Group 1 Complexes of an (Amido-amino)silane and Their Use in the Synthesis of the Bi(III) Amide, Bi(Me2Si{NAr}{N(H)Ar})Cl2(Ar = 2,6-i-Pr2C6H3)
Schwamm, Ryan J.; Coles, Martyn P.; Fitchett, Christopher M.; Organometallics 34 (2015) 2500–; doi:10.1021/om5012227

data_4085430
_publ_section_title
;
 Group 1 Complexes of an (Amido-amino)silane and Their Use in the
 Synthesis of the Bi(III) Amide, Bi(Me2Si{NAr}{N(H)Ar})Cl2(Ar =
 2,6-i-Pr2C6H3)
;
_journal_issue                   11
_journal_name_full               Organometallics
_journal_page_first              2500
_journal_paper_doi               10.1021/om5012227
_journal_volume                  34
_journal_year                    2015
_chemical_formula_moiety         'C78 H123 K3 N6 Si3, 2(C3.5), 2(C7 H8)'
_chemical_formula_sum            'C99 H139 K3 N6 Si3'
_chemical_formula_weight         1614.72
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_audit_creation_date             2014-08-06
_audit_creation_method
;
Olex2 1.2
(compiled 2014.07.22 svn.r2960 for OlexSys, GUI svn.r4862)
;
_cell_angle_alpha                84.9008(19)
_cell_angle_beta                 83.8507(18)
_cell_angle_gamma                76.4098(19)
_cell_formula_units_Z            2
_cell_length_a                   16.6239(3)
_cell_length_b                   17.1021(4)
_cell_length_c                   17.7075(4)
_cell_measurement_reflns_used    25315
_cell_measurement_temperature    120.01(10)
_cell_measurement_theta_max      76.5580
_cell_measurement_theta_min      3.5000
_cell_volume                     4854.61(19)
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET)
(compiled Jan 14 2014,18:38:05)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET)
(compiled Jan 14 2014,18:38:05)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET)
(compiled Jan 14 2014,18:38:05)
;
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'olex2.refine (Bourhis et al., 2013)'
_computing_structure_solution    'ShelXS (Sheldrick, 2008)'
_diffrn_ambient_environment      N~2~
_diffrn_ambient_temperature      120.01(10)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 10.6501
_diffrn_detector_type            Atlas
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measurement_details
;
  1 omega -120.00  -37.00   1.0000   12.0000
omega____ theta____ kappa____ phi______ frames
    -      -38.5000 -176.0000  -64.0000 83

  2 omega -107.00  -13.00   1.0000   12.0000
omega____ theta____ kappa____ phi______ frames
    -      -38.5000  -57.0000 -180.0000 94

  3 omega  -49.00   33.00   1.0000   12.0000
omega____ theta____ kappa____ phi______ frames
    -      -38.5000   37.0000  -30.0000 82

  4 omega  -69.00   33.00   1.0000   12.0000
omega____ theta____ kappa____ phi______ frames
    -      -38.5000   77.0000  -30.0000 102

  5 omega  -49.00   33.00   1.0000   12.0000
omega____ theta____ kappa____ phi______ frames
    -      -38.5000   37.0000  120.0000 82

  6 omega   23.00   96.00   1.0000   12.0000
omega____ theta____ kappa____ phi______ frames
    -       42.6255 -125.0000  150.0000 73

  7 omega   90.00  178.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000   30.0000  -30.0000 88

  8 omega   38.00   91.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000  -30.0000  -30.0000 53

  9 omega   31.00  109.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000  -94.0000  120.0000 78

 10 omega   42.00  122.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000 -125.0000   30.0000 80

 11 omega   34.00   93.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000  -94.0000 -180.0000 59

 12 omega   43.00   69.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000 -125.0000  120.0000 26

 13 omega   94.00  121.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000   30.0000 -120.0000 27

 14 omega  127.00  178.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000   30.0000 -150.0000 51

 15 omega  101.00  138.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000   30.0000   30.0000 37

 16 omega   78.00  104.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000  -61.0000    0.0000 26

 17 omega   93.00  118.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000   30.0000 -150.0000 25

 18 omega  113.00  152.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000   77.0000   90.0000 39

