Crystal structures, Hirshfeld atom refinements and Hirshfeld surface analyses of tris(4,5-dihydrofuran-2-yl)methylsilane and tris(4,5-dihydrofuran-2-yl)phenylsilane
Krupp, Anna; Barth, Eva Rebecca; Seymen, Rana; Strohmann, Carsten; Acta Crystallographica Section E 76 (2020) 1514–1519; doi:10.1107/S2056989020011470

data_2243565
_publ_section_title
;
 Crystal structures, Hirshfeld atom refinements and Hirshfeld surface
 analyses of tris(4,5-dihydrofuran-2-yl)methylsilane and
 tris(4,5-dihydrofuran-2-yl)phenylsilane
;
_journal_issue                   9
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              1514
_journal_page_last               1519
_journal_paper_doi               10.1107/S2056989020011470
_journal_volume                  76
_journal_year                    2020
_chemical_formula_iupac          'C18 H20 O3 Si'
_chemical_formula_moiety         'C18 H20 O3 Si'
_chemical_formula_sum            'C18 H20 O3 Si'
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_chemical_name_systematic
;
Tris(4,5-dihydrofuran-2-yl)phenylsilane
;
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2ybc'
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Olex2 1.3
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;
SAINT (Bruker, 2016)
;
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APEX2 (Bruker, 2018)
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SAINT (Bruker, 2016)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>,  2009) and MERCURY (Macrae <i>et
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publCIF (Westrip, 2010)
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SHELXL  (Sheldrick, 2015b)
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SHELXT (Sheldrick, 2015a)
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;
(SADABS; Bruker, 2016)
;
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0530P)^2^+0.5057P] where P=(Fo^2^+2Fc^2^)/3'
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