Isolation and Reactivity of Trifluoromethyl Iodonium Salts.
Brantley, Johnathan N.; Samant, Andrew V.; Toste, F. Dean; ACS central science 2 (2016) 341–350; doi:10.1021/acscentsci.6b00119

data_4516758
_publ_section_title
;
 Isolation and Reactivity of Trifluoromethyl Iodonium Salts.
;
_journal_issue                   5
_journal_name_full               'ACS central science'
_journal_page_first              341
_journal_page_last               350
_journal_paper_doi               10.1021/acscentsci.6b00119
_journal_volume                  2
_journal_year                    2016
_chemical_formula_sum            'C10 H11 B F7 I O S0'
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_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_limit_l_min       -22
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_diffrn_source                   'microfocus sealed tube'
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_exptl_absorpt_correction_T_max  0.745
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_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colourless
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_exptl_crystal_description       plate
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_refine_ls_R_factor_all          0.0565
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0691P)^2^+8.2812P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_total             4884
_reflns_threshold_expression     'I > 2\s(I)'
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_shelx_estimated_absorpt_t_min   0.866
_shelx_estimated_absorpt_t_max   0.952
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_shelx_hkl_checksum              46622