Thorium Mono- and Bis(imido) Complexes Made by Reprotonation of cyclo-Metalated Amides.
Bell, Nicola L.; Maron, Laurent; Arnold, Polly L.; Journal of the American Chemical Society  (2015) 150814165612001–; doi:10.1021/jacs.5b06630

data_4124278
_publ_section_title
;
 Thorium Mono- and Bis(imido) Complexes Made by Reprotonation of
 cyclo-Metalated Amides.
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              150814165612001
_journal_paper_doi               10.1021/jacs.5b06630
_journal_year                    2015
_chemical_formula_sum            'C44 H86 K2 N4 O2 Si4 Th'
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
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Analytical numeric absorption correction using a multifaceted crystal
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(Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0512P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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'Adding full bibliography for 4124276--4124278.cif.'
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