LMucko/crystallography-open-database huggingface dataset:
Chemistry of C-Trimethylsilyl-Substituted Heterocarboranes. 30. Synthetic and Structural Studies on Oxide Ion Encapsulating Tetralanthanide Tetrahedra Surrounded by "Carbons Apart" C2B4-Carborane Ligands (Ln(III) = La, Nd, Gd, Tb, Ho, Lu)
Wang, Jianhui; Li, Shoujian; Zheng, Chong; Li, Ang; Hosmane, Narayan S.; Maguire, John A.; Roesky, Herbert W.; Cummins, Christopher C.; Kaim, Wolfgang; Organometallics 23 (2004) 4621–4629; doi:10.1021/om0496176

data_4062756
_publ_section_title
;
 Chemistry of C-Trimethylsilyl-Substituted Heterocarboranes.
 30. Synthetic and Structural Studies on Oxide Ion Encapsulating
 Tetralanthanide Tetrahedra Surrounded by "Carbons Apart"
 C2B4-Carborane Ligands (Ln(III) = La, Nd, Gd, Tb, Ho, Lu)
;
_journal_coden_ASTM              ORGND7
_journal_issue                   20
_journal_name_full               Organometallics
_journal_page_first              4621
_journal_page_last               4629
_journal_paper_doi               10.1021/om0496176
_journal_volume                  23
_journal_year                    2004
_chemical_formula_sum            'C56 H136 B16 Cl2 Ho4 O7 Si8'
_chemical_formula_weight         2049.95
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 117.820(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   28.403(5)
_cell_length_b                   12.835(2)
_cell_length_c                   27.879(5)
_cell_measurement_temperature    173(2)
_cell_volume                     8989(3)
_diffrn_ambient_temperature      173(2)
_exptl_crystal_density_diffrn    1.515
_cod_depositor_comments
;
 Updated bibliographic information.

 Antanas Vaitkus,
 2019-09-24
;
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4062756
Chemistry of C-Trimethylsilyl-Substituted Heterocarboranes. 30. Synthetic and Structural Studies on Oxide Ion Encapsulating Tetralanthanide Tetrahedra Surrounded by "Carbons Apart" C2B4-Carborane Ligands (Ln(III) = La, Nd, Gd, Tb, Ho, Lu)
Wang, Jianhui; Li, Shoujian; Zheng, Chong; Li, Ang; Hosmane, Narayan S.; Maguire, John A.; Roesky, Herbert W.; Cummins, Christopher C.; Kaim, Wolfgang; Organometallics 23 (2004) 4621–4629; doi:10.1021/om0496176

data_4062757
_publ_section_title
;
 Chemistry of C-Trimethylsilyl-Substituted Heterocarboranes.
 30. Synthetic and Structural Studies on Oxide Ion Encapsulating
 Tetralanthanide Tetrahedra Surrounded by "Carbons Apart"
 C2B4-Carborane Ligands (Ln(III) = La, Nd, Gd, Tb, Ho, Lu)
;
_journal_coden_ASTM              ORGND7
_journal_issue                   20
_journal_name_full               Organometallics
_journal_page_first              4621
_journal_page_last               4629
_journal_paper_doi               10.1021/om0496176
_journal_volume                  23
_journal_year                    2004
_chemical_formula_sum            'C48 H120 B16 Cl2 Lu4 O5 Si8'
_chemical_formula_weight         1945.90
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.000(5)
_cell_angle_beta                 104.153(5)
_cell_angle_gamma                90.000(5)
_cell_formula_units_Z            4
_cell_length_a                   23.544(5)
_cell_length_b                   18.440(5)
_cell_length_c                   22.480(5)
_cell_measurement_temperature    213(2)
_cell_volume                     9464(4)
_diffrn_ambient_temperature      213(2)
_exptl_crystal_density_diffrn    1.366
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

 Updated bibliographic information.

