LMucko/crystallography-open-database huggingface dataset:
organofunctionalized derivatives of alpha-carborane as molecular precursors to non-oxide ceramics of boron
Johnson, S. E.; Gomez, F. A.; Hawthorne, M. F.; Thorne, K. J.; Mackenzie, J. D.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 113–125; doi:

data_4030497
_publ_section_title
;
 organofunctionalized derivatives of alpha-carborane as molecular
 precursors to non-oxide ceramics of boron
;
_journal_issue                   Supp
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              113
_journal_page_last               125
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'C12 H30 B20'
_chemical_formula_weight         390.58
_space_group_IT_number           33
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      33
_symmetry_space_group_name_Hall  'P -2n -2ac'
_symmetry_space_group_name_H-M   'P c 21 n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   6.7064(4)
_cell_length_b                   11.2290(6)
_cell_length_c                   30.710(2)
_cell_volume                     2312.7(2)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.5418
_exptl_absorpt_coefficient_mu    0.3
_exptl_crystal_density_diffrn    1.12
_refine_ls_number_reflns         1312
_refine_ls_R_factor_gt           0.065
_refine_ls_wR_factor_gt          0.076
_cod_data_source_file            EJSSIC-1992-29-Suppl-113-125.cif
_cod_data_source_block           C12H30B20
_cod_database_code               4030497
Novel main group thiolates as possible sulfide precursors in CVD. Preparation, structures, and properties of Tl(SC6H11) and Pb(Sc6H4-p-CH3)2
Krebs, B.; Brommelhaus, A.; Kersting, B.; Nienhaus, M.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 167–170; doi:

data_4030498
_publ_section_title
;
 Novel main group thiolates as possible sulfide precursors in CVD.
 Preparation, structures, and properties of Tl(SC6H11) and
 Pb(Sc6H4-p-CH3)2
;
_journal_issue                   Supp
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              167
_journal_page_last               170
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'C6 H11 S Tl'
_chemical_formula_weight         319.60
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 92.13(3)
_cell_angle_gamma                90
_cell_formula_units_Z            16
_cell_length_a                   9.104(3)
_cell_length_b                   28.309(8)
_cell_length_c                   11.968(3)
_cell_volume                     3082.3(15)
_diffrn_ambient_temperature      150
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71019
_exptl_absorpt_coefficient_mu    2.134
_exptl_crystal_density_diffrn    2.75
_exptl_crystal_density_meas      2.73
_refine_ls_number_parameters     290
_refine_ls_number_reflns         5792
_refine_ls_R_factor_gt           0.0323
_refine_ls_wR_factor_gt          0.0459
_cod_data_source_file            EJSSIC-1992-29-Suppl-167-180-1.cif
_cod_data_source_block           C6H11STl
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4030498
Novel main group thiolates as possible sulfide precursors in CVD. Preparation, structures, and properties of Tl(SC6H11) and Pb(Sc6H4-p-CH3)2
Krebs, B.; Brommelhaus, A.; Kersting, B.; Nienhaus, M.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 167–170; doi:

data_4030499
_publ_section_title
;
 Novel main group thiolates as possible sulfide precursors in CVD.
 Preparation, structures, and properties of Tl(SC6H11) and
 Pb(Sc6H4-p-CH3)2
;
_journal_issue                   Supp
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              167
_journal_page_last               170
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'C14 H14 Pb S2'
_chemical_formula_weight         453.58
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 94.60(8)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   31.929(34)
_cell_length_b                   5.966(5)
_cell_length_c                   7.178(6)
_cell_volume                     1363(2)
_diffrn_ambient_temperature      150
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71019
_exptl_absorpt_coefficient_mu    1.274
_exptl_crystal_density_diffrn    2.21
_exptl_crystal_density_meas      2.20
_refine_ls_number_parameters     154
_refine_ls_number_reflns         2614
_refine_ls_R_factor_gt           0.0309
_refine_ls_wR_factor_gt          0.0419
_cod_data_source_file            EJSSIC-1992-29-Suppl-167-180-2.cif
_cod_data_source_block           C14H14S2Pb
_cod_original_cell_volume        1362(2)
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4030499
Preparation and crystal structure of a sodium silicon nitride, NaSi2N3
Jacobs, H.; Mengis, H.; European Journal of Solid State and Inorganic Chemistry 30 (1993) 45–53; doi:

