New platinum(II) complexes with benzothiazole ligands
Carmona-Negrón, José A.; Cádiz, Mayra E.; Moore, Curtis E.; Rheingold, Arnold L.; Meléndez, Enrique; Acta Crystallographica Section E 72 (2016) 412–416; doi:10.1107/S2056989016002826

data_2241577
_publ_section_title
;
 New platinum(II) complexes with benzothiazole ligands
;
_journal_coeditor_code           BG2580
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              412
_journal_page_last               416
_journal_paper_doi               10.1107/S2056989016002826
_journal_volume                  72
_journal_year                    2016
_chemical_formula_iupac          '(C8 H20 N) [Pt Br3 (C8 H7 N S)]'
_chemical_formula_moiety         'C8 H20 N +, C8 H7 Br3 N Pt S -'
_chemical_formula_sum            'C16 H27 Br3 N2 Pt S'
_chemical_formula_weight         714.27
_chemical_name_systematic
;
Tetraethylammonium
tribromido(2-methyl-1,3-benzothiazole-\k<i>N</i>)platinate(II)
;
_space_group_crystal_system      orthorhombic
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_space_group_name_Hall           '-P 2ac 2ab'
_space_group_name_H-M_alt        'P b c a'
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
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Olex2 1.2
(compiled 2015.09.30 svn.r3233 for OlexSys, GUI svn.r5103)
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SAINT (Bruker, 2013)
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APEX2 (Bruker, 2013)
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SAINT (Bruker, 2013)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>,  2009)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>,  2009)
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SHELXL2014 (Sheldrick, 2015b)
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SHELXT (Sheldrick, 2015a)
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_diffrn_detector_area_resol_mean 7.9
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_diffrn_measurement_device       'Kappa Four-Circle Diffractometer'
_diffrn_measurement_device_type  'Bruker APEXII CCD'
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_diffrn_reflns_theta_min         2.063
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;
(SADABS; Bruker, 2014)
;
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_exptl_crystal_size_mid          0.16
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_refine_diff_density_min         -0.933
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_refine_ls_number_reflns         4418
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.033
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_refine_ls_shift/su_max          0.003
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0352P)^2^+9.4131P] where P=(Fo^2^+2Fc^2^)/3'
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_refine_ls_wR_factor_ref         0.0810
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_reflns_threshold_expression     'I > 2\s(I)'
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