Heterometallic hexanuclear Ni<sub>4</sub>M<sub>2</sub> (M = Dy, Y) complexes: structure and single-molecule magnet for the Dy(iii) derivative.
Pei, Shaomin; Hu, Zhaobo; Chen, Zilu; Yu, Shui; Li, Bo; Liang, Yuning; Liu, Dongcheng; Yao, Di; Liang, Fupei; Dalton transactions (Cambridge, England : 2003) 47 (2018) 1801–1807; doi:10.1039/c7dt04003b

data_7045261
_publ_section_title
;
 Heterometallic hexanuclear Ni<sub>4</sub>M<sub>2</sub> (M = Dy, Y)
 complexes: structure and single-molecule magnet for the Dy(iii)
 derivative.
;
_journal_issue                   6
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1801
_journal_page_last               1807
_journal_paper_doi               10.1039/c7dt04003b
_journal_volume                  47
_journal_year                    2018
_chemical_formula_moiety         'C28 H62 Dy2 N8 Ni4 O22, H2 O'
_chemical_formula_sum            'C28 H64 Dy2 N8 Ni4 O23'
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_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-C 2yc'
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_symmetry_space_group_name_Hall  '-C 2yc'
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2017-10-17 deposited with the CCDC.
2018-01-11 downloaded from the CCDC.
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
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(compiled Aug 13 2014,18:06:01)
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
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Empirical absorption correction using spherical harmonics,
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_exptl_crystal_colour            'light green'
_exptl_crystal_density_diffrn    2.069
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0198P)^2^+20.6705P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0565
_refine_ls_wR_factor_ref         0.0590
_reflns_Friedel_coverage         0.000
_reflns_number_gt                3678
_reflns_number_total             4029
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7045261--7045262.cif.'
_cod_database_code               7045261
_shelx_shelxl_version_number     2014/7
_shelx_estimated_absorpt_t_min   0.280
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