Schiff Bases and Their Complexes with Metal Ions. I. 2-Hydroxy-<i>N</i>-<i>n</i>-propyl-1-naphthaldimine (1) and Bis(2-hydroxy-κ<i>O</i>-<i>N</i>-<i>n</i>-propyl-1-naphthaldiminato-κ<i>N</i>)nickel(II) (2)
Hökelek, T.; Gündüz, N.; Hayvali, Z.; Kilic, Z.; Acta Crystallographica Section C 51 (1995) 880–884; doi:10.1107/S0108270194009480

data_2003409
_publ_section_title
;Schiff Bases and Their Complexes with Metal Ions. I.
 2-Hydroxy-<i>N</i>-<i>n</i>-propyl-1-naphthaldimine (1) and
 Bis(2-hydroxy-\k<i>O</i>-<i>N</i>-<i>n</i>-propyl-1-naphthaldiminato-\k<i>N</i>)nickel(II)
 (2)
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              880
_journal_page_last               884
_journal_paper_doi               10.1107/S0108270194009480
_journal_volume                  51
_journal_year                    1995
_chemical_formula_sum            'C14 H15 N O'
_chemical_formula_weight         213.28
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90
_cell_angle_beta                 96.41(4)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   10.167(5)
_cell_length_b                   8.797(3)
_cell_length_c                   13.155(7)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293
_cell_measurement_theta_max      15
_cell_measurement_theta_min      10
_cell_volume                     1169.2(9)
_diffrn_measurement_device       CAD-4
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54180
_diffrn_reflns_av_R_equivalents  'not calculated'
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -1
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -1
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            3390
_diffrn_reflns_theta_max         75
_diffrn_standards_decay_%        1
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.56
_exptl_absorpt_correction_T_max  1.00
_exptl_absorpt_correction_T_min  0.909
_exptl_absorpt_correction_type   'empirical (North, Phillips & Mathews, 1968)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.212
_exptl_crystal_description       prismatic
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.30
_refine_diff_density_max         0.26
_refine_diff_density_min         -0.35
_refine_ls_extinction_method     none
_refine_ls_hydrogen_treatment
'H atoms positioned geometrically and not refined'
_refine_ls_number_parameters     145
_refine_ls_number_reflns         581
_refine_ls_R_factor_obs          0.055
_refine_ls_shift/esd_max         0.005
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      'Weighting scheme: see text'
_refine_ls_wR_factor_obs         0.064
_reflns_number_observed          777
_reflns_number_total             1683
_reflns_observed_criterion       F>=3\s(F)
_cod_data_source_file            ab1153.cif
_cod_data_source_block           1
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               2003409