Synthesis and structural study of new metallasilsesquioxanes of potassium and uranium.
Gießmann, Stephan; Lorenz, Volker; Liebing, Phil; Hilfert, Liane; Fischer, Axel; Edelmann, Frank T.; Dalton transactions (Cambridge, England : 2003) 46 (2017) 2415–2419; doi:10.1039/c7dt00006e

data_7041851
_publ_section_title
;
 Synthesis and structural study of new metallasilsesquioxanes of potassium
 and uranium.
;
_journal_issue                   8
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2415
_journal_page_last               2419
_journal_paper_doi               10.1039/c7dt00006e
_journal_volume                  46
_journal_year                    2017
_chemical_formula_moiety         'C100 H194 K6 O32 Si14'
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_chemical_properties_physical    ', Air-sensitive,Moisture-sensitive'
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_audit_update_record
;
2016-12-19 deposited with the CCDC.
2017-01-26 downloaded from the CCDC.
;
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_computing_cell_refinement       'SMART CCD System (Bruker)'
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_diffrn_measurement_device_type  'SMART CCD System (Bruker)'
_diffrn_measurement_method       'omega scans'
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'Re-crystallisation from solvent: 1,2-Dimethoxyethane'
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0342P)^2^+0.7959P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_depositor_comments
'Adding full bibliography for 7041851--7041852.cif.'
_cod_original_cell_volume        3333.3(2)
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