Di-μ-chlorobis[chloro(4,7-diphenyl-1,10-phenanthroline)copper(II)]
Atria, A.M.; Baggio, R.F.; Garland, M.T.; Spodine, E.; Acta Crystallographica Section C 50 (1994) 864–866; doi:10.1107/S010827019301217X

data_2009755
_publ_section_title
;
 Di-\m-chlorobis[chloro(4,7-diphenyl-1,10-phenanthroline)copper(II)]
;
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              864
_journal_page_last               866
_journal_paper_doi               10.1107/S010827019301217X
_journal_volume                  50
_journal_year                    1994
_chemical_formula_moiety         'Cu 2+, 2C6 H5 , C12 H6 N2, 2Cl 1-'
_chemical_formula_sum            'C24 H16 Cl2 Cu N2'
_chemical_formula_weight         466.8
_chemical_name_systematic
;
Di-chloro-4,7-diphenyl-1,10-phenantroline copper (II).
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                66.770(10)
_cell_angle_beta                 70.410(10)
_cell_angle_gamma                87.560(10)
_cell_formula_units_Z            2
_cell_length_a                   10.165(2)
_cell_length_b                   10.191(2)
_cell_length_c                   11.004(2)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293
_cell_measurement_theta_max      10
_cell_measurement_theta_min      5
_cell_volume                     981.6(3)
_computing_cell_refinement       'Siemens P3/P4-PC version V4.27 (1991)'
_computing_data_collection       'Siemens P3/P4-PC version V4.27 (1991)'
_computing_data_reduction        'XDISK in SHELXTL/PC (Sheldrick,1991)'
_computing_molecular_graphics    'XP in SHELXTL/PC (Sheldrick,1991)'
_computing_publication_material  'XPUBL in SHELXTL/PC (Sheldrick,1991)'
_computing_structure_refinement  'XLS in SHELXTL/PC (Sheldrick,1991)'
_computing_structure_solution    'XS in SHELXTL/PC (Sheldrick,1991)'
_diffrn_ambient_temperature      293
_diffrn_measurement_device       'Siemens R3m difractometer'
_diffrn_measurement_method       \q/2\q
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.031
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -11
_diffrn_reflns_number            3294
_diffrn_reflns_reduction_process 3098
_diffrn_reflns_theta_max         22.5
_diffrn_reflns_theta_min         1.5
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 98
_diffrn_standards_number         2
_exptl_absorpt_coefficient_mu    1.398
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            Light_green
_exptl_crystal_density_diffrn    1.579
_exptl_crystal_description       Polyhedra
_exptl_crystal_F_000             474
_exptl_crystal_size_max          .22
_exptl_crystal_size_mid          .18
_exptl_crystal_size_min          .14
_refine_diff_density_max         .34
_refine_diff_density_min         -.47
_refine_ls_goodness_of_fit_obs   1.35
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_constraints    0
_refine_ls_number_parameters     262
_refine_ls_number_reflns         2454
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          6.25
_refine_ls_R_factor_obs          0.036
_refine_ls_shift/esd_max         0.069
_refine_ls_shift/esd_mean        0.003
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      unit
_refine_ls_wR_factor_all         6.25
_refine_ls_wR_factor_obs         0.036
_reflns_number_observed          2454
_reflns_number_total             3098
_reflns_observed_criterion       F>4.0\s(F)
_cod_data_source_file            as1079.cif
_cod_data_source_block           cudif
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'None' changed to 'none'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               2009755