Tetrakis[{μ~3~-ethoxy(<i>N</i>-methylimino)methanethiolato}copper(I)]
Kuroda-Sowa, T.; Munakata, M.; Miyazaki, M.; Maekawa, M.; Acta Crystallographica Section C 50 (1994) 1026–1028; doi:10.1107/S0108270193013083

data_2009892
_publ_section_title
;
 Tetrakis[{\m~3~-ethoxy(<i>N</i>-methylimino)methanethiolato}copper(I)]
;
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1026
_journal_page_last               1028
_journal_paper_doi               10.1107/S0108270193013083
_journal_volume                  50
_journal_year                    1994
_chemical_formula_moiety         'C8 H16 Cu2 N2 O2 S2'
_chemical_formula_sum            'C8 H16 Cu2 N2 O2 S2'
_chemical_formula_weight         363.44
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.
_cell_angle_beta                 106.618(4)
_cell_angle_gamma                90.
_cell_formula_units_Z            8
_cell_length_a                   17.6990(10)
_cell_length_b                   10.201(2)
_cell_length_c                   15.4469(9)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    296
_cell_measurement_theta_max      23.57
_cell_measurement_theta_min      21.63
_cell_volume                     2672.4(6)
_diffrn_measurement_device       'Rigaku AFC5R'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.018
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            3342
_diffrn_reflns_theta_max         27.5
_diffrn_standards_decay_%        none
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    3.48
_exptl_absorpt_correction_T_max  1.0
_exptl_absorpt_correction_T_min  0.90
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.81
_exptl_crystal_description       plate
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.25
_exptl_crystal_size_min          0.15
_refine_diff_density_max         0.29
_refine_diff_density_min         -0.30
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   1.75
_refine_ls_hydrogen_treatment    'refxyz & Uiso'
_refine_ls_number_parameters     209
_refine_ls_number_reflns         2255
_refine_ls_R_factor_obs          0.027
_refine_ls_shift/esd_max         0.17
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 4F~o~^2^/\s^2^(F~o~^2^)'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.020
_reflns_number_observed          2255
_reflns_number_total             3235
_reflns_observed_criterion       I>3.00\s(I)
_cod_data_source_file            oh1057.cif
_cod_data_source_block           oh1057_structure_1_of_1
_cod_depositor_comments
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The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value '4F~o~^2^/\s^2^(F~o~^2^)' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to 'w =
4F~o~^2^/\s^2^(F~o~^2^)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        2672.4(8)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               2009892