Bis(β-diketone)-based metallacycles with haloalkane-induced fluorescence enhancement.
Yan, Ming-Jie; Liu, Tian-Fu; Huang, Sheng-Li; Yang, Guo-Yu; Dalton transactions (Cambridge, England : 2003) 50 (2021) 8680–8684; doi:10.1039/d1dt01580j

data_7707564
_publ_section_title
;
 Bis(\b-diketone)-based metallacycles with haloalkane-induced fluorescence
 enhancement.
;
_journal_issue                   25
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              8680
_journal_page_last               8684
_journal_paper_doi               10.1039/d1dt01580j
_journal_volume                  50
_journal_year                    2021
_chemical_formula_sum            'C104 H112 N4 O8 Ru4'
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_audit_update_record
;
2021-01-08 deposited with the CCDC.	2021-06-01 downloaded from the CCDC.
;
_cell_angle_alpha                76.380(2)
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_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
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_diffrn_radiation_type           MoK\a
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_refine_ls_restrained_S_all      1.042
_refine_ls_R_factor_all          0.0818
_refine_ls_R_factor_gt           0.0562
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0859P)^2^+1.1682P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.1603
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_reflns_number_gt                8454
_reflns_number_total             12639
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d1dt01580j2.cif
_cod_data_source_block           q_a_sqd
_cod_depositor_comments          'Adding full bibliography for 7707564.cif.'
_cod_database_code               7707564
_shelx_shelxl_version_number     2018/3
_platon_squeeze_void_probe_radius 1.20
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