LMucko/crystallography-open-database huggingface dataset:
Reactions of Iminophosphorano(8-quinolyl)methane with AlMe~3~: Unexpected Formation of Aluminum Iminophosphorano(2-methyl-8-quinolyl)methandiide Complex
Wang, Zhong-Xia; Li, Ye-Xin; Organometallics 22 (2003) 4900–4904; doi:10.1021/om034045v

data_4062393
_publ_section_title
;
 Reactions of Iminophosphorano(8-quinolyl)methane with AlMe~3~: Unexpected
 Formation of Aluminum Iminophosphorano(2-methyl-8-quinolyl)methandiide
 Complex
;
_journal_issue                   24
_journal_name_full               Organometallics
_journal_page_first              4900
_journal_page_last               4904
_journal_paper_doi               10.1021/om034045v
_journal_volume                  22
_journal_year                    2003
_chemical_formula_sum            'C30 H37 Al2 N2 P'
_chemical_formula_weight         510.55
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 95.960(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   9.998(3)
_cell_length_b                   22.527(6)
_cell_length_c                   13.184(4)
_cell_measurement_temperature    293(2)
_cell_volume                     2953.3(15)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.148
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4062393
Reactivity of [NBu~4~][(C~6~F~5~)~2~M(μ-PPh~2~)~2~M'(acac-O,O')] (M, M' = Pt, Pd) toward Silver Centers. Synthesis of Polynuclear Complexes Containing M-Ag Bonds (M = Pd, Pt)
Alonso, Ester; Forniés, Juan; Fortuño, Consuelo; Martín, Antonio; Orpen, A. Guy; Organometallics 22 (2003) 5011–5019; doi:10.1021/om034047f

data_4062394
_publ_section_title
;
 Reactivity of [NBu~4~][(C~6~F~5~)~2~M(\m-PPh~2~)~2~M'(acac-O,O')]
 (M, M' = Pt, Pd) toward Silver Centers. Synthesis of Polynuclear
 Complexes Containing M-Ag Bonds (M = Pd, Pt)
;
_journal_issue                   24
_journal_name_full               Organometallics
_journal_page_first              5011
_journal_page_last               5019
_journal_paper_doi               10.1021/om034047f
_journal_volume                  22
_journal_year                    2003
_chemical_formula_sum            'C60 H68 F10 N O3 P2 Pd Pt'
_chemical_formula_weight         1404.58
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 100.2130(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   22.9957(13)
_cell_length_b                   12.0462(6)
_cell_length_c                   21.6125(12)
_cell_measurement_temperature    100(2)
_cell_volume                     5892.0(6)
_diffrn_ambient_temperature      100(2)
_exptl_crystal_density_diffrn    1.583
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4062394
Reactivity of [NBu~4~][(C~6~F~5~)~2~M(μ-PPh~2~)~2~M'(acac-O,O')] (M, M' = Pt, Pd) toward Silver Centers. Synthesis of Polynuclear Complexes Containing M-Ag Bonds (M = Pd, Pt)
Alonso, Ester; Forniés, Juan; Fortuño, Consuelo; Martín, Antonio; Orpen, A. Guy; Organometallics 22 (2003) 5011–5019; doi:10.1021/om034047f

data_4062395
_publ_section_title
;
 Reactivity of [NBu~4~][(C~6~F~5~)~2~M(\m-PPh~2~)~2~M'(acac-O,O')]
 (M, M' = Pt, Pd) toward Silver Centers. Synthesis of Polynuclear
 Complexes Containing M-Ag Bonds (M = Pd, Pt)
;
_journal_issue                   24
_journal_name_full               Organometallics
_journal_page_first              5011
_journal_page_last               5019
_journal_paper_doi               10.1021/om034047f
_journal_volume                  22
_journal_year                    2003
_chemical_formula_sum            'C60 H43 Ag Cl3 F10 O2 P3 Pt2'
_chemical_formula_weight         1683.25
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 96.63(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   13.261(5)
_cell_length_b                   22.962(7)
_cell_length_c                   20.048(7)
_cell_measurement_temperature    293(2)
_cell_volume                     6063.8(36)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.844
_refine_ls_R_factor_obs          0.0414
_refine_ls_wR_factor_obs         0.0968
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4062395
Reactivity of [NBu~4~][(C~6~F~5~)~2~M(μ-PPh~2~)~2~M'(acac-O,O')] (M, M' = Pt, Pd) toward Silver Centers. Synthesis of Polynuclear Complexes Containing M-Ag Bonds (M = Pd, Pt)
Alonso, Ester; Forniés, Juan; Fortuño, Consuelo; Martín, Antonio; Orpen, A. Guy; Organometallics 22 (2003) 5011–5019; doi:10.1021/om034047f