 19 omega   44.00   69.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000  -61.0000  120.0000 25

 20 omega   89.00  137.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000  -61.0000  120.0000 48

 21 omega   43.00   97.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000  -61.0000  -60.0000 54

 22 omega   87.00  177.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000   15.0000 -180.0000 90

 23 omega   43.00   87.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000  -45.0000  150.0000 44

 24 omega   32.00  104.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000  -94.0000   30.0000 72

 25 omega   90.00  160.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000   30.0000  -90.0000 70

 26 omega   51.00   83.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000 -125.0000 -180.0000 32

 27 omega   97.00  122.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000 -125.0000 -180.0000 25

 28 omega   93.00  122.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000 -125.0000  -30.0000 29

 29 omega   41.00   72.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000 -125.0000  -30.0000 31

 30 omega   49.00   97.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000 -125.0000  -60.0000 48

 31 omega   85.00  120.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000 -125.0000  -90.0000 35

 32 omega   56.00   98.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000  -45.0000    0.0000 42

 33 omega   55.00   90.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000  -30.0000 -120.0000 35

 34 omega   80.00  109.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000 -125.0000  120.0000 29

 35 omega  108.00  137.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000  -61.0000    0.0000 29

 36 omega   45.00   97.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000  -77.0000  -90.0000 52

