Coordination capabilities of bis-(2-pyridyl)amides in the field of divalent germanium, tin and lead compounds.
Zechovský, Jan; Mrózek, Ondřej; Samsonov, Maksim; Jambor, Roman; R°uŽička, Aleš; Dostál, Libor; Dalton transactions (Cambridge, England : 2003) 50 (2021) 6321–6332; doi:10.1039/d1dt00717c

data_7707036
_publ_section_title
;
 Coordination capabilities of bis-(2-pyridyl)amides in the field of
 divalent germanium, tin and lead compounds.
;
_journal_issue                   18
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              6321
_journal_page_last               6332
_journal_paper_doi               10.1039/d1dt00717c
_journal_volume                  50
_journal_year                    2021
_chemical_formula_sum            'C24 H24 Ge N6'
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;
2020-09-21 deposited with the CCDC.	2021-03-29 downloaded from the CCDC.
;
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_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker D8 - Venture'
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_diffrn_reflns_Laue_measured_fraction_full 0.997
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_diffrn_reflns_point_group_measured_fraction_full 0.997
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_diffrn_reflns_theta_max         27.574
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;
SADABS-2016/2 - Bruker AXS area detector
scaling and absorption correction
;
_exptl_crystal_colour            yellow
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0298P)^2^+0.6353P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.0666
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_reflns_number_gt                4703
_reflns_number_total             5147
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7707027--7707037.cif.'
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_exptl_absorpt_special_details
;
The ratio of minimum to maximum
apparent transmission was 0.588
;
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