LMucko/crystallography-open-database huggingface dataset:
Structural studies of silver (I) salts of the cyclic sulfonimides (CF2)n(SO2)2NH (n = 3, 4)
Desmarteau, D. D.; Zuberi, S. S.; Pennington, W. T.; Randolph, B. B.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 777–789; doi:

data_4030447
_publ_section_title
;
 Structural studies of silver (I) salts of the cyclic sulfonimides
 (CF2)n(SO2)2NH (n = 3, 4)
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              777
_journal_page_last               789
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'C3 H2 Ag F6 N O5 S2'
_chemical_formula_weight         418.05
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      11
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 94.06(7)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   10.904(9)
_cell_length_b                   8.489(7)
_cell_length_c                   5.560(5)
_cell_volume                     513.4(8)
_diffrn_ambient_temperature      294
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    2.44
_exptl_crystal_density_diffrn    2.70
_exptl_crystal_F_000             400
_refine_ls_number_reflns         937
_refine_ls_R_factor_gt           0.0544
_refine_ls_wR_factor_gt          0.0730
_cod_data_source_file            EJSSIC-1992-29-777-789-1.cif
_cod_data_source_block           1
_cod_original_sg_symbol_H-M      'P 21/m'
_cod_database_code               4030447
Structural studies of silver (I) salts of the cyclic sulfonimides (CF2)n(SO2)2NH (n = 3, 4)
Desmarteau, D. D.; Zuberi, S. S.; Pennington, W. T.; Randolph, B. B.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 777–789; doi:

data_4030448
_publ_section_title
;
 Structural studies of silver (I) salts of the cyclic sulfonimides
 (CF2)n(SO2)2NH (n = 3, 4)
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              777
_journal_page_last               789
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'C4 H2 Ag F6 N O5 S2'
_chemical_formula_weight         430.05
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 103.13(1)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   12.651(2)
_cell_length_b                   7.453(2)
_cell_length_c                   12.682(2)
_cell_volume                     1164.5(4)
_diffrn_ambient_temperature      294
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    2.19
_exptl_crystal_density_diffrn    2.67
_exptl_crystal_F_000             896
_refine_ls_number_reflns         1813
_refine_ls_R_factor_gt           0.0517
_refine_ls_wR_factor_gt          0.0756
_cod_data_source_file            EJSSIC-1992-29-777-789-2.cif
_cod_data_source_block           2
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4030448
Combinatorial Screening of Luminescent and Structural Properties in a Ce(3+)-Doped Ln-Al-Si-O-N (Ln = Y, La, Gd, Lu) System: The Discovery of a Novel Gd3Al3+xSi3-xO12+xN2-x:Ce(3+) Phosphor.
Park, Woon Bae; Singh, Satendra Pal; Kim, Minseuk; Sohn, Kee-Sun; Inorganic chemistry 54 (2015) 1829–1840; doi:10.1021/ic502721h

