Migratory Transmetalation in Diphenoxo-Bridged CuIIMII Complexes of a Dinucleating Macrocycle with N(amine)2O2 and N(imine)2O2 Metal-Binding Sites
Masami Yonemura; Yukiko Matsumura; Hideki Furutachi; Masaaki Ohba; Hisashi Ōkawa; David E. Fenton; Inorganic Chemistry 36 (1997) 2711–2717; doi:10.1021/ic9614430

data_4323473
_publ_section_title
;
 Migratory Transmetalation in Diphenoxo-Bridged CuIIMII Complexes of a
 Dinucleating Macrocycle with N(amine)2O2 and N(imine)2O2 Metal-Binding
 Sites
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              2711
_journal_page_last               2717
_journal_paper_doi               10.1021/ic9614430
_journal_volume                  36
_journal_year                    1997
_chemical_formula_sum            'C33 H38 Br2 Cl Cu N5 O9 Pb'
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_symmetry_cell_setting           triclinic
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_audit_creation_date             'Wed Mar 12 21:14:32 1997'
_audit_creation_method           'from TEXRAY.INF file'
_cell_angle_alpha                95.32(1)
_cell_angle_beta                 92.23(1)
_cell_angle_gamma                82.81(1)
_cell_formula_units_Z            2.00
_cell_length_a                   13.998(2)
_cell_length_b                   15.568(2)
_cell_length_c                   8.699(2)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    20.0
_cell_measurement_theta_max      23.91
_cell_measurement_theta_min      20.92
_cell_volume                     1872.0(6)
_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
_computing_data_reduction        'teXsan: PROCESS (MSC)'
_computing_publication_material  'teXsan: FINISH (MSC)'
_computing_structure_refinement  'teXsan: LS (MSC)'
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_diffrn_ambient_temperature      20.0
_diffrn_measurement_device       AFC7R
_diffrn_measurement_method       'omega/2-theta scans'
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_exptl_absorpt_coefficient_mu_cm 73.383
_exptl_absorpt_correction_T_max  1.000
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      sigma
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_cod_data_source_file            ic9614430_1.cif
_cod_data_source_block           '[CuPb(L)(BzO)(DMF)]ClO4'
_cod_original_cell_volume        1871.9(5)
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_cod_database_code               4323473