1,1'-Diacetyloctamethylferrocene: an overlooked and overdue synthon leading to the facile synthesis of an octamethylferrocenophane.
Roemer, Max; Skelton, Brian W.; Piggott, Matthew J.; Koutsantonis, George A.; Dalton transactions (Cambridge, England : 2003) 45 (2016) 18817–18821; doi:10.1039/c6dt03820d

data_7040934
_publ_section_title
;
 1,1'-Diacetyloctamethylferrocene: an overlooked and overdue synthon
 leading to the facile synthesis of an octamethylferrocenophane.
;
_journal_issue                   47
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              18817
_journal_page_last               18821
_journal_paper_doi               10.1039/c6dt03820d
_journal_volume                  45
_journal_year                    2016
_chemical_formula_moiety         'C18 H26 Fe, Cl, H2 O'
_chemical_formula_sum            'C18 H28 Cl Fe O'
_chemical_formula_weight         351.7
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_symmetry_space_group_name_Hall  '-P 1'
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;
2016-08-12 deposited with the CCDC.
2016-10-17 downloaded from the CCDC.
;
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'CrysAlisPro convention (1999,Acta A55,543-557)'
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_diffrn_radiation_type           MoK\a
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;
       CrysAlisPro 1.171.38.41 (Rigaku Oxford Diffraction, 2015)
;
_exptl_crystal_colour            'dark green'
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_exptl_crystal_description       plate
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_exptl_crystal_size_min          0.197
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0412P)^2^+0.1747P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.084
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c6dt03820d2.cif
_cod_data_source_block           gk438
_cod_depositor_comments
'Adding full bibliography for 7040934--7040938.cif.'
_cod_database_code               7040934
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