Accessing Ni(0) to Ni(IV) <i>via</i> nickel-carbon-phosphorus bond reorganization.
Lin, Lirong; Tresp, David S.; Spasyuk, Denis M.; Lalancette, Roger A.; Prokopchuk, Demyan E.; Chemical communications (Cambridge, England) 60 (2024) 674–677; doi:10.1039/d3cc04687g

data_7132385
_publ_section_title
;
 Accessing Ni(0) to Ni(IV) <i>via</i> nickel-carbon-phosphorus bond
 reorganization.
;
_journal_issue                   6
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              674
_journal_page_last               677
_journal_paper_doi               10.1039/d3cc04687g
_journal_volume                  60
_journal_year                    2024
_chemical_formula_moiety         'C42 H66 Ni P2'
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;
2023-11-16 deposited with the CCDC.	2023-11-22 downloaded from the CCDC.
;
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_diffrn_source                   'micro-focus sealed X-ray tube'
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;
CrysAlisPro 1.171.42.102a (Rigaku Oxford Diffraction, 2023)
Numerical absorption correction based on gaussian integration over
a multifaceted crystal model
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            yellow
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0411P)^2^+4.1527P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7132385--7132386.cif.'
_cod_database_code               7132385
_shelx_shelxl_version_number     2018/3
_shelx_estimated_absorpt_t_min   0.819
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_oxdiff_exptl_absorpt_empirical_full_min 0.789
_oxdiff_exptl_absorpt_empirical_full_max 1.312
_oxdiff_exptl_absorpt_empirical_details
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_shelx_res_checksum              90625
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