6,6'-[(1<i>E</i>,1'<i>E</i>)-Oxybis(4,1-phenylene)bis(azanylylidene)bis(methanylylidene)]bis(2-methylphenol): supramolecular assemblies in two dimensions mediated by weak C—H···N, C—H···O and C—H···π interactions
Arafath, Md. Azharul; Kwong, Huey Chong; Adam, Farook; Razali, Mohd. R.; Acta Crystallographica Section E 74 (2018) 687–690; doi:10.1107/S2056989018005959

data_2242459
_publ_section_title
;
 6,6'-[(1<i>E</i>,1'<i>E</i>)-Oxybis(4,1-phenylene)bis(azanylylidene)bis(methanylylidene)]bis(2-methylphenol):
 supramolecular assemblies in two dimensions mediated by weak
 C---H&#x00B7;&#x00B7;&#x00B7;N, C---H&#x00B7;&#x00B7;&#x00B7;O and
 C---H&#x00B7;&#x00B7;&#x00B7;\p interactions
;
_journal_coeditor_code           JJ2197
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              687
_journal_page_last               690
_journal_paper_doi               10.1107/S2056989018005959
_journal_volume                  74
_journal_year                    2018
_chemical_formula_iupac          'C28 H24 N2 O3'
_chemical_formula_moiety         'C28 H24 N2 O3'
_chemical_formula_sum            'C28 H24 N2 O3'
_chemical_formula_weight         436.49
_chemical_name_systematic
6,6'-[(1<i>E</i>,1'<i>E</i>)-Oxybis(4,1-phenylene)bis(azanylylidene)bis(methanylylidene)]bis(2-methylphenol)
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2014/7
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_cell_angle_beta                 96.7616(10)
_cell_angle_gamma                110.4087(10)
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_cell_length_c                   11.3087(4)
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_cell_measurement_theta_max      30.20
_cell_measurement_theta_min      2.20
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;
SAINT (Bruker, 2012)
;
_computing_data_collection
;
APEX2 (Bruker, 2012)
;
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SAINT (Bruker, 2012)
;
_computing_molecular_graphics
;
SHELXL2013 (Sheldrick, 2015) and Mercury (Macrae <i>et al.</i>,
2006)
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SHELXL2013 (Sheldrick, 2015) and PLATON (Spek, 2009)
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SHELXL2013 (Sheldrick, 2015)
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SHELXS97 (Sheldrick, 2008)
;
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;
Bruker APEXII DUO CCD area-detector
;
_diffrn_measurement_method       '\f and \w scans'
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_diffrn_reflns_limit_k_max       15
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;
(SADABS; Bruker, 2012)
;
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_exptl_crystal_size_mid          0.310
_exptl_crystal_size_min          0.131
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_refine_ls_number_reflns         6513
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_refine_ls_R_factor_all          0.0545
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0747P)^2^+0.3053P] where P=(Fo^2^+2Fc^2^)/3'
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_refine_ls_wR_factor_ref         0.1311
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_reflns_threshold_expression     'I > 2\s(I)'
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_shelx_estimated_absorpt_t_min   0.970
_shelx_estimated_absorpt_t_max   0.989
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