Synthesis and Properties of Ethene-Bridged Terthiophenes.
Mitsudo, Koichi; Sato, Hidehiko; Yamasaki, Arata; Kamimoto, Natsuyo; Goto, Jun; Mandai, Hiroki; Suga, Seiji; Organic letters 17 (2015) 4858–4861; doi:10.1021/acs.orglett.5b02417

data_1532457
_publ_section_title
;
 Synthesis and Properties of Ethene-Bridged Terthiophenes.
;
_journal_issue                   19
_journal_name_full               'Organic letters'
_journal_page_first              4858
_journal_page_last               4861
_journal_paper_doi               10.1021/acs.orglett.5b02417
_journal_volume                  17
_journal_year                    2015
_chemical_formula_moiety         'C32 H40 S3'
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Rigaku CrystalClear-SM Expert 2.0 r16
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_computing_data_collection
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Rigaku CrystalClear-SM Expert 2.0 r16
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_computing_data_reduction
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Rigaku CrystalClear-SM Expert 2.0 r16
;
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_diffrn_ambient_temperature      110(2)
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Rigaku CrystalClear-SM Expert 2.0 r16
;
_diffrn_measurement_method       'profile data from \w-scans'
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_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
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_diffrn_reflns_point_group_measured_fraction_full 0.989
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_exptl_absorpt_process_details   'REQAB (Rigaku, 1998)'
_exptl_crystal_colour            Orange
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_exptl_crystal_description       Block
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_refine_ls_restrained_S_all      0.996
_refine_ls_R_factor_all          0.0666
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0627P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1303
_refine_ls_wR_factor_ref         0.1388
_reflns_Friedel_coverage         0.000
_reflns_number_gt                4716
_reflns_number_total             6349
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            ol5b02417_si_004.cif
_cod_data_source_block           1c-1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3271 2015-04-21 07:52:19Z andrius 

 Adding full bibliography for 1532457--1532461.cif.
;
_cod_database_code               1532457
_shelx_estimated_absorpt_t_min   0.867
_shelx_estimated_absorpt_t_max   0.925
_shelxl_version_number           2014-3
_shelx_res_checksum              45943
_shelx_hkl_checksum              6096