Synthesis of multifunctional metal-organic frameworks and tuning the functionalities with pendant ligands.
Prasad, Thazhe Kootteri; Suh, Myunghyun Paik; Dalton transactions (Cambridge, England : 2003) 49 (2020) 15034–15040; doi:10.1039/d0dt03012k

data_7705663
_publ_section_title
;
 Synthesis of multifunctional metal-organic frameworks and tuning the
 functionalities with pendant ligands.
;
_journal_issue                   42
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              15034
_journal_page_last               15040
_journal_paper_doi               10.1039/d0dt03012k
_journal_volume                  49
_journal_year                    2020
_chemical_formula_sum            'C156 H144 O64 Zn16'
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_chemical_properties_physical    Air-sensitive,Moisture-sensitive
_space_group_crystal_system      cubic
_space_group_IT_number           225
_space_group_name_Hall           '-F 4 2 3'
_space_group_name_H-M_alt        'F m -3 m'
_audit_creation_method           SHELXL-2013
_audit_update_record
;
2020-06-22 deposited with the CCDC.	2020-10-06 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_cell_measurement_theta_max      23.286
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_computing_data_collection       'ADSC Q210 ADX program'
_computing_data_reduction        HKL3000sm
_computing_molecular_graphics    'Mercury (Bruno, et.al., 2002)'
_computing_publication_material  'WinGX (Farrugia, 2012)'
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_computing_structure_solution    'SHELXL-2013 (Sheldrick, 2013)'
_diffrn_ambient_temperature      293(2)
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_diffrn_measured_fraction_theta_max 0.862
_diffrn_measurement.details
' 1.00 degrees, 1.0 sec, detector distance 100.00 mm'
_diffrn_measurement_device_type  'ADSC Quantum-210 detector '
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_diffrn_reflns_Laue_measured_fraction_full 0.730
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_diffrn_source                   'PLSII 2D bending magnet'
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_exptl_crystal_preparation       Luminescent
_exptl_crystal_recrystallization_method 'Solvothermal synthesis'
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_refine_ls_extinction_method     none
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_refine_ls_matrix_type           full
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_refine_ls_R_factor_all          0.1011
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_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.2000P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.3096
_reflns_Friedel_coverage         0.000
_reflns_number_gt                621
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           SNU-174
_cod_depositor_comments
'Adding full bibliography for 7705661--7705665.cif.'
_cod_original_cell_volume        27560(27)
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_shelxl_version_number           2013-4
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