data_4342127
_publ_section_title
;
 Combinatorial Screening of Luminescent and Structural Properties in a
 Ce(3+)-Doped Ln-Al-Si-O-N (Ln = Y, La, Gd, Lu) System: The Discovery of a
 Novel Gd3Al3+xSi3-xO12+xN2-x:Ce(3+) Phosphor.
;
_journal_issue                   4
_journal_name_full               'Inorganic chemistry'
_journal_page_first              1829
_journal_page_last               1840
_journal_paper_doi               10.1021/ic502721h
_journal_volume                  54
_journal_year                    2015
_chemical_formula_structural     Gd3Al3.774Si2.226O12.774N1.226
_chemical_formula_sum            'Al3.774 Gd3 N1.226 O12.774 Si2.226'
_chemical_formula_weight         857.63
_space_group_IT_number           5
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'C 2y'
_symmetry_space_group_name_H-M   'C 1 2 1'
_cell_angle_alpha                90.00000
_cell_angle_beta                 89.8430(9)
_cell_angle_gamma                90.00000
_cell_formula_units_Z            2
_cell_length_a                   13.67681(15)
_cell_length_b                   7.86858(9)
_cell_length_c                   4.85157(3)
_cell_measurement_temperature    298
_cell_volume                     522.110(9)
_computing_structure_refinement  FULLPROF
_diffrn_ambient_temperature      298
_diffrn_measurement_device_type  '8C2 HRPD beamline Pohang Light Source'
_diffrn_radiation_type           Synchrotron
_diffrn_radiation_wavelength     1.4647
_diffrn_source                   '8C2 HRPD beamline Pohang Light Source'
_exptl_crystal_density_diffrn    5.455
_pd_char_colour                  White
_pd_meas_2theta_range_inc        0.010000
_pd_meas_2theta_range_max        130.50000
_pd_meas_2theta_range_min        10.00000
_pd_meas_number_of_points        12051
_pd_meas_scan_method             cont
_pd_proc_2theta_range_inc        0.010000
_pd_proc_2theta_range_max        130.5000
_pd_proc_2theta_range_min        10.0000
_pd_proc_ls_prof_R_factor        5.5758
_pd_proc_ls_prof_wR_expected     5.4478
_pd_proc_ls_prof_wR_factor       7.1185
_pd_proc_wavelength              1.464700
_pd_spec_mount_mode              reflection
_refine_ls_goodness_of_fit_all   1.3077
_refine_ls_number_parameters     73
_refine_ls_number_reflns         576
_refine_ls_number_restraints     0
_refine_ls_R_I_factor            3.4335
_cod_data_source_file            ic502721h_si_002.cif
_cod_data_source_block           monoclinic
_cod_depositor_comments          'Adding full bibliography for 4342127.cif.'
_cod_original_sg_symbol_H-M      'C 2'
_cod_original_formula_sum        Al3.774Gd3N1.226O12.774Si2.226
_cod_database_code               4342127
_pd_proc_ls_prof_cr_factor       10.8908
_pd_proc_ls_prof_cwr_factor      11.6788
_pd_proc_ls_prof_cwr_expected    8.9378
_pd_proc_ls_prof_chi2            1.7074
_pd_proc_ls_prof_echi2           1.7155
Gold-Gold Bonding: The Key to Stabilizing the 19-Electron Ternary Phases LnAuSb (Ln = La-Nd and Sm).
Seibel, Elizabeth M.; Schoop, Leslie M.; Xie, Weiwei; Gibson, Quinn D.; Webb, James B.; Fuccillo, Michael K.; Krizan, Jason W.; Cava, Robert J.; Journal of the American Chemical Society 137 (2015) 1282–1289; doi:10.1021/ja511394q

data_4123309
_publ_section_title
;
 Gold-Gold Bonding: The Key to Stabilizing the 19-Electron Ternary Phases
 LnAuSb (Ln = La-Nd and Sm).
;
_journal_issue                   3
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              1282
_journal_page_last               1289
_journal_paper_doi               10.1021/ja511394q
_journal_volume                  137
_journal_year                    2015
_chemical_formula_sum            'Au La Sb'
_chemical_formula_weight         457.63
_space_group_IT_number           194
_symmetry_cell_setting           hexagonal
_symmetry_Int_Tables_number      194
_symmetry_space_group_name_Hall  '-P 6c 2c'
_symmetry_space_group_name_H-M   'P 63/m m c'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            4
_cell_length_a                   4.63839(2)
_cell_length_b                   4.63839(2)
_cell_length_c                   16.83143(14)
_cell_measurement_temperature    295
_cell_volume                     313.607(3)
_diffrn_ambient_temperature      295
_diffrn_radiation_wavelength     0.41372
_diffrn_source                   Synchrotron
_pd_meas_2theta_range_inc        0.004
_pd_meas_2theta_range_max        49.984
_pd_meas_2theta_range_min        0.500
_pd_meas_number_of_points        12372
_pd_phase_name                   LaAuSb
_pd_proc_ls_prof_R_factor        12.8
_pd_proc_ls_prof_wR_expected     8.34
_pd_proc_ls_prof_wR_factor       13.9
_refine_ls_goodness_of_fit_all   1.644
_refine_ls_R_I_factor            20.9
_cod_data_source_file            ja511394q_si_003.cif
_cod_data_source_block           VESTA_phase_1
_cod_depositor_comments
'Adding full bibliography for 4123309--4123311.cif.'
_cod_original_cell_volume        313.603(1)
_cod_original_formula_sum        'Au1 La1 Sb1'
_cod_database_code               4123309
_pd_proc_ls_prof_cr_factor       13.9
_pd_proc_ls_prof_cwr_factor      14.4
_pd_proc_ls_prof_cwr_expected    8.77
_pd_proc_ls_prof_chi2            2.703
_pd_proc_ls_prof_echi2           2.703
Gold-Gold Bonding: The Key to Stabilizing the 19-Electron Ternary Phases LnAuSb (Ln = La-Nd and Sm).
Seibel, Elizabeth M.; Schoop, Leslie M.; Xie, Weiwei; Gibson, Quinn D.; Webb, James B.; Fuccillo, Michael K.; Krizan, Jason W.; Cava, Robert J.; Journal of the American Chemical Society 137 (2015) 1282–1289; doi:10.1021/ja511394q

