Heptanickel(ii) double-cubane core in wells-dawson heteropolytungstate, [Ni7(OH)6(H2O)6(P2W15O56)2](16.).
Bassil, Bassem S.; Xiang, Yixian; Haider, Ali; Hurtado, Jaime; Novitchi, Ghenadie; Powell, Annie K.; Bossoh, A. Martin; Mbomekallé, Israël M; de Oliveira, Pedro; Kortz, Ulrich; Chemical communications (Cambridge, England) 52 (2016) 2601–2604; doi:10.1039/c5cc09823h

data_7118392
_publ_section_title
;
 Heptanickel(ii) double-cubane core in wells-dawson heteropolytungstate,
 [Ni7(OH)6(H2O)6(P2W15O56)2](16.).
;
_journal_issue                   12
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              2601
_journal_page_last               2604
_journal_paper_doi               10.1039/c5cc09823h
_journal_volume                  52
_journal_year                    2016
_chemical_formula_sum            'Cs1.5 H130 Na14.5 Ni7 O180 P4 W30'
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_cell_length_b                   12.7765(4)
_cell_length_c                   25.7791(10)
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_cell_measurement_temperature    100(2)
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_cell_volume                     3966.0(2)
_computing_cell_refinement       'Bruker SAINT'
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_diffrn_radiation_type           MoK\a
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_diffrn_reflns_av_unetI/netI     0.0453
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0430P)^2^+470.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           try
_cod_depositor_comments          'Adding full bibliography for 7118392.cif.'
_cod_original_formula_sum        'Cs1.50 H130 Na14.50 Ni7 O180 P4 W30'
_cod_database_code               7118392
_shelx_estimated_absorpt_t_min   0.0336
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