Synthesis of novel series of 7,7′-(substituted methylene)bis-imidazo[1,2-b]pyrazoles via an acid catalyzed one-pot three-component reaction
Driowya, Mohsine; Allouchi, Hassan; Gally, José Manuel; Bonnet, Pascal; Guillaumet, Gérald; New Journal of Chemistry 42 (2018) 5728–; doi:10.1039/C7NJ05088G

data_7057144
_publ_section_title
;
 Synthesis of novel series of 7,7&#x2032;-(substituted
 methylene)bis-imidazo[1,2-b]pyrazoles via an acid catalyzed one-pot
 three-component reaction
;
_journal_issue                   8
_journal_name_full               'New Journal of Chemistry'
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_journal_paper_doi               10.1039/C7NJ05088G
_journal_volume                  42
_journal_year                    2018
_chemical_formula_sum            'C50 H62 N11'
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2017-12-18 deposited with the CCDC.
2018-03-08 downloaded from the CCDC.
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  1 omega   -8.00   49.00   1.0000  100.0000
omega____ theta____ kappa____ phi______ frames
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  2 omega   22.00   86.00   1.0000  100.0000
omega____ theta____ kappa____ phi______ frames
    -       19.6530   77.0000 -150.0000 64

  3 omega  -16.00  106.00   1.0000  100.0000
omega____ theta____ kappa____ phi______ frames
    -       19.6530   77.0000  150.0000 122

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Analytical numeric absorption correction using a multifaceted crystal
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(Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
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_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
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'w=1/[\s^2^(Fo^2^)+(0.0770P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_cod_depositor_comments
'Adding full bibliography for 7057143--7057144.cif.'
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