Cobalt(II) and copper(II) supramolecular networks with 1-iminoisoindoline asymmetric pincer
Zabierowski, Piotr; Matoga, Dariusz; Nitek, Wojciech; RSC Adv.  (2015) –; doi:10.1039/C5RA02063H

data_7219726
_publ_section_title
;
 Cobalt(II) and copper(II) supramolecular networks with 1-iminoisoindoline
 asymmetric pincer
;
_journal_name_full               'RSC Adv.'
_journal_paper_doi               10.1039/C5RA02063H
_journal_year                    2015
_chemical_formula_moiety         'C24 H22 Co N4 O4, 1.6(O), H2 O'
_chemical_formula_sum            'C24 H27.2 Co N4 O6.6'
_chemical_formula_weight         536.23
_chemical_name_systematic        5
_space_group_IT_number           14
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_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2ybc'
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_atom_sites_solution_hydrogens   mixed
_audit_creation_date             2015-02-20T18:24:58-00:00
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_audit_update_record
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2015-02-24 deposited with the CCDC.
2015-02-27 downloaded from the CCDC.
;
_cell_angle_alpha                90
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        CrysAlisPro, Agilent Technologies,
        Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
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        CrysAlisPro, Agilent Technologies,
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        CrysAlisPro, Agilent Technologies,
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        (compiled Feb  1 2013,16:14:44)
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_computing_structure_refinement  'SHELXL-2012 (Sheldrick, 2012)'
_diffrn_ambient_temperature      120(2)
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_exptl_absorpt_coefficient_mu    0.792
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        CrysAlisPro, Agilent Technologies,
        Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
        (compiled Feb  1 2013,16:14:44)
        Empirical absorption correction using spherical harmonics,
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_exptl_crystal_colour            red
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_refine_ls_R_factor_gt           0.0541
_refine_ls_shift/su_max          0
_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
 w=1/[\s^2^(Fo^2^)+(0.0460P)^2^+2.5332P]
 where P=(Fo^2^+2Fc^2^)/3
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1214
_refine_ls_wR_factor_ref         0.1409
_reflns_number_gt                3806
_reflns_number_total             5633
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c5ra02063h2.cif
_cod_data_source_block           5
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C24 H27.20 Co N4 O6.60'
_cod_database_code               7219726
_shelx_estimated_absorpt_t_min   0.8
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