Half-sandwich lanthanide crown ether complexes with the slow relaxation of magnetization and photoluminescence behaviors.
Gao, Feng; Yang, Feng-Lei; Feng, Xiaowan; Xu, Huimin; Sun, Wang; Liu, Huan; Li, Xiu-Ling; Dalton transactions (Cambridge, England : 2003) 46 (2017) 1317–1323; doi:10.1039/c6dt04353d

data_7041528
_publ_section_title
;
 Half-sandwich lanthanide crown ether complexes with the slow relaxation
 of magnetization and photoluminescence behaviors.
;
_journal_issue                   4
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1317
_journal_page_last               1323
_journal_paper_doi               10.1039/c6dt04353d
_journal_volume                  46
_journal_year                    2017
_chemical_formula_sum            'C8 H16 Dy N3 O13'
_chemical_formula_weight         524.74
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2016/6
_audit_update_record
;
2016-12-02 deposited with the CCDC.
2016-12-21 downloaded from the CCDC.
;
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_cell_volume                     1567.3(3)
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_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      123(2)
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_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0401P)^2^+0.8342P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           1
_cod_depositor_comments
'Adding full bibliography for 7041526--7041529.cif.'
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