data_4030500
_publ_section_title
;
 Preparation and crystal structure of a sodium silicon nitride, NaSi2N3
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              45
_journal_page_last               53
_journal_volume                  30
_journal_year                    1993
_chemical_formula_sum            'N3 Na Si2'
_chemical_formula_weight         121.18
_space_group_IT_number           36
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      36
_symmetry_space_group_name_Hall  'C 2c -2'
_symmetry_space_group_name_H-M   'C m c 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.468(1)
_cell_length_b                   5.502(1)
_cell_length_c                   4.878(5)
_cell_volume                     254.1(3)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.5418
_exptl_crystal_density_diffrn    3.17
_pd_proc_ls_prof_R_factor        0.0837
_pd_proc_ls_prof_wR_factor       0.0943
_refine_ls_number_parameters     27
_refine_ls_number_reflns         200
_refine_ls_R_I_factor            0.0325
_cod_data_source_file            EJSSIC-1993-30-45-53.cif
_cod_data_source_block           NaSi2N3
_cod_database_code               4030500
Crystal structure of KPbFeF6.H2O
Decap, G.; Retoux, R.; Calage, Y.; European Journal of Solid State and Inorganic Chemistry 30 (1993) 63–70; doi:

data_4030501
_publ_section_title
;
 Crystal structure of KPbFeF6.H2O
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              63
_journal_page_last               70
_journal_volume                  30
_journal_year                    1993
_chemical_formula_sum            'F6 Fe H2 K O Pb'
_chemical_formula_weight         434.15
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                86.35(1)
_cell_angle_beta                 82.63(1)
_cell_angle_gamma                89.62(1)
_cell_formula_units_Z            2
_cell_length_a                   5.955(1)
_cell_length_b                   6.125(1)
_cell_length_c                   8.694(2)
_cell_volume                     313.85(10)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    27.813
_exptl_crystal_density_diffrn    4.593
_refine_ls_number_parameters     92
_refine_ls_number_reflns         1932
_refine_ls_R_factor_gt           0.0289
_refine_ls_wR_factor_gt          0.0284
_cod_data_source_file            EJSSIC-1993-30-63-70.cif
_cod_data_source_block           KPb
_cod_original_formula_sum        'H2 F6 Fe K O Pb'
_cod_database_code               4030501
Crystal structures of MSnF3 for M = K, Rb, Tl; ionic mobolity
Foulon, J. D.; Durand, J.; Larbot, A.; Cot, L.; Soufiane, A.; European Journal of Solid State and Inorganic Chemistry 30 (1993) 87–99; doi:

data_4030502
_publ_section_title
;
 Crystal structures of MSnF3 for M = K, Rb, Tl; ionic mobolity
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              87
_journal_page_last               99
_journal_volume                  30
_journal_year                    1993
_chemical_formula_sum            'F3 K Sn'
_chemical_formula_weight         214.8
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                80.02(1)
_cell_angle_beta                 72.39(1)
_cell_angle_gamma                74.50(1)
_cell_formula_units_Z            8
_cell_length_a                   8.080(1)
_cell_length_b                   9.975(2)
_cell_length_c                   10.321(2)
_cell_volume                     760.2(2)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    7.70
_exptl_crystal_density_diffrn    3.754
_exptl_crystal_F_000             768
_refine_ls_number_parameters     181
_refine_ls_number_reflns         2696
_refine_ls_R_factor_gt           0.0312
_refine_ls_wR_factor_gt          0.0370
_cod_data_source_file            EJSSIC-1993-30-87-99-1.cif
_cod_data_source_block           KSnF3
_cod_database_code               4030502
Crystal structures of MSnF3 for M = K, Rb, Tl; ionic mobolity
Foulon, J. D.; Durand, J.; Larbot, A.; Cot, L.; Soufiane, A.; European Journal of Solid State and Inorganic Chemistry 30 (1993) 87–99; doi:

data_4030503
_publ_section_title
;
 Crystal structures of MSnF3 for M = K, Rb, Tl; ionic mobolity
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              87
_journal_page_last               99
_journal_volume                  30
_journal_year                    1993
_chemical_formula_sum            'F3 Rb Sn'
_chemical_formula_weight         261.2
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 112.60(1)
_cell_angle_gamma                90
_cell_formula_units_Z            16
_cell_length_a                   16.011(1)
_cell_length_b                   13.586(2)
_cell_length_c                   8.233(1)
_cell_volume                     1653.4(4)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    17.77
_exptl_crystal_density_diffrn    4.197
_exptl_crystal_F_000             1824
_refine_ls_number_parameters     93
_refine_ls_number_reflns         1165
_refine_ls_R_factor_gt           0.0584
_refine_ls_wR_factor_gt          0.0831
_cod_data_source_file            EJSSIC-1993-30-87-99-2.cif
_cod_data_source_block           RbSnF3
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4030503
Crystal structures of MSnF3 for M = K, Rb, Tl; ionic mobolity
Foulon, J. D.; Durand, J.; Larbot, A.; Cot, L.; Soufiane, A.; European Journal of Solid State and Inorganic Chemistry 30 (1993) 87–99; doi:

