Syntheses, Structures, and Characterization of Quaternary Tellurites, Li3MTe4O11 (M = Al, Ga, and Fe).
Lü, Minfeng; Jo, Hongil; Oh, Seung-Jin; Lee, Suheon; Choi, Kwang-Yong; Yu, Yang; Ok, Kang Min; Inorganic chemistry 56 (2017) 5873–5879; doi:10.1021/acs.inorgchem.7b00530

data_4345749
_publ_section_title
;
 Syntheses, Structures, and Characterization of Quaternary Tellurites,
 Li3MTe4O11 (M = Al, Ga, and Fe).
;
_journal_issue                   10
_journal_name_full               'Inorganic chemistry'
_journal_page_first              5873
_journal_page_last               5879
_journal_paper_doi               10.1021/acs.inorgchem.7b00530
_journal_volume                  56
_journal_year                    2017
_chemical_formula_sum            'Ga2 Li6 O22 Te8'
_chemical_formula_weight         1553.88
_chemical_name_systematic        ' ?'
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 109.726(4)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   18.7906(10)
_cell_length_b                   5.1841(2)
_cell_length_c                   10.7786(5)
_cell_measurement_reflns_used    5065
_cell_measurement_temperature    298.0
_cell_measurement_theta_max      28.405
_cell_measurement_theta_min      3.893
_cell_volume                     988.35(8)
_diffrn_ambient_temperature      298.0
_diffrn_measured_fraction_theta_full 0.98
_diffrn_measured_fraction_theta_max 0.97
_diffrn_measurement_device       CCD
_diffrn_measurement_device_type  'Bruker SMART BREEZE'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0318
_diffrn_reflns_av_unetI/netI     0.0199
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       6
_diffrn_reflns_limit_k_min       -6
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            8364
_diffrn_reflns_theta_full        28.61
_diffrn_reflns_theta_max         28.65
_diffrn_reflns_theta_min         2.3
_exptl_absorpt_coefficient_mu    14.41
_exptl_absorpt_correction_T_max  0.7457
_exptl_absorpt_correction_T_min  0.4350
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   Bruker
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    5.2213
_exptl_crystal_description       brick
_exptl_crystal_F_000             1344
_exptl_crystal_size_max          0.80
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.20
_refine_diff_density_max         1.79
_refine_diff_density_min         -1.20
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_gt    1.87
_refine_ls_goodness_of_fit_ref   1.82
_refine_ls_number_constraints    0
_refine_ls_number_parameters     65
_refine_ls_number_reflns         1237
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0257
_refine_ls_R_factor_gt           0.0234
_refine_ls_shift/su_max          0.0234
_refine_ls_shift/su_mean         0.0024
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w=1/(\s^2^(F)+0.0001F^2^)
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.0305
_refine_ls_wR_factor_ref         0.0311
_reflns_number_gt                1139
_reflns_number_total             1237
_reflns_threshold_expression     I>3\s(I)
_cod_data_source_file            ic7b00530_si_002.cif
_cod_data_source_block           Li3GaTe4O11
_cod_depositor_comments
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The following automatic conversions were performed:

'_diffrn_radiation_probe' value 'X-ray' changed to 'x-ray' according
to
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 

 Adding full bibliography for 4345748--4345749.cif.
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_cod_database_code               4345749