A Homologous Series of Cobalt, Rhodium, and Iridium Metalloradicals
Ayumi Takaoka; Jonas C. Peters; Inorganic Chemistry 51 (2012) 16–18; doi:10.1021/ic202079r

data_4327866
_publ_section_title
;
 A Homologous Series of Cobalt, Rhodium, and Iridium Metalloradicals
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              16
_journal_page_last               18
_journal_paper_doi               10.1021/ic202079r
_journal_volume                  51
_journal_year                    2012
_chemical_formula_sum            'C71 H75 B Co F24 P4 Si'
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_chemical_name_systematic
; 
 ? 
;
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_cell_length_a                   38.7112(11)
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_cell_measurement_theta_min      2.17
_cell_volume                     15839.8(8)
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_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
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_diffrn_measured_fraction_theta_max 0.996
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_diffrn_measurement_method       'phi and omega scans'
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_diffrn_radiation_type           MoK\a
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_diffrn_reflns_theta_max         26.37
_diffrn_reflns_theta_min         1.48
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
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