Intramolecular Cyclizations of Vinyl-Substituted N,N-Dialkyl Arylamines Enabled by Borane-Assisted Hydride Transfer
Tian, Jun-Jie; Zeng, Ning-Ning; Liu, Ning; Tu, Xian-Shuang; Wang, Xiao-Chen; ACS Catalysis 9 (2018) 295–; doi:10.1021/acscatal.8b04485

data_4515457
_publ_section_title
;
 Intramolecular Cyclizations of Vinyl-Substituted N,N-Dialkyl Arylamines
 Enabled by Borane-Assisted Hydride Transfer
;
_journal_issue                   1
_journal_name_full               'ACS Catalysis'
_journal_page_first              295
_journal_paper_doi               10.1021/acscatal.8b04485
_journal_volume                  9
_journal_year                    2018
_chemical_formula_sum            'C27 H25 N'
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_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      113(2)
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_diffrn_measurement_device_type  'rigaku saturn'
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1250P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                3544
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           shelxl
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'MULTI-SCAN' was
changed to 'multi-scan' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/current/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_original_cell_volume        1970.2(8)
_cod_database_code               4515457
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_shelx_res_checksum              56703
_shelx_hkl_checksum              51428