LMucko/crystallography-open-database huggingface dataset:
Structure of dilithium tetraammonium <i>cyclo</i>-hexaphosphate tetrahydrate
Elmokhtar, O. S. M. M.; Rzaigui, M.; Jouini, A.; Acta Crystallographica Section C 49 (1993) 435–437; doi:10.1107/S0108270192008023

data_2001843
_publ_section_title
;
 Structure of dilithium tetraammonium <i>cyclo</i>-hexaphosphate
 tetrahydrate
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              435
_journal_page_last               437
_journal_paper_doi               10.1107/S0108270192008023
_journal_volume                  49
_journal_year                    1993
_chemical_formula_moiety         'H16 Li2 N4 O18 P6,4(H2 O1)'
_chemical_formula_sum            'H24 Li2 N4 O22 P6'
_chemical_formula_weight         631.93
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 106.260(10)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   9.429(2)
_cell_length_b                   15.824(3)
_cell_length_c                   7.9310(10)
_cell_volume                     1136.0(4)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.7107
_exptl_absorpt_coefficient_mu    0.562
_exptl_crystal_density_diffrn    1.85
_exptl_crystal_F_000             648
_cod_data_source_file            du0331.cif
_cod_data_source_block           du0331_structure_1_of_1
_cod_original_cell_volume        1136
_cod_database_code               2001843
Seven-coordinate manganese(II) complexes of 2,6-bis[1-(2-hydroxyethylimino)ethyl]pyridine
Brooker, S.; McKee, V.; Acta Crystallographica Section C 49 (1993) 441–445; doi:10.1107/S0108270192007157

data_2001844
_publ_section_title
;
 Seven-coordinate manganese(II) complexes of
 2,6-bis[1-(2-hydroxyethylimino)ethyl]pyridine
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              441
_journal_page_last               445
_journal_paper_doi               10.1107/S0108270192007157
_journal_volume                  49
_journal_year                    1993
_chemical_formula_moiety         'C13 H23 Mn1 N3 O4,2(Cl1 O4)'
_chemical_formula_sum            'C13 H23 Cl2 Mn N3 O12'
_chemical_formula_weight         539.2
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 94.41(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   16.142(3)
_cell_length_b                   12.222(3)
_cell_length_c                   11.047(3)
_cell_volume                     2173.0(9)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    0.893
_exptl_crystal_density_diffrn    1.648
_exptl_crystal_F_000             1108
_cod_data_source_file            mu0301.cif
_cod_data_source_block           mu0301_structure_1_of_3
_cod_original_cell_volume        2173.0(10)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_original_formula_sum        'C13 H23 Cl2 Mn1 N3 O12'
_cod_database_code               2001844
Seven-coordinate manganese(II) complexes of 2,6-bis[1-(2-hydroxyethylimino)ethyl]pyridine
Brooker, S.; McKee, V.; Acta Crystallographica Section C 49 (1993) 441–445; doi:10.1107/S0108270192007157

data_2001845
_publ_section_title
;
 Seven-coordinate manganese(II) complexes of
 2,6-bis[1-(2-hydroxyethylimino)ethyl]pyridine
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              441
_journal_page_last               445
_journal_paper_doi               10.1107/S0108270192007157
_journal_volume                  49
_journal_year                    1993
_chemical_formula_sum            'C15 H19 Mn N5 O2 S2'
_chemical_formula_weight         420
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'I 1 2/a 1'
_cell_angle_alpha                90
_cell_angle_beta                 101.46(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.902(2)
_cell_length_b                   12.581(2)
_cell_length_c                   15.203(3)
_cell_volume                     1856.2(6)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    0.917
_exptl_crystal_density_diffrn    1.504
_exptl_crystal_F_000             868
_cod_data_source_file            mu0301.cif
_cod_data_source_block           mu0301_structure_2_of_3
_cod_original_sg_symbol_H-M      'I 2/a'
_cod_original_formula_sum        'C15 H19 Mn1 N5 O2 S2'
_cod_database_code               2001845
Seven-coordinate manganese(II) complexes of 2,6-bis[1-(2-hydroxyethylimino)ethyl]pyridine
Brooker, S.; McKee, V.; Acta Crystallographica Section C 49 (1993) 441–445; doi:10.1107/S0108270192007157

