Group 2 metal bis(arenecarbochalcogenoate)(crown ether) complexes: isolation and structural analysis.
Tatematsu, Yoshiharu; Kato, Shinzi; Nakata, Norio; Ebihara, Masahiro; Niyomura, Osamu; Sugamata, Koh; Yukimoto, Mariko; Minoura, Mao; Dalton transactions (Cambridge, England : 2003) 47 (2018) 9787–9794; doi:10.1039/c8dt01959b

data_7046878
_publ_section_title
;
 Group 2 metal bis(arenecarbochalcogenoate)(crown ether) complexes:
 isolation and structural analysis.
;
_journal_issue                   29
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              9787
_journal_page_last               9794
_journal_paper_doi               10.1039/c8dt01959b
_journal_volume                  47
_journal_year                    2018
_chemical_formula_moiety         'C28 H38 Ba O8 S2, C3 H6 O'
_chemical_formula_sum            'C31 H44 Ba O9 S2'
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_space_group_name_Hall           '-P 1'
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_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2018-06-21 deposited with the CCDC.
2018-06-26 downloaded from the CCDC.
;
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_cell_measurement_theta_min      10.1
_cell_volume                     1741.4(5)
_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
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'Yadokari-XG 2009 (Wakita, Nemoto et al., 2009)'
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_computing_structure_solution    'SIR97 (Altomare et al., 1999)'
_diffrn_ambient_temperature      193(2)
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_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Rigaku AFC7R'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_monochromator  graphite
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_diffrn_reflns_point_group_measured_fraction_full 1.000
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_diffrn_standards_decay_%        0.15
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_exptl_absorpt_correction_type   psi-scan
_exptl_absorpt_process_details   '(North, Phillips & Mathews, 1968)'
_exptl_crystal_colour            colorless
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0207P)^2^+0.3827P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7046874--7046878.cif.'
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