The preparation and characterisation of cyclam/anthraquinone macrocyle/intercalator complexes and their interactions with DNAElectronic supplementary information (ESI) available: Figs. S1?8; gel electrophoresis patterns, 1H NMR spectra, and overlap interactions between the macrocycle and DNA. See http://www.rsc.org/suppdata/dt/b3/b302123h/
Ellis, Leanne T.; Perkins, David F.; Turner, Peter; Hambley, Trevor W.; Dalton Transactions  (2003) 2728–; doi:10.1039/b302123h

data_7012875
_publ_section_title
;
 The preparation and characterisation of cyclam/anthraquinone
 macrocyle/intercalator complexes and their interactions with
 DNAElectronic supplementary information (ESI) available: Figs. S1?8;
 gel electrophoresis patterns, 1H NMR spectra, and overlap interactions
 between the macrocycle and DNA. See
 http://www.rsc.org/suppdata/dt/b3/b302123h/
;
_journal_issue                   13
_journal_name_full               'Dalton Transactions'
_journal_page_first              2728
_journal_paper_doi               10.1039/b302123h
_journal_year                    2003
_chemical_formula_sum            'C30 H42 Cu F12 N7 O2.2 P2'
_chemical_formula_weight         889.38
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_audit_creation_date             19100-12-01
_audit_creation_method           'by teXsan v1.8'
_audit_update_record
;
?
;
_cell_angle_alpha                95.644(5)
_cell_angle_beta                 95.614(4)
_cell_angle_gamma                105.800(4)
_cell_formula_units_Z            2
_cell_length_a                   8.304(2)
_cell_length_b                   9.899(3)
_cell_length_c                   22.647(6)
_cell_measurement_reflns_used    0
_cell_measurement_temperature    273.2
_cell_measurement_theta_max      0.0
_cell_measurement_theta_min      0.0
_cell_volume                     1767.4(8)
_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
_computing_data_reduction        'teXsan (MSC, 1992-1997)'
_computing_publication_material  'teXsan (MSC, 1992-1997)'
_computing_structure_refinement  'teXsan (MSC, 1992-1997)'
_computing_structure_solution
;
SAPI91 (Fan, 1991)
;
_diffrn_ambient_temperature      273.2
_diffrn_measurement_device_type  unknown
_diffrn_orient_matrix_UB_11      0.00000
_diffrn_orient_matrix_UB_12      0.00000
_diffrn_orient_matrix_UB_13      0.00000
_diffrn_orient_matrix_UB_21      0.00000
_diffrn_orient_matrix_UB_22      0.00000
_diffrn_orient_matrix_UB_23      0.00000
_diffrn_orient_matrix_UB_31      0.00000
_diffrn_orient_matrix_UB_32      0.00000
_diffrn_orient_matrix_UB_33      0.00000
_diffrn_radiation_detector       'scintillation counter'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.00000
_diffrn_reflns_av_sigmaI/netI    0.050
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            8116
_diffrn_reflns_reduction_process 'Lp corrections applied'
_diffrn_reflns_theta_max         28.32
_diffrn_reflns_theta_min         1.83
_diffrn_standards_decay_%        0.00
_diffrn_standards_interval_count 0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.814
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            unknown
_exptl_crystal_density_diffrn    1.671
_exptl_crystal_density_meas      ?
_exptl_crystal_description       unknown
_exptl_crystal_F_000             911.20
_exptl_crystal_size_max          0.00
_exptl_crystal_size_mid          0.00
_exptl_crystal_size_min          0.00
_refine_diff_density_max         0.50
_refine_diff_density_min         -0.54
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   2.791
_refine_ls_goodness_of_fit_ref   3.245
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_constraints    0
_refine_ls_number_parameters     660
_refine_ls_number_reflns         5864
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0728
_refine_ls_R_factor_gt           0.0505
_refine_ls_shift/su_max          0.0831
_refine_ls_shift/su_mean         0.0030
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo)]'
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_all         0.0381
_refine_ls_wR_factor_ref         0.0371
_reflns_number_gt                5864
_reflns_number_total             8116
_reflns_threshold_expression     I>2.50\s(I)
_cod_data_source_file            b302123h.txt
_cod_data_source_block           lte17x_in_P-1_
_cod_original_cell_volume        1767.5(7)
_cod_original_sg_symbol_H-M      'P -1       '
_cod_original_formula_sum        'C30 H42 Cu F12 N7 O2.20 P2 '
_cod_database_code               7012875