Total Synthesis of Paralemnolide A.
Abe, Hideki; Ogura, Yuta; Kobayashi, Toyoharu; Ito, Hisanaka; Organic letters 19 (2017) 5996–5999; doi:10.1021/acs.orglett.7b03038

data_1547697
_publ_section_title
;
 Total Synthesis of Paralemnolide A.
;
_journal_issue                   21
_journal_name_full               'Organic letters'
_journal_page_first              5996
_journal_page_last               5999
_journal_paper_doi               10.1021/acs.orglett.7b03038
_journal_volume                  19
_journal_year                    2017
_chemical_formula_moiety         'C26 H37 Br O5 Si'
_chemical_formula_sum            'C26 H37 Br O5 Si'
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2017-01-25 # Formatted by publCIF

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pubCIF (Westrip, 2010) and enCIFer (Allen et al. 2004)
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'SHELXTL XT Intrinsic Phasing (Sheldrick, 2013)'
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;
Crystal Faces plugin in Bruker APEX2 software
;
_exptl_crystal_colour            colurless
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0363P)^2^+0.9844P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0715
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_cod_depositor_comments
'Adding full bibliography for 1547697--1547699.cif.'
_cod_database_code               1547697
_shelx_estimated_absorpt_t_min   0.493
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_shelx_res_checksum              83548
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