Isothiourea-mediated asymmetric functionalization of 3-alkenoic acids.
Morrill, Louis C.; Smith, Samuel M.; Slawin, Alexandra M. Z.; Smith, Andrew D.; The Journal of organic chemistry 79 (2014) 1640–1655; doi:10.1021/jo402591v

data_4028985
_publ_section_title
;
 Isothiourea-mediated asymmetric functionalization of 3-alkenoic acids.
;
_journal_issue                   4
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              1640
_journal_page_last               1655
_journal_paper_doi               10.1021/jo402591v
_journal_volume                  79
_journal_year                    2014
_chemical_formula_moiety         'C18 H13 F3 O2'
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_atom_sites_solution_secondary   difmap
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_cell_angle_beta                 97.367(11)
_cell_angle_gamma                90.0000
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_cell_length_a                   14.802(6)
_cell_length_b                   5.944(3)
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_diffrn_ambient_temperature      173
_diffrn_measured_fraction_theta_full 0.995
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_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       platelet
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_exptl_crystal_size_mid          0.030
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_refine_ls_structure_factor_coef Fsqd
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'w = 1/[\s^2^(Fo^2^)+(0.0767P)^2^+0.3074P] where P=(Fo^2^+2Fc^2^)/3'
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