The Hydrothermal and Structural Chemistry of Oxovanadium-Arylphosphonate Networks and Frameworks
Wayne Ouellette; Guangbin Wang; Hongxue Liu; Gordon T. Yee; Charles J. O'Connor; Jon Zubieta; Inorganic Chemistry 48 (2009) 953–963; doi:10.1021/ic801450m

data_4301277
_publ_contact_author_address
;Department of Chemistry
111 College Place
Syracuse University
Syracuse, NY 13244    
;
_publ_contact_author_name        'Jon Zubieta'
_publ_section_title
;
The Hydrothermal and Structural Chemistry of Oxovanadium-Arylphosphonate
Networks and Frameworks
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              953
_journal_page_last               963
_journal_paper_doi               10.1021/ic801450m
_journal_volume                  48
_journal_year                    2009
_chemical_formula_sum            'C24 H26.5 O16 P3 V1.5'
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_chemical_name_systematic
; 
 ? 
;
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_cell_volume                     7445.1(7)
_computing_cell_refinement       'Bruker SMART'
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_computing_molecular_graphics    'Bruker SHELXTL'
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_diffrn_ambient_temperature      90(2)
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_diffrn_radiation_monochromator  graphite
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_diffrn_reflns_limit_l_min       -38
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_diffrn_source                   'fine-focus sealed tube'
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_exptl_absorpt_correction_T_min  0.8466
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS SHELXL-97 (SHELDRICK, 1997)'
_exptl_crystal_colour            green
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.1153P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                5730
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_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic801450m_si_005_6.cif
_cod_data_source_block
pnma_[V3O3(H2O)(H3L5)2]_._7.5H2O_(6_._7.5H2O)_Compound_6
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_formula_sum        'C24 H26.50 O16 P3 V1.50'
_cod_database_code               4301277