Reactions of nickelocene with an Ru5 cluster: crystal structures of two nickel‒ruthenium clusters containing C2 ligands
Adams, Chris J.; Bruce, Michael I.; Halet, Jean-François; Kahlal, Samia; Skelton, Brian W.; White, Allan H.; Journal of the Chemical Society, Dalton Transactions  (2001) 414–; doi:10.1039/b005210h

data_7010032
_publ_section_title
;
 Reactions of nickelocene with an Ru5 cluster: crystal structures of
 two nickel--ruthenium clusters containing C2 ligands
;
_journal_issue                   4
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              414
_journal_paper_doi               10.1039/b005210h
_journal_year                    2001
_chemical_formula_structural     '[Ru4Ni2(CO)8(PPh3)2(C2)(SMe)2(cp)2]'
_chemical_formula_sum            'C46 H36 Ni2 O8 P2 Ru4 S2'
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_diffrn_reflns_limit_h_max       13
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_diffrn_reflns_limit_k_max       13
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_diffrn_reflns_theta_min         2
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_diffrn_standards_number         6
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_exptl_absorpt_correction_T_max  .84
_exptl_absorpt_correction_T_min  .82
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_exptl_absorpt_process_details   'XTAL absorb'
_exptl_crystal_density_diffrn    1.863
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_exptl_crystal_size_mid          .16
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         .045
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_reflns_limit_k_max              13
_reflns_limit_k_min              0
_reflns_limit_l_max              44
_reflns_limit_l_min              0
_reflns_number_gt                1437
_reflns_number_observed          1437
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_reflns_threshold_expression     'I    > 3.00 sig(I   )'
_cod_data_source_file            b005210h.txt
_cod_data_source_block           br306
_cod_depositor_comments
;
The following automatic conversions were performed:
'_refine_ls_matrix_type' value 'Full' changed to 'full' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_cell_volume        4864.8(18)
_cod_original_sg_symbol_Hall     p_4w_2c
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_cod_database_code               7010032