Direct access to multi-functionalized benzenes via [4 + 2] annulation of α-cyano-β-methylenones and α,β-unsaturated aldehydes
Jia, Qianfa; Lan, Yunfei; Ye, Xin; Lin, Yinhe; Ren, Qiao; RSC Advances 10 (2020) 29171–29174; doi:10.1039/D0RA05251E

data_7241012
_publ_section_title
;
 Direct access to multi-functionalized benzenes via [4 + 2] annulation of
 \a-cyano-\b-methylenones and \a,\b-unsaturated aldehydes
;
_journal_issue                   49
_journal_name_full               'RSC Advances'
_journal_page_first              29171
_journal_page_last               29174
_journal_paper_doi               10.1039/D0RA05251E
_journal_volume                  10
_journal_year                    2020
_chemical_formula_sum            'C26 H17 N O'
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_audit_update_record
;
2019-10-01 deposited with the CCDC.	2020-07-28 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_cell_length_c                   26.6169(3)
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_computing_structure_refinement  'SHELXL-2014 (Sheldrick, 2014)'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0827P)^2^+1.4719P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_data_source_file            d0ra05251e2.cif
_cod_data_source_block           2019-9-26
_cod_depositor_comments          'Adding full bibliography for 7241012.cif.'
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               7241012
_shelx_estimated_absorpt_t_min   0.767
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