Intriguing Two-Dimensional Assembly of Cobaloxime with a [Zn2(OOCR)4] Center
Sarvendra Kumar; B. D. Gupta; Inorganic Chemistry 50 (2011) 9207–9209; doi:10.1021/ic201435j

data_4326407
_publ_section_title
;
 Intriguing Two-Dimensional Assembly of Cobaloxime with a [Zn2(OOCR)4]
 Center
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              9207
_journal_page_last               9209
_journal_paper_doi               10.1021/ic201435j
_journal_volume                  50
_journal_year                    2011
_chemical_formula_sum            'C15 H22 Co N5 O6'
_chemical_formula_weight         427.31
_chemical_name_systematic
;
 ?
;
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_atom_sites_solution_secondary   difmap
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_cell_angle_beta                 92.741(5)
_cell_angle_gamma                90.00
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_cell_length_a                   8.042(3)
_cell_length_b                   33.383(10)
_cell_length_c                   13.643(4)
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_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      25.56
_cell_measurement_theta_min      2.36
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_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0591
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_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       37
_diffrn_reflns_limit_k_min       -40
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_diffrn_reflns_limit_l_min       -8
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_diffrn_reflns_theta_full        25.50
_diffrn_reflns_theta_max         25.50
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_exptl_absorpt_correction_T_max  0.8130
_exptl_absorpt_correction_T_min  0.7844
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.552
_exptl_crystal_description       prism
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_exptl_crystal_size_min          0.22
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_refine_ls_extinction_method     none
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_refine_ls_R_factor_all          0.0775
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0810P)^2^+0.8460P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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