Silver-mediated three-component cycloaddition reaction for direct synthesis of 1-N-vinyl-substituted 1,2,3-triazoles.
Chen, Jinpeng; Liang, Taoyuan; Zhao, He; Lin, Chuyuan; Chen, Lu; Zhang, Min; Organic & biomolecular chemistry 17 (2019) 4843–4849; doi:10.1039/c9ob00686a

data_7156782
_publ_section_title
;
 Silver-mediated three-component cycloaddition reaction for direct
 synthesis of 1-N-vinyl-substituted 1,2,3-triazoles.
;
_journal_issue                   19
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              4843
_journal_page_last               4849
_journal_paper_doi               10.1039/c9ob00686a
_journal_volume                  17
_journal_year                    2019
_chemical_formula_moiety         'C18 H15 N3 O'
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_audit_update_record
;
2019-03-21 deposited with the CCDC.    2019-04-17 downloaded from the CCDC.
;
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_exptl_absorpt_correction_type   none
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_exptl_crystal_description       BLOCK
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_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     SHELXL
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0719P)^2^+0.1393P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1204
_refine_ls_wR_factor_ref         0.1250
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2433
_reflns_number_total             2702
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c9ob00686a2.cif
_cod_data_source_block           1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'NONE' changed to 'none'
according to
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 

 Adding full bibliography for 7156782.cif.
;
_cod_original_cell_volume        768.5(10)
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_shelx_res_checksum              97326
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