New microporous coordination polymer affording guest-coordination sites at channel wallsElectronic supplementary information (ESI) available: Fig. S1: XRPD patterns of (a) simulation, (b) 2 and (c) 3. See http://www.rsc.org/suppdata/cc/b1/b108695b/
Noro, Shin-ichiro; Kitagawa, Susumu; Yamashita, Masahiro; Wada, Tatsuo; Chemical Communications  (2002) 222–; doi:10.1039/b108695b

data_7114288
_publ_section_title
;
 New microporous coordination polymer affording guest-coordination sites
 at channel wallsElectronic supplementary information (ESI) available:
 Fig. S1: XRPD patterns of (a) simulation, (b) 2 and (c) 3. See
 http://www.rsc.org/suppdata/cc/b1/b108695b/
;
_journal_issue                   3
_journal_name_full               'Chemical Communications'
_journal_page_first              222
_journal_paper_doi               10.1039/b108695b
_journal_year                    2002
_chemical_formula_sum            'C20 H26 Cu N4 O13 Zn'
_chemical_formula_weight         659.37
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                92.801(4)
_cell_angle_beta                 107.034(4)
_cell_angle_gamma                92.175(5)
_cell_formula_units_Z            2
_cell_length_a                   10.5857(9)
_cell_length_b                   20.308(2)
_cell_length_c                   6.3289(6)
_cell_measurement_reflns_used    5561
_cell_measurement_temperature    296.2
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      2.9
_cell_volume                     1297.4(2)
_computing_cell_refinement       PROCESS-AUTO
_computing_data_collection       PROCESS-AUTO
_computing_data_reduction        'teXsan Ver. 1.11'
_computing_publication_material  'teXsan Ver. 1.11'
_computing_structure_refinement  'teXsan Ver. 1.10'
_computing_structure_solution    MITHRIL90
_diffrn_detector_area_resol_mean 10.00
_diffrn_measured_fraction_theta_full 0.9685
_diffrn_measured_fraction_theta_max 0.9685
_diffrn_measurement_device_type  'Rigaku RAXIS-RAPID Imaging Plate'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.049
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       26
_diffrn_reflns_limit_k_min       -26
_diffrn_reflns_limit_l_max       7
_diffrn_reflns_limit_l_min       -8
_diffrn_reflns_number            11493
_diffrn_reflns_theta_full        27.49
_diffrn_reflns_theta_max         27.49
_exptl_absorpt_coefficient_mu    1.817
_exptl_absorpt_correction_T_max  0.865
_exptl_absorpt_correction_T_min  0.679
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(Higashi, 1995)'
_exptl_crystal_colour            sky-blue
_exptl_crystal_density_diffrn    1.688
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prismatic
_exptl_crystal_size_max          0.250
_exptl_crystal_size_mid          0.080
_exptl_crystal_size_min          0.080
_refine_diff_density_max         0.85
_refine_diff_density_min         -0.45
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.240
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     355
_refine_ls_number_reflns         4088
_refine_ls_R_factor_gt           0.0478
_refine_ls_shift/su_max          0.0005
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^) + (0.06000(Max(Fo^2^,0) + 2Fc^2^)/3)^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1097
_reflns_number_gt                4088
_reflns_number_total             5752
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
_cod_data_source_file            b108695b.txt
_cod_data_source_block           {[ZnCu(24pydca)2(H2O)3(DMF)](DMF)}n
_cod_original_cell_volume        1297.3(2)
_cod_original_sg_symbol_H-M      'P -1         '
_cod_original_formula_sum        'C20 H26 Cu N4 O13 Zn '
_cod_database_code               7114288