Cu(ii) salen and 1,2,4-triazole complexes from thiosemicarbazone: synthesis, physicochemical and structural properties and cytotoxic activities
Avcu Altiparmak, Elif; Erdemir, Gökçe; Özdemir, Namık; Kuruca, Serap Erdem; Bal-Demirci, Tülay; New Journal of Chemistry 44 (2020) 5333–5342; doi:10.1039/C9NJ04455H

data_7059394
_publ_section_title
;
 Cu(ii) salen and 1,2,4-triazole complexes from thiosemicarbazone:
 synthesis, physicochemical and structural properties and cytotoxic
 activities
;
_journal_issue                   14
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              5333
_journal_page_last               5342
_journal_paper_doi               10.1039/C9NJ04455H
_journal_volume                  44
_journal_year                    2020
_chemical_formula_moiety         'C11 H15 Cu N5 O S, H2 O'
_chemical_formula_sum            'C11 H17 Cu N5 O2 S'
_chemical_formula_weight         346.89
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_space_group_name_Hall           '-P 2yn'
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_audit_update_record
;
2018-10-30 deposited with the CCDC.	2020-03-06 downloaded from the CCDC.
;
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'WinGX (Farrugia, 2012) and PLATON (Spek, 2009)'
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_diffrn_measurement_method       'rotation method, \w scan'
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'sealed X-ray tube, 12 x 0.4 mm long-fine focus'
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0550P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1067
_refine_ls_wR_factor_ref         0.1211
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2374
_reflns_number_total             3644
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c9nj04455h2.cif
_cod_data_source_block           namiko66
_cod_depositor_comments
;Adding full bibliography for 7059394--7059395.cif.

 Adding full bibliography for 7059394--7059395.cif.
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               7059394
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_shelx_res_checksum              10729