<i>catena</i>-Poly[[(1,10-phenanthroline-κ^2^<i>N,N</i>')silver(I)]-μ-chloro]
Odoko, Mamiko; Wang, Yue; Okabe, Nobuo; Acta Crystallographica Section E 60 (2004) m1522–m1524; doi:10.1107/S1600536804023724

data_2204258
_publ_section_title
<i>catena</i>-Poly[[(1,10-phenanthroline-\k^2^<i>N,N</i>')silver(I)]-\m-chloro]
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1522
_journal_page_last               m1524
_journal_paper_doi               10.1107/S1600536804023724
_journal_volume                  60
_journal_year                    2004
_chemical_formula_iupac          '[Ag Cl (C12 H8 N2)]'
_chemical_formula_moiety         'C12 H8 Ag Cl N2'
_chemical_formula_sum            'C12 H8 Ag Cl N2'
_chemical_formula_weight         323.52
_space_group_IT_number           5
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'C 2y'
_symmetry_space_group_name_H-M   'C 1 2 1'
_cell_angle_alpha                90
_cell_angle_beta                 104.92(4)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   12.566(14)
_cell_length_b                   10.235(11)
_cell_length_c                   4.279(4)
_cell_measurement_reflns_used    2250
_cell_measurement_temperature    296.1
_cell_measurement_theta_max      27.4
_cell_measurement_theta_min      3.4
_cell_volume                     531.8(10)
_computing_cell_refinement       PROCESS-AUTO
_computing_data_collection       'PROCESS-AUTO (Rigaku/MSC, 2004)'
_computing_data_reduction
'CrystalStructure (Rigaku/MSC, 2004) and CRYSTALS (Watkin et al., 1996)'
_computing_molecular_graphics    'ORTEPII (Johnson, 1996)'
_computing_publication_material  CrystalStructure
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution
'SIR97 (Altomare et al., 1999) and DIRDIF99 (Beurskens et al., 1999)'
_diffrn_detector_area_resol_mean 10.00
_diffrn_measured_fraction_theta_full 0.9954
_diffrn_measured_fraction_theta_max 0.9954
_diffrn_measurement_device_type  'Rigaku R-AXIS RAPID'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.043
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       5
_diffrn_reflns_limit_l_min       -5
_diffrn_reflns_number            2616
_diffrn_reflns_theta_full        27.40
_diffrn_reflns_theta_max         27.40
_exptl_absorpt_coefficient_mu    2.114
_exptl_absorpt_correction_T_max  0.810
_exptl_absorpt_correction_T_min  0.456
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(ABSCOR; Higashi, 1995)'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    2.020
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             316.00
_exptl_crystal_size_max          0.10
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.41
_refine_diff_density_min         -0.52
_refine_ls_abs_structure_details 'Flack (1983), 564 Friedel pairs [CHECK?]'
_refine_ls_abs_structure_Flack   0.53(6)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.887
_refine_ls_hydrogen_treatment    refall
_refine_ls_number_parameters     75
_refine_ls_number_reflns         1215
_refine_ls_R_factor_gt           0.0360
_refine_ls_shift/su_max          0.0000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^)+(0.0268P)^2^] where P = (Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.0660
_reflns_number_gt                686
_reflns_number_total             1215
_reflns_threshold_expression     F^2^>2\s(F^2^)
_cod_data_source_file            ac6117.cif
_cod_data_source_block           I
_cod_original_cell_volume        531.7(8)
_cod_original_sg_symbol_Hall     c_2y
_cod_original_sg_symbol_H-M      'C 2'
_cod_database_code               2204258
_cod_database_fobs_code          2204258