data_2001846
_publ_section_title
;
 Seven-coordinate manganese(II) complexes of
 2,6-bis[1-(2-hydroxyethylimino)ethyl]pyridine
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              441
_journal_page_last               445
_journal_paper_doi               10.1107/S0108270192007157
_journal_volume                  49
_journal_year                    1993
_chemical_formula_sum            'C13 H19 Mn N9 O2'
_chemical_formula_weight         388
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_H-M   'P b c n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   18.643(7)
_cell_length_b                   12.616(3)
_cell_length_c                   7.127(3)
_cell_volume                     1676.3(10)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    0.783
_exptl_crystal_density_diffrn    1.539
_exptl_crystal_F_000             804
_cod_data_source_file            mu0301.cif
_cod_data_source_block           mu0301_structure_3_of_3
_cod_original_cell_volume        1676.0(10)
_cod_original_sg_symbol_H-M      'P bcn'
_cod_original_formula_sum        'C13 H19 Mn1 N9 O2'
_cod_database_code               2001846
Structure of μ-carbonato-1κ^2^<i>O</i>^1^,<i>O</i>^2^:2κ^2^<i>O</i>^1^,<i>O</i>^3^-bis[(acetylacetonato)(<i>N</i>,<i>N</i>,<i>N'</i>,<i>N'</i>-tetramethylethylenediamine)nickel(II)] (acetylacetonato)aqua(methanol)(<i>N</i>,<i>N</i>,<i>N'</i>,<i>N'</i>-tetramethylethylenediamine)nickel(II) tetraphenylborate
Yamada, K.; Hori, K.; Fukuda, Y.; Acta Crystallographica Section C 49 (1993) 445–448; doi:10.1107/S0108270192007091

data_2001847
_publ_section_title
;Structure of
 \m-carbonato-1\k^2^<i>O</i>^1^,<i>O</i>^2^:2\k^2^<i>O</i>^1^,<i>O</i>^3^-bis[(acetylacetonato)(<i>N</i>,<i>N</i>,<i>N'</i>,<i>N'</i>-tetramethylethylenediamine)nickel(II)]
 (acetylacetonato)aqua(methanol)(<i>N</i>,<i>N</i>,<i>N'</i>,<i>N'</i>-tetramethylethylenediamine)nickel(II)
 tetraphenylborate
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              445
_journal_page_last               448
_journal_paper_doi               10.1107/S0108270192007091
_journal_volume                  49
_journal_year                    1993
_chemical_formula_sum            'C59 H95 B N6 Ni3 O11'
_chemical_formula_weight         1251.32
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                97.41(6)
_cell_angle_beta                 95.29(6)
_cell_angle_gamma                117.83(3)
_cell_formula_units_Z            2
_cell_length_a                   16.965(9)
_cell_length_b                   18.847(8)
_cell_length_c                   12.108(7)
_cell_volume                     3343(3)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    .894
_exptl_crystal_density_diffrn    1.243
_exptl_crystal_F_000             1336
_cod_data_source_file            as1009.cif
_cod_data_source_block           as1009_structure_1_of_1
_cod_original_cell_volume        3344(3)
_cod_original_formula_sum        'C59 H95 B1 N6 Ni3 O11'
_cod_database_code               2001847
The first zwitterionic and bent-sandwiched hafnacarborane 4',5,5',6-Li(THF)-1,1'-<i>commo</i>-Hf(THF)Cl[2-(SiMe~3~)-3-(Me)-2,3-C~2~B~4~H~4~]~2~
Zhang, H.; Jia, L.; Hosmane, N. S.; Acta Crystallographica Section C 49 (1993) 453–456; doi:10.1107/S0108270192008138

