Spectroscopic studies of lanthanide complexes of varying nuclearity based on a compartmentalised ligand.
Olea-Román, Daniela; Bélanger-Desmarais, Nicolas; Flores-Álamo, Marcos; Bazán, Claudia; Thouin, Félix; Reber, Christian; Castillo-Blum, Silvia E; Dalton transactions (Cambridge, England : 2003) 44 (2015) 17175–17188; doi:10.1039/c5dt02563j

data_7036293
_publ_section_title
;
 Spectroscopic studies of lanthanide complexes of varying nuclearity based
 on a compartmentalised ligand.
;
_journal_issue                   39
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              17175
_journal_page_last               17188
_journal_paper_doi               10.1039/c5dt02563j
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety         'C40 H29 Cl2 N4 O9 Tb Zn2, N O3, 2(C2 H6 O)'
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2015-08-13 deposited with the CCDC.
2015-08-27 downloaded from the CCDC.
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          'Ortep-3 for Windows (Farrugia, 1997)'
      L. J. Farrugia, J. Appl. Crystallogr., 1997, 30, 565.
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        'WinGX publication routines (Farrugia, 1999)'                 
    L. J. Farrugia, J. Appl. Crystallogr., 1999, 32, 837-838.
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      'SHELXS-2014 (Sheldrick, 2008)'
      G. M. Sheldrick, Acta Crystallogr., Sect. A: 
      Found. Crystallogr., 2008, 64, 112-122.
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_diffrn_ambient_temperature      130(2)
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        CrysAlisPro, Agilent Technologies,
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Analytical numeric absorption correction using a multifaceted crystal
                        model based on expressions derived by R.C. Clark & J.S.
        (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
;
_exptl_crystal_colour            brown
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The SQUEEZE/PLATON program has been used to model some disorder
of ethanol solvent.
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_refine_ls_R_factor_all          0.0444
_refine_ls_R_factor_gt           0.0387
_refine_ls_shift/su_max          0.002
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0592P)^2^+34.6389P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c5dt02563j2.cif
_cod_data_source_block           23-trinuclear-tb299-rev1
_cod_depositor_comments
'Adding full bibliography for 7036293--7036295.cif.'
_cod_original_sg_symbol_H-M      'C 2/c'
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