Counterion effect on the formation of coordination polymer networks between AgNO3 and L (2,2′-oxybis(ethane-2,1-diyl) diisonicotinate). Part 2
Sague, Jorge L.; Meuwly, Markus; Fromm, Katharina M.; CrystEngComm 10 (2008) 1542–; doi:10.1039/b803158d

data_7202038
_publ_section_title
;
 Counterion effect on the formation of coordination polymer networks
 between AgNO3 and L (2,2&#x2032;-oxybis(ethane-2,1-diyl)
 diisonicotinate). Part 2
;
_journal_issue                   11
_journal_name_full               CrystEngComm
_journal_page_first              1542
_journal_paper_doi               10.1039/b803158d
_journal_volume                  10
_journal_year                    2008
_chemical_compound_source        'L6 and AgNO3 in THF/Water'
_chemical_formula_sum            'C32 H32 Ag2 N6 O16'
_chemical_formula_weight         972.38
_chemical_melting_point          210
_chemical_name_common            L6AgNO3
_chemical_name_systematic
;
?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 94.74(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   6.6811(13)
_cell_length_b                   12.263(3)
_cell_length_c                   22.585(4)
_cell_measurement_temperature    386(2)
_cell_measurement_theta_max      27.15
_cell_measurement_theta_min      1.81
_cell_volume                     1844.1(7)
_computing_cell_refinement       'STOE X-AREA'
_computing_data_collection       'STOE X-AREA'
_computing_data_reduction        'STOE X-RED'
_computing_molecular_graphics    'ORTEPII (Johnson, 1976)'
_computing_publication_material  'SHELXL97, SCHAKAL and PLATON (Spek, 2003)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXL97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector                 'image plate (34 cm diameter)'
_diffrn_detector_area_resol_mean 6.67
_diffrn_measured_fraction_theta_full 0.930
_diffrn_measured_fraction_theta_max 0.930
_diffrn_measurement_device_type  'STOE IPDS 2T'
_diffrn_measurement_method       'rotation method'
_diffrn_radiation_monochromator  'plane graphite'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.2612
_diffrn_reflns_av_sigmaI/netI    0.2127
_diffrn_reflns_limit_h_max       7
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_number            13141
_diffrn_reflns_theta_full        27.15
_diffrn_reflns_theta_max         27.15
_diffrn_reflns_theta_min         1.81
_diffrn_source                   'sealed X-ray tube,12x0.4 mm long-fine focus'
_diffrn_source_current           40
_diffrn_source_power             2.00
_diffrn_source_type              'STOE IPDS II'
_diffrn_source_voltage           50
_diffrn_standards_decay_%        0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    1.144
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    1.751
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       'Rod-like crystal'
_exptl_crystal_F_000             976
_exptl_crystal_recrystallization_method 'Solvent diffusion'
_refine_diff_density_max         0.471
_refine_diff_density_min         -1.178
_refine_diff_density_rms         0.113
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.032
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     239
_refine_ls_number_reflns         3804
_refine_ls_number_restraints     12
_refine_ls_restrained_S_all      1.031
_refine_ls_R_factor_all          0.2719
_refine_ls_R_factor_gt           0.1237
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0581P)^2^+11.1621P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2162
_refine_ls_wR_factor_ref         0.2764
_reflns_number_gt                1360
_reflns_number_total             3804
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            b803158d.txt
_cod_data_source_block           Compound-2
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7202038