data_4123310
_publ_section_title
;
 Gold-Gold Bonding: The Key to Stabilizing the 19-Electron Ternary Phases
 LnAuSb (Ln = La-Nd and Sm).
;
_journal_issue                   3
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              1282
_journal_page_last               1289
_journal_paper_doi               10.1021/ja511394q
_journal_volume                  137
_journal_year                    2015
_chemical_formula_sum            'Au Nd Sb'
_chemical_formula_weight         462.97
_space_group_IT_number           194
_symmetry_cell_setting           hexagonal
_symmetry_Int_Tables_number      194
_symmetry_space_group_name_Hall  '-P 6c 2c'
_symmetry_space_group_name_H-M   'P 63/m m c'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            4
_cell_length_a                   4.58003
_cell_length_b                   4.58003
_cell_length_c                   16.47753
_cell_measurement_temperature    295
_cell_volume                     299.336
_diffrn_ambient_temperature      295
_diffrn_radiation_wavelength     0.41372
_diffrn_source                   Synchrotron
_pd_meas_2theta_range_inc        0.004
_pd_meas_2theta_range_max        49.984
_pd_meas_2theta_range_min        0.500
_pd_meas_number_of_points        12372
_pd_phase_name                   'NdAuSb                        '
_pd_proc_ls_prof_R_factor        12.6
_pd_proc_ls_prof_wR_expected     7.62
_pd_proc_ls_prof_wR_factor       13.7
_refine_ls_goodness_of_fit_all   1.805
_refine_ls_R_I_factor            7.68
_cod_data_source_file            ja511394q_si_001.cif
_cod_data_source_block           VESTA_phase_1
_cod_depositor_comments
'Adding full bibliography for 4123309--4123311.cif.'
_cod_original_cell_volume        299.34(1)
_cod_original_formula_sum        'Au1 Nd1 Sb1'
_cod_database_code               4123310
_pd_proc_ls_prof_cr_factor       12.7
_pd_proc_ls_prof_cwr_factor      13.8
_pd_proc_ls_prof_cwr_expected    7.66
_pd_proc_ls_prof_chi2            3.256
_pd_proc_ls_prof_echi2           3.256
Gold-Gold Bonding: The Key to Stabilizing the 19-Electron Ternary Phases LnAuSb (Ln = La-Nd and Sm).
Seibel, Elizabeth M.; Schoop, Leslie M.; Xie, Weiwei; Gibson, Quinn D.; Webb, James B.; Fuccillo, Michael K.; Krizan, Jason W.; Cava, Robert J.; Journal of the American Chemical Society 137 (2015) 1282–1289; doi:10.1021/ja511394q

