Synthesis and Complexation Properties of the Anions (η5-C5Me5)Ru(PR2O)32- as Ligands
Thomas Rüther; Ulli Englert; Ulrich Koelle; Inorganic Chemistry 37 (1998) 4265–4271; doi:10.1021/ic971319w

data_4322948
_publ_contact_author
;
     Ulli Englert
     Institut fuer Anorganische Chemie
     RWTH Aachen
     Prof.-Pirlet-Str.1
     52074 Aachen
     Germany
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_publ_contact_author_email       ullrich.englert@ac.rwth-aachen.de
_publ_contact_author_fax         '(0241) 8888288'
_publ_contact_author_phone       '(0241) 804666'
_publ_section_title
;
 Synthesis and Complexation Properties of the Anions
 (\h5-C5Me5)Ru(PR2O)32- as Ligands
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_journal_name_full               'Inorganic Chemistry'
_journal_page_first              4265
_journal_page_last               4271
_journal_paper_doi               10.1021/ic971319w
_journal_volume                  37
_journal_year                    1998
_chemical_compound_source        'see paper'
_chemical_formula_sum            'C149 H159 O13 P9 Ru3 Ti3'
_chemical_formula_weight         2883.60
_chemical_name_common            ' compound no. 9'
_space_group_IT_number           205
_symmetry_cell_setting           cubic
_symmetry_space_group_name_Hall  '-P 2ac 2ab 3'
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_atom_type_scat_source           International_Tables_for_Xray_Crystallography
_audit_creation_date             24-03-98
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_computing_publication_material  CIF_VAX_MolEN_(Fair,_1990)
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_diffrn_standards_interval_time  80
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_exptl_absorpt_coefficient_mu    0.601
_exptl_absorpt_correction_T_max  0.011
_exptl_absorpt_correction_T_min  0.008
_exptl_absorpt_correction_type   refined_empirical_(Walker_&_Stuart,_1983)
_exptl_crystal_colour            'orange red'
_exptl_crystal_density_diffrn    1.31
_exptl_crystal_density_meas      ?
_exptl_crystal_description       'isometric block'
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_cod_data_source_file            ic971319w.cif
_cod_data_source_block           TR3
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'none' was changed to '?' - the
value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value '4Fo^2^/ (\s^2^(Fo^2^) + 0.0016
Fo^4^)' was changed to 'calc'. New tag '_refine_ls_weighting_details'
was created. The value of the new tag was set to 'w = 4Fo^2^/
(\s^2^(Fo^2^) + 0.0016 Fo^4^)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        2930(3)
_cod_database_code               4322948