 37 omega  148.00  177.00   1.0000   50.0000
omega____ theta____ kappa____ phi______ frames
    -      111.0000   30.0000 -120.0000 29
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       '\w scans'
_diffrn_orient_matrix_UB_11      0.0098489000
_diffrn_orient_matrix_UB_12      -0.0847353000
_diffrn_orient_matrix_UB_13      0.0406522000
_diffrn_orient_matrix_UB_21      0.0333655000
_diffrn_orient_matrix_UB_22      -0.0380177000
_diffrn_orient_matrix_UB_23      -0.0761198000
_diffrn_orient_matrix_UB_31      0.0891761000
_diffrn_orient_matrix_UB_32      0.0008863000
_diffrn_orient_matrix_UB_33      0.0156062000
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0329
_diffrn_reflns_av_unetI/netI     0.0326
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.982
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            58119
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.982
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         77.036
_diffrn_reflns_theta_min         2.664
_diffrn_source                   'sealed X-ray tube'
_diffrn_source_type              'SuperNova (Cu) X-ray Source'
_exptl_absorpt_coefficient_mu    1.942
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.78062
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.31 (release 14-01-2014 CrysAlis171 .NET)
(compiled Jan 14 2014,18:38:05)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.105
_exptl_crystal_description       plate
_exptl_crystal_F_000             1748
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.03
_refine_diff_density_max         0.878
_refine_diff_density_min         -0.653
_refine_diff_density_rms         0.064
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.040
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1097
_refine_ls_number_reflns         20190
_refine_ls_number_restraints     175
_refine_ls_restrained_S_all      1.066
_refine_ls_R_factor_all          0.0761
_refine_ls_R_factor_gt           0.0666
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1025P)^2^+3.8816P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1844
_refine_ls_wR_factor_ref         0.1950
_reflns_Friedel_coverage         0.000
_reflns_number_gt                17108
_reflns_number_total             20190
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            om5012227_si_002.cif
_cod_data_source_block           Compound4-55mc53
_cod_depositor_comments
'Adding full bibliography for 4085428--4085431.cif.'
_cod_original_cell_volume        4854.59(19)
_cod_database_code               4085430
_shelxl_version_number           2014/6
_chemical_oxdiff_formula         C91H61N2P1ZN1
_reflns_odcompleteness_completeness 99.76
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     74.33
_olex2_refinement_description
;
1. Others
 Fixed Sof: C93(0.5) C95(0.5) C96(0.5) C98(0.5) C99(0.5) C100(0.5) C101(0.5)
 C102(0.5)
 Fixed Uiso: H1(0.064) H3(0.049) H5(0.087) H3A(0.058) H4(0.061) H5A(0.057)
 H7(0.069) H8A(0.081) H8B(0.081) H8C(0.081) H9A(0.144) H9B(0.144) H9C(0.144)
 H10(0.07) H11A(0.14) H11B(0.14) H11C(0.14) H12A(0.131) H12B(0.131) H12C(0.131)
 H15(0.044) H16(0.049) H17(0.048) H19(0.045) H20A(0.097) H20B(0.097)
 H20C(0.097) H21A(0.1) H21B(0.1) H21C(0.1) H22(0.055) H23A(0.176) H23B(0.176)
 H23C(0.176) H24A(0.127) H24B(0.127) H24C(0.127) H25A(0.107) H25B(0.107)
 H25C(0.107) H26A(0.131) H26B(0.131) H26C(0.131) H29(0.085) H30(0.092)