 Antanas Vaitkus,
 2019-09-24
;
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4062757
; Organometallics  (2004) –; doi:10.1021/om049618y

data_4062758
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om049618y
_journal_year                    2004
_chemical_formula_sum            'C6 H14 B Br2 N O2'
_chemical_formula_weight         302.81
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 107.3070(16)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   13.8260(4)
_cell_length_b                   6.9220(3)
_cell_length_c                   11.6390(5)
_cell_measurement_temperature    110(2)
_cell_volume                     1063.46(7)
_diffrn_ambient_temperature      110(2)
_exptl_crystal_density_diffrn    1.891
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4062758
; Organometallics  (2004) –; doi:10.1021/om049618y

data_4062759
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om049618y
_journal_year                    2004
_chemical_formula_sum            'C8 H18 B Br2 N O2'
_chemical_formula_weight         330.86
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                105.1380(12)
_cell_angle_beta                 98.8870(14)
_cell_angle_gamma                98.772(3)
_cell_formula_units_Z            2
_cell_length_a                   6.8310(2)
_cell_length_b                   9.6340(3)
_cell_length_c                   10.7050(5)
_cell_measurement_temperature    110(2)
_cell_volume                     658.00(4)
_diffrn_ambient_temperature      110(2)
_exptl_crystal_density_diffrn    1.670
_cod_database_code               4062759
; Organometallics  (2004) –; doi:10.1021/om049618y

data_4062760
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om049618y
_journal_year                    2004
_chemical_formula_sum            'C8 H18 B Br2 N O2'
_chemical_formula_weight         330.86
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 110.5331(7)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   16.3860(2)
_cell_length_b                   6.96400(10)
_cell_length_c                   11.7720(4)
_cell_measurement_temperature    110(2)
_cell_volume                     1257.99(5)
_diffrn_ambient_temperature      110(2)
_exptl_crystal_density_diffrn    1.747
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4062760
Bis(imino)arylrhodium(III) Halide and Methyl Compounds
Hoogervorst, Wilhelmus J.; Goubitz, Kees; Fraanje, Jan; Lutz, Martin; Spek, Anthony L.; Ernsting, Jan Meine; Elsevier, Cornelis J.; Organometallics  (2004) –; doi:10.1021/om049619q

data_4062761
_publ_section_title
;
Bis(imino)arylrhodium(III) Halide and Methyl Compounds
;
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om049619q
_journal_year                    2004
_chemical_formula_moiety         'C18 H27 Br Cl N2 O Rh, 1.5(C4 H8 O)'
_chemical_formula_sum            'C24 H39 Br Cl N2 O2.5 Rh'
_chemical_formula_weight         613.84
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 91.5006(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.5951(1)
_cell_length_b                   11.4836(1)
_cell_length_c                   15.8397(1)
_cell_measurement_temperature    150(2)
_cell_volume                     2653.89(3)
_diffrn_ambient_temperature      150(2)
_exptl_crystal_density_diffrn    1.536
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C24 H39 Br Cl N2 O2.50 Rh'
_cod_database_code               4062761
Bis(imino)arylrhodium(III) Halide and Methyl Compounds
Hoogervorst, Wilhelmus J.; Goubitz, Kees; Fraanje, Jan; Lutz, Martin; Spek, Anthony L.; Ernsting, Jan Meine; Elsevier, Cornelis J.; Organometallics  (2004) –; doi:10.1021/om049619q

data_4062762
_publ_section_title
;
Bis(imino)arylrhodium(III) Halide and Methyl Compounds
;
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om049619q
_journal_year                    2004
_chemical_formula_moiety         'C14 H21 Br2 N2 O Rh'
_chemical_formula_sum            'C14 H21 Br2 N2 O Rh'
_chemical_formula_weight         496.06
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 119.2738(7)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   17.9937(2)
_cell_length_b                   11.8451(2)
_cell_length_c                   8.8178(1)
_cell_measurement_temperature    150(2)
_cell_volume                     1639.39(4)
_diffrn_ambient_temperature      150(2)
_exptl_crystal_density_diffrn    2.010
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4062762
Bis(imino)arylrhodium(III) Halide and Methyl Compounds
Hoogervorst, Wilhelmus J.; Goubitz, Kees; Fraanje, Jan; Lutz, Martin; Spek, Anthony L.; Ernsting, Jan Meine; Elsevier, Cornelis J.; Organometallics  (2004) –; doi:10.1021/om049619q

