Rh(ii)-Catalyzed formation of pyrrolo[2,3-b]quinolines from azide-methylenecyclopropanes and isonitriles.
Chen, Kai; Tang, Xiang-Ying; Shi, Min; Chemical communications (Cambridge, England) 52 (2016) 1967–1970; doi:10.1039/c5cc09236a

data_7118596
_publ_section_title
;
 Rh(ii)-Catalyzed formation of pyrrolo[2,3-b]quinolines from
 azide-methylenecyclopropanes and isonitriles.
;
_journal_issue                   9
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              1967
_journal_page_last               1970
_journal_paper_doi               10.1039/c5cc09236a
_journal_volume                  52
_journal_year                    2016
_chemical_formula_sum            'C23 H19 N2'
_chemical_formula_weight         323.40
_chemical_name_systematic
; 
 ? 
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
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_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2013
_audit_update_record
;
2014-05-21 deposited with the CCDC.
2015-12-03 downloaded from the CCDC.
;
_cell_angle_alpha                109.644(3)
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_cell_measurement_theta_min      6.385
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_computing_molecular_graphics    'Bruker SHELXTL'
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_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'CCD area detector'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0588P)^2^+0.0777P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_total             3064
_reflns_threshold_expression     'I > 2\s(I)'
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_shelx_res_checksum              32680