data_2001848
_publ_section_title
;The first zwitterionic and bent-sandwiched hafnacarborane
 4',5,5',6-Li(THF)-1,1'-<i>commo</i>-Hf(THF)Cl[2-(SiMe~3~)-3-(Me)-2,3-C~2~B~4~H~4~]~2~
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              453
_journal_page_last               456
_journal_paper_doi               10.1107/S0108270192008138
_journal_volume                  49
_journal_year                    1993
_chemical_formula_moiety         'C20 H48 B8 Cl1 Hf1 Li1 O2 Si2'
_chemical_formula_sum            'C20 H48 B8 Cl Hf Li O2 Si2'
_chemical_formula_weight         684.1
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 90.41(3)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   16.821(5)
_cell_length_b                   16.277(5)
_cell_length_c                   12.131(5)
_cell_volume                     3321(2)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    3.474
_exptl_crystal_density_diffrn    1.368
_exptl_crystal_F_000             1376
_cod_data_source_file            cr1005.cif
_cod_data_source_block           cr1005_structure_1_of_1
_cod_depositor_comments
;
 Marking attached hydrogen atoms.

 Antanas Vaitkus,
 2017-03-27
;
_cod_original_formula_sum        'C20 H48 B8 Cl1 Hf1 Li1 O2 Si2'
_cod_database_code               2001848
Structure of the dinuclear platinum monohydrido bridged complex [(PEt~3~)~2~HPt(μ-H)PtH(PEt~3~)~2~][BPh~4~]
Bachechi, F.; Acta Crystallographica Section C 49 (1993) 460–464; doi:10.1107/S0108270192007674

data_2001849
_publ_section_title
;
 Structure of the dinuclear platinum monohydrido bridged complex
 [(PEt~3~)~2~HPt(\m-H)PtH(PEt~3~)~2~][BPh~4~]
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              460
_journal_page_last               464
_journal_paper_doi               10.1107/S0108270192007674
_journal_volume                  49
_journal_year                    1993
_chemical_formula_moiety         'C24 H63 P4 Pt2, C24 H20 B1'
_chemical_formula_sum            'C48 H83 B P4 Pt2'
_chemical_formula_weight         1185.1
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yac'
_symmetry_space_group_name_H-M   'C 2/n 1 1'
_cell_angle_alpha                90
_cell_angle_beta                 93.10(3)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   23.284(10)
_cell_length_b                   20.923(7)
_cell_length_c                   21.822(8)
_cell_volume                     10615(7)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    5.47
_exptl_crystal_density_diffrn    1.483
_exptl_crystal_F_000             4736
_cod_data_source_file            na1006.cif
_cod_data_source_block           na1006_structure_1_of_1
_cod_original_cell_volume        10615(6)
_cod_original_sg_symbol_H-M      'C 2/n'
_cod_original_formula_sum        'C48 H83 B1 P4 Pt2'
_cod_database_code               2001849
Structure of bis(dimethylammonium) bis(tetrabutylammonium) β-octamolybdate
Wang, Q.; Xu, X.; Wang, X.; Acta Crystallographica Section C 49 (1993) 464–467; doi:10.1107/S0108270192007868

data_2001850
_publ_section_title
;
 Structure of bis(dimethylammonium) bis(tetrabutylammonium)
 \b-octamolybdate
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              464
_journal_page_last               467
_journal_paper_doi               10.1107/S0108270192007868
_journal_volume                  49
_journal_year                    1993
_chemical_formula_moiety         '2(C2 H8 N1),2(C16 H36 N1),Mo8 O26'
_chemical_formula_sum            'C36 H88 Mo8 N4 O26'
_chemical_formula_weight         1760.63
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 99.24(2)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   10.287(2)
_cell_length_b                   14.033(4)
_cell_length_c                   21.241(4)
_cell_volume                     3026.5(12)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.7107
_exptl_absorpt_coefficient_mu    1.64
_exptl_crystal_density_diffrn    1.93
_exptl_crystal_F_000             1752
_cod_data_source_file            cr0415.cif
_cod_data_source_block           cr0415_structure_1_of_1
_cod_depositor_comments
;
 Updating space group information and adding the symmetry operation list.

