Facile synthesis of silver alkynide cluster and coordination polymers using picolinic acid as co-ligand
Gupta, Arvind Kumar Kumar; Orthaber, Andreas; Dalton Transactions  (2019) –; doi:10.1039/C9DT03697K

data_7701370
_publ_section_title
;
 Facile synthesis of silver alkynide cluster and coordination polymers
 using picolinic acid as co-ligand
;
_journal_name_full               'Dalton Transactions'
_journal_paper_doi               10.1039/C9DT03697K
_journal_year                    2019
_chemical_formula_moiety         'C74 H86 Ag15 N4 O8, Cl O4'
_chemical_formula_sum            'C74 H86 Ag15 Cl N4 O12'
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_space_group_name_Hall           '-P 1'
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;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_audit_update_record
;
2019-10-10 deposited with the CCDC.    2019-10-14 downloaded from the CCDC.
;
_cell_angle_alpha                74.668(2)
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_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      25.0
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_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker Apex-II'
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_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1338P)^2^+74.6510P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_gt                9556
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_reflns_threshold_expression     'I > 2\s(I)'
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_shelx_res_checksum              27176
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_olex2_submission_special_instructions 'No special instructions were received'