Silver(I) Complex Assemblies with Nonplanar Aromatic Compounds
Megumu Munakata; Liang Ping Wu; Kunihisa Sugimoto; Takayoshi Kuroda-Sowa; Masahiko Maekawa; Yusaku Suenaga; Naoto Maeno; Motoshi Fujita; Inorganic Chemistry 38 (1999) 5674–5680; doi:10.1021/ic990391m

data_4322498
_publ_section_title
;
 Silver(I) Complex Assemblies with Nonplanar Aromatic Compounds
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              5674
_journal_page_last               5680
_journal_paper_doi               10.1021/ic990391m
_journal_volume                  38
_journal_year                    1999
_chemical_formula_sum            'C30 H21 Ag Cl O4'
_chemical_formula_weight         588.81
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 100.015(1)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   12.317(4)
_cell_length_b                   7.961(1)
_cell_length_c                   24.741(1)
_cell_measurement_reflns_used    5286
_cell_measurement_temperature    296.2
_cell_measurement_theta_max      27.5
_cell_volume                     2389.0(8)
_computing_data_reduction        'teXsan Ver. 1.10'
_computing_publication_material  'teXsan Ver. 1.10'
_computing_structure_refinement  'teXsan Ver. 1.10'
_computing_structure_solution    SIR88
_diffrn_measurement_device_type  'Quantum CCD/Rigaku AFC7'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.038
_diffrn_reflns_limit_h_max       0
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       0
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       0
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            5286
_exptl_absorpt_coefficient_mu    0.990
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.637
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_size_max          0.250
_exptl_crystal_size_mid          0.150
_exptl_crystal_size_min          0.040
_refine_diff_density_max         0.80
_refine_diff_density_min         -0.96
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.812
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     325
_refine_ls_number_reflns         4147
_refine_ls_R_factor_gt           0.0560
_refine_ls_shift/su_max          0.0010
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^) + (0.06000(Max(Fo^2^,0) + 2Fc^2^)/3)^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1555
_reflns_number_gt                3228
_reflns_number_total             0
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
_cod_data_source_file            ic990391m_2.cif
_cod_data_source_block           ag-bif-clo4
_cod_original_cell_volume        2389.0(6)
_cod_original_formula_sum        'C30 H21 Ag Cl O4 '
_cod_database_code               4322498