Studies on Pd-catalyzed asymmetric hydroesterification of enimides. A possible approach to optically active β-amino acid derivatives
Li, Junhua; Yang, Yan; Wang, Zichu; Shi, Yian; New Journal of Chemistry 46 (2022) 9507–9510; doi:10.1039/D2NJ01027E

data_7061491
_publ_section_title
;
 Studies on Pd-catalyzed asymmetric hydroesterification of enimides. A
 possible approach to optically active \b-amino acid derivatives
;
_journal_issue                   20
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              9507
_journal_page_last               9510
_journal_paper_doi               10.1039/D2NJ01027E
_journal_volume                  46
_journal_year                    2022
_chemical_absolute_configuration ad
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_audit_update_record
;
2021-08-27 deposited with the CCDC.	2022-04-25 downloaded from the CCDC.
;
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_cell_volume                     2010.6(10)
_computing_cell_refinement       'Bruker SAINT'
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; 
 Flack x determined using 2103 quotients [(I+)-(I-)]/[(I+)+(I-)] 
 (Parsons and Flack (2004), Acta Cryst. A60, s61). 
;
_refine_ls_abs_structure_Flack   0.06(5)
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_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     SHELXL
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_refine_ls_shift/su_mean         0.003
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.1228P)^2^+0.3590P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_Friedel_fraction_full    0.599
_reflns_Friedel_fraction_max     0.592
_reflns_number_gt                6025
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_cod_depositor_comments          'Adding full bibliography for 7061491.cif.'
_cod_database_code               7061491
_shelx_estimated_absorpt_t_min   0.964
_shelx_estimated_absorpt_t_max   0.976
_shelxl_version_number           2013-4
_shelx_res_checksum              65550