<i>catena</i>-Poly[trimethyltin(IV)-μ-3,4-dichlorophenylacetato]
Saeed, M. Adeel; Craig, D. C.; Badshah, Amin; Ali, Saqib; Rauf, M. Khawar; Acta Crystallographica Section E 61 (2005) m2595–m2597; doi:10.1107/S160053680503638X

data_2207552
_publ_section_title
;
 <i>catena</i>-Poly[trimethyltin(IV)-\m-3,4-dichlorophenylacetato]
;
_journal_coeditor_code           HG6259
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m2595
_journal_page_last               m2597
_journal_paper_doi               10.1107/S160053680503638X
_journal_volume                  61
_journal_year                    2005
_chemical_formula_iupac          '[Sn (C H3)3 (C8 H5 Cl2 O2)]'
_chemical_formula_moiety         'C11 H14 Cl2 O2 Sn'
_chemical_formula_sum            'C11 H14 Cl2 O2 Sn'
_chemical_formula_weight         367.8
_chemical_melting_point          388
_chemical_name_systematic
;
catena-Poly[trimethyltin(IV)-\m-3,4-dichlorophenylacetato]
;
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_type_scat_source
'International Tables for X-ray Crystallography, Vol. IV'
_cell_angle_alpha                90
_cell_angle_beta                 96.010(10)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   12.660(3)
_cell_length_b                   9.8010(10)
_cell_length_c                   23.462(5)
_cell_measurement_reflns_used    10
_cell_measurement_temperature    294
_cell_measurement_theta_max      12
_cell_measurement_theta_min      11
_cell_volume                     2895.2(10)
_computing_cell_refinement       'CAD-4 Software'
_computing_data_collection       'CAD-4 Software (Enraf--Nonius, 1989)'
_computing_data_reduction        'local program'
_computing_molecular_graphics    'ORTEPII (Johnson, 1976)'
_computing_publication_material  'local programs'
_computing_structure_refinement  'RAELS (Rae, 1996)'
_computing_structure_solution    'SIR92 (Altomare <i>et al.</i>,  1994)'
_diffrn_measured_fraction_theta_full 1.00
_diffrn_measured_fraction_theta_max 1.00
_diffrn_measurement_device_type  'Enraf--Nonius CAD-4'
_diffrn_measurement_method       \w--2\q
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.017
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            2619
_diffrn_reflns_theta_full        25
_diffrn_reflns_theta_max         25
_diffrn_standards_decay_%        12
_diffrn_standards_interval_time  30
_diffrn_standards_number         1
_exptl_absorpt_coefficient_mu    2.131
_exptl_absorpt_correction_T_max  0.87
_exptl_absorpt_correction_T_min  0.64
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details   '(de Meulenaer & Tompa, 1965)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.69
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       lath
_exptl_crystal_F_000             1440.0
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.03
_refine_diff_density_max         0.97
_refine_diff_density_min         -1.05
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.79
_refine_ls_hydrogen_treatment    constr
_refine_ls_number_parameters     146
_refine_ls_number_reflns         2012
_refine_ls_R_factor_gt           0.043
_refine_ls_shift/su_max          0.011
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(F) + 0.0004F^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.055
_reflns_number_gt                2012
_reflns_number_total             2550
_reflns_threshold_expression     I>2\s(I)
_cod_data_source_file            hg6259.cif
_cod_data_source_block           I
_cod_original_cell_volume        2895.0(10)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               2207552
_cod_database_fobs_code          2207552