The First Nitrosyl Complexes of Niobium and Tantalum
P. James Daff; Peter Legzdins; Steven J. Rettig; Journal of the American Chemical Society 120 (1998) 2688–2689; doi:10.1021/ja9738079

data_4116706
_publ_contact_author_address
;
University of British Columbia
Department of Chemistry
2036 Main Mall
Vancouver, BC V6T 1Z1
Canada
;
_publ_contact_author_email       ' legzdins@chem.ubc.ca '
_publ_contact_author_fax         ' 604-822-2847 '
_publ_contact_author_name        ' Peter Legzdins '
_publ_contact_author_phone       ' 604-822-2471 '
_publ_section_title
;
 The First Nitrosyl Complexes of Niobium and Tantalum
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              2688
_journal_page_last               2689
_journal_paper_doi               10.1021/ja9738079
_journal_volume                  120
_journal_year                    1998
_chemical_formula_moiety         'C15 H33 N Nb O3 P3 Si '
_chemical_formula_sum            'C15 H33 N Nb O3 P3 Si'
_chemical_formula_weight         489.34
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;
nonsense geometrical parameters between disorder components have not
been edited out
;
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_cell_volume                     2348.9(5)
_computing_cell_refinement       'd*TREK (MSC, 1997)'
_computing_data_collection       'd*TREK (MSC, 1997)'
_computing_data_reduction        'teXsan (MSC, 1992-1997)'
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;
SIR92 (Altomare, et. al. 1993)
;
_diffrn_ambient_temperature      180.2
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo^2)]'
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_cod_data_source_block           compound_3
_cod_original_cell_volume        2348.8(6)
_cod_original_sg_symbol_H-M      'P n m a '
_cod_original_formula_sum        'C15 H33 N Nb O3 P3 Si '
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