Syntheses, structures and anti-tumor activity of four organotin(iv) dicarboxylates based on (1,3,4-thiadiazole-2,5-diyldithio)diacetic acid
Yan, Fei-Fei; Ma, Chun-Lin; Li, Qian-Li; Zhang, Shao-Liang; Ru, Jing; Cheng, Shuang; Zhang, Ru-Fen; New Journal of Chemistry 42 (2018) 11601–; doi:10.1039/C8NJ00431E

data_7057492
_publ_section_title
;
 Syntheses, structures and anti-tumor activity of four organotin(iv)
 dicarboxylates based on (1,3,4-thiadiazole-2,5-diyldithio)diacetic acid
;
_journal_issue                   14
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              11601
_journal_paper_doi               10.1039/C8NJ00431E
_journal_volume                  42
_journal_year                    2018
_chemical_formula_sum            'C10 H16 N2 O5 S3 Sn2'
_chemical_formula_weight         577.81
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2017/1
_audit_update_record
;
2017-10-24 deposited with the CCDC.
2018-06-04 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_cell_angle_gamma                90
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_cell_volume                     1841.1(3)
_computing_cell_refinement       'Bruker SMART'
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_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2017/1 (Sheldrick, 2017)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_av_R_equivalents  0.0795
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_diffrn_reflns_theta_max         25.020
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_refine_ls_shift/su_mean         0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0677P)^2^+6.2950P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                2504
_reflns_number_total             3239
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c8nj00431e2.cif
_cod_data_source_block           160915e
_cod_depositor_comments
'Adding full bibliography for 7057489--7057492.cif.'
_cod_database_code               7057492
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