New Triosmium Complexes Containing a Partially Hydrogenated Bis(ferrocenyl)butadiyne Ligand. Their Structures and Electrochemical Responses
Adams, Richard D.; Qu, Bo; Organometallics 19 (2000) 4090–; doi:10.1021/om000432i

data_4077545
_publ_section_title
;
 New Triosmium Complexes Containing a Partially Hydrogenated
 Bis(ferrocenyl)butadiyne Ligand. Their Structures and Electrochemical
 Responses
;
_journal_issue                   20
_journal_name_full               Organometallics
_journal_page_first              4090
_journal_paper_doi               10.1021/om000432i
_journal_volume                  19
_journal_year                    2000
_chemical_formula_sum            'C42 H32 Cl2 Fe2 O9 Os3 Pt'
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_audit_creation_date             1999-05-30
_audit_creation_method           'by teXsan v1.8'
_audit_update_record
;
?
;
_cell_angle_alpha                96.41(2)
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_cell_length_b                   18.684(5)
_cell_length_c                   10.826(2)
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_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
_computing_data_reduction        'teXsan (MSC, 1992-1997)'
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;
SIR92 (Altomare, et. al. 1993)
;
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\DF (DIFABS; Walker & Stuart, 1983)
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_cod_data_source_file            om000432i.cif
_cod_data_source_block           afc6s.xtl_master_file
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'w = 1/[\s^2^(Fo) +
0.00164|Fo|^2^]' was changed to 'calc'. New tag
'_refine_ls_weighting_details' was created. The value of the new tag
was set to 'w = 1/[\s^2^(Fo) + 0.00164|Fo|^2^]'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        2158.4(9)
_cod_original_sg_symbol_H-M      'P -1       '
_cod_original_formula_sum        'C42 H32 Cl2 Fe2 O9 Os3 Pt '
_cod_database_code               4077545