 H31(0.086) H33(0.088) H34A(0.096) H34B(0.096) H34C(0.096) H35A(0.181)
 H35B(0.181) H35C(0.181) H36(0.099) H37A(0.189) H37B(0.189) H37C(0.189)
 H38A(0.153) H38B(0.153) H38C(0.153) H41(0.054) H42(0.059) H43(0.055)
 H45(0.054) H46A(0.12) H46B(0.12) H46C(0.12) H47A(0.109) H47B(0.109)
 H47C(0.109) H48(0.06) H49A(0.155) H49B(0.155) H49C(0.155) H50A(0.119)
 H50B(0.119) H50C(0.119) H51A(0.071) H51B(0.071) H51C(0.071) H52A(0.07)
 H52B(0.07) H52C(0.07) H55(0.063) H56(0.091) H57(0.1) H59(0.059) H60A(0.11)
 H60B(0.11) H60C(0.11) H61A(0.18) H61B(0.18) H61C(0.18) H62A(0.066) H62B(0.065)
 H63A(0.114) H63B(0.114) H63C(0.114) H63D(0.115) H63E(0.115) H63F(0.115)
 H64A(0.122) H64B(0.122) H64C(0.122) H64D(0.119) H64E(0.119) H64F(0.119)
 H65A(0.095) H65B(0.095) H65C(0.095) H66A(0.111) H66B(0.111) H66C(0.111)
 H69(0.056) H70(0.055) H71(0.052) H73(0.064) H74A(0.145) H74B(0.145)
 H74C(0.145) H75A(0.076) H75B(0.076) H75C(0.076) H76(0.05) H77A(0.09)
 H77B(0.09) H77C(0.09) H78A(0.083) H78B(0.083) H78C(0.083) H80(0.143)
 H81(0.202) H82(0.199) H83(0.238) H84(0.176) H85A(0.255) H85B(0.255)
 H85C(0.255) H87(0.132) H88(0.127) H89(0.152) H90(0.143) H91(0.141) H92A(0.393)
 H92B(0.393) H92C(0.393)
 Fixed X: H1(1.1305) H3(0.6102) H5(0.5262) H3A(1.3049) H4(1.4044) H5A(1.3851)
 H7(1.1269) H8A(1.1191) H8B(1.0478) H8C(1.072) H9A(1.2304) H9B(1.1454)
 H9C(1.2158) H10(1.2057) H11A(1.3279) H11B(1.2586) H11C(1.2344) H12A(1.3164)
 H12B(1.3057) H12C(1.377) H15(0.8636) H16(0.9067) H17(1.0142) H19(0.9398)
 H20A(0.7907) H20B(0.8037) H20C(0.8051) H21A(0.997) H21B(0.922) H21C(0.9105)
 H22(1.1336) H23A(1.0452) H23B(1.1364) H23C(1.0701) H24A(1.1634) H24B(1.2282)
 H24C(1.2016) H25A(0.9633) H25B(0.9634) H25C(0.9091) H26A(0.9959) H26B(1.0293)
 H26C(1.0915) H29(0.8506) H30(0.7924) H31(0.6656) H33(0.76) H34A(0.8535)
 H34B(0.8966) H34C(0.9145) H35A(0.8713) H35B(0.8548) H35C(0.7841) H36(0.5517)
 H37A(0.5341) H37B(0.4875) H37C(0.5829) H38A(0.5081) H38B(0.441) H38C(0.5028)
 H41(0.8955) H42(0.8493) H43(0.7395) H45(0.8202) H46A(0.9727) H46B(0.9591)
 H46C(0.953) H47A(0.7704) H47B(0.8501) H47C(0.8555) H48(0.6417) H49A(0.7132)
 H49B(0.6182) H49C(0.6775) H50A(0.5788) H50B(0.5263) H50C(0.5592) H51A(0.5251)
 H51B(0.5118) H51C(0.5503) H52A(0.6836) H52B(0.6382) H52C(0.7332) H55(0.4878)
 H56(0.5941) H57(0.6837) H59(0.4408) H60A(0.3581) H60B(0.3135) H60C(0.3484)
 H61A(0.4411) H61B(0.4041) H61C(0.5003) H62A(0.7047) H62B(0.7008) H63A(0.7952)
 H63B(0.8026) H63C(0.7545) H63D(0.8003) H63E(0.8073) H63F(0.7629) H64A(0.6222)
 H64B(0.6751) H64C(0.5914) H64D(0.6338) H64E(0.6763) H64F(0.5915) H65A(0.6773)
 H65B(0.6028) H65C(0.6849) H66A(0.488) H66B(0.4743) H66C(0.5328) H69(1.0588)
 H70(1.0824) H71(1.2187) H73(1.2079) H74A(1.102) H74B(1.0809) H74C(1.0371)
 H75A(1.0852) H75B(1.1265) H75C(1.1795) H76(1.4018) H77A(1.3422) H77B(1.4347)
 H77C(1.3652) H78A(1.3745) H78B(1.4415) H78C(1.3496) H80(0.2121) H81(0.3172)
 H82(0.3068) H83(0.1705) H84(0.0571) H85A(0.0782) H85B(0.0137) H85C(0.0467)
 H87(0.7025) H88(0.6357) H89(0.5752) H90(0.5689) H91(0.6288) H92A(0.6852)
 H92B(0.6979) H92C(0.7663)
 Fixed Y: H1(0.4245) H3(0.1731) H5(-0.3226) H3A(0.4467) H4(0.3309) H5A(0.2407)
 H7(0.5215) H8A(0.4641) H8B(0.5263) H8C(0.4368) H9A(0.5843) H9B(0.6175)
 H9C(0.5546) H10(0.2348) H11A(0.2852) H11B(0.2453) H11C(0.3318) H12A(0.1394)
 H12B(0.1228) H12C(0.1632) H15(0.215) H16(0.0785) H17(0.0358) H19(0.3731)
 H20A(0.3452) H20B(0.429) H20C(0.3597) H21A(0.3436) H21B(0.4189) H21C(0.3348)
