A New Twist on Pincer Ligands and Complexes
Ma, Liqing; Woloszynek, Robert A.; Chen, Weizhong; Ren, Tong; Protasiewicz, John D.; Organometallics 25 (2006) 3301–; doi:10.1021/om060256z

data_4075371
_publ_section_title
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 A New Twist on Pincer Ligands and Complexes
;
_journal_issue                   14
_journal_name_full               Organometallics
_journal_page_first              3301
_journal_paper_doi               10.1021/om060256z
_journal_volume                  25
_journal_year                    2006
_chemical_formula_sum            'C42 H31 Br O2 P2 Pd'
_chemical_formula_weight         815.92
_chemical_name_systematic
; 
 ? 
;
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_cell_length_c                   19.7745(3)
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_computing_data_collection       'Bruker APEX2'
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_diffrn_measured_fraction_theta_max 0.917
_diffrn_measurement_device_type  'Bruker Kappa APEX II CCD area detector'
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_diffrn_reflns_limit_l_min       -30
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_exptl_absorpt_correction_T_min  0.6472
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_exptl_crystal_colour            'clear, light brown'
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_exptl_crystal_density_meas      0
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0349P)^2^+0.3357P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0774
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_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om060256zsi20060321_102604.cif
_cod_data_source_block           case02
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Orthorhombic' changed to
'orthorhombic' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      Pbcn
_cod_database_code               4075371