Powder study of <i>trans</i>-tetrachloridobis(isopropylamine)platinum(IV)
Sergei D. Kirik; Aleksandr K. Starkov; Acta Crystallographica Section E 63 (2007) m1705–m1706; doi:10.1107/S1600536807024233

data_2213870
_publ_contact_author_address
;
  Institute of Chem. & Chem. Tech.,
  660049 Krasnoyarsk,
  Russian Federation
;
_publ_contact_author_email       kirik@icct.ru
_publ_contact_author_fax         '+7 (3912) 238658'
_publ_contact_author_name        ' Dr Sergei Kirik  '
_publ_contact_author_phone       '+7 (3912) 495663'
_publ_section_title
;
 Powder study of
 <i>trans</i>-tetrachloridobis(isopropylamine)platinum(IV)
;
_journal_coeditor_code           LH2358
_journal_date_accepted           2007-05-16
_journal_date_recd_electronic    2007-03-30
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1705
_journal_page_last               m1706
_journal_paper_category          QM
_journal_paper_doi               10.1107/S1600536807024233
_journal_volume                  63
_journal_year                    2007
_chemical_formula_analytical     Pt(NH2C3H7)2Cl4
_chemical_formula_iupac          '[Pt Cl4 (C3 H9 N)2]'
_chemical_formula_moiety         'C6 H18 Cl4 N2 Pt'
_chemical_formula_structural     trans-Pt(NH2C3H7)2Cl4
_chemical_formula_sum            'C6 H18 Cl4 N2 Pt'
_chemical_formula_weight         455.11
_chemical_name_common
'trans-bis(isopropylamine) tetrachloro platimun(IV)'
_chemical_name_systematic
trans-tetrachloridobis(isopropylamine)platinum(IV)
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 93.8680(10)
_cell_angle_gamma                90.000
_cell_formula_units_Z            2
_cell_length_a                   8.88860(10)
_cell_length_b                   8.9464(2)
_cell_length_c                   8.3255(2)
_cell_measurement_temperature    293
_cell_volume                     660.54(2)
_computing_cell_refinement       'POWDER (Kirik <i>et al.</i>,  1979)'
_computing_data_collection       'DRON-4 (refernce?)'
_computing_molecular_graphics    'XP (Siemens, 1989) and PLATON (Spek, 2003)'
_computing_structure_refinement  'Modified DBWM'
_computing_structure_solution    'Modified DBWM (Wiles & Young, 1981)'
_diffrn_ambient_temperature      293
_diffrn_measurement_device       'DRON-4 powder diffractometer'
_diffrn_measurement_method       '\q/2\q scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.5418
_diffrn_reflns_av_R_equivalents  0
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       8
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       7
_diffrn_reflns_limit_l_min       -7
_diffrn_reflns_number            692
_diffrn_reflns_theta_max         45.
_diffrn_reflns_theta_min         2.5
_exptl_absorpt_coefficient_mu    27.026
_exptl_absorpt_correction_type   none
_exptl_absorpt_process_details   none
_exptl_crystal_density_diffrn    2.288
_exptl_crystal_F_000             428.0
_refine_ls_goodness_of_fit_all   1.46
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_constraints    0
_refine_ls_number_parameters     42
_refine_ls_number_restraints     0
_refine_ls_shift/su_max          0.1
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_scheme      sigma
_reflns_number_total             533
_cod_data_source_file            lh2358.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:
'_geom_bond_publ_flag' value 'NO' changed to 'no' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29 (9
times).

'_geom_angle_publ_flag' value 'NO' changed to 'no' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29 (9 times).

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_geom_bond_publ_flag' value 'NO' changed to 'no' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29 (9
times).

'_geom_angle_publ_flag' value 'NO' changed to 'no' according
to /home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary
named 'cif_core.dic' version 2.4.1 from 2010-06-29 (9 times).

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_Hall     -P_2ybc
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               2213870