Synthesis, structure, and spin crossover above room temperature of a mononuclear and related dinuclear double helicate iron(ii) complexes.
Hagiwara, Hiroaki; Tanaka, Tomoko; Hora, Shiori; Dalton transactions (Cambridge, England : 2003) 45 (2016) 17132–17140; doi:10.1039/c6dt02766k

data_7040294
_publ_section_title
;
 Synthesis, structure, and spin crossover above room temperature of a
 mononuclear and related dinuclear double helicate iron(ii) complexes.
;
_journal_issue                   43
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              17132
_journal_page_last               17140
_journal_paper_doi               10.1039/c6dt02766k
_journal_volume                  45
_journal_year                    2016
_chemical_formula_sum            'C22 H26 F12 Fe N10 P2'
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_symmetry_space_group_name_Hall  '-P 2yab'
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_audit_update_record
;
2016-08-09 deposited with the CCDC.
2016-08-12 downloaded from the CCDC.
;
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'Re-crystallisation from solvent: Methanol/acetonitrile'
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0442P)^2^+2.7278P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_depositor_comments
'Adding full bibliography for 7040294--7040296.cif.'
_cod_original_cell_volume        2854.4(6)
_cod_original_sg_symbol_H-M      P21/a
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