Investigations of Some Disordered Quaternary Compounds in the Systems Ag/Pb/Sb/Se and Ag/Pb/Sb/Te
Grauer, Maxim; Benndorf, Christopher; Rohr, Valentin; Paulmann, Carsten; Oeckler, Oliver; Crystals 14 (2024) 789–; doi:10.3390/cryst14090789

data_1572812
_publ_contact_author
;
 Prof. Dr. Oliver Oeckler
 Institute for Mineralogy, Crystallography and Materials Science
 Faculty of Chemistry and Mineralogy
 Leipzig University
 Scharnhorststr. 20
 04275 Leipzig, Germany
;
_publ_section_title
;
 Investigations of Some Disordered Quaternary Compounds in the Systems
 Ag/Pb/Sb/Se and Ag/Pb/Sb/Te
;
_journal_issue                   9
_journal_name_full               Crystals
_journal_page_first              789
_journal_paper_doi               10.3390/cryst14090789
_journal_volume                  14
_journal_year                    2024
_chemical_formula_moiety         'Ag0.61 Pb1.79 Sb2.61 Se6'
_chemical_formula_sum            'Ag0.61 Pb1.79 Sb2.61 Se6'
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_chemical_name_common            'silver lead antimony selenide'
_chemical_name_systematic        'silver lead antimony selenide'
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_space_group_name_Hall           '-C 2c 2'
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'CrysAlisPro 1.171.41.123a (Rigaku Oxford Diffraction, 2022)'
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'CrysAlisPro 1.171.41.123a (Rigaku Oxford Diffraction, 2022)'
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'Four circle Kappa diffractometer with Euler cradle'
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'Water cooled Double Crystal Monochromator Si(111)'
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_exptl_crystal_colour            'metallic grey'
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_exptl_crystal_description       cuboid
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_exptl_crystal_size_min          0.02
_refine_diff_density_max         1.746
_refine_diff_density_min         -2.632
_refine_diff_density_rms         0.312
_refine_ls_extinction_method     none
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0313P)^2^+4.0000P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_gt                1160
_reflns_number_total             1325
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           Ag0.61Pb1.79Sb2.61Se6
_cod_database_code               1572812
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_shelx_res_checksum              34205
_shelx_hkl_checksum              68634