Rearrangements of 3H-PyrazolesAdducts of Dimethyl Acetylenedicarboxylate with Diphenyldiazomethane and 9-Diazofluorene
Vasin, V.A.; Razin, V.V.; Bezrukova, E.V.; Popkova, Yu.A.; Somov, N.V.; Russian Journal of Organic Chemistry 54 (2018) 892–900; doi:10.1134/S1070428018060118

data_4038964
_publ_section_title
;
 Rearrangements of 3H-PyrazolesAdducts of Dimethyl Acetylenedicarboxylate
 with Diphenyldiazomethane and 9-Diazofluorene
;
_journal_issue                   6
_journal_name_full
;
 Russian Journal of Organic Chemistry
;
_journal_page_first              892
_journal_page_last               900
_journal_paper_doi               10.1134/S1070428018060118
_journal_volume                  54
_journal_year                    2018
_chemical_formula_sum            'C19 H16 N2 O4'
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'CrysAlisPro convention (1999,Acta A55,543-557)'
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;
        CrysAlisPro 1.171.39.8e (Rigaku Oxford Diffraction, 2015)
        Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
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'w=1/[\s^2^(Fo^2^)+(0.0827P)^2^+0.0526P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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