The dehydration process in the <small>DL</small>-phenylglycinium trifluoromethanesulfonate monohydrate crystal revealed by XRD, vibrational and DSC studies
Wołoszyn, Łukasz; Ilczyszyn, Maria M.; Kinzhybalo, Vasyl; Acta Crystallographica Section C 75 (2019) –; doi:10.1107/S2053229619014402

data_2021816
_publ_section_title
;
 The dehydration process in the <small>DL</small>-phenylglycinium
 trifluoromethanesulfonate monohydrate crystal revealed by XRD,
 vibrational and DSC studies
;
_journal_coeditor_code           JX3047
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first
;
;
_journal_paper_doi               10.1107/S2053229619014402
_journal_volume                  75
_journal_year                    2019
_chemical_formula_iupac          'C8 H10 N O2 +, C F3 O3 S -, H2 O'
_chemical_formula_moiety         'C8 H10 N O2 +, C F3 O3 S -, H2 O'
_chemical_formula_sum            'C9 H12 F3 N O6 S'
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_chemical_name_systematic
;
<i>DL</i>-Phenylglycinium trifluoromethanesulfonate monohydrate
;
_space_group_crystal_system      monoclinic
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Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
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;
CrysAlis PRO (Rigaku OD, 2018)
;
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CrysAlis PRO (Rigaku OD, 2018)
;
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CrysAlis PRO (Rigaku OD, 2018)
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OLEX2 (Dolomanov <i>et al.</i>,  2009)
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OLEX2 (Dolomanov <i>et al.</i>,  2009)
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SHELXL2018 (Sheldrick, 2015b)
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SHELXT (Sheldrick, 2015a)
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;
(CrysAlis PRO; Rigaku OD, 2018)
;
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0884P)^2^+2.4562P] where P=(Fo^2^+2Fc^2^)/3'
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