Synthesis of non-symmetrically sulphonated phosphine sulphonate based Pd(ii) catalyst salts for olefin polymerisation reactions.
Anselment, Timo M. J.; Anderson, Carly E.; Rieger, Bernhard; Boeddinghaus, M. Bele; Fässler, Thomas F; Dalton transactions (Cambridge, England : 2003) 40 (2011) 8304–8313; doi:10.1039/c1dt10372e

data_7016403
_publ_section_title
;
 Synthesis of non-symmetrically sulphonated phosphine sulphonate based
 Pd(ii) catalyst salts for olefin polymerisation reactions.
;
_journal_issue                   33
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              8304
_journal_page_last               8313
_journal_paper_doi               10.1039/c1dt10372e
_journal_volume                  40
_journal_year                    2011
_chemical_formula_sum            'C43 H64 Cl K2 O18 P Pd S2'
_chemical_formula_weight         1184.10
_chemical_name_systematic        ' ?'
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_cell_length_c                   16.890(1)
_cell_measurement_temperature    110(2)
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_computing_structure_refinement  'Jana2006 (Petricek 2006)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      110(2)
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_diffrn_measurement_device       'Bruker APEX II'
_diffrn_radiation_monochromator  graphite
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_refine_ls_R_factor_gt           0.1088
_refine_ls_shift/su_max          0.0069
_refine_ls_shift/su_mean         0.0003
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     w=1/(\s^2^(I)+0.0004I^2^)
_refine_ls_weighting_scheme      sigma
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