Aza-tricycles containing a perfluoroalkyl group: synthesis, structure and fluorescence.
Fu, Qiang; Wang, Rui; Liang, Fushun; Guan, Wei; Organic & biomolecular chemistry 16 (2018) 8950–8954; doi:10.1039/c8ob02749h

data_7156571
_publ_section_title
;
 Aza-tricycles containing a perfluoroalkyl group: synthesis, structure and
 fluorescence.
;
_journal_issue                   46
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              8950
_journal_page_last               8954
_journal_paper_doi               10.1039/c8ob02749h
_journal_volume                  16
_journal_year                    2018
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_space_group_name_Hall           '-P 2ybc'
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_symmetry_space_group_name_Hall  '-P 2ybc'
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_audit_update_record
;
2017-10-05 deposited with the CCDC.
2018-11-13 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_refine_diff_density_max         3.133
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_refine_ls_extinction_coef       0.006(2)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2014/7 (Sheldrick 2014'
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_refine_ls_shift/su_mean         0.102
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_total             2926
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c8ob02749h2.cif
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'Adding full bibliography for 7156570--7156572.cif.'
_cod_database_code               7156571
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