Neutron and X-ray diffraction study of ferrite nanocrystals obtained by microwave-assisted growth. A structural comparison with the thermal synthetic route
Solano, Eduardo; Frontera, Carlos; Puig, Teresa; Obradors, Xavier; Ricart, Susagna; Ros, Josep; Journal of Applied Crystallography 47 (2014) 414–420; doi:10.1107/S1600576713032895

data_2300615
_publ_section_title
;
 Neutron and X-ray diffraction study of ferrite nanocrystals obtained by
 microwave-assisted growth. A structural comparison with the thermal
 synthetic route
;
_journal_coeditor_code           kk5153
_journal_issue                   1
_journal_name_full               'Journal of Applied Crystallography'
_journal_page_first              414
_journal_page_last               420
_journal_paper_doi               10.1107/S1600576713032895
_journal_volume                  47
_journal_year                    2014
_chemical_formula_sum            'Fe2 O4 Zn'
_chemical_formula_weight         241.072
_chemical_name_systematic
;
Fe2O4Zn1
;
_space_group_IT_number           227
_symmetry_cell_setting           cubic
_symmetry_space_group_name_Hall  '-F 4vw 2vw 3'
_symmetry_space_group_name_H-M   'F d -3 m :2'
_cell_angle_alpha                90.00000
_cell_angle_beta                 90.00000
_cell_angle_gamma                90.00000
_cell_formula_units_Z            8
_cell_length_a                   8.3910(4)
_cell_length_b                   8.3910(4)
_cell_length_c                   8.3910(4)
_cell_measurement_temperature    300
_cell_volume                     590.80(5)
_computing_structure_refinement  FULLPROF
_diffrn_ambient_temperature      300
_diffrn_radiation_type           'Constant Wavelength Neutron Diffraction'
_diffrn_radiation_wavelength     2.52268
_diffrn_source                   'nuclear reactor'
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.100078
_pd_meas_2theta_range_max        128.69000
_pd_meas_2theta_range_min        0.79000
_pd_meas_number_of_points        1280
_pd_proc_2theta_range_inc        0.100078
_pd_proc_2theta_range_max        128.9662
_pd_proc_2theta_range_min        1.0662
_pd_proc_ls_pref_orient_corr     ' ?'
_pd_proc_ls_prof_R_factor        0.9393
_pd_proc_ls_prof_wR_expected     0.8140
_pd_proc_ls_prof_wR_factor       1.1978
_pd_proc_wavelength              2.522680
_pd_spec_mounting                ' ?'
_refine_ls_number_parameters     23
_refine_ls_number_reflns         95
_refine_ls_number_restraints     0
_refine_ls_R_I_factor            0.9945
_cod_data_source_file            kk5153sup1.cif
_cod_data_source_block           ZnFe2O4
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Cubic' changed to 'cubic' according
to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/IUCr/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4268 2015-11-12 08:31:59Z antanas 
;
_cod_original_sg_symbol_H-M      'F d -3 m'
_cod_original_formula_sum        'Fe2 O4 Zn1 '
_cod_database_code               2300615
_publcif_datablock.id            {2d0f1cd0-6630-42f1-89fd-b2c860cebf08}
_pd_proc_ls_prof_cr_factor       9.2702
_pd_proc_ls_prof_cwr_factor      7.2818
_pd_proc_ls_prof_cwr_expected    4.9488
_pd_proc_ls_prof_chi2            2.1651
_pd_proc_ls_prof_echi2           2.1651
_refine_ls_goodenes_of_fit_all   1.4714
_publcif_info_exptl_table_max_cols 4
_publcif_info_exptl_table_use_headnotes n
_cod_database_fobs_code 2300615