One-dimensional polymeric iodoplumbate hybrids with lanthanide complex cations: syntheses, crystal structures, and photoelectric and photocatalytic properties
Chen, Niannian; Gao, Yan; Tian, Yiming; Wu, Bing; Jia, Dingxian; Zhao, Shengxian; New Journal of Chemistry 44 (2020) 19166–19173; doi:10.1039/D0NJ04549G

data_7060068
_publ_section_title
;
 One-dimensional polymeric iodoplumbate hybrids with lanthanide complex
 cations: syntheses, crystal structures, and photoelectric and
 photocatalytic properties
;
_journal_issue                   44
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              19166
_journal_page_last               19173
_journal_paper_doi               10.1039/D0NJ04549G
_journal_volume                  44
_journal_year                    2020
_chemical_formula_moiety         'C24 H56 Gd I13 N8 O8 Pb5'
_chemical_formula_sum            'C24 H56 Gd I13 N8 O8 Pb5'
_chemical_formula_weight         3427.66
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_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2020-09-11 deposited with the CCDC.	2020-10-15 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
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_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Rigaku Saturn'
_diffrn_measurement_method       \w
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_diffrn_reflns_av_unetI/netI     0.1117
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_diffrn_reflns_Laue_measured_fraction_max 0.998
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_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
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_diffrn_reflns_point_group_measured_fraction_full 0.998
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_diffrn_reflns_theta_full        25.242
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_exptl_absorpt_coefficient_mu    18.311
_exptl_absorpt_correction_T_max  0.1208
_exptl_absorpt_correction_T_min  0.0240
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Jacobson, R. (1998) Private communication'
_exptl_crystal_colour            Yellow
_exptl_crystal_density_diffrn    3.187
_exptl_crystal_description       Platelet
_exptl_crystal_F_000             5932
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_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0553P)^2^+179.2714P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2190
_refine_ls_wR_factor_ref         0.2357
_reflns_Friedel_coverage         0.000
_reflns_number_gt                9452
_reflns_number_total             13061
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d0nj04549g2.cif
_cod_data_source_block           m14
_cod_depositor_comments
'Adding full bibliography for 7060067--7060069.cif.'
_cod_original_cell_volume        7143(3)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               7060068
_shelx_shelxl_version_number     2014/7
_shelx_estimated_absorpt_t_min   0.024
_shelx_estimated_absorpt_t_max   0.121
_shelx_res_checksum              84574