Tin(ii) ketoacidoximates: synthesis, X-ray structures and processing to tin(ii) oxide.
Khanderi, Jayaprakash; Davaasuren, Bambar; Alshankiti, Buthainah Ameen; Rothenberger, Alexander; Dalton transactions (Cambridge, England : 2003) 44 (2015) 19820–19828; doi:10.1039/c5dt03103f

data_7036917
_publ_section_title
;
 Tin(ii) ketoacidoximates: synthesis, X-ray structures and processing to
 tin(ii) oxide.
;
_journal_issue                   46
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              19820
_journal_page_last               19828
_journal_paper_doi               10.1039/c5dt03103f
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety         'C12 H26 N4 O11 Sn'
_chemical_formula_sum            'C12 H26 N4 O11 Sn'
_chemical_formula_weight         521.06
_chemical_name_common
'Diaqua tris[2-(methoxyimino) propionato] tin(II) ammonium salt'
_chemical_name_systematic
;
Diaqua tris[2-(methoxyimino) propionato] tin(II) ammonium salt
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2013
_audit_update_record
;
2015-10-07 deposited with the CCDC.
2015-10-21 downloaded from the CCDC.
;
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_cell_angle_gamma                90.000(5)
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_diffrn_measurement_device_type  'STOE IPDS 2'
_diffrn_measurement_method       'rotation method'
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_limit_h_min       -24
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'sealed X-ray tube, 12 x 0.4 mm long-fine focus'
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'Re-crystallisation from solvent: Water'
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_refine_ls_extinction_method     none
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_refine_ls_hydrogen_treatment    mixed
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0265P)^2^+3.0230P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0489
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_reflns_number_gt                4983
_reflns_number_total             5499
_reflns_threshold_expression     'I > 2\s(I)'
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'Adding full bibliography for 7036916--7036918.cif.'
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