Monofunctional platinum(ii) anticancer complexes based on multidentate phenanthridine-containing ligand frameworks.
Lozada, Issiah B.; Huang, Bin; Stilgenbauer, Morgan; Beach, Travis; Qiu, Zihan; Zheng, Yaorong; Herbert, David E.; Dalton transactions (Cambridge, England : 2003) 49 (2020) 6557–6560; doi:10.1039/d0dt01275k

data_7704128
_publ_section_title
;
 Monofunctional platinum(ii) anticancer complexes based on multidentate
 phenanthridine-containing ligand frameworks.
;
_journal_issue                   20
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              6557
_journal_page_last               6560
_journal_paper_doi               10.1039/d0dt01275k
_journal_volume                  49
_journal_year                    2020
_chemical_formula_sum            'C22 H24 N2 O'
_chemical_formula_weight         332.43
_chemical_name_common            (4-nacac-2-tertbutyl-phenanthridine)
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2019-10-16 deposited with the CCDC.	2020-04-15 downloaded from the CCDC.
;
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_cell_measurement_temperature    150(2)
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_cell_volume                     1778.68(18)
_computing_cell_refinement       'Bruker SAINT'
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_diffrn_radiation.monochromator  'TRIUMPH curved--crystal'
_diffrn_radiation_type           MoK\a
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0454P)^2^+1.9858P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7704128--7704129.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7704128
_shelx_shelxl_version_number     2014/7
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_shelx_res_checksum              3690