N-Coordinated Tin(II) Trifluoromethanesulfonates and Their Reactions with Transition Metal Carbonyls.
Bouska, Marek; Dostál, Libor; Lutter, Michael; Glowacki, Britta; Ruzickova, Zdenka; Beck, Daniel; Jambor, Roman; Jurkschat, Klaus; Inorganic chemistry 54 (2015) 6792–6800; doi:10.1021/acs.inorgchem.5b00678

data_4343447
_publ_section_title
;
 N-Coordinated Tin(II) Trifluoromethanesulfonates and Their Reactions with
 Transition Metal Carbonyls.
;
_journal_issue                   14
_journal_name_full               'Inorganic chemistry'
_journal_page_first              6792
_journal_page_last               6800
_journal_paper_doi               10.1021/acs.inorgchem.5b00678
_journal_volume                  54
_journal_year                    2015
_chemical_formula_moiety         'C20 H27 N2 O, C5 Cl3 O5 Sn W'
_chemical_formula_sum            'C25 H27 Cl3 N2 O6 Sn W'
_chemical_formula_weight         860.38
_chemical_name_systematic
; 
 ? 
;
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_computing_data_collection
'COLLECT (Hooft, 1998) and DENZO (Otwinowski & Minor, 1997)'
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_computing_molecular_graphics    'PLATON (Spek, 2003)'
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_diffrn_measurement_device_type  'Bruker Nonius KappaCCD area detector'
_diffrn_measurement_method       '\f and \w scans to fill the Ewald sphere'
_diffrn_radiation_monochromator  graphite
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_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            30544
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
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;
Gaussian integration (Coppens, 1970)
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_exptl_crystal_colour            yellow
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_exptl_crystal_description       block
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_refine_ls_extinction_method     SHELXL
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_refine_ls_R_factor_all          0.0249
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0243P)^2^+1.3731P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0531
_refine_ls_wR_factor_ref         0.0558
_reflns_number_gt                6744
_reflns_number_total             7099
_reflns_threshold_expression     >2sigma(I)
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_cod_data_source_block           Supp
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3271 2015-04-21 07:52:19Z andrius 

 Adding full bibliography for 4343443--4343447.cif.
;
_cod_original_cell_volume        1553.02(15)
_cod_database_code               4343447
_shelxl_version_number           2013-4
_shelx_res_checksum              54241
_shelx_hkl_checksum              92289