Bridging selenocarbonyl ligands: An open and shut case.
Hill, Anthony; Watson, Lachlan J.; Frogley, Benjamin; Chemical Communications  (2019) –; doi:10.1039/C9CC07757J

data_7124386
_publ_section_title
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 Bridging selenocarbonyl ligands: An open and shut case.
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/C9CC07757J
_journal_year                    2019
_chemical_formula_moiety         'C46 H62 B2 N14 O4 Pt Se2 W2'
_chemical_formula_sum            'C46 H62 B2 N14 O4 Pt Se2 W2'
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_space_group_name_Hall           '-P 2yn'
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_symmetry_space_group_name_Hall  '-P 2yn'
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_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2019-08-27 deposited with the CCDC.    2019-10-28 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'New Xcalibur, Atlas'
_diffrn_measurement_method       '\w scans'
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_diffrn_reflns_point_group_measured_fraction_full 0.997
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_diffrn_reflns_theta_min         3.506
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_exptl_absorpt_correction_T_max  1.00000
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_exptl_absorpt_process_details
;
CrysAlisPro 1.171.40.36a (Rigaku Oxford Diffraction, 2018)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            orange
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_exptl_crystal_description       needle
_exptl_crystal_F_000             1544
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_exptl_crystal_size_min          0.043
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0160P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           Compound_5
_cod_database_code               7124386
_shelx_shelxl_version_number     2014/7
_shelx_res_checksum              19074
_shelx_hkl_checksum              28544