Copper(II)- and gold(III)-mediated cyclization of a thiourea to a substituted 2-aminobenzothiazole
Schroeder, Zachary W.; Hiscock, L. K.; Dawe, Louise Nicole; Acta Crystallographica Section C 73 (2017) 905–910; doi:10.1107/S205322961701381X

data_2020901
_publ_section_title
;
 Copper(II)- and gold(III)-mediated cyclization of a thiourea to a
 substituted 2-aminobenzothiazole
;
_journal_coeditor_code           YF3126
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              905
_journal_page_last               910
_journal_paper_doi               10.1107/S205322961701381X
_journal_volume                  73
_journal_year                    2017
_chemical_formula_iupac          '[Cu (C13 H11 N3 O1 S1)2 (H2 O)] (N O3)2'
_chemical_formula_moiety         'C26 H24 Cu N6 O3 S2 2+, 2(N O3 -)'
_chemical_formula_sum            'C26 H24 Cu N8 O9 S2'
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'Aquabis[5-methoxy-<i>N</i>-(pyridin-2-yl-\k<i>N</i>)benzothiazol-2-amine-\k<i>N</i>^3^]copper(II) dinitrate'
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<i>OLEX2</i> 1.2
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CrysAlis PRO (Rigaku OD, 2015)
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CrysAlis PRO (Rigaku OD, 2015)
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CrysAlis PRO (Rigaku OD, 2015)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>,  2009)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>,  2009)
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SHELXL2016 (Sheldrick, 2015b)
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SHELXT (Sheldrick, 2015a)
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;
(CrysAlis PRO; Rigaku OD, 2015)
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'w=1/[\s^2^(Fo^2^)+(0.0189P)^2^+9.2626P] where P=(Fo^2^+2Fc^2^)/3'
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