Hydrodeoxygenative Cyclotetramerization of Carbon Monoxide by a Trinuclear Titanium Polyhydride Complex.
Hu, Shaowei; Shima, Takanori; Hou, Zhaomin; Journal of the American Chemical Society 142 (2020) 19889–19894; doi:10.1021/jacs.0c10403

data_4135352
_publ_section_title
;
 Hydrodeoxygenative Cyclotetramerization of Carbon Monoxide by a
 Trinuclear Titanium Polyhydride Complex.
;
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_journal_name_full               'Journal of the American Chemical Society'
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_journal_page_last               19894
_journal_paper_doi               10.1021/jacs.0c10403
_journal_volume                  142
_journal_year                    2020
_chemical_formula_sum            'C41 H70 O5 Si3 Ti3'
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2018-09-10 # Formatted by publCIF

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;
 Flack x determined using 2654 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0481P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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'Adding full bibliography for 4135351--4135354.cif.'
_cod_original_cell_volume        1177.2(4)
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