data_4123311
_publ_section_title
;
 Gold-Gold Bonding: The Key to Stabilizing the 19-Electron Ternary Phases
 LnAuSb (Ln = La-Nd and Sm).
;
_journal_issue                   3
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              1282
_journal_page_last               1289
_journal_paper_doi               10.1021/ja511394q
_journal_volume                  137
_journal_year                    2015
_chemical_formula_sum            'Au Ce Sb'
_chemical_formula_weight         458.84
_space_group_IT_number           194
_symmetry_cell_setting           hexagonal
_symmetry_Int_Tables_number      194
_symmetry_space_group_name_Hall  '-P 6c 2c'
_symmetry_space_group_name_H-M   'P 63/m m c'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            4
_cell_length_a                   4.61403(2)
_cell_length_b                   4.61403(2)
_cell_length_c                   16.6348(1)
_cell_measurement_temperature    295
_cell_volume                     306.697(3)
_diffrn_ambient_temperature      295
_diffrn_radiation_wavelength     0.41372
_diffrn_source                   Synchrotron
_pd_meas_2theta_range_inc        0.004
_pd_meas_2theta_range_max        49.984
_pd_meas_2theta_range_min        0.500
_pd_meas_number_of_points        12372
_pd_phase_name                   CeAuSb
_pd_proc_ls_prof_R_factor        12.0
_pd_proc_ls_prof_wR_expected     6.95
_pd_proc_ls_prof_wR_factor       13.4
_refine_ls_goodness_of_fit_all   1.9
_refine_ls_R_I_factor            15.3
_cod_data_source_file            ja511394q_si_002.cif
_cod_data_source_block           VESTA_phase_1
_cod_depositor_comments
'Adding full bibliography for 4123309--4123311.cif.'
_cod_original_formula_sum        'Au1 La1 Sb1'
_cod_database_code               4123311
_pd_proc_ls_prof_cr_factor       12.2
_pd_proc_ls_prof_cwr_factor      13.4
_pd_proc_ls_prof_cwr_expected    7.05
_pd_proc_ls_prof_chi2            3.628
_pd_proc_ls_prof_echi2           3.628
"Naked" SF5- anion: The crystal and molecular structure of [Cs+.(18-crown-6)2][SF5-]
Clark, M.; Kellen-Yuen, C. J.; Robinson, K. D.; Zhang, H.; Yang, Z.-Y.; Madappat, K. V.; Fuller, J. W.; Atwood, J. L.; Thrasher, J. S.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 809–833; doi:

data_4030474
_publ_section_title
;
 "Naked" SF5- anion: The crystal and molecular structure of
 [Cs+.(18-crown-6)2][SF5-]
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              809
_journal_page_last               833
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'C24 H48 Cs F5 O12 S'
_chemical_formula_weight         788.57
_space_group_IT_number           85
_symmetry_cell_setting           tetragonal
_symmetry_Int_Tables_number      85
_symmetry_space_group_name_Hall  '-P 4a'
_symmetry_space_group_name_H-M   'P 4/n :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   13.503(3)
_cell_length_b                   13.503(3)
_cell_length_c                   19.471(5)
_cell_volume                     3550.2(14)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    1.168
_exptl_crystal_density_diffrn    1.48
_exptl_crystal_F_000             1616
_refine_ls_number_parameters     204
_refine_ls_number_reflns         858
_refine_ls_R_factor_gt           0.028
_refine_ls_wR_factor_gt          0.032
_cod_data_source_file            EJSSIC-1992-29-809-833.cif
_cod_data_source_block           naked-SF5
_cod_original_cell_volume        3550.2(18)
_cod_original_sg_symbol_H-M      'P 4/n'
_cod_database_code               4030474
The crystal structure of (pentafluoro-lamda6-sulfanyl)(fluorosulfonyl) diethylacetamide
Keszler, D. A.; Winter, B.; Gard, G. L.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 835–855; doi:

