Intramolecular H-bond stabilization of a primary hydroxylamine in salen-type metal complexes.
Singh, Hardeep; MacKay, Alyson; Sheibany, Nooshin; Chen, Fei; Mosser, Maëlle; Rouet, Pierre-Étienne; Rousseau, Frédéric; Askari, Mohammad S.; Ottenwaelder, Xavier; Chemical communications (Cambridge, England) 57 (2021) 10403–10406; doi:10.1039/d1cc03077a

data_7128998
_publ_section_title
;
 Intramolecular H-bond stabilization of a primary hydroxylamine in
 salen-type metal complexes.
;
_journal_issue                   80
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              10403
_journal_page_last               10406
_journal_paper_doi               10.1039/d1cc03077a
_journal_volume                  57
_journal_year                    2021
_chemical_formula_moiety         'C23 H31 N3 O5 S'
_chemical_formula_sum            'C23 H31 N3 O5 S'
_chemical_formula_weight         461.57
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_audit_creation_method           SHELXL-2017/1
_audit_update_record
;
2021-06-09 deposited with the CCDC.	2021-08-02 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
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_exptl_crystal_colour            yellow
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_refine_ls_number_reflns         4385
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.108
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0506P)^2^+5.8209P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d1cc03077a2.cif
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_cod_depositor_comments
'Adding full bibliography for 7128990--7128999.cif.'
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