Intermediates for the Convenient Synthesis of Bicyclic Aziridinocarbamates
Mague, Joel T.; Ensley, Harry E.; Ling, Jing; Acta Crystallographica Section C 53 (1997) 1347–1350; doi:10.1107/S0108270197006070

data_2006497
_publ_section_title
;
 Intermediates for the Convenient Synthesis of Bicyclic
 Aziridinocarbamates
;
_journal_issue                   9
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1347
_journal_page_last               1350
_journal_paper_doi               10.1107/S0108270197006070
_journal_volume                  53
_journal_year                    1997
_chemical_formula_structural     'C6 H10 I1 N1 O2'
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_chemical_name_systematic
;
4,4-dimethyl-5-iodo-2-oxazineone
;
_space_group_IT_number           2
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_atom_type_scat_source
International_Tables_for_Xray_Crystallography_(Vol._IV)
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_cell_angle_beta                 113.56(3)
_cell_angle_gamma                83.54(5)
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_cell_length_a                   6.686(3)
_cell_length_b                   11.304(9)
_cell_length_c                   6.399(2)
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_cell_measurement_temperature    293
_cell_measurement_theta_max      16
_cell_measurement_theta_min      13
_cell_volume                     439.8(4)
_computing_cell_refinement       'CAD-4 Software'
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_computing_structure_solution    'Patterson and Fourier methods'
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_diffrn_measurement_device       Enraf_Nonius_CAD4
_diffrn_measurement_method       \q/2\q
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_exptl_absorpt_correction_type   \y_scans_(North,_Phillips_&_Mathews,_1968)
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     '4Fo^2^/[\s^2^(Fo^2^) + 0.0036Fo^4^]'
_refine_ls_weighting_scheme      calc
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