Salen-Based Coordination Polymers of Iron and the Rare Earth Elements
Asamanjoy Bhunia; Yanhua Lan; Valeriu Mereacre; Michael T. Gamer; Annie K. Powell; Peter W. Roesky; Inorganic Chemistry 50 (2011) 12697–12704; doi:10.1021/ic2018264

data_4327153
_publ_contact_author
;
      Prof. Dr. Peter Roesky
      Karlsruher Institut f\"ur Technologie (KIT) 
      Engesserstr. 15, Geb. 30.45
      76128 Karlsruhe
      Bundesrepublik Deutschland
;
_publ_contact_author_email       roesky@kit.edu
_publ_contact_author_fax         '+49/(0)721 608 44854'
_publ_contact_author_phone       '+49/(0)721 608 46117'
_publ_section_title
;
 Salen-Based Coordination Polymers of Iron and the Rare Earth Elements
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              12697
_journal_page_last               12704
_journal_paper_doi               10.1021/ic2018264
_journal_volume                  50
_journal_year                    2011
_chemical_formula_moiety         'C51 H59 Cl2 Dy2 Fe2 N11 O23, 4(C3 H7 N O)'
_chemical_formula_sum            'C63 H87 Cl2 Dy2 Fe2 N15 O27'
_chemical_formula_weight         1994.08
_chemical_name_systematic
;
 ?
;
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_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      29.61
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_computing_cell_refinement       'STOE X-AREA, PLATON (A.L.Spek, 2005)'
_computing_data_collection       'STOE X-AREA'
_computing_data_reduction        'STOE X-RED, PLATON (A.L.Spek, 2005)'
_computing_molecular_graphics    'Diamond 2.1e/3'
_computing_publication_material  'X-STEP32, Microsoft Word'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'STOE IPDS 2'
_diffrn_measurement_method       'area detector'
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_diffrn_reflns_limit_l_min       -25
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_diffrn_reflns_theta_max         25.12
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_refine_ls_R_factor_all          0.0804
_refine_ls_R_factor_gt           0.0678
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'calc w=1/[\s^2^(Fo^2^)+(0.1085P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
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