Dinuclear Pd(I)-Pd(I) and Pt(II)...Pt(II) Complexes Supported by Tridentate Pyphos Ligands (Pyphos = 6-(Diphenylphosphino)-2-pyridonate)
Kazushi Mashima; Mitsuhiro Tanaka; Kazuhide Tani; Hiroshi Nakano; Akira Nakamura; Inorganic Chemistry 35 (1996) 5244–5248; doi:10.1021/ic951658u

data_4323885
_publ_section_title
;
 Dinuclear Pd(I)-Pd(I) and Pt(II)...Pt(II) Complexes Supported by
 Tridentate Pyphos Ligands (Pyphos = 6-(Diphenylphosphino)-2-pyridonate)
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              5244
_journal_page_last               5248
_journal_paper_doi               10.1021/ic951658u
_journal_volume                  35
_journal_year                    1996
_chemical_formula_sum            'C70 H56 Cl4 N4 O4 P4 Pt2'
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_audit_creation_date             'Fri Nov 24 14:54:28 1995'
_audit_creation_method           'from TEXRAY.INF file'
_cell_angle_alpha                90
_cell_angle_beta                 109.782(8)
_cell_angle_gamma                90
_cell_formula_units_Z            4.00
_cell_length_a                   19.646(2)
_cell_length_b                   11.411(4)
_cell_length_c                   30.368(3)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    20.0
_cell_measurement_theta_max      50.00
_cell_measurement_theta_min      49.37
_cell_volume                     6406(2)
_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
_computing_data_reduction        'teXsan: PROCESS (MSC)'
_computing_publication_material  'teXsan: FINISH (MSC)'
_computing_structure_refinement  'teXsan: LS (MSC)'
_computing_structure_solution    SHELXS86
_diffrn_ambient_temperature      20.0
_diffrn_measurement_device       AFC7R
_diffrn_measurement_method       'omega/2-theta scans'
_diffrn_orient_matrix_UB_11      0.04597
_diffrn_orient_matrix_UB_12      -0.01348
_diffrn_orient_matrix_UB_13      -0.00653
_diffrn_orient_matrix_UB_21      -0.02798
_diffrn_orient_matrix_UB_22      -0.00531
_diffrn_orient_matrix_UB_23      -0.03424
_diffrn_orient_matrix_UB_31      0.00545
_diffrn_orient_matrix_UB_32      0.08643
_diffrn_orient_matrix_UB_33      -0.00312
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Rigaku rotating anode'
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_exptl_absorpt_correction_T_min  0.204
_exptl_absorpt_correction_type   psi-scan
_exptl_crystal_colour            yellow
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      sigma
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_cod_data_source_file            ic951658u_2.cif
_cod_data_source_block           Pt2(pyphos)4
_cod_original_cell_volume        6406(1)
_cod_original_sg_symbol_H-M      'C 2/c '
_cod_original_formula_sum        'C70 H56 O4 N4 P4 Pt2 Cl4'
_cod_database_code               4323885