Catalyst-Free Synthesis of Aryl Diamines via a Three-Step Reaction Process.
Bulut, Safak; Queen, Wendy L.; The Journal of organic chemistry 83 (2018) 3806–3818; doi:10.1021/acs.joc.8b00151

data_4035499
_publ_section_title
;
 Catalyst-Free Synthesis of Aryl Diamines via a Three-Step Reaction
 Process.
;
_journal_issue                   7
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              3806
_journal_page_last               3818
_journal_paper_doi               10.1021/acs.joc.8b00151
_journal_volume                  83
_journal_year                    2018
_chemical_formula_sum            'C38 H54 N4 O11'
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_diffrn_reflns_point_group_measured_fraction_full 0.996
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_diffrn_reflns_theta_max         21.089
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_exptl_crystal_colour            'clear colourless'
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_refine_ls_matrix_type           full
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_refine_ls_number_reflns         1863
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_cod_original_sg_symbol_H-M      'P 21/n'
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