Further Evidence for the Stabilization of U(V) within a Tetraoxo Core.
Stritzinger, Jared T.; Alekseev, Evgeny V.; Polinski, Matthew J.; Cross, Justin N.; Eaton, Teresa M.; Albrecht-Schmitt, Thomas E; Inorganic chemistry 53 (2014) 5294–5299; doi:10.1021/ic500523a

data_4338308
_publ_section_title
;
 Further Evidence for the Stabilization of U(V) within a Tetraoxo Core.
;
_journal_issue                   10
_journal_name_full               'Inorganic chemistry'
_journal_page_first              5294
_journal_page_last               5299
_journal_paper_doi               10.1021/ic500523a
_journal_volume                  53
_journal_year                    2014
_chemical_formula_moiety         K13[(U02)19(U04)(BO3)10(OH)2(O10)]-H2O
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_chemical_melting_point          ?
_chemical_name_systematic
; 
 ? 
;
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_computing_molecular_graphics    'SHELXP-91 (Sheldrick, 1997)'
_computing_publication_material  'SHELXCIF-97 (Sheldrick, 2000)'
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_diffrn_measurement_device_type  'BRUKER apex II'
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_exptl_absorpt_correction_type   multi-scan
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_exptl_crystal_colour            Brown
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0300P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_data_source_file            ic500523a_si_002.cif
_cod_data_source_block           pbam
_cod_depositor_comments
;
The following automatic conversions were performed:

'_chemical_melting_point' value 'N/A' was changed to '?' - the value
is undefined or not given.

'_symmetry_cell_setting' value
'Orthorhombic' changed to 'orthorhombic' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from
2011-04-26.

'_exptl_absorpt_correction_type' value 'Multi-Scan'
changed to 'multi-scan' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 

 Adding full bibliography for 4338307--4338308.cif.

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        4630.3(5)
_cod_original_sg_symbol_H-M      Pbam
_cod_database_code               4338308