Eu~2~(PO~3~H)~3~
Foulon, J.-D.; Durand, J.; Cot, L.; Tijani, N.; Rafiq, M.; Acta Crystallographica Section C 51 (1995) 348–350; doi:10.1107/S0108270193007796

data_2003252
_publ_section_title
;
 Eu~2~(PO~3~H)~3~
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              348
_journal_page_last               350
_journal_paper_doi               10.1107/S0108270193007796
_journal_volume                  51
_journal_year                    1995
_chemical_formula_moiety         'Eu2 (P1 O3 H1 )3'
_chemical_formula_sum            'Eu2 H3 O9 P3'
_chemical_formula_weight         543,8
_space_group_IT_number           12
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90
_cell_angle_beta                 123.79(1)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   14.822(3)
_cell_length_b                   7.055(1)
_cell_length_c                   10.205(2)
_cell_measurement_reflns_used    20
_cell_measurement_temperature    293
_cell_measurement_theta_max      12.5
_cell_measurement_theta_min      5
_cell_volume                     886.9(3)
_diffrn_measurement_device       'Siemens P3'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.033
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       -1
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -1
_diffrn_reflns_number            2180
_diffrn_reflns_theta_max         27.5
_diffrn_standards_decay_%        <3
_diffrn_standards_interval_count 50
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    14.67
_exptl_absorpt_correction_T_max  0.83
_exptl_absorpt_correction_T_min  0.59
_exptl_absorpt_correction_type   'empirique (Walker & Stuart, 1983)'
_exptl_crystal_colour            jaune
_exptl_crystal_density_diffrn    4.074
_exptl_crystal_density_meas      4.06(1)
_exptl_crystal_description       parallelepiped
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.04
_refine_diff_density_max         1.32
_refine_diff_density_min         -2.00
_refine_ls_extinction_method     aucun
_refine_ls_goodness_of_fit_obs   3.34
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     86
_refine_ls_number_reflns         945
_refine_ls_R_factor_obs          0.026
_refine_ls_shift/esd_max         0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     'w = 1/[\s^2^(F)+0.000030F^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.032
_reflns_number_observed          945
_reflns_number_total             1099
_reflns_observed_criterion       F>=5\s(F)
_cod_data_source_file            du1051.cif
_cod_data_source_block           du1051_structure_1_of_1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value '1/[\s^2^(F)+0.000030F^2^]' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to 'w =
1/[\s^2^(F)+0.000030F^2^]'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_formula_sum        'H3 Eu2 O9 P3'
_cod_database_code               2003252