Electron-Transfer Oxidation by Phase-Separating Reagents
Robert E. Patterson; Scott W. Gordon-Wylie; Christine G. Woomer; Richard E. Norman; Susan T. Weintraub; Colin P. Horwitz; Terrence J. Collins; Inorganic Chemistry 37 (1998) 4748–4750; doi:10.1021/ic9803661

data_4323003
_publ_contact_author
;
Terrance J. Collins
Department of Chemistry
Carnegie Mellon University
Mellon Institute
4400 Fifth Avenue
Pittsburgh, PA 15213-2683  USA
;
_publ_contact_author_email       'tc1u@andrew.cmu.edu '
_publ_contact_author_fax         '(412) 268-1061'
_publ_contact_author_phone       '(412) 268-6335'
_publ_section_title
;
 Electron-Transfer Oxidation by Phase-Separating Reagents
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              4748
_journal_page_last               4750
_journal_paper_doi               10.1021/ic9803661
_journal_volume                  37
_journal_year                    1998
_chemical_compound_source        'see experimental'
_chemical_formula_sum            'C34 H52 Co N5 O5'
_chemical_formula_weight         669.75
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_audit_creation_date             'Jul 03 1997'
_audit_creation_method           'from TEXRAY.INF file'
_audit_update_record             '13-03-98 updated Robert E. Patterson'
_cell_angle_alpha                90
_cell_angle_beta                 96.55(3)
_cell_angle_gamma                90
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_cell_length_b                   16.33(1)
_cell_length_c                   36.679(6)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    294
_cell_measurement_theta_max      12.42
_cell_measurement_theta_min      11.05
_cell_volume                     7032(6)
_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
_computing_data_reduction        'teXsan (MSC, 1992)'
_computing_publication_material  'teXsan (MSC, 1992)'
_computing_structure_refinement  'teXsan (MSC, 1992)'
_computing_structure_solution    'SIR92 (Altomare, et al., 1994)'
_diffrn_ambient_temperature      294
_diffrn_measurement_device       AFC7R
_diffrn_measurement_method       'omega/2-theta scans'
_diffrn_orient_matrix_UB_11      -0.0064403
_diffrn_orient_matrix_UB_12      -0.0183743
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_diffrn_reflns_av_R_equivalents  0.022
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_diffrn_reflns_limit_k_min       0
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_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
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_refine_ls_number_restraints     0
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_refine_ls_structure_factor_coef F
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_reflns_number_total             9581
_reflns_observed_criterion       I>3.00\s(I)
_cod_data_source_file            ic9803661.cif
_cod_data_source_block           tjcollins
_cod_original_cell_volume        7030(6)
_cod_original_sg_symbol_H-M      'P 21/c '
_cod_original_formula_sum        'C34 H52 O5 N5 Co1 '
_cod_database_code               4323003