Ruthenium-catalyzed formation of aryl(diphenyl)phosphine oxides by reactions of propargylic alcohols with diphenylphosphine oxide.
Onodera, Gen; Matsumoto, Hideyuki; Milton, Marilyn Daisy; Nishibayashi, Yoshiaki; Uemura, Sakae; Organic letters 7 (2005) 4029–4032; doi:10.1021/ol0515311

data_1506688
_publ_section_title
;
 Ruthenium-catalyzed formation of aryl(diphenyl)phosphine oxides by
 reactions of propargylic alcohols with diphenylphosphine oxide.
;
_journal_issue                   18
_journal_name_full               'Organic letters'
_journal_page_first              4029
_journal_page_last               4032
_journal_paper_doi               10.1021/ol0515311
_journal_volume                  7
_journal_year                    2005
_chemical_formula_moiety         'C29 H24 O1.50 P '
_chemical_formula_sum            'C29 H24 O1.5 P'
_chemical_formula_weight         427.48
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_symmetry_cell_setting           monoclinic
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_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.0000
_cell_angle_beta                 95.607(11)
_cell_angle_gamma                90.0000
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_cell_length_b                   10.982(4)
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_cell_measurement_temperature    296.1
_cell_measurement_theta_max      27.5
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_diffrn_measurement_device_type  'Rigaku RAXIS-RAPID'
_diffrn_measurement_method       \w
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_diffrn_reflns_limit_h_min       -29
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_exptl_absorpt_coefficient_mu    0.139
_exptl_absorpt_correction_T_max  0.946
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_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
    Higashi, T. (1995). Program for Absorption Correction.
    Rigaku Corporation, Tokyo, Japan.
;
_exptl_crystal_colour            white
_exptl_crystal_density_diffrn    1.226
_exptl_crystal_density_method    'not measured'
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