Tripodal Amido Boron and Aluminum Complexes
Hongping Zhu; Eugene Y.-X. Chen; Inorganic Chemistry 46 (2007) 1481–1487; doi:10.1021/ic0620889

data_4307608
_publ_section_title
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Tripodal Amido Boron and Aluminum Complexes
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_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1481
_journal_page_last               1487
_journal_paper_doi               10.1021/ic0620889
_journal_volume                  46
_journal_year                    2007
_chemical_formula_sum            'C32 H48 Al N3 O Si3'
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_chemical_name_systematic
; 
 ? 
;
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_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
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_diffrn_reflns_limit_h_min       -22
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_diffrn_reflns_limit_k_min       -23
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_diffrn_reflns_limit_l_min       -29
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_diffrn_reflns_theta_max         35.04
_diffrn_reflns_theta_min         1.16
_exptl_absorpt_coefficient_mu    0.198
_exptl_absorpt_correction_T_max  0.9469
_exptl_absorpt_correction_T_min  0.9304
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS, Sheldrick, 1997'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.199
_exptl_crystal_density_meas      ?
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_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0592P)^2^+1.0862P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1083
_refine_ls_wR_factor_ref         0.1216
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_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic0620889si20061101_052151_4.cif
_cod_data_source_block           complex_6
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
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_cod_original_cell_volume        3335.1(2)
_cod_database_code               4307608