A diphenylformamidinate-bridged terpyridineplatinum(II) dimer
Bailey, J. A.; Miskowski, V. M.; Gray, H. B.; Acta Crystallographica Section C 49 (1993) 793–796; doi:10.1107/S0108270192010229

data_2001813
_publ_section_title
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 A diphenylformamidinate-bridged terpyridineplatinum(II) dimer
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_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              793
_journal_page_last               796
_journal_paper_doi               10.1107/S0108270192010229
_journal_volume                  49
_journal_year                    1993
_chemical_formula_sum            'C43 H35 Cl3 N8 O13 Pt2'
_chemical_formula_weight         1368.33
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2c -2n'
_symmetry_space_group_name_H-M   'P n a 21'
_atom_type_scat_source           'Cromer (1974); Cromer & Waber (1974)'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   13.409(3)
_cell_length_b                   20.196(5)
_cell_length_c                   16.517(4)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    295
_cell_measurement_theta_max      14
_cell_measurement_theta_min      13
_cell_volume                     4472.9(18)
_diffrn_measurement_device       CAD-4
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.008
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            14036
_diffrn_reflns_theta_max         20
_diffrn_standards_decay_%        0
_diffrn_standards_number         4
_exptl_absorpt_coefficient_mu    65.61
_exptl_absorpt_correction_type   'empirical [0.885 to 1.169 (relative)]'
_exptl_crystal_colour            'deep red'
_exptl_crystal_density_diffrn    2.03
_exptl_crystal_description       'irregular parallelepiped'
_exptl_crystal_size_max          0.27
_exptl_crystal_size_mid          0.23
_exptl_crystal_size_min          0.21
_refine_diff_density_max         0.74
_refine_diff_density_min         -0.72
_refine_ls_extinction_coef       0.258E-6(6)
_refine_ls_extinction_method     'Larson (1967)'
_refine_ls_goodness_of_fit_obs   2.07
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     487
_refine_ls_number_reflns         4175
_refine_ls_R_factor_obs          0.030
_refine_ls_shift/esd_max         '0.23 for O12; 0.13 for all others'
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     'w = 1/\s^2^(F~o~^2^)'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.003
_reflns_number_observed          4175
_reflns_number_total             4176
_reflns_observed_criterion       All
_cod_data_source_file            sp1005.cif
_cod_data_source_block           sp1005_structure_1_of_1
_cod_depositor_comments
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The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value '1/\s^2^(F~o~^2^)' was changed to
'calc'. New tag '_refine_ls_weighting_details' was created. The value
of the new tag was set to 'w = 1/\s^2^(F~o~^2^)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
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_cod_database_code               2001813