Neutron and X-ray diffraction study of ferrite nanocrystals obtained by microwave-assisted growth. A structural comparison with the thermal synthetic route
Solano, Eduardo; Frontera, Carlos; Puig, Teresa; Obradors, Xavier; Ricart, Susagna; Ros, Josep; Journal of Applied Crystallography 47 (2014) 414–420; doi:10.1107/S1600576713032895

data_2300618
_publ_section_title
;
 Neutron and X-ray diffraction study of ferrite nanocrystals obtained by
 microwave-assisted growth. A structural comparison with the thermal
 synthetic route
;
_journal_coeditor_code           kk5153
_journal_issue                   1
_journal_name_full               'Journal of Applied Crystallography'
_journal_page_first              414
_journal_page_last               420
_journal_paper_doi               10.1107/S1600576713032895
_journal_volume                  47
_journal_year                    2014
_chemical_formula_moiety         'Fe2 Mn1 O4'
_chemical_formula_sum            'Fe2 Mn O4'
_chemical_formula_weight         230.630
_chemical_name_systematic        ' Fe2MnO4'
_space_group_IT_number           227
_symmetry_cell_setting           cubic
_symmetry_space_group_name_Hall  '-F 4vw 2vw 3'
_symmetry_space_group_name_H-M   'F d -3 m :2'
_cell_angle_alpha                90.00000
_cell_angle_beta                 90.00000
_cell_angle_gamma                90.00000
_cell_formula_units_Z            8
_cell_length_a                   8.3711(4)
_cell_length_b                   8.3711(4)
_cell_length_c                   8.3711(4)
_cell_measurement_temperature    300
_cell_volume                     586.61(5)
_computing_structure_refinement  FULLPROF
_diffrn_ambient_temperature      300
_diffrn_radiation_monochromator  none
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.020006
_pd_meas_2theta_range_max        80.00000
_pd_meas_2theta_range_min        10.06000
_pd_meas_number_of_points        3498
_pd_meas_scan_method             step
_pd_proc_2theta_range_inc        0.020006
_pd_proc_2theta_range_max        80.0302
_pd_proc_2theta_range_min        10.0902
_pd_proc_ls_pref_orient_corr     ' ?'
_pd_proc_ls_prof_R_factor        6.0630
_pd_proc_ls_prof_wR_expected     7.1393
_pd_proc_ls_prof_wR_factor       8.0017
_pd_proc_wavelength              1.540590
_pd_spec_mounting                ' ?'
_refine_ls_number_parameters     22
_refine_ls_number_reflns         38
_refine_ls_number_restraints     0
_refine_ls_R_I_factor            2.4194
_cod_data_source_file            kk5153sup3.cif
_cod_data_source_block           MnFe2O4
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Cubic' changed to 'cubic' according
to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/IUCr/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4268 2015-11-12 08:31:59Z antanas 
;
_cod_original_cell_volume        586.60(4)
_cod_original_sg_symbol_H-M      'F d -3 m'
_cod_original_formula_sum        'Fe2 Mn1 O4'
_cod_database_code               2300618
_pd_proc_ls_prof_cr_factor       14.1292
_pd_proc_ls_prof_cwr_factor      14.3884
_pd_proc_ls_prof_cwr_expected    12.8376
_pd_proc_ls_prof_chi2            1.2562
_pd_proc_ls_prof_echi2           1.2569
_cod_database_fobs_code 2300618