Chlorosilane-Promoted Addition Reaction of Isocyanides to 3,4-Dihydroisoquinoline N-Oxides
Takahiro Soeta; Shuhei Fujinami; Yutaka Ukaji; Journal of Organic Chemistry 77 (2012) 9878–9883; doi:10.1021/jo301791m

data_4027673
_publ_section_title
;
 Chlorosilane-Promoted Addition Reaction of Isocyanides to
 3,4-Dihydroisoquinoline N-Oxides
;
_journal_name_full               'Journal of Organic Chemistry'
_journal_page_first              9878
_journal_page_last               9883
_journal_paper_doi               10.1021/jo301791m
_journal_volume                  77
_journal_year                    2012
_chemical_formula_moiety         'C14 H20 N2 O2 '
_chemical_formula_sum            'C14 H20 N2 O2'
_chemical_formula_weight         248.32
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_symmetry_space_group_name_H-M   'P b c a'
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_cell_angle_beta                 90
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_cell_measurement_temperature    123.2
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_cell_measurement_theta_min      3.3
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_computing_cell_refinement       CRYSTALCLEAR
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_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(Jacobson, 1998)'
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_exptl_crystal_description       Prism
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_exptl_crystal_size_min          0.070
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo) + 0.00106|Fo|^2^]'
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_cod_original_formula_sum        'C14 H20 N2 O2 '
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