Crystallization of the chalcogenide compound Sb~8~Te~3~
Kifune, Kouichi; Fujita, Tomoko; Kubota, Yoshiki; Yamada, Noboru; Matsunaga, Toshiyuki; Acta Crystallographica Section B 67 (2011) 381–385; doi:10.1107/S0108768111033738

data_2310028
_publ_section_title
;
 Crystallization of the chalcogenide compound Sb~8~Te~3~
;
_journal_coeditor_code           SO5052
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              381
_journal_page_last               385
_journal_paper_doi               10.1107/S0108768111033738
_journal_volume                  67
_journal_year                    2011
_chemical_formula_sum            'Sb8 Te3'
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_space_group_ssg_name            R-3m(00\g)
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_computing_publication_material
'Jana2000 (Petricek, Dusek & Palatinus, 2000)'
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'Jana2000 (Petricek, Dusek & Palatinus, 2000)'
_diffrn_ambient_temperature      831
_diffrn_measurement_device_type  'Debye-Scherrer camera'
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_diffrn_radiation_type           synchrotron
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_exptl_absorpt_coefficient_mu    18.433
_exptl_absorpt_process_details
'(Jana2000; Petricek, Dusek & Palatinus, 2000)'
_exptl_crystal_colour            black
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_exptl_crystal_F_000             1846
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_pd_meas_scan_method             fixed
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_pd_proc_ls_background_function  '36 Legendre polynoms'
_pd_proc_ls_pref_orient_corr     'March & Dollase'
_pd_proc_ls_profile_function     Pseudo-Voigt
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_pd_proc_ls_prof_wR_expected     0.0243
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_pd_spec_mounting                'sealed quartz capillary tube'
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_pd_spec_shape                   cylinder
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_pd_spec_size_equat              0.3
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_refine_ls_R_factor_gt           0.0560
_refine_ls_shift/su_max          0.4812
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_refine_ls_weighting_scheme      sigma
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