data_4062763
_publ_section_title
;
Bis(imino)arylrhodium(III) Halide and Methyl Compounds
;
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om049619q
_journal_year                    2004
_chemical_formula_moiety         'C32 H34 Br2 N2 P Rh'
_chemical_formula_sum            'C32 H34 Br2 N2 P Rh'
_chemical_formula_weight         740.31
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 121.8235(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   23.0455(1)
_cell_length_b                   13.4782(1)
_cell_length_c                   28.5576(2)
_cell_measurement_temperature    150(2)
_cell_volume                     7536.91(8)
_diffrn_ambient_temperature      150(2)
_exptl_crystal_density_diffrn    1.305
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4062763
Bis(imino)arylrhodium(III) Halide and Methyl Compounds
Hoogervorst, Wilhelmus J.; Goubitz, Kees; Fraanje, Jan; Lutz, Martin; Spek, Anthony L.; Ernsting, Jan Meine; Elsevier, Cornelis J.; Organometallics  (2004) –; doi:10.1021/om049619q

data_4062764
_publ_section_title
;
Bis(imino)arylrhodium(III) Halide and Methyl Compounds
;
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om049619q
_journal_year                    2004
_chemical_formula_sum            'C17 H26 Br N2 Rh'
_chemical_formula_weight         441.22
_space_group_IT_number           19
_space_group_name_Hall           'P 2ac 2ab'
_space_group_name_H-M_alt        'P 21 21 21'
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90.00000
_cell_angle_beta                 90.00000
_cell_angle_gamma                90.00000
_cell_formula_units_Z            8
_cell_length_a                   9.8568(8)
_cell_length_b                   15.2410(10)
_cell_length_c                   25.541(4)
_cell_measurement_temperature    293
_cell_volume                     3837.0(7)
_exptl_crystal_density_diffrn    1.528
_cod_original_sg_symbol_Hall     'p 2ac 2ab'
_cod_original_formula_sum        'C17 H26 Br1 N2 Rh1'
_cod_database_code               4062764
; Organometallics  (2004) –; doi:10.1021/om0496232

data_4062765
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om0496232
_journal_year                    2004
_chemical_formula_sum            'C14 H15 Cl N2 Pt'
_chemical_formula_weight         441.82
_space_group_IT_number           7
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P -2yc'
_symmetry_space_group_name_H-M   'P 1 c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 104.71(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   17.456(4)
_cell_length_b                   13.216(3)
_cell_length_c                   12.616(3)
_cell_measurement_temperature    150(2)
_cell_volume                     2815.1(10)
_diffrn_ambient_temperature      150(2)
_exptl_crystal_density_diffrn    2.085
_cod_original_sg_symbol_H-M      'P c'
_cod_database_code               4062765
; Organometallics  (2004) –; doi:10.1021/om0496232

data_4062766
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om0496232
_journal_year                    2004
_chemical_formula_sum            'C16 H17.5 Cl1.5 N2 Pd'
_chemical_formula_weight         397.40
_space_group_IT_number           33
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2c -2n'
_symmetry_space_group_name_H-M   'P n a 21'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            16
_cell_length_a                   21.336(4)
_cell_length_b                   21.469(4)
_cell_length_c                   14.219(3)
_cell_measurement_temperature    150(2)
_cell_volume                     6513(2)
_diffrn_ambient_temperature      150(2)
_exptl_crystal_density_diffrn    1.621
_cod_database_code               4062766
; Organometallics  (2004) –; doi:10.1021/om0496232

data_4062767
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om0496232
_journal_year                    2004
_chemical_formula_sum            'C69 H109 Cl K9 N4 O8 Pt2'
_chemical_formula_weight         1900.15
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 114.75(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   23.154(5)
_cell_length_b                   14.737(3)
_cell_length_c                   27.657(6)
_cell_measurement_temperature    150(2)
_cell_volume                     8570(3)
_diffrn_ambient_temperature      150(2)
_exptl_crystal_density_diffrn    1.473
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4062767
GOLD(III) PHENYLPHOSPHIDES AND -PHOSPHODIIDES
; Organometallics  (2004) –; doi:10.1021/om049624u

data_4062768
_publ_section_title
;
GOLD(III) PHENYLPHOSPHIDES AND -PHOSPHODIIDES
;
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om049624u
_journal_year                    2004
_chemical_formula_sum            'C78 H36 Au2 F30 N P3'
_chemical_formula_weight         2043.92
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                99.841(3)
_cell_angle_beta                 105.470(3)
_cell_angle_gamma                109.980(3)
_cell_formula_units_Z            2
_cell_length_a                   13.1839(12)
_cell_length_b                   17.2921(14)
_cell_length_c                   18.2913(16)
_cell_measurement_temperature    143(2)
_cell_volume                     3615.5(5)
_diffrn_ambient_temperature      143(2)
_exptl_crystal_density_diffrn    1.877
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_geom_bond_publ_flag' value 'Y' changed to 'y' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29 (10 times).

