Diastereoselective synthesis of spiro[carbazole-3,5'-pyrimidines] and spiro[carbazole-3,1'-cyclohexanes] <i>via</i> four-component reaction.
Zhan, Shao-Cong; Fang, Ren-Jie; Sun, Jing; Yan, Chao-Guo; Organic & biomolecular chemistry 19 (2021) 6322–6327; doi:10.1039/d1ob01113h

data_7158141
_publ_section_title
;
 Diastereoselective synthesis of spiro[carbazole-3,5'-pyrimidines] and
 spiro[carbazole-3,1'-cyclohexanes] <i>via</i> four-component reaction.
;
_journal_issue                   28
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              6322
_journal_page_last               6327
_journal_paper_doi               10.1039/d1ob01113h
_journal_volume                  19
_journal_year                    2021
_chemical_formula_moiety         'C34 H31 N3 O8'
_chemical_formula_sum            'C34 H31 N3 O8'
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_audit_update_record
;
2021-04-20 deposited with the CCDC.	2021-06-22 downloaded from the CCDC.
;
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_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
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_diffrn_measured_fraction_theta_max 0.973
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1043P)^2^+2.4570P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                3219
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d1ob01113h2.cif
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_cod_depositor_comments
'Adding full bibliography for 7158139--7158148.cif.'
_cod_original_cell_volume        1708.79(17)
_cod_database_code               7158141
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_shelx_res_checksum              25250
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