Single-molecule magnet behavior in an octanuclear dysprosium(iii) aggregate inherited from helical triangular Dy3 SMM-building blocks.
Zhang, Li; Zhang, Peng; Zhao, Lang; Wu, Jianfeng; Guo, Mei; Tang, Jinkui; Dalton transactions (Cambridge, England : 2003) 45 (2016) 10556–10562; doi:10.1039/c6dt01718e

data_7039303
_publ_section_title
;
 Single-molecule magnet behavior in an octanuclear dysprosium(iii)
 aggregate inherited from helical triangular Dy3 SMM-building blocks.
;
_journal_issue                   26
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              10556
_journal_page_last               10562
_journal_paper_doi               10.1039/c6dt01718e
_journal_volume                  45
_journal_year                    2016
_chemical_formula_sum            'C118 H150 Dy8 N26 O48'
_chemical_formula_weight         4000.63
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_hydrogens   mixed
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_audit_update_record
;
2016-05-14 deposited with the CCDC.
2016-05-17 downloaded from the CCDC.
;
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_computing_cell_refinement       'Bruker SMART'
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_computing_publication_material  'Bruker SHELXTL'
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_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      186(2)
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_diffrn_measured_fraction_theta_max 0.980
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_Laue_measured_fraction_full 0.980
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0689P)^2^+2.6492P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_total             12646
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments          'Adding full bibliography for 7039303.cif.'
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