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4062768
GOLD(III) PHENYLPHOSPHIDES AND -PHOSPHODIIDES
; Organometallics  (2004) –; doi:10.1021/om049624u

data_4062769
_publ_section_title
;
GOLD(III) PHENYLPHOSPHIDES AND -PHOSPHODIIDES
;
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om049624u
_journal_year                    2004
_chemical_formula_sum            'C61 H36 Au3 Cl3 F15 P3'
_chemical_formula_weight         1844.06
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 110.268(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   23.9558(18)
_cell_length_b                   20.5905(16)
_cell_length_c                   26.249(2)
_cell_measurement_temperature    143(2)
_cell_volume                     12145.9(16)
_diffrn_ambient_temperature      143(2)
_exptl_crystal_density_diffrn    2.017
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4062769
GOLD(III) PHENYLPHOSPHIDES AND -PHOSPHODIIDES
; Organometallics  (2004) –; doi:10.1021/om049624u

data_4062770
_publ_section_title
;
GOLD(III) PHENYLPHOSPHIDES AND -PHOSPHODIIDES
;
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om049624u
_journal_year                    2004
_chemical_formula_sum            'C54.25 H18.25 Au3 Cl0.75 F30 P3'
_chemical_formula_weight         1950.34
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 102.6827(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.3742(2)
_cell_length_b                   21.4249(3)
_cell_length_c                   19.2234(3)
_cell_measurement_temperature    173(2)
_cell_volume                     5775.70(15)
_diffrn_ambient_temperature      173(2)
_exptl_crystal_density_diffrn    2.243
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4062770
Filippou, Alexander C.; Philippopoulos, Athanassios I.; Portius, Peter; Schnakenburg, Gregor; Organometallics  (2004) –; doi:10.1021/om049625m

data_4062771
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om049625m
_journal_year                    2004
_chemical_formula_moiety         'C62 H64 Ge P4 W, 1.5(C6 H6)'
_chemical_formula_sum            'C71 H73 Ge P4 W'
_chemical_formula_weight         1306.61
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                97.65(4)
_cell_angle_beta                 104.64(4)
_cell_angle_gamma                112.72(4)
_cell_formula_units_Z            2
_cell_length_a                   14.406(5)
_cell_length_b                   14.792(6)
_cell_length_c                   16.554(6)
_cell_measurement_temperature    180(2)
_cell_volume                     3041.0(19)
_diffrn_ambient_temperature      180(2)
_exptl_crystal_density_diffrn    1.427
_cod_database_code               4062771
Filippou, Alexander C.; Philippopoulos, Athanassios I.; Portius, Peter; Schnakenburg, Gregor; Organometallics  (2004) –; doi:10.1021/om049625m

data_4062772
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om049625m
_journal_year                    2004
_chemical_formula_moiety         'C63 H63 Ge N O1 P4 W, C4 H8 O'
_chemical_formula_sum            'C67 H71 Ge N O2 P4 W'
_chemical_formula_weight         1302.57
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 95.18(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   13.358(4)
_cell_length_b                   17.610(4)
_cell_length_c                   25.160(8)
_cell_measurement_temperature    180(2)
_cell_volume                     5894(3)
_diffrn_ambient_temperature      180(2)
_exptl_crystal_density_diffrn    1.468
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4062772
Filippou, Alexander C.; Philippopoulos, Athanassios I.; Portius, Peter; Schnakenburg, Gregor; Organometallics  (2004) –; doi:10.1021/om049625m

data_4062773
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om049625m
_journal_year                    2004
_chemical_formula_moiety         'C63 H63 Ge N P4 W, 0.5(C7 H8)'
_chemical_formula_sum            'C66.5 H67 Ge N P4 W'
_chemical_formula_weight         1260.53
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-I 2ya'
_symmetry_space_group_name_H-M   'I 1 2/a 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 97.563(18)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   24.601(4)
_cell_length_b                   13.466(3)
_cell_length_c                   34.549(5)
_cell_measurement_temperature    180(2)
_cell_volume                     11346(3)
_diffrn_ambient_temperature      180(2)
_exptl_crystal_density_diffrn    1.476
_cod_original_sg_symbol_H-M      'I 2/a'
_cod_original_formula_sum        'C66.50 H67 Ge N P4 W'
_cod_database_code               4062773