Postsynthetic modification of single Pd sites into uncoordinated polypyridine groups of a MOF as the highly efficient catalyst for Heck and Suzuki reactions
Dong, Dapeng; Li, Zhenghua; Liu, Dedi; Yu, Naisen; Zhao, Haiyan; Chen, Huiying; Liu, Jia; Liu, Dongping; New Journal of Chemistry 42 (2018) 9317–; doi:10.1039/C8NJ00518D

data_7057332
_publ_section_title
;
 Postsynthetic modification of single Pd sites into uncoordinated
 polypyridine groups of a MOF as the highly efficient catalyst for Heck
 and Suzuki reactions
;
_journal_issue                   11
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              9317
_journal_paper_doi               10.1039/C8NJ00518D
_journal_volume                  42
_journal_year                    2018
_chemical_formula_sum            'C66 H42 Ho N9 O6'
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_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2018-03-23 deposited with the CCDC.
2018-04-23 downloaded from the CCDC.
;
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_computing_structure_refinement  'SHELXL-2014 (Sheldrick 2014)'
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_diffrn_ambient_temperature      296(2)
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_type           MoK\a
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0364P)^2^+8.9624P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments          'Adding full bibliography for 7057332.cif.'
_cod_original_cell_volume        5392.8(7)
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