data_4030475
_publ_section_title
;
 The crystal structure of (pentafluoro-lamda6-sulfanyl)(fluorosulfonyl)
 diethylacetamide
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              835
_journal_page_last               855
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'C6 H11 F6 N O3 S2'
_chemical_formula_weight         323.30
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2yab'
_symmetry_space_group_name_H-M   'P 1 21/a 1'
_cell_angle_alpha                90
_cell_angle_beta                 102.404(9)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   10.945(2)
_cell_length_b                   8.932(2)
_cell_length_c                   12.564(1)
_cell_volume                     1199.6(4)
_diffrn_ambient_temperature      296
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    0.522
_exptl_crystal_density_diffrn    1.790
_exptl_crystal_F_000             656
_refine_ls_number_parameters     162
_refine_ls_number_reflns         1577
_refine_ls_R_factor_gt           0.065
_refine_ls_wR_factor_gt          0.079
_cod_data_source_file            EJSSIC-1992-29-835-855.cif
_cod_data_source_block           pentafluoro
_cod_original_sg_symbol_H-M      'P 21/a'
_cod_database_code               4030475
Preparation and X-ray structures of gold(I) complexes with some fluoro-phosphorus(III) ligands
Lin, Y.; Jones, P. G.; Schmutzler, R.; Sheldrick, G. M.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 887–898; doi:

data_4030476
_publ_section_title
;
 Preparation and X-ray structures of gold(I) complexes with some
 fluoro-phosphorus(III) ligands
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              887
_journal_page_last               898
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'C2 H6 Au Cl F2 N P'
_chemical_formula_weight         345.5
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 98.51(3)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   19.575(7)
_cell_length_b                   6.278(2)
_cell_length_c                   11.608(4)
_cell_volume                     1410.8(8)
_diffrn_ambient_temperature      178
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    2.14
_exptl_crystal_density_diffrn    3.25
_exptl_crystal_F_000             1232
_refine_ls_number_parameters     74
_refine_ls_number_reflns         1350
_refine_ls_R_factor_gt           0.033
_refine_ls_wR_factor_gt          0.043
_cod_data_source_file            EJSSIC-1992-29-887-898-1.cif
_cod_data_source_block           complex-3
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4030476
Preparation and X-ray structures of gold(I) complexes with some fluoro-phosphorus(III) ligands
Lin, Y.; Jones, P.G.; Schmutzler, R.; Sheldrick, G. M.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 887–898; doi:

data_4030477
_publ_section_title
;
 Preparation and X-ray structures of gold(I) complexes with some
 fluoro-phosphorus(III) ligands
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              887
_journal_page_last               898
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'C8 H9 Au Cl F2 P'
_chemical_formula_weight         406.5
_space_group_IT_number           64
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      64
_symmetry_space_group_name_Hall  '-C 2ac 2'
_symmetry_space_group_name_H-M   'C m c a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   6.620(3)
_cell_length_b                   28.350(8)
_cell_length_c                   11.343(2)
_cell_volume                     2128.8(12)
_diffrn_ambient_temperature      178
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    1.42
_exptl_crystal_density_diffrn    2.54
_exptl_crystal_F_000             1488
_refine_ls_number_parameters     52
_refine_ls_number_reflns         1836
_refine_ls_R_factor_gt           0.036
_refine_ls_wR_factor_gt          0.046
_cod_data_source_file            EJSSIC-1992-29-887-898-2.cif
_cod_data_source_block           complex-2
_cod_original_sg_symbol_Hall     '-C 2bc 2'
_cod_database_code               4030477
X-ray powder diffraction study of Li4TbF8
El-Ghozzi, M.; Avignant, D.; Cousseins, J. C.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 981–992; doi:

data_4030478
_publ_section_title
;
 X-ray powder diffraction study of Li4TbF8
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              981
_journal_page_last               992
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'F8 Li4 Tb'
_chemical_formula_weight         338.69
_space_group_IT_number           62
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      62
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.6582(9)
_cell_length_b                   9.7411(8)
_cell_length_c                   5.7155(4)
_cell_volume                     537.72(8)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.542
_exptl_crystal_density_diffrn    4.184
_exptl_crystal_F_000             596
_pd_proc_ls_prof_R_factor        0.0844
_pd_proc_ls_prof_wR_expected     0.0215
_pd_proc_ls_prof_wR_factor       0.0908
_refine_ls_number_parameters     43
_refine_ls_number_reflns         428
_refine_ls_R_I_factor            0.0615
_cod_data_source_file            EJJSSIC-1992-981-992.cif
_cod_data_source_block           Li4TbF8
_cod_database_code               4030478