The synthesis and strecker reaction of 2-chlorotetrafluoroethanesulfinyl ketimines.
Yang, Kai; Liu, Li-Juan; Liu, Jin-Tao; The Journal of organic chemistry 79 (2014) 3215–3220; doi:10.1021/jo500008e

data_4029232
_publ_section_title
;
 The synthesis and strecker reaction of 2-chlorotetrafluoroethanesulfinyl
 ketimines.
;
_journal_issue                   7
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              3215
_journal_page_last               3220
_journal_paper_doi               10.1021/jo500008e
_journal_volume                  79
_journal_year                    2014
_chemical_absolute_configuration ad
_chemical_formula_sum            'C11 H9 Cl F4 N2 O S'
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_chemical_name_systematic
; 
 ? 
;
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_exptl_crystal_colour            colorless
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_exptl_crystal_description       prismatic
_exptl_crystal_F_000             498
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_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0817P)^2^+0.0746P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1234
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_reflns_number_gt                2381
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_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            jo500008e_si_001.cif
_cod_data_source_block           cd211504
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Trigonal' changed to 'trigonal'
according to
/usr/data/users/saulius/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 

 Adding full bibliography for
 ./tmp-cod-update-bibliographies-12971/cifs/4029232.cif.
;
_cod_original_cell_volume        1043.5(9)
_cod_original_sg_symbol_H-M      P3(1)
_cod_database_code               4029232