Dynamic covalent self-assembly and self-sorting processes in the formation of imine-based macrocycles and macrobicyclic cages.
Yang, Zhaozheng; Esteve, Ferran; Antheaume, Cyril; Lehn, Jean-Marie; Chemical science 14 (2023) 6631–6642; doi:10.1039/d3sc01174g

data_1569427
_publ_section_title
;
 Dynamic covalent self-assembly and self-sorting processes in the
 formation of imine-based macrocycles and macrobicyclic cages.
;
_journal_issue                   24
_journal_name_full               'Chemical science'
_journal_page_first              6631
_journal_page_last               6642
_journal_paper_doi               10.1039/d3sc01174g
_journal_volume                  14
_journal_year                    2023
_chemical_formula_moiety         'C72 H66 N8, 3(C H Cl3)'
_chemical_formula_sum            'C75 H69 Cl9 N8'
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_space_group_name_Hall           '-P 1'
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_audit_update_record
;
2020-07-23 deposited with the CCDC.	2023-05-26 downloaded from the CCDC.
;
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_cell_measurement_temperature    120(2)
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_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker PHOTON-III CPAD'
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_refine_ls_extinction_method     none
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0933P)^2^+4.9129P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_Friedel_coverage         0.000
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_reflns_threshold_expression     'I > 2\s(I)'
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