Supramolecular triangular and linear arrays of metal-radical solids using pyrazolato-silver(I) motifs.
Yamada, Susumu; Ishida, Takayuki; Nogami, Takashi; Dalton transactions (Cambridge, England : 2003)  (2004) 898–903; doi:10.1039/b312406a

data_7013697
_publ_section_title
;
 Supramolecular triangular and linear arrays of metal-radical solids
 using pyrazolato-silver(I) motifs.
;
_journal_issue                   6
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              898
_journal_page_last               903
_journal_paper_doi               10.1039/b312406a
_journal_year                    2004
_chemical_formula_moiety         'C17 H25 Ag N6 O2 '
_chemical_formula_sum            'C17 H25 Ag N6 O2'
_chemical_formula_weight         453.29
_space_group_IT_number           19
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      19
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_audit_creation_date             'Mon Aug 18 15:42:20 2003'
_audit_creation_method           'by teXsan'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   6.9851(4)
_cell_length_b                   12.5908(7)
_cell_length_c                   22.479(2)
_cell_measurement_reflns_used    20746
_cell_measurement_temperature    90.2
_cell_measurement_theta_max      27.1
_cell_measurement_theta_min      3.1
_cell_volume                     1977.0(2)
_computing_cell_refinement       PROCESS-AUTO
_computing_data_collection       PROCESS-AUTO
_computing_data_reduction        'teXsan Ver. 1.11'
_computing_publication_material  'teXsan Ver. 1.11'
_computing_structure_refinement  'teXsan Ver. 1.10'
_computing_structure_solution    SIR92
_diffrn_detector_area_resol_mean 10.00
_diffrn_measured_fraction_theta_full 0.9652
_diffrn_measured_fraction_theta_max 0.9652
_diffrn_measurement_device_type  'Rigaku RAXIS-RAPID Imaging Plate'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.049
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_number            10383
_diffrn_reflns_theta_full        27.10
_diffrn_reflns_theta_max         27.10
_exptl_absorpt_coefficient_mu    1.040
_exptl_absorpt_correction_T_max  0.697
_exptl_absorpt_correction_T_min  0.476
_exptl_absorpt_correction_type   integration
_exptl_absorpt_process_details   '(Higashi, 1999)'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.523
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.100
_refine_diff_density_max         0.67
_refine_diff_density_min         -1.44
_refine_ls_extinction_coef       0.001(1)
_refine_ls_extinction_method     'Zachariasen(1967) type 2 Gaussian isotropic'
_refine_ls_goodness_of_fit_ref   1.676
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     236
_refine_ls_number_reflns         2415
_refine_ls_R_factor_gt           0.0462
_refine_ls_shift/su_max          0.0003
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^) + (0.06500(Max(Fo^2^,0) + 2Fc^2^)/3)^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1275
_reflns_number_gt                2283
_reflns_number_total             2415
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
_cod_data_source_file            b312406a.txt
_cod_data_source_block           '[Ag(pzbisIN)]n_'
_cod_original_sg_symbol_H-M      'P 21 21 21   '
_cod_original_formula_sum        'C17 H25 Ag N6 O2 '
_cod_database_code               7013697