data_4030504
_publ_section_title
;
 Crystal structures of MSnF3 for M = K, Rb, Tl; ionic mobolity
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              87
_journal_page_last               99
_journal_volume                  30
_journal_year                    1993
_chemical_formula_sum            'F3 Sn Tl'
_chemical_formula_weight         380.1
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 113.04(1)
_cell_angle_gamma                90
_cell_formula_units_Z            16
_cell_length_a                   15.892(3)
_cell_length_b                   13.579(2)
_cell_length_c                   8.226(1)
_cell_volume                     1633.5(5)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    45.41
_exptl_crystal_density_diffrn    6.182
_exptl_crystal_F_000             2528
_refine_ls_number_parameters     93
_refine_ls_number_reflns         1451
_refine_ls_R_factor_gt           0.0809
_refine_ls_wR_factor_gt          0.1149
_cod_data_source_file            EJSSIC-1993-30-87-99-3.cif
_cod_data_source_block           TlSnF3
_cod_original_cell_volume        1633.6(5)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4030504
Synthesis of the new one-dimensional quaternary compound K2CuTaSe4 and its structural relationship to other compounds in the K/Cu/M/Q (M = Nb, Ta; Q = S, Se) system
Lu, Y.-J.; Wu, P.; Ibers, J. A.; European Journal of Solid State and Inorganic Chemistry 30 (1993) 101–110; doi:

data_4030505
_publ_section_title
;
 Synthesis of the new one-dimensional quaternary compound K2CuTaSe4 and
 its structural relationship to other compounds in the K/Cu/M/Q (M = Nb,
 Ta; Q = S, Se) system
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              101
_journal_page_last               110
_journal_volume                  30
_journal_year                    1993
_chemical_formula_sum            'Cu K2 Se4 Ta'
_chemical_formula_weight         638.54
_space_group_IT_number           70
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      70
_symmetry_space_group_name_Hall  '-F 2uv 2vw'
_symmetry_space_group_name_H-M   'F d d d :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   5.735(3)
_cell_length_b                   13.481(7)
_cell_length_c                   23.941(12)
_cell_volume                     1851.0(16)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.70930
_exptl_absorpt_coefficient_mu    30.652
_exptl_crystal_density_diffrn    4.583
_exptl_crystal_F_000             2208
_refine_ls_number_parameters     17
_refine_ls_number_reflns         423
_refine_ls_R_factor_gt           0.067
_refine_ls_R_I_factor            0.131
_cod_data_source_file            EJSSIC-1993-30-101-110.cif
_cod_data_source_block           K2CuTaSe4
_cod_original_sg_symbol_H-M      'F d d d'
_cod_database_code               4030505
Crystal structure of Cs3Sb3O6(GeO7), its relationship with K3Sb3O6(PO4)2
Pagnoux, C.; Verbaere, A.; Piffard, Y.; Tournoux, M.; European Journal of Solid State and Inorganic Chemistry 30 (1993) 111–123; doi:

data_4030506
_publ_section_title
;
 Crystal structure of Cs3Sb3O6(GeO7), its relationship with K3Sb3O6(PO4)2
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              111
_journal_page_last               123
_journal_volume                  30
_journal_year                    1993
_chemical_formula_sum            'Cs3 Ge2 O13 Sb3'
_chemical_formula_weight         1117.1
_space_group_IT_number           194
_symmetry_cell_setting           hexagonal
_symmetry_Int_Tables_number      194
_symmetry_space_group_name_Hall  '-P 6c 2c'
_symmetry_space_group_name_H-M   'P 63/m m c'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            2
_cell_length_a                   7.3309(5)
_cell_length_b                   7.3309(5)
_cell_length_c                   16.775(2)
_cell_volume                     780.74(12)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    16.27
_exptl_crystal_density_diffrn    4.754
_exptl_crystal_F_000             971
_refine_ls_number_parameters     35
_refine_ls_number_reflns         378
_refine_ls_R_factor_gt           0.041
_refine_ls_wR_factor_gt          0.047
_cod_data_source_file            EJSSIC-1993-30-111-123.cif
_cod_data_source_block           Cs3Sb3
_cod_original_cell_volume        780.74(16)
_cod_database_code               4030506
The (MIII1/2M'V3/3)(PO4)3 compounds, M = Sb, Nd, Eu, Bi; M' = Sb, Nb, Ta. Preparation and structure
Jouanneaux, A.; Fitch, A. N.; Oyetola, S.; Verbaere, A.; Guyomard, D.; Piffard, Y.; European Journal of Solid State and Inorganic Chemistry 30 (1993) 125–137; doi:

