(Hexasulfanediyl)di(pyridine-<i>N</i>)zinc
Li, Hongjun; Du, Shaowu; Wu, Xintao; Acta Crystallographica Section C 50 (1994) 498–500; doi:10.1107/S0108270193010868

data_2009581
_publ_section_title
;
 (Hexasulfanediyl)di(pyridine-<i>N</i>)zinc
;
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              498
_journal_page_last               500
_journal_paper_doi               10.1107/S0108270193010868
_journal_volume                  50
_journal_year                    1994
_chemical_formula_sum            'C10 H10 N2 S6 Zn'
_chemical_formula_weight         415.94
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90
_cell_angle_beta                 118.61(4)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   13.608(8)
_cell_length_b                   8.998(6)
_cell_length_c                   15.334(8)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    296
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      6
_cell_volume                     1648.3(18)
_diffrn_measurement_device       'Rigaku AFC5R'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0774
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            2664
_diffrn_reflns_theta_max         30.05
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    2.243
_exptl_absorpt_correction_T_max  1.0
_exptl_absorpt_correction_T_min  0.7234
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            Yellow
_exptl_crystal_density_diffrn    1.68
_exptl_crystal_description       Prism
_refine_diff_density_max         0.52
_refine_diff_density_min         -0.51
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   1.57
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     88
_refine_ls_number_reflns         1599
_refine_ls_R_factor_obs          0.050
_refine_ls_shift/esd_max         0.010
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w=1/\s^2^(F~o~)
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.059
_reflns_number_observed          1599
_reflns_number_total             2564
_reflns_observed_criterion       I>3\s(I)
_cod_data_source_file            al1062.cif
_cod_data_source_block           al1062_structure_1_of_1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'w=1/\s^2^(F~o~)' was changed to
'calc'. New tag '_refine_ls_weighting_details' was created. The value
of the new tag was set to 'w=1/\s^2^(F~o~)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        1648(2)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_original_formula_sum        'C10 H10 N2 S6 Zn1'
_cod_database_code               2009581