Modular synthesis of oligoacetylacetones via site-selective silylation of acetylacetone derivatives.
Sarkar, Parantap; Inaba, Yuya; Shirakura, Hayato; Yoneda, Tomoki; Inokuma, Yasuhide; Organic & biomolecular chemistry 18 (2020) 3297–3302; doi:10.1039/d0ob00501k

data_7157458
_publ_section_title
;
 Modular synthesis of oligoacetylacetones via site-selective silylation of
 acetylacetone derivatives.
;
_journal_issue                   17
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              3297
_journal_page_last               3302
_journal_paper_doi               10.1039/d0ob00501k
_journal_volume                  18
_journal_year                    2020
_chemical_formula_moiety         'C20 H38 O4 Si2'
_chemical_formula_sum            'C10 H19 O2 Si'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0924P)^2^+0.7584P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_data_source_block           Compound5a
_cod_depositor_comments
'Adding full bibliography for 7157456--7157460.cif.'
_cod_original_cell_volume        1198.7(4)
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7157458
_shelx_shelxl_version_number     2017/1
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