 H22(0.157) H23A(0.1052) H23B(0.0533) H23C(0.0222) H24A(0.0095) H24B(0.0348)
 H24C(0.0828) H25A(0.4643) H25B(0.4606) H25C(0.4134) H26A(0.257) H26B(0.322)
 H26C(0.2454) H29(0.2916) H30(0.388) H31(0.386) H33(0.1345) H34A(0.0818)
 H34B(0.0644) H34C(0.1338) H35A(0.2305) H35B(0.1584) H35C(0.2364) H36(0.2385)
 H37A(0.3954) H37B(0.3302) H37C(0.3187) H38A(0.3015) H38B(0.3342) H38C(0.3865)
 H41(-0.1262) H42(-0.0782) H43(0.0332) H45(-0.0424) H46A(-0.1191) H46B(-0.1049)
 H46C(-0.0312) H47A(-0.1554) H47B(-0.1811) H47C(-0.1976) H48(0.1557)
 H49A(0.2082) H49B(0.2313) H49C(0.1611) H50A(0.0706) H50B(0.1471) H50C(0.0673)
 H51A(0.1112) H51B(0.0705) H51C(0.0171) H52A(-0.0581) H52B(0.0035) H52C(-0.005)
 H55(-0.0979) H56(-0.1528) H57(-0.2725) H59(-0.1823) H60A(-0.1913) H60B(-
 0.1288) H60C(-0.0987) H61A(-0.0277) H61B(-0.0543) H61C(-0.077) H62A(-0.3829)
 H62B(-0.3576) H63A(-0.3391) H63B(-0.4325) H63C(-0.3798) H63D(-0.3524) H63E(-
 0.4421) H63F(-0.4102) H64A(-0.425) H64B(-0.4854) H64C(-0.4283) H64D(-0.454)
 H64E(-0.4867) H64F(-0.4228) H65A(-0.3833) H65B(-0.4111) H65C(-0.4147) H66A(-
 0.187) H66B(-0.2749) H66C(-0.2446) H69(0.2428) H70(0.1325) H71(0.0638)
 H73(0.3151) H74A(0.2625) H74B(0.3568) H74C(0.314) H75A(0.3943) H75B(0.4376)
 H75C(0.3955) H76(0.1068) H77A(-0.0184) H77B(-0.0247) H77C(-0.0169)
 H78A(0.1754) H78B(0.0947) H78C(0.1002) H80(0.8858) H81(0.8044) H82(0.7348)
 H83(0.7435) H84(0.8359) H85A(0.9732) H85B(0.9369) H85C(0.9003) H87(0.5353)
 H88(0.4802) H89(0.383) H90(0.3343) H91(0.3912) H92A(0.5665) H92B(0.4869)
 H92C(0.4988)
 Fixed Z: H1(0.3206) H3(0.5174) H5(0.2148) H3A(0.0939) H4(0.1138) H5A(0.2146)
 H7(0.211) H8A(0.0679) H8B(0.1101) H8C(0.1434) H9A(0.1484) H9B(0.1133)
 H9C(0.0708) H10(0.3275) H11A(0.398) H11B(0.4409) H11C(0.4004) H12A(0.269)
 H12B(0.3576) H12C(0.3202) H15(0.1109) H16(0.1446) H17(0.2223) H19(0.1727)
 H20A(0.1309) H20B(0.1498) H20C(0.2141) H21A(0.0498) H21B(0.0483) H21C(0.0285)
 H22(0.2903) H23A(0.3816) H23B(0.3824) H23C(0.3442) H24A(0.2203) H24B(0.2656)
 H24C(0.1893) H25A(0.2565) H25B(0.3453) H25C(0.3082) H26A(0.3976) H26B(0.434)
 H26C(0.4031) H29(0.4603) H30(0.3706) H31(0.331) H33(0.5541) H34A(0.4542)
 H34B(0.5304) H34C(0.4717) H35A(0.5763) H35B(0.6323) H35C(0.6219) H36(0.3758)
 H37A(0.3036) H37B(0.2862) H37C(0.2621) H38A(0.4898) H38B(0.4319) H38C(0.447)
 H41(0.2378) H42(0.1202) H43(0.1129) H45(0.4147) H46A(0.3392) H46B(0.4263)
 H46C(0.3661) H47A(0.4015) H47B(0.446) H47C(0.3597) H48(0.2636) H49A(0.1597)
 H49B(0.1478) H49C(0.1042) H50A(0.1638) H50B(0.2033) H50C(0.2524) H51A(0.3791)
 H51B(0.4609) H51C(0.3928) H52A(0.4951) H52B(0.555) H52C(0.5304) H55(0.371)
 H56(0.4447) H57(0.4156) H59(0.2106) H60A(0.3236) H60B(0.2625) H60C(0.3306)
 H61A(0.2403) H61B(0.1716) H61C(0.1776) H62A(0.2768) H62B(0.223) H63A(0.35)
 H63B(0.3564) H63C(0.4223) H63D(0.3061) H63E(0.2887) H63F(0.3662) H64A(0.4151)
 H64B(0.3573) H64C(0.3351) H64D(0.3422) H64E(0.2643) H64F(0.2668) H65A(0.0358)
 H65B(0.0836) H65C(0.1212) H66A(0.0668) H66B(0.0692) H66C(0.0034) H69(-0.0409)
 H70(0.0455) H71(0.0604) H73(-0.1683) H74A(-0.2083) H74B(-0.2196) H74C(-0.1507)
 H75A(-0.0607) H75B(-0.1309) H75C(-0.0643) H76(-0.0384) H77A(0.0472)
 H77B(0.0143) H77C(-0.041) H78A(0.0731) H78B(0.0835) H78C(0.118) H80(0.0102)
 H81(0.0594) H82(0.1729) H83(0.2386) H84(0.1812) H85A(0.0383) H85B(0.093)
 H85C(0.0144) H87(0.6746) H88(0.775) H89(0.7606) H90(0.6488) H91(0.5415)
 H92A(0.5238) H92B(0.4821) H92C(0.5317)
;