Bis(μ-2-methylquinolin-8-olato)-κ^3^<i>N</i>,<i>O</i>:<i>O</i>;κ^3^<i>O</i>:<i>N</i>,<i>O</i>-bis[(methanol-κ<i>O</i>)(nitrato-κ^2^<i>O</i>,<i>O</i>')lead(II)]
Mohammadnezhad Sh., Gholamhossein; Amini, Mostafa M.; Ng, Seik Weng; Acta Crystallographica Section E 65 (2009) m259–; doi:10.1107/S1600536809003547

data_2221202
_publ_section_title
Bis(\m-2-methylquinolin-8-olato)-\k^3^<i>N</i>,<i>O</i>:<i>O</i>;\k^3^<i>O</i>:<i>N</i>,<i>O</i>-bis[(methanol-\k<i>O</i>)(nitrato-\k^2^<i>O</i>,<i>O</i>')lead(II)]
_journal_coeditor_code           TK2363
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m259
_journal_paper_doi               10.1107/S1600536809003547
_journal_volume                  65
_journal_year                    2009
_chemical_formula_iupac          '[Pb2 (C10 H8 N O)2 (N O3)2 (C H4 O)2]'
_chemical_formula_moiety         'C22 H24 N4 O10 Pb2'
_chemical_formula_sum            'C22 H24 N4 O10 Pb2'
_chemical_formula_weight         918.83
_chemical_name_systematic
;
Bis(\m-2-methylquinolin-8-olato)-
\k^3^<i>N</i>,<i>O</i>:<i>O</i>;\k^3^<i>O</i>:<i>N</i>,<i>O</i>-
bis[(methanol-\k<i>O</i>)(nitrato-\k^2^<i>O</i>,<i>O</i>')lead(II)]
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL97
_cell_angle_alpha                103.9760(10)
_cell_angle_beta                 98.2620(10)
_cell_angle_gamma                108.1900(10)
_cell_formula_units_Z            1
_cell_length_a                   8.25790(10)
_cell_length_b                   8.80520(10)
_cell_length_c                   9.67650(10)
_cell_measurement_reflns_used    5067
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      28.3
_cell_measurement_theta_min      2.2
_cell_volume                     630.069(14)
_computing_cell_refinement       'SAINT (Bruker, 2008)'
_computing_data_collection       'APEX2 (Bruker, 2008)'
_computing_data_reduction        'SAINT (Bruker, 2008)'
_computing_molecular_graphics    'X-SEED (Barbour, 2001)'
_computing_publication_material  'publCIF (Westrip, 2009)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Bruker SMART APEX'
_diffrn_measurement_method       \w
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.019
_diffrn_reflns_av_sigmaI/netI    0.027
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            5958
_diffrn_reflns_theta_full        27.5
_diffrn_reflns_theta_max         27.5
_diffrn_reflns_theta_min         2.2
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    13.407
_exptl_absorpt_correction_T_max  0.554
_exptl_absorpt_correction_T_min  0.175
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Sheldrick, 1996)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.422
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             428
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.05
_refine_diff_density_max         1.41
_refine_diff_density_min         -2.12
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.08
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     174
_refine_ls_number_reflns         2872
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.08
_refine_ls_R_factor_all          0.022
_refine_ls_R_factor_gt           0.021
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w = 1/[\s^2^(Fo^2^)+(0.0341P)^2^+1.3909P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.057
_refine_ls_wR_factor_ref         0.058
_reflns_number_gt                2754
_reflns_number_total             2872
_reflns_threshold_expression     I>2\s(I)
_cod_data_source_file            tk2363.cif
_cod_data_source_block           I
_cod_original_cell_volume        630.070(10)
_cod_database_code               2221202
_cod_database_fobs_code          2221202