Solid-state structures of the covalent hydrides germane and stannane
Maley, Iain J.; Brown, Daniel H.; Ibberson, Richard M.; Pulham, Colin R.; Acta Crystallographica Section B 64 (2008) 312–317; doi:10.1107/S0108768108010379

data_2104156
_publ_section_title
;
 Solid-state structures of the covalent hydrides germane and stannane
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              312
_journal_page_last               317
_journal_paper_doi               10.1107/S0108768108010379
_journal_volume                  64
_journal_year                    2008
_chemical_formula_moiety         'D4  Sn'
_chemical_formula_sum            'D4 Sn'
_chemical_formula_weight         126.75
_chemical_melting_point          123
_chemical_name_common            stannane
_chemical_name_systematic
;
perdeuterostannane
;
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_cell_angle_gamma                90.0
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_cell_length_c                   8.75705(12)
_cell_measurement_temperature    5
_cell_volume                     308.219(9)
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_computing_data_collection       'ISIS instrument control program (ICP)'
_computing_data_reduction        'Standard HRPD normalisation routines'
_computing_structure_refinement  TOPAS
_diffrn_measurement_device_type  HRPD
_diffrn_radiation_probe          neutron
_diffrn_radiation_type           'time-of-flight neutron'
_diffrn_radiation_wavelength     1.24-5.36
_exptl_crystal_density_diffrn    2.731
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_refine_ls_goodness_of_fit_all   2.03
_refine_ls_hydrogen_treatment    refall
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_refine_ls_number_parameters     35
_refine_ls_number_restraints     0
_refine_ls_shift/su_max          0.02
_refine_ls_shift/su_mean         0.00
_refine_ls_weighting_scheme      sigma
_cod_data_source_file            ws5063.cif
_cod_data_source_block           SnD4_5K
_cod_depositor_comments
;
The following automatic conversions were performed:
'_geom_bond_publ_flag' value 'N' changed to 'n' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29 (4
times).

'_geom_angle_publ_flag' value 'N' changed to 'n' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29 (6 times).

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_geom_bond_publ_flag' value 'N' changed to 'n' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29 (4
times).

'_geom_angle_publ_flag' value 'N' changed to 'n' according
to /home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary
named 'cif_core.dic' version 2.4.1 from 2010-06-29 (6 times).

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        308.220(10)
_cod_original_sg_symbol_Hall     '-C 2yc '
_cod_original_sg_symbol_H-M      C2/c
_cod_original_formula_sum        'D4  Sn'
_cod_database_code               2104156