The intramolecular amination of allenes.
Feast, George C; Page, Lee W; Robertson, Jeremy; Chemical communications (Cambridge, England) 46 (2010) 2835–2837; doi:10.1039/b926179f

data_7105438
_publ_section_title
;
 The intramolecular amination of allenes.
;
_journal_issue                   16
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              2835
_journal_page_last               2837
_journal_paper_doi               10.1039/b926179f
_journal_volume                  46
_journal_year                    2010
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_symmetry_space_group_name_Hall  '-P 1'
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_computing_publication_material  'CRYSTALS (Betteridge et al., 2003)'
_computing_structure_refinement  'CRYSTALS (Betteridge et al., 2003)'
_computing_structure_solution    'SIR92 (Altomare et al., 1994)'
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_diffrn_measurement_device       'Nonius KappaCCD'
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_exptl_absorpt_correction_T_min  0.77
_exptl_absorpt_correction_type   multi-scan
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_exptl_crystal_density_meas      ?
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
Method= Modified Sheldrick
w=1/[\s^2^(F^2^) + ( 0.04P)^2^ + 0.44P]
,where P=(max(Fo^2^,0) + 2Fc^2^)/3
;
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     I>2.0\s(I)
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_oxford_refine_ls_r_factor_ref   0.0360
_oxford_refine_ls_scale          2.280(19)
_oxford_reflns_number_all        2766
_oxford_reflns_threshold_expression_ref I>-10.0\s(I)
_oxford_structure_analysis_title 3-96
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_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P -1 '
_cod_original_formula_sum        'C10 H17 N1 O5 S1'
_cod_database_code               7105438