 Antanas Vaitkus,
 2018-06-15
;
_cod_original_cell_volume        3026.4
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               2001850
Structure of tetrakis(μ-acetato)-bis(4-pyridylmethanol)dicopper(II)
Hoang, N. N.; Valach, F.; Melník, M.; Acta Crystallographica Section C 49 (1993) 467–469; doi:10.1107/S010827019200386X

data_2001851
_publ_section_title
;
 Structure of tetrakis(\m-acetato)-bis(4-pyridylmethanol)dicopper(II)
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              467
_journal_page_last               469
_journal_paper_doi               10.1107/S010827019200386X
_journal_volume                  49
_journal_year                    1993
_chemical_formula_sum            'C20 H26 Cu2 N2 O10'
_chemical_formula_weight         581.53
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                91.4070(10)
_cell_angle_beta                 98.2470(10)
_cell_angle_gamma                114.242(3)
_cell_formula_units_Z            1
_cell_length_a                   7.301(4)
_cell_length_b                   8.216(4)
_cell_length_c                   10.709(5)
_cell_volume                     577.2(5)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    1.90
_exptl_crystal_density_diffrn    1.67
_exptl_crystal_density_meas      1.63
_exptl_crystal_F_000             298
_cod_data_source_file            al0509.cif
_cod_data_source_block           al0509_structure_1_of_1
_cod_original_cell_volume        577.27
_cod_database_code               2001851
Structure and solid-state tin-119 and tellurium-125 NMR spectra of 2,2,4,4,6,6-hexakis(trimethylsilylmethyl)cyclotristannatellurane
Einstein, F. W. B.; Gay, I. D.; Jones, C. H. W.; Riesen, A.; Sharma, R. D.; Acta Crystallographica Section C 49 (1993) 470–472; doi:10.1107/S0108270192008400

data_2001852
_publ_section_title
;
 Structure and solid-state tin-119 and tellurium-125 NMR spectra of
 2,2,4,4,6,6-hexakis(trimethylsilylmethyl)cyclotristannatellurane
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              470
_journal_page_last               472
_journal_paper_doi               10.1107/S0108270192008400
_journal_volume                  49
_journal_year                    1993
_chemical_formula_sum            'C24 H66 Si6 Sn3 Te3'
_chemical_formula_weight         1262.2
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 107.86(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   18.392(3)
_cell_length_b                   12.723(3)
_cell_length_c                   22.183(3)
_cell_volume                     4940.7(17)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    3.414
_exptl_crystal_density_diffrn    1.698
_exptl_crystal_F_000             2399
_cod_data_source_file            cd1004.cif
_cod_data_source_block           cd1004_structure_1_of_1
_cod_original_cell_volume        4941
_cod_database_code               2001852
Structures of bis(triphenylphosphine)gold(I) hexafluorophosphate, [Au(PPh~3~)~2~]PF~6~ (1), and bis(triphenylphosphine)gold(I) nitrate, [Au(PPh~3~)~2~]NO~3~ (2)
Staples, R. J.; King, C.; Khan, M. N. I.; Winpenny, R. E. P.; Fackler, Jnr, J. P.; Acta Crystallographica Section C 49 (1993) 472–475; doi:10.1107/S0108270192008680

