[{PtCl(dmso)}~2~(μ-OH)~2~]
Burgarcic, Z.; Lövqvist, K.; Oskarsson, A.; Acta Crystallographica Section C 50 (1994) 1028–1031; doi:10.1107/S0108270193011989

data_2009825
_publ_section_title
;
 [{PtCl(dmso)}~2~(\m-OH)~2~]
;
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1028
_journal_page_last               1031
_journal_paper_doi               10.1107/S0108270193011989
_journal_volume                  50
_journal_year                    1994
_chemical_formula_sum            'C4 H14 Cl2 O4 Pt2 S2'
_chemical_formula_weight         651.34
_space_group_IT_number           61
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.
_cell_angle_beta                 90.
_cell_angle_gamma                90.
_cell_formula_units_Z            8
_cell_length_a                   11.487(2)
_cell_length_b                   12.0670(10)
_cell_length_c                   18.967(3)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    295(2)
_cell_measurement_theta_max      22.6
_cell_measurement_theta_min      6.4
_cell_volume                     2629.1(7)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  ' 0.0082 (based on standard reflections)'
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            2571
_diffrn_reflns_theta_max         28
_diffrn_standards_decay_%        <2.5
_diffrn_standards_interval_time  120
_diffrn_standards_number         2
_exptl_absorpt_coefficient_mu    22.19
_exptl_absorpt_correction_T_max  0.2182
_exptl_absorpt_correction_T_min  0.0978
_exptl_absorpt_correction_type   integration
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    3.29
_exptl_crystal_description       prism
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.12
_refine_diff_density_max         2.27
_refine_diff_density_min         -1.89
_refine_ls_extinction_coef       10130.000000
_refine_ls_extinction_method     'Becker & Coppens'
_refine_ls_goodness_of_fit_obs   1.09
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     118
_refine_ls_number_reflns         1497
_refine_ls_R_factor_obs          0.038
_refine_ls_shift/esd_max         0.06
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details
'w = 1/[\s^2^/4|F~o~|^2^ + 0.03|F~o~|^2^ + 8.0]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.048
_reflns_number_observed          1497
_reflns_number_total             2511
_reflns_observed_criterion       I>2\s(I)
_cod_data_source_file            ab1105.cif
_cod_data_source_block           ab1105_structure_1_of_1
_cod_depositor_comments
;
 Marking attached hydrogen atoms.

 Antanas Vaitkus,
 2017-08-07

The following automatic conversions were performed:

'_cell_measurement_temperature' value 'Room temperature' was changed
to '295(2)' - the room/ambient temperature average [293;298] in
Kelvins(K) was taken.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 

The following automatic conversions were performed:

'_cell_measurement_temperature' value 'Room temperature' was changed
to '295(2)' - the room/ambient temperature average [293;298] in
Kelvins(K) was taken.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value ' w = 1/[\s^2^/4|F~o~|^2^ +
0.03|F~o~|^2^ + 8.0]' was changed to 'calc'. New tag
'_refine_ls_weighting_details' was created. The value of the new tag
was set to 'w = 1/[\s^2^/4|F~o~|^2^ + 0.03|F~o~|^2^ + 8.0]'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        2629.0(5)
_cod_database_code               2009825