A)=
 Sof(H15B)=Sof(H15C)=Sof(C16)=Sof(H16A)=Sof(H16B)=Sof(H16C)=Sof(C18)=Sof(C19)=
 Sof(H19)=Sof(C20)=Sof(H20)=Sof(C21)=Sof(H21)=Sof(C22)=Sof(H22)=Sof(C23)=
 Sof(H23)=Sof(C24)=Sof(H24A)=Sof(H24B)=Sof(H24C)=Sof(C25)=Sof(H25A)=Sof(H25B)=
 Sof(H25C)=Sof(C26)=Sof(H26A)=Sof(H26B)=Sof(H26C)=FVAR(2)
 Sof(Si6A)=Sof(C31A)=Sof(C36A)=Sof(H36A)=Sof(C35A)=Sof(H35A)=Sof(C34A)=
 Sof(H34A)=Sof(C33A)=Sof(H33A)=Sof(C32A)=Sof(H32A)=Sof(C37A)=Sof(H37D)=
 Sof(H37E)=Sof(H37F)=Sof(C38A)=Sof(H38D)=Sof(H38E)=Sof(H38F)=Sof(C39A)=
 Sof(H39D)=Sof(H39E)=Sof(H39F)=1-FVAR(3)
 Sof(Si6)=Sof(C31)=Sof(C36)=Sof(H36)=Sof(C35)=Sof(H35)=Sof(C34)=Sof(H34)=
 Sof(C33)=Sof(H33)=Sof(C32)=Sof(H32)=Sof(C37)=Sof(H37A)=Sof(H37B)=Sof(H37C)=
 Sof(C38)=Sof(H38A)=Sof(H38B)=Sof(H38C)=Sof(C39)=Sof(H39A)=Sof(H39B)=Sof(H39C)=
 FVAR(3)
 Sof(Si7A)=Sof(N7A)=Sof(C40A)=Sof(H40D)=Sof(H40E)=Sof(H40F)=Sof(C41A)=
 Sof(H41D)=Sof(H41E)=Sof(H41F)=Sof(C42A)=Sof(H42D)=Sof(H42E)=Sof(H42F)=
 Sof(C43A)=Sof(C44A)=Sof(C45A)=Sof(H45A)=Sof(C46A)=Sof(H46A)=Sof(C47A)=
 Sof(H47A)=Sof(C48A)=Sof(H48A)=Sof(C49A)=Sof(H49A)=1-FVAR(4)
 Sof(Si7)=Sof(N7)=Sof(C40)=Sof(H40A)=Sof(H40B)=Sof(H40C)=Sof(C41)=Sof(H41A)=
 Sof(H41B)=Sof(H41C)=Sof(C42)=Sof(H42A)=Sof(H42B)=Sof(H42C)=Sof(C43)=Sof(C44)=
 Sof(C45)=Sof(H45)=Sof(C46)=Sof(H46)=Sof(C47)=Sof(H47)=Sof(C48)=Sof(H48)=
 Sof(C49)=Sof(H49)=FVAR(4)
6.a Secondary CH2 refined with riding coordinates:
 C53(H53A,H53B), C54(H54A,H54B), C55(H55A,H55B), C56(H56A,H56B)
6.b Aromatic/amide H refined with riding coordinates:
 C6(H6), C7(H7), C8(H8), C9(H9), C10(H10), C6A(H6A), C7A(H7A), C8A(H8A),
 C9A(H9A), C10A(H10A), C19(H19), C20(H20), C21(H21), C22(H22), C23(H23),
 C19A(H19A), C20A(H20A), C21A(H21A), C22A(H22A), C23A(H23A), C36(H36), C35(H35),
  C34(H34), C33(H33), C32(H32), C36A(H36A), C35A(H35A), C34A(H34A), C33A(H33A),
 C32A(H32A), C45(H45), C45A(H45A), C46(H46), C46A(H46A), C47(H47), C47A(H47A),
 C48(H48), C48A(H48A), C49(H49), C49A(H49A)
6.c Fitted hexagon refined as free rotating group:
 C5(C6,C7,C8,C9,C10), C18(C19,C20,C21,C22,C23), C18A(C19A,C20A,C21A,C22A,C23A),
  C31(C36,C35,C34,C33,C32), C31A(C36A,C35A,C34A,C33A,C32A)
6.d Idealised Me refined as rotating group:
 C1(H1A,H1B,H1C), C1A(H1AA,H1AB,H1AC), C2(H2A,H2B,H2C), C2A(H2AA,H2AB,H2AC),
 C3(H3A,H3B,H3C), C3A(H3AA,H3AB,H3AC), C11(H11A,H11B,H11C), C11A(H11D,H11E,
 H11F), C12(H12A,H12B,H12C), C12A(H12D,H12E,H12F), C13(H13A,H13B,H13C),
 C13A(H13D,H13E,H13F), C14(H14A,H14B,H14C), C14A(H14D,H14E,H14F), C15(H15A,H15B,
 H15C), C15A(H15D,H15E,H15F), C16(H16A,H16B,H16C), C16A(H16D,H16E,H16F),
 C24(H24A,H24B,H24C), C24A(H24D,H24E,H24F), C25(H25A,H25B,H25C), C25A(H25D,H25E,
 H25F), C26(H26A,H26B,H26C), C26A(H26D,H26E,H26F), C27(H27A,H27B,H27C),
 C28(H28A,H28B,H28C), C29(H29A,H29B,H29C), C37(H37A,H37B,H37C), C37A(H37D,H37E,
 H37F), C38(H38A,H38B,H38C), C38A(H38D,H38E,H38F), C39(H39A,H39B,H39C),
 C39A(H39D,H39E,H39F), C40(H40A,H40B,H40C), C40A(H40D,H40E,H40F), C41(H41A,H41B,
 H41C), C41A(H41D,H41E,H41F), C42(H42A,H42B,H42C), C42A(H42D,H42E,H42F),
 C50(H50A,H50B,H50C), C51(H51A,H51B,H51C), C52(H52A,H52B,H52C)
;
_olex2_submission_special_instructions 'No special instructions were received'