2-D Interwoven and 3-D 5-fold Interpenetrating Silver(I) Complexes of 1-(Isocyanidomethyl)-1H-benzotriazole and 1,3-Bis(dicyanomethylidene)indan
Ichiro Ino; Jian Chu Zhong; Megumu Munakata; Takayoshi Kuroda-Sowa; Masahiko Maekawa; Yusaku Suenaga; Yoshinobu Kitamori; Inorganic Chemistry 39 (2000) 4273–4279; doi:10.1021/ic000459u

data_4321369
_publ_section_title
;
 2-D Interwoven and 3-D 5-fold Interpenetrating Silver(I) Complexes of
 1-(Isocyanidomethyl)-1H-benzotriazole and
 1,3-Bis(dicyanomethylidene)indan
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              4273
_journal_page_last               4279
_journal_paper_doi               10.1021/ic000459u
_journal_volume                  39
_journal_year                    2000
_chemical_formula_moiety         'C2 H2 Ag Cl I N O4 '
_chemical_formula_sum            'C2 H2 Ag Cl I N O4'
_chemical_formula_weight         374.27
_space_group_IT_number           29
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      29
_symmetry_space_group_name_Hall  'P 2c -2ac'
_symmetry_space_group_name_H-M   'P c a 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   14.503(1)
_cell_length_b                   5.104(2)
_cell_length_c                   10.2019(9)
_cell_measurement_reflns_used    890
_cell_measurement_temperature    295.2
_cell_measurement_theta_max      27.5
_cell_volume                     755.2(3)
_computing_data_reduction        'teXsan Ver. 1.10'
_computing_publication_material  'teXsan Ver. 1.10'
_computing_structure_refinement  'teXsan Ver. 1.10'
_computing_structure_solution    SIR92
_diffrn_measured_fraction_theta_full 0.9716
_diffrn_measured_fraction_theta_max 0.9716
_diffrn_measurement_device_type  'Quantum CCD/Rigaku AFC7'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.018
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       6
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            890
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_exptl_absorpt_coefficient_mu    7.061
_exptl_absorpt_correction_T_max  0.244
_exptl_absorpt_correction_T_min  0.244
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(Jacobson, 1998)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    3.292
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       brick
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.200
_refine_diff_density_max         2.02
_refine_diff_density_min         -2.99
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   2.618
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     92
_refine_ls_number_reflns         890
_refine_ls_R_factor_gt           0.0460
_refine_ls_shift/su_max          0.0004
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^) + (0.06000(Max(Fo^2^,0) + 2Fc^2^)/3)^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1589
_reflns_number_gt                878
_reflns_number_total             890
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
_cod_data_source_file            ic000459u_1.cif
_cod_data_source_block           '[Ag(L1)(ClO4)]n(1)'
_cod_original_sg_symbol_H-M      'P c a 21 '
_cod_original_formula_sum        'C2 H2 Ag Cl I N O4 '
_cod_database_code               4321369