Tetrapotassium tetrahydrogen-β-hexamolybdoplatinate(IV) dihydrate, K~4~[H~4~β-PtMo~6~O~24~].2H~2~O
Joo, H.C.; Park, K.M.; Lee, U.; Acta Crystallographica Section C 50 (1994) 1659–1661; doi:10.1107/S0108270194004816

data_2010166
_publ_section_title
;
 Tetrapotassium tetrahydrogen-\b-hexamolybdoplatinate(IV) dihydrate,
 K~4~[H~4~\b-PtMo~6~O~24~].2H~2~O
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_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1659
_journal_page_last               1661
_journal_paper_doi               10.1107/S0108270194004816
_journal_volume                  50
_journal_year                    1994
_chemical_formula_moiety         'H4 K4 Mo6 O24 Pt,2(H2 O1)'
_chemical_formula_sum            'H8 K4 Mo6 O26 Pt'
_chemical_formula_weight         1351.47
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                113.680(10)
_cell_angle_beta                 110.540(10)
_cell_angle_gamma                81.970(10)
_cell_formula_units_Z            2
_cell_length_a                   10.636(2)
_cell_length_b                   12.041(2)
_cell_length_c                   10.5670(10)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    298
_cell_measurement_theta_max      19.98
_cell_measurement_theta_min      19.895
_cell_volume                     1160.6(3)
_diffrn_measurement_device       'Rigaku AFC-5S'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0053
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            10231
_diffrn_reflns_theta_max         35
_diffrn_standards_decay_%        <1
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    9.76
_exptl_absorpt_correction_T_max  0.647
_exptl_absorpt_correction_T_min  0.213
_exptl_crystal_colour            'Lemon yellow'
_exptl_crystal_density_diffrn    3.87
_exptl_crystal_description       'hexagonal prism'
_exptl_crystal_size_max          0.3
_exptl_crystal_size_mid          0.3
_exptl_crystal_size_min          0.1
_refine_diff_density_max         3.26
_refine_diff_density_min         -4.15
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   3.84
_refine_ls_number_parameters     335
_refine_ls_number_reflns         9170
_refine_ls_R_factor_obs          0.044
_refine_ls_shift/esd_max         0.068
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(|F~o~|) + |0.02F~o~|^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.058
_reflns_number_observed          9126
_reflns_number_total             9170
_reflns_observed_criterion       I>3.0\s(I)
_cod_data_source_file            du1074.cif
_cod_data_source_block           du1074_structure_1_of_1
_cod_depositor_comments
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The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'w = 1/[\s^2^(|F~o~|) +
|0.02F~o~|^2^]' was changed to 'calc'. New tag
'_refine_ls_weighting_details' was created. The value of the new tag
was set to 'w = 1/[\s^2^(|F~o~|) + |0.02F~o~|^2^]'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
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_cod_original_formula_sum        'H8 K4 Mo6 O26 Pt1'
_cod_database_code               2010166