data_4062396
_publ_section_title
;
 Reactivity of [NBu~4~][(C~6~F~5~)~2~M(\m-PPh~2~)~2~M'(acac-O,O')]
 (M, M' = Pt, Pd) toward Silver Centers. Synthesis of Polynuclear
 Complexes Containing M-Ag Bonds (M = Pd, Pt)
;
_journal_issue                   24
_journal_name_full               Organometallics
_journal_page_first              5011
_journal_page_last               5019
_journal_paper_doi               10.1021/om034047f
_journal_volume                  22
_journal_year                    2003
_chemical_formula_sum            'C61 H45 Ag Cl4 F10 O2 P3 Pd Pt'
_chemical_formula_weight         1644.04
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 93.780(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.3204(18)
_cell_length_b                   23.828(4)
_cell_length_c                   20.266(3)
_cell_measurement_temperature    100(2)
_cell_volume                     5936.5(15)
_diffrn_ambient_temperature      100(2)
_exptl_crystal_density_diffrn    1.839
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4062396
Synthesis of New Chiral N-Heterocyclic Carbene-Imine Ligands and Their Application to an Asymmetric Allylic Alkylation Reaction
Bonnet, Ludovic G.; Douthwaite, Richard E.; Kariuki, Benson M.; Organometallics 22 (2003) 4187–4189; doi:10.1021/om034050z

data_4062397
_publ_section_title
;
 Synthesis of New Chiral N-Heterocyclic Carbene-Imine Ligands and Their
 Application to an Asymmetric Allylic Alkylation Reaction
;
_journal_issue                   21
_journal_name_full               Organometallics
_journal_page_first              4187
_journal_page_last               4189
_journal_paper_doi               10.1021/om034050z
_journal_volume                  22
_journal_year                    2003
_chemical_absolute_configuration ad
_chemical_formula_sum            'C25 H29 Cl2 N3 Pd'
_chemical_formula_weight         548.81
_space_group_IT_number           19
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   11.0731(6)
_cell_length_b                   18.2240(10)
_cell_length_c                   12.0902(6)
_cell_measurement_temperature    195(2)
_cell_volume                     2439.8(2)
_diffrn_ambient_temperature      195(2)
_exptl_crystal_density_diffrn    1.494
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4062397
Divergent Isomerization Behavior and Rh(I) Coordination Chemistry of Indenyl Ligands Bearing Either One or Two Pnictogen Donor Fragments
; Organometallics  (2003) –; doi:

data_4062398
_publ_section_title
;
 Divergent Isomerization Behavior and Rh(I) Coordination Chemistry
of Indenyl Ligands Bearing Either One or Two Pnictogen Donor
Fragments
;
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C23 H22 N P'
_chemical_formula_weight         343.39
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 102.876(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.5175(12)
_cell_length_b                   8.2259(8)
_cell_length_c                   18.4451(18)
_cell_measurement_temperature    193(2)
_cell_volume                     1851.5(3)
_diffrn_ambient_temperature      193(2)
_exptl_crystal_density_diffrn    1.232
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4062398
; Organometallics  (2003) –; doi:

data_4062399
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C31 H44 Cl N P Rh'
_chemical_formula_weight         600.00
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 105.2511(13)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.7645(10)
_cell_length_b                   7.9199(6)
_cell_length_c                   25.1578(18)
_cell_measurement_temperature    193(2)
_cell_volume                     2838.2(4)
_diffrn_ambient_temperature      193(2)
_exptl_crystal_density_diffrn    1.404
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4062399
; Organometallics  (2003) –; doi:

data_4062400
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C23 H33 Cl P Rh'
_chemical_formula_weight         478.82
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                75.0404(10)
_cell_angle_beta                 75.3897(10)
_cell_angle_gamma                70.3824(10)
_cell_formula_units_Z            2
_cell_length_a                   7.7514(5)
_cell_length_b                   10.6743(7)
_cell_length_c                   14.4876(9)
_cell_measurement_temperature    193(2)
_cell_volume                     1072.66(12)
_diffrn_ambient_temperature      193(2)
_exptl_crystal_density_diffrn    1.482
_exptl_crystal_density_meas      0
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4062400
; Organometallics  (2003) –; doi:

data_4062401
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C53 H70 Li2 P2 Rh2'
_chemical_formula_weight         988.73
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-I 2ya'
_symmetry_space_group_name_H-M   'I 1 2/a 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 97.5269(11)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   18.8574(10)
_cell_length_b                   17.4958(9)
_cell_length_c                   14.0506(7)
_cell_measurement_temperature    193(2)
_cell_volume                     4595.7(4)
_diffrn_ambient_temperature      193(2)
_exptl_crystal_density_diffrn    1.429
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'I 2/a'
_cod_database_code               4062401
; Organometallics  (2003) –; doi:

data_4062402
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C47 H69 Cl2 N2 P Ru'
_chemical_formula_weight         864.98
_space_group_IT_number           19
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.497(3)
_cell_length_b                   15.426(3)
_cell_length_c                   23.201(5)
_cell_measurement_temperature    293(2)
_cell_volume                     4472.9(15)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.284
_cod_database_code               4062402
Dizirconium Complexes Supported by Preorganized Binucleating Bis(amidinates)
Hagadorn, John R.; McNevin, Michael J.; Wiedenfeld, Grant; Shoemaker, Richard; Organometallics 22 (2003) 4818–4824; doi:10.1021/om034063c

