Syntheses, Crystal Structures, and Properties of Unsymmetrical (μ-Oxo)diiron(III) Complexes Containing Polyimidazole Ligands
Jianping Wang; Mark S. Mashuta; Ziming Sun; John F. Richardson; David N. Hendrickson; Robert M. Buchanan; Inorganic Chemistry 35 (1996) 6642–6643; doi:10.1021/ic9607494

data_4323974
_publ_contact_author
;
    Professor Robert M. Buchanan
 Department of Chemistry and Center for Chemical Catalysis
 University of Lousiville
 Louisville
 KY  40292
 USA
;
_publ_contact_author_email       ' RMBUCH01@ulkyvm.louisville.edu '
_publ_contact_author_fax         ' (502)852-8149 '
_publ_contact_author_phone       ' (502)852-6580 '
_publ_section_title
;
 Syntheses, Crystal Structures, and Properties of Unsymmetrical
 (\m-Oxo)diiron(III) Complexes Containing Polyimidazole Ligands
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              6642
_journal_page_last               6643
_journal_paper_doi               10.1021/ic9607494
_journal_volume                  35
_journal_year                    1996
_chemical_formula_sum            'C38 H57 Cl3 Fe2 N14 O15'
_chemical_formula_weight         1168.01
_space_group_IT_number           19
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      19
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_audit_creation_date             'Wed Feb  7 09:21:03 1996'
_audit_creation_method           'from TEXRAY.INF file'
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_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
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_cell_length_b                   24.030(7)
_cell_length_c                   10.137(3)
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_cell_measurement_temperature    296(2)
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_cell_measurement_theta_min      30.0
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_computing_cell_refinement       'Enraf Nonius Diffractometer Control, 1988'
_computing_data_collection       'Enraf Nonius Diffractometer Control, 1988'
_computing_data_reduction        teXsan
_computing_publication_material  teXsan
_computing_structure_refinement  teXsan
_computing_structure_solution    SIR92
_diffrn_ambient_temperature      296(2)
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_diffrn_reflns_limit_l_min       -12
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_diffrn_standards_interval_time  60
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_refine_ls_structure_factor_coef F
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_cod_data_source_file            ic9607494_2.cif
_cod_data_source_block           compound#2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'w=1/\s^2^(F)' was changed to
'calc'. New tag '_refine_ls_weighting_details' was created. The value
of the new tag was set to 'w=1/\s^2^(F)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        5256(2)
_cod_original_sg_symbol_H-M      'P 21 21 21 '
_cod_original_formula_sum        'C38 H57 Cl3 Fe2 N14 O15 '
_cod_database_code               4323974