4-(Phenyldiazenyl)naphthalen-1-amine and its hydrochloride
Yatsenko, A. V.; Chernyshev, V. V.; Paseshnichenko, K. A.; Schenk, H.; Acta Crystallographica Section C 57 (2001) 295–297; doi:10.1107/S0108270100018692

data_2011791
_publ_section_title
;
 4-(Phenyldiazenyl)naphthalen-1-amine and its hydrochloride
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              295
_journal_page_last               297
_journal_paper_doi               10.1107/S0108270100018692
_journal_volume                  57
_journal_year                    2001
_chemical_formula_moiety         'C16 H14 N3 + , Cl -'
_chemical_formula_sum            'C16 H14 Cl N3'
_chemical_formula_weight         283.76
_chemical_name_systematic
;
[4-(phenyldiazenyl)naphthalen-1-yl]ammonium chloride
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 95.32(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   7.426(3)
_cell_length_b                   13.305(4)
_cell_length_c                   14.027(4)
_cell_measurement_reflns_used    75
_cell_measurement_temperature    295(2)
_cell_measurement_theta_max      22.5
_cell_measurement_theta_min      4.5
_cell_volume                     1379.9(8)
_computing_cell_refinement       'LSPAID (Visser, 1986)'
_computing_data_collection       'local program'
_computing_molecular_graphics    'PLUTON92 (Spek, 1992)'
_computing_publication_material  'PARST (Nardelli, 1983)'
_computing_structure_refinement  MRIA
_computing_structure_solution    'MRIA (Zlokazov & Chernyshev, 1992)'
_diffrn_ambient_temperature      295(2)
_diffrn_measurement_device_type
;
DRON-3M diffractometer (Burevestnik, Russia)
;
_diffrn_radiation_monochromator  'Ni filtered'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.5418
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       10
_diffrn_reflns_limit_l_min       -10
_exptl_absorpt_coefficient_mu    2.378
_exptl_absorpt_correction_type   none
_exptl_crystal_density_diffrn    1.366
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             592
_refine_diff_density_max         .9
_refine_diff_density_min         -1.3
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   1.60
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           fullcycle
_refine_ls_number_constraints    0
_refine_ls_number_parameters     107
_refine_ls_number_restraints     10
_refine_ls_shift/su_max          .04
_refine_ls_shift/su_mean         .01
_refine_ls_structure_factor_coef Inet
_refine_ls_weighting_scheme      sigma
_cod_data_source_file            br1305.cif
_cod_data_source_block           II
_cod_original_cell_volume        1380.0(10)
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C16 H14 Cl1 N3'
_cod_database_code               2011791