data_4062403
_publ_section_title
;
 Dizirconium Complexes Supported by Preorganized Binucleating Bis(amidinates)
;
_journal_issue                   23
_journal_name_full               Organometallics
_journal_page_first              4818
_journal_page_last               4824
_journal_paper_doi               10.1021/om034063c
_journal_volume                  22
_journal_year                    2003
_chemical_formula_sum            'C39 H50 Cl4 N4 O Zr2'
_chemical_formula_weight         915.07
_chemical_name_common            (iPr4Xan)Zr2Cp2Cl4
_space_group_IT_number           33
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2c -2n'
_symmetry_space_group_name_H-M   'P n a 21'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.7785(4)
_cell_length_b                   18.0385(5)
_cell_length_c                   17.8506(5)
_cell_measurement_temperature    137(2)
_cell_volume                     4114.7(2)
_diffrn_ambient_temperature      137(2)
_exptl_crystal_density_diffrn    1.477
_cod_database_code               4062403
Dizirconium Complexes Supported by Preorganized Binucleating Bis(amidinates)
Hagadorn, John R.; McNevin, Michael J.; Wiedenfeld, Grant; Shoemaker, Richard; Organometallics 22 (2003) 4818–4824; doi:10.1021/om034063c

data_4062404
_publ_section_title
;
 Dizirconium Complexes Supported by Preorganized Binucleating Bis(amidinates)
;
_journal_issue                   23
_journal_name_full               Organometallics
_journal_page_first              4818
_journal_page_last               4824
_journal_paper_doi               10.1021/om034063c
_journal_volume                  22
_journal_year                    2003
_chemical_formula_sum            'C39 H54 N4 O Zr2'
_chemical_formula_weight         777.30
_chemical_name_common            (iPr4Xan)Zr2Cp2H4
_space_group_IT_number           33
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2c -2n'
_symmetry_space_group_name_H-M   'P n a 21'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   23.1814(6)
_cell_length_b                   13.7921(4)
_cell_length_c                   11.6429(3)
_cell_measurement_temperature    138(2)
_cell_volume                     3722.47(17)
_diffrn_ambient_temperature      138(2)
_exptl_crystal_density_diffrn    1.387
_cod_database_code               4062404
Dizirconium Complexes Supported by Preorganized Binucleating Bis(amidinates)
Hagadorn, John R.; McNevin, Michael J.; Wiedenfeld, Grant; Shoemaker, Richard; Organometallics 22 (2003) 4818–4824; doi:10.1021/om034063c

data_4062405
_publ_section_title
;
 Dizirconium Complexes Supported by Preorganized Binucleating Bis(amidinates)
;
_journal_issue                   23
_journal_name_full               Organometallics
_journal_page_first              4818
_journal_page_last               4824
_journal_paper_doi               10.1021/om034063c
_journal_volume                  22
_journal_year                    2003
_chemical_formula_sum            'C41 H76 N10 O Zr2'
_chemical_formula_weight         907.56
_chemical_name_common            (iPr4Xan)Zr2(NMe2)6
_space_group_IT_number           154
_symmetry_cell_setting           hexagonal
_symmetry_space_group_name_Hall  'P 32 2"'
_symmetry_space_group_name_H-M   'P 32 2 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            3
_cell_length_a                   13.3607(3)
_cell_length_b                   13.3607(3)
_cell_length_c                   23.5264(8)
_cell_measurement_temperature    143(2)
_cell_volume                     3637.01(17)
_diffrn_ambient_temperature      143(2)
_exptl_crystal_density_diffrn    1.243
_cod_original_sg_symbol_H-M      'P 3 2 21'
_cod_database_code               4062405
; Organometallics  (2003) –; doi:

data_4062406
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C35 H35 Ta'
_chemical_formula_weight         636.58
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 91.7040(11)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   9.21300(10)
_cell_length_b                   30.2980(6)
_cell_length_c                   9.5180(2)
_cell_measurement_temperature    110(2)
_cell_volume                     2655.64(8)
_diffrn_ambient_temperature      110(2)
_exptl_crystal_density_diffrn    1.592
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4062406
; Organometallics  (2003) –; doi:

data_4062407
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C45.5 H57 N2 O2 Ta'
_chemical_formula_weight         844.88
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 107.9610(6)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   32.3570(4)
_cell_length_b                   12.1320(2)
_cell_length_c                   21.2870(3)
_cell_measurement_temperature    110(2)
_cell_volume                     7949.1(2)
_diffrn_ambient_temperature      110(2)
_exptl_crystal_density_diffrn    1.412
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_original_formula_sum        'C45.50 H57 N2 O2 Ta'
_cod_database_code               4062407
; Organometallics  (2003) –; doi:

data_4062408
_journal_name_full               Organometallics
_journal_year                    2003
_chemical_formula_sum            'C41 H44 N O3 Ta'
_chemical_formula_weight         779.72
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 114.2270(6)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   25.8800(4)
_cell_length_b                   19.1250(3)
_cell_length_c                   15.2890(3)
_cell_measurement_temperature    110(2)
_cell_volume                     6900.9(2)
_diffrn_ambient_temperature      110(2)
_exptl_crystal_density_diffrn    1.501
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4062408