Influence of annealing conditions on the structure and luminescence properties of KGd1−xEux(MoO4)2 (0 ≤ x ≤ 1)
Morozov, Vladimir A.; Posokhova, Svetlana M.; Deyneko, Dina V.; Savina, Aleksandra A.; Morozov, Anatolii V.; Tyablikov, Oleg A.; Redkin, Boris S.; Spassky, Dmitry A.; Hadermann, Joke; Lazoryak, Bogdan I.; CrystEngComm 21 (2019) 6460–; doi:10.1039/C9CE01244C

data_7234030
_publ_section_title
;
 Influence of annealing conditions on the structure and luminescence
 properties of KGd1&#x2212;xEux(MoO4)2 (0 &#x2264; x &#x2264; 1)
;
_journal_issue                   42
_journal_name_full               CrystEngComm
_journal_page_first              6460
_journal_paper_doi               10.1039/C9CE01244C
_journal_volume                  21
_journal_year                    2019
_chemical_formula_analytical     'Gd1 K1 Mo2 O8'
_chemical_formula_iupac          'Gd1 K1 Mo2 O8'
_chemical_formula_moiety         '(K1+)1, (Gd3+)1, (MoO4 2-)2'
_chemical_formula_structural     'Gd1 K1 Mo2 O8'
_chemical_formula_sum            'Gd K Mo2 O8'
_chemical_formula_weight         516.2
_chemical_melting_point          1271
_chemical_name_common            'Gd1 K1 Mo2 O8'
_space_group_IT_number           60
_space_group_name_Hall           '-P 2n 2ab'
_space_group_name_H-M_alt        'P b c n'
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      60
_symmetry_space_group_name_Hall  '-P 2n 2ab'
_symmetry_space_group_name_H-M   'P b c n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   5.11465(4)
_cell_length_b                   18.0858(2)
_cell_length_c                   8.04600(5)
_cell_measurement_temperature    293
_cell_volume                     744.275(11)
_computing_cell_refinement       '(Jana2000; Petricek and Dusek, 2000)'
_computing_publication_material  '(Jana2000; Petricek and Dusek, 2000)'
_computing_structure_refinement  '(Jana2000; Petricek and Dusek, 2000)'
_diffrn_ambient_temperature      293
_diffrn_detector                 'linear position sensitive detector'
_diffrn_measurement_device       STADI-P
_diffrn_radiation_monochromator  'curved Ge monochromator'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Co K\a'
_diffrn_radiation_wavelength     1.78892
_diffrn_source                   'Rietveld Refinement'
_diffrn_source_type              'X-ray tube'
_exptl_absorpt_coefficient_mu    74.039
_exptl_crystal_density_diffrn    4.6069
_exptl_crystal_F_000             462
_pd_char_colour                  white
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.01
_pd_meas_2theta_range_max        100.090
_pd_meas_2theta_range_min        4.900
_pd_meas_number_of_points        9520
_pd_meas_scan_method             step
_pd_proc_2theta_range_inc        0.01
_pd_proc_2theta_range_max        100.09
_pd_proc_2theta_range_min        4.9
_pd_proc_ls_background_function  '18 Legendre polynoms'
_pd_proc_ls_pref_orient_corr     'March & Dollase'
_pd_proc_ls_profile_function     Pseudo-Voigt
_pd_proc_ls_prof_R_factor        0.0572
_pd_proc_ls_prof_wR_expected     0.0423
_pd_proc_ls_prof_wR_factor       0.0836
_pd_proc_wavelength              1.78892
_refine_diff_density_max         1.21
_refine_diff_density_min         -0.75
_refine_ls_goodness_of_fit_all   1.98
_refine_ls_number_constraints    6
_refine_ls_number_parameters     45
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0349
_refine_ls_R_factor_gt           0.0349
_refine_ls_shift/su_max          0.0402
_refine_ls_shift/su_mean         0.0080
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_all         0.0491
_refine_ls_wR_factor_gt          0.0491
_cod_data_source_file            c9ce01244c6.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:

'_diffrn_radiation_probe' value 'X-ray' changed to 'x-ray' according
to
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 

 Adding full bibliography for 7234030.cif.
;
_cod_original_cell_volume        744.276(12)
_cod_original_sg_symbol_Hall     '-P -2xab;-2yc;-2zabc'
_cod_original_formula_sum        'Gd1 K1 Mo2 O8'
_cod_database_code               7234030