Reversibility in Reactions of Linker-Bridged Distannenes with Terminal Alkynes at Ambient Temperature.
Schneider, Julia; Henning, Jens; Edrich, Jessica; Schubert, Hartmut; Wesemann, Lars; Inorganic chemistry 54 (2015) 6020–6027; doi:10.1021/acs.inorgchem.5b00896

data_4343092
_publ_section_title
;
 Reversibility in Reactions of Linker-Bridged Distannenes with Terminal
 Alkynes at Ambient Temperature.
;
_journal_issue                   12
_journal_name_full               'Inorganic chemistry'
_journal_page_first              6020
_journal_page_last               6027
_journal_paper_doi               10.1021/acs.inorgchem.5b00896
_journal_volume                  54
_journal_year                    2015
_chemical_formula_sum            'C60 H58 Sn2'
_chemical_formula_weight         1016.44
_chemical_name_systematic
;
 ?
;
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_diffrn_ambient_temperature      100(2)
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_diffrn_measurement_method       '\f and \w scans'
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_diffrn_reflns_point_group_measured_fraction_full 0.996
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_exptl_absorpt_correction_type   numerical
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_exptl_crystal_colour            'clear green-violet'
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_exptl_crystal_density_method    'not measured'
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_refine_ls_number_reflns         11045
_refine_ls_number_restraints     0
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_refine_ls_R_factor_all          0.0255
_refine_ls_R_factor_gt           0.0210
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0254P)^2^+0.9901P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                9735
_reflns_number_total             11045
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           shelx
_cod_depositor_comments
'Adding full bibliography for 4343090--4343095.cif.'
_cod_database_code               4343092
_shelx_estimated_absorpt_t_min   0.645
_shelx_estimated_absorpt_t_max   0.851
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_shelx_res_checksum              85687
_shelx_hkl_checksum              734