Solvothermal Synthesis of −LIT-type Zeolite
Takako, Nagase; Takuji, Ikeda; Chie, Abe; Yasuhisa, Hasegawa; Yoshimichi, Kiyozumi; Takaaki, Hanaoka; Crystal Growth & Design 12 (2012) 1752–; doi:10.1021/cg201138f

data_4505870
_publ_section_title
;
 Solvothermal Synthesis of &#x2212;LIT-type Zeolite
;
_journal_issue                   4
_journal_name_full               'Crystal Growth &amp; Design'
_journal_page_first              1752
_journal_paper_doi               10.1021/cg201138f
_journal_volume                  12
_journal_year                    2012
_chemical_formula_analytical     'Al4 H2 K5.8652 O26 Si8'
_chemical_formula_moiety         'Al4 H2 K5.8652 O26 Si8'
_chemical_formula_structural     'Al4 H2 K5.8652 O26 Si8'
_chemical_formula_sum            'Al4 H2 K5.8652 O26 Si8'
_chemical_formula_weight         980.742
_chemical_name_systematic        ' ?'
_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      4
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90
_cell_angle_beta                 89.997(7)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   15.1324(2)
_cell_length_b                   10.2258(1)
_cell_length_c                   8.42153(8)
_cell_measurement_temperature    297
_cell_volume                     1303.16(2)
_computing_cell_refinement       'RIETAN-FP (Izumi and Momma, 2007)'
_computing_molecular_graphics    'VESTA (Momma and Izumi, 2008)'
_computing_structure_refinement  'RIETAN-FP (Izumi and Momma, 2007)'
_diffrn_ambient_temperature      297
_diffrn_radiation_type           'Cu K\a~1~'
_diffrn_radiation_wavelength     1.540590
_diffrn_source                   'X-ray tube'
_diffrn_source_target            Cu
_exptl_crystal_density_diffrn    2.4994
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             972.35
_pd_calc_method                  'Rietveld Refinement'
_pd_char_colour                  white
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.0170
_pd_meas_2theta_range_max        100.1014
_pd_meas_2theta_range_min        8.0000
_pd_meas_number_of_points        5304
_pd_meas_scan_method             step
_pd_proc_2theta_range_inc        0.0170
_pd_proc_2theta_range_max        100.1014
_pd_proc_2theta_range_min        9.0073
_pd_proc_ls_background_function  'composite background function'
_pd_proc_ls_pref_orient_corr     ' ?'
_pd_proc_ls_profile_function     'split pseudo-Voigt function'
_pd_proc_ls_prof_R_factor        0.02318
_pd_proc_ls_prof_wR_expected     0.02308
_pd_proc_ls_prof_wR_factor       0.02997
_pd_spec_mounting                ' ?'
_pd_spec_mount_mode              transmission
_pd_spec_shape                   cylinder
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   1.2982
_refine_ls_hydrogen_treatment    none
_refine_ls_matrix_type           full
_refine_ls_number_constraints    63
_refine_ls_number_parameters     142
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.01157
_refine_ls_R_Fsqd_factor         0.01157
_refine_ls_R_I_factor            0.01770
_refine_ls_shift/su_max          0.0
_refine_ls_weighting_details     1/<i>y</i>~i~
_refine_ls_weighting_scheme      sigma
_cod_data_source_file            cg201138f_si_002.cif
_cod_data_source_block           single_phase
_cod_original_cell_volume        1303.15(2)
_cod_original_sg_symbol_H-M      'P 21'
_cod_database_code               4505870