Reductive Transformations of a Pyrazolate-Based Bioinspired Diiron-Dinitrosyl Complex.
Kindermann, Nicole; Schober, Anne; Demeshko, Serhiy; Lehnert, Nicolai; Meyer, Franc; Inorganic chemistry 55 (2016) 11538–11550; doi:10.1021/acs.inorgchem.6b02080

data_4349186
_publ_section_title
;
 Reductive Transformations of a Pyrazolate-Based Bioinspired
 Diiron-Dinitrosyl Complex.
;
_journal_issue                   21
_journal_name_full               'Inorganic chemistry'
_journal_page_first              11538
_journal_page_last               11550
_journal_paper_doi               10.1021/acs.inorgchem.6b02080
_journal_volume                  55
_journal_year                    2016
_chemical_formula_moiety         'C27 H50 Fe2 N10 O2 2+, 2(Cl O4 -)'
_chemical_formula_sum            'C27 H50 Cl2 Fe2 N10 O10'
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_space_group_name_H-M_alt        'P 1 21/n 1'
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_cell_angle_beta                 114.98(3)
_cell_angle_gamma                90
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_cell_length_b                   21.472(4)
_cell_length_c                   14.142(3)
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_cell_measurement_theta_min      1.747
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_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Stoe IPDS II'
_diffrn_measurement_method       \w
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0407P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_cod_data_source_block           1a-nk138-2
_cod_original_cell_volume        3723.3(15)
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