A four-component domino reaction for the synthesis of novel bridgehead nitrogen-containing pyrido[1,2-d][1,4]diazepines
Wang, Rui; Zhang, Wei; Tang, Ying; Qi, Ze-Hui; Yu, Yuan-Hui; Tan, Hong-Bo; Tang, Dian-Yong; Xu, Zhi-Gang; Chen, Zhong-Zhu; New Journal of Chemistry 46 (2022) 592–598; doi:10.1039/D1NJ04233E

data_7061089
_publ_section_title
;
 A four-component domino reaction for the synthesis of novel bridgehead
 nitrogen-containing pyrido[1,2-d][1,4]diazepines
;
_journal_issue                   2
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              592
_journal_page_last               598
_journal_paper_doi               10.1039/D1NJ04233E
_journal_volume                  46
_journal_year                    2022
_chemical_formula_sum            'C34 H32 N2 O6'
_chemical_formula_weight         564.61
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_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2021-07-26 deposited with the CCDC.	2021-11-26 downloaded from the CCDC.
;
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_computing_structure_solution    'Bruker SHELXTL'
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_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.1037P)^2^+0.0374P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                3005
_reflns_number_total             5062
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d1nj04233e2.cif
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_cod_depositor_comments
'Adding full bibliography for 7061088--7061090.cif.'
_cod_original_cell_volume        1449.2(4)
_cod_database_code               7061089
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_shelx_res_checksum              24024