data_2001853
_publ_section_title
;
 Structures of bis(triphenylphosphine)gold(I) hexafluorophosphate,
 [Au(PPh~3~)~2~]PF~6~ (1), and bis(triphenylphosphine)gold(I) nitrate,
 [Au(PPh~3~)~2~]NO~3~ (2)
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              472
_journal_page_last               475
_journal_paper_doi               10.1107/S0108270192008680
_journal_volume                  49
_journal_year                    1993
_chemical_formula_moiety         'C36 H30 Au1 P2,F6 P1'
_chemical_formula_sum            'C36 H30 Au F6 P3'
_chemical_formula_weight         866.5
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 96.720(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.9270(10)
_cell_length_b                   20.086(5)
_cell_length_c                   17.500(5)
_cell_volume                     3465.4(14)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    4.428
_exptl_crystal_density_diffrn    1.66
_exptl_crystal_F_000             1696
_cod_data_source_file            br1000.cif
_cod_data_source_block           br1000_structure_1_of_2
_cod_original_cell_volume        3465.0(10)
_cod_original_formula_sum        'C36 H30 Au1 F6 P3'
_cod_database_code               2001853
Structures of bis(triphenylphosphine)gold(I) hexafluorophosphate, [Au(PPh~3~)~2~]PF~6~ (1), and bis(triphenylphosphine)gold(I) nitrate, [Au(PPh~3~)~2~]NO~3~ (2)
Staples, R. J.; King, C.; Khan, M. N. I.; Winpenny, R. E. P.; Fackler, Jnr, J. P.; Acta Crystallographica Section C 49 (1993) 472–475; doi:10.1107/S0108270192008680

data_2001854
_publ_section_title
;
 Structures of bis(triphenylphosphine)gold(I) hexafluorophosphate,
 [Au(PPh~3~)~2~]PF~6~ (1), and bis(triphenylphosphine)gold(I) nitrate,
 [Au(PPh~3~)~2~]NO~3~ (2)
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              472
_journal_page_last               475
_journal_paper_doi               10.1107/S0108270192008680
_journal_volume                  49
_journal_year                    1993
_chemical_formula_moiety         'C36 H30 Au1 P2,N1 O3'
_chemical_formula_sum            'C36 H30 Au N O3 P2'
_chemical_formula_weight         783.5
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 112.40(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   17.502(5)
_cell_length_b                   11.0200(10)
_cell_length_c                   18.012(3)
_cell_volume                     3211.9(12)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    4.704
_exptl_crystal_density_diffrn    1.59
_exptl_crystal_F_000             1544
_cod_data_source_file            br1000.cif
_cod_data_source_block           br1000_structure_2_of_2
_cod_original_cell_volume        3212.0(10)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_original_formula_sum        'C36 H30 Au1 N1 O3 P2'
_cod_database_code               2001854
Structures of {diethyl 2-[(8-hydroxy-κ<i>O</i>-2-quinolyl-κ<i>N</i>)methyl]malonato(2–)-κ<i>C</i>^2^}(pyridine)palladium(II) and the analogous ethyl complex
Yoneda, A.; Newkome, G. R.; Morimoto, Y.; Higuchi, Y.; Yasuoka, N.; Acta Crystallographica Section C 49 (1993) 476–478; doi:10.1107/S0108270192010801

data_2001855
_publ_section_title
;Structures of {diethyl
 2-[(8-hydroxy-\k<i>O</i>-2-quinolyl-\k<i>N</i>)methyl]malonato(2--)-\k<i>C</i>^2^}(pyridine)palladium(II)
 and the analogous ethyl complex
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              476
_journal_page_last               478
_journal_paper_doi               10.1107/S0108270192010801
_journal_volume                  49
_journal_year                    1993
_chemical_formula_sum            'C22 H26 N2 O7 Pd'
_chemical_formula_weight         536.82
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                128.34(2)
_cell_angle_beta                 91.930(10)
_cell_angle_gamma                97.18(2)
_cell_formula_units_Z            2
_cell_length_a                   11.6740(10)
_cell_length_b                   11.740(3)
_cell_length_c                   10.863(3)
_cell_volume                     1146.7(6)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.7107
_exptl_absorpt_coefficient_mu    0.84
_exptl_crystal_density_diffrn    1.555
_exptl_crystal_density_meas      1.441
_exptl_crystal_F_000             528
_cod_data_source_file            as0558.cif
_cod_data_source_block           as0558_structure_1_of_2
_cod_original_cell_volume        1146.7(8)
_cod_original_formula_sum        'C22 H26 N2 O7 Pd1'
_cod_database_code               2001855