data_4030507
_publ_section_title
;
 The (MIII1/2M'V3/3)(PO4)3 compounds, M = Sb, Nd, Eu, Bi; M' = Sb, Nb, Ta.
 Preparation and structure
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              125
_journal_page_last               137
_journal_volume                  30
_journal_year                    1993
_chemical_formula_sum            'O12 P3 Sb0.5 Ta1.5'
_chemical_formula_weight         617.216
_space_group_IT_number           167
_symmetry_cell_setting           trigonal
_symmetry_Int_Tables_number      167
_symmetry_space_group_name_Hall  '-R 3 2"c'
_symmetry_space_group_name_H-M   'R -3 c :H'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            6
_cell_length_a                   8.6417(3)
_cell_length_b                   8.6417(3)
_cell_length_c                   22.1498(3)
_cell_volume                     1432.51(7)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_wavelength     1.50481
_exptl_crystal_density_diffrn    4.293
_pd_proc_ls_prof_wR_expected     0.066
_pd_proc_ls_prof_wR_factor       0.120
_refine_ls_number_parameters     20
_refine_ls_number_reflns         235
_refine_ls_R_I_factor            0.045
_cod_data_source_file            EJSSIC-1993-30-125-137-1.cif
_cod_data_source_block           SbTa
_cod_original_cell_volume        1432.51(12)
_cod_original_sg_symbol_H-M      'R -3 c'
_cod_database_code               4030507
The (MIII1/2M'V3/3)(PO4)3 compounds, M = Sb, Nd, Eu, Bi; M' = Sb, Nb, Ta. Preparation and structure
Jouanneaux, A.; Fitch, A. N.; Oyetola, S.; Verbaere, A.; Guyomard, D.; Piffard, Y.; European Journal of Solid State and Inorganic Chemistry 30 (1993) 125–137; doi:

data_4030508
_publ_section_title
;
 The (MIII1/2M'V3/3)(PO4)3 compounds, M = Sb, Nd, Eu, Bi; M' = Sb, Nb, Ta.
 Preparation and structure
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              125
_journal_page_last               137
_journal_volume                  30
_journal_year                    1993
_chemical_formula_sum            'Nb1.5 O12 P3 Sb0.5'
_chemical_formula_weight         485.154
_space_group_IT_number           60
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      60
_symmetry_space_group_name_Hall  '-P 2n 2ab'
_symmetry_space_group_name_H-M   'P b c n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   12.0769(1)
_cell_length_b                   8.6732(1)
_cell_length_c                   8.7293(1)
_cell_volume                     914.354(17)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_wavelength     1.50481
_exptl_crystal_density_diffrn    3.524
_pd_proc_ls_prof_wR_expected     0.072
_pd_proc_ls_prof_wR_factor       0.130
_refine_ls_number_parameters     38
_refine_ls_number_reflns         678
_refine_ls_R_I_factor            0.067
_cod_data_source_file            EJSSIC-1993-30-125-137-2.cif
_cod_data_source_block           SbTa
_cod_database_code               4030508
Ethylenediamine complexes of magnesium: the search for volatile compounds
Bradley, D. C.; Frigo, D. M.; Harding, I. S.; Motevalli, M.; European Journal of Solid State and Inorganic Chemistry 30 (1993) 241–258; doi:

data_4030509
_publ_section_title
;
 Ethylenediamine complexes of magnesium: the search for volatile compounds
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              241
_journal_page_last               258
_journal_volume                  30
_journal_year                    1993
_chemical_formula_sum            'C20 H52 Mg2 N8'
_chemical_formula_weight         453.297
_space_group_IT_number           61
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      61
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   10.424(5)
_cell_length_b                   16.907(7)
_cell_length_c                   15.601(2)
_cell_volume                     2749.5(18)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    2.83
_exptl_crystal_density_diffrn    1.095
_refine_ls_number_parameters     240
_refine_ls_number_reflns         1421
_refine_ls_R_factor_gt           0.0409
_refine_ls_wR_factor_gt          0.0434
_cod_data_source_file            EJSSIC-1993-30-241-258.cif
_cod_data_source_block           C20H52N8Mg2
_cod_original_formula_sum        'C20 H52 N8 Mg2'
_cod_database_code               4030509