Ethylenediamine complexes of the beryllium halides and pseudo-halides.
Buchner, Magnus R.; Müller, Matthias; Dalton transactions (Cambridge, England : 2003) 50 (2021) 7246–7255; doi:10.1039/d1dt01154e

data_7707223
_publ_section_title
;
 Ethylenediamine complexes of the beryllium halides and pseudo-halides.
;
_journal_issue                   21
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7246
_journal_page_last               7255
_journal_paper_doi               10.1039/d1dt01154e
_journal_volume                  50
_journal_year                    2021
_chemical_formula_sum            'C6 H24 Be Br2 N6'
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_audit_update_record
;
2021-04-07 deposited with the CCDC.	2021-04-27 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'STOE STADIVARI'
_diffrn_measurement_method       'rotation method, \w scans'
_diffrn_radiation_type           CuK\a
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_diffrn_reflns_av_unetI/netI     0.0126
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_diffrn_reflns_theta_min         3.575
_diffrn_source                   'GeniX 3D HF Cu'
_exptl_absorpt_coefficient_mu    7.061
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            colorless
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_exptl_crystal_description       block
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_exptl_crystal_size_max          0.06
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_exptl_crystal_size_min          0.045
_exptl_transmission_factor_max   0.7404
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_refine_diff_density_max         0.511
_refine_diff_density_min         -0.531
_refine_diff_density_rms         0.072
_refine_ls_extinction_coef       0.00114(19)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2014/7 (Sheldrick 2014'
_refine_ls_goodness_of_fit_ref   1.067
_refine_ls_hydrogen_treatment    mixed
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_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.067
_refine_ls_R_factor_all          0.0238
_refine_ls_R_factor_gt           0.0215
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0341P)^2^+0.4703P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0543
_refine_ls_wR_factor_ref         0.0556
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2683
_reflns_number_total             2883
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d1dt01154e2.cif
_cod_data_source_block           4
_cod_depositor_comments
'Adding full bibliography for 7707219--7707225.cif.'
_cod_database_code               7707223
_shelx_shelxl_version_number     2014/7
_shelx_res_checksum              94676
_shelx_hkl_checksum              92508