LMucko/crystallography-open-database huggingface dataset:
[(tBu2PCH2SiMe2)2N]RuMe2: Synthesis and Reactivity of an Unsaturated Ruthenium Dialkyl Radical Species
Ingleson, Michael J.; Pink, Maren; Huffman, John C.; Fan, Hongjun; Caulton, Kenneth G.; Organometallics 25 (2006) 1112–1119; doi:10.1021/om0508536

data_4060861
_publ_section_title
;
 [(tBu2PCH2SiMe2)2N]RuMe2: Synthesis and Reactivity of an
 Unsaturated Ruthenium Dialkyl Radical Species
;
_journal_coden_ASTM              ORGND7
_journal_issue                   5
_journal_name_full               Organometallics
_journal_page_first              1112
_journal_page_last               1119
_journal_paper_doi               10.1021/om0508536
_journal_volume                  25
_journal_year                    2006
_chemical_formula_sum            'C23 H55 Cl N2 O P2 Ru Si2'
_chemical_formula_weight         630.33
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 114.7750(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   16.0426(7)
_cell_length_b                   12.9141(6)
_cell_length_c                   16.5029(8)
_cell_measurement_temperature    120(2)
_cell_volume                     3104.3(2)
_diffrn_ambient_temperature      120(2)
_exptl_crystal_density_diffrn    1.349
_cod_duplicate_entry             4074749
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4060861
[(tBu2PCH2SiMe2)2N]RuMe2: Synthesis and Reactivity of an Unsaturated Ruthenium Dialkyl Radical Species
Ingleson, Michael J.; Pink, Maren; Huffman, John C.; Fan, Hongjun; Caulton, Kenneth G.; Organometallics 25 (2006) 1112–1119; doi:10.1021/om0508536

data_4060862
_publ_section_title
;
 [(tBu2PCH2SiMe2)2N]RuMe2: Synthesis and Reactivity of an
 Unsaturated Ruthenium Dialkyl Radical Species
;
_journal_coden_ASTM              ORGND7
_journal_issue                   5
_journal_name_full               Organometallics
_journal_page_first              1112
_journal_page_last               1119
_journal_paper_doi               10.1021/om0508536
_journal_volume                  25
_journal_year                    2006
_chemical_formula_moiety         'C25 H55 N O2 P2 Ru Si2'
_chemical_formula_sum            'C25 H55 N O2 P2 Ru Si2'
_chemical_formula_weight         620.89
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 109.978(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.1346(11)
_cell_length_b                   29.621(3)
_cell_length_c                   11.2384(12)
_cell_measurement_temperature    130(2)
_cell_volume                     3170.7(6)
_diffrn_ambient_temperature      130(2)
_exptl_crystal_density_diffrn    1.301
_cod_duplicate_entry             4074750
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4060862
[(tBu2PCH2SiMe2)2N]RuMe2: Synthesis and Reactivity of an Unsaturated Ruthenium Dialkyl Radical Species
Ingleson, Michael J.; Pink, Maren; Huffman, John C.; Fan, Hongjun; Caulton, Kenneth G.; Organometallics 25 (2006) 1112–1119; doi:10.1021/om0508536

data_4060863
_publ_section_title
;
 [(tBu2PCH2SiMe2)2N]RuMe2: Synthesis and Reactivity of an
 Unsaturated Ruthenium Dialkyl Radical Species
;
_journal_coden_ASTM              ORGND7
_journal_issue                   5
_journal_name_full               Organometallics
_journal_page_first              1112
_journal_page_last               1119
_journal_paper_doi               10.1021/om0508536
_journal_volume                  25
_journal_year                    2006
_chemical_formula_sum            'C71 H168 I6 N3 P6 Ru3 Si6'
_chemical_formula_weight         2483.05
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 92.910(6)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.533(3)
_cell_length_b                   17.061(4)
_cell_length_c                   47.050(11)
_cell_measurement_temperature    130(2)
_cell_volume                     10047(4)
_diffrn_ambient_temperature      130(2)
_exptl_crystal_density_diffrn    1.642
_cod_duplicate_entry             4074751
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4060863
Thulium Alkylidene Complexes: Synthesis, X-ray Structures, and Reactivity
Cantat, Thibault; Jaroschik, Florian; Ricard, Louis; Le Floch, Pascal; Nief, François; Mézailles, Nicolas; Organometallics 25 (2006) 1329–1332; doi:10.1021/om050877c

data_4060864
_publ_section_title
;
 Thulium Alkylidene Complexes: Synthesis, X-ray Structures, and Reactivity
;
_journal_coden_ASTM              ORGND7
_journal_issue                   5
_journal_name_full               Organometallics
_journal_page_first              1329
_journal_page_last               1332
_journal_paper_doi               10.1021/om050877c
_journal_volume                  25
_journal_year                    2006
_chemical_formula_sum            'C73 H80 I2 O4 P4 S4 Tm2'
_chemical_formula_weight         1865.15
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 95.8700(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   19.7560(10)
_cell_length_b                   20.6800(10)
_cell_length_c                   18.3020(10)
_cell_measurement_temperature    150.0(1)
_cell_volume                     7438.1(7)
_diffrn_ambient_temperature      150.0(1)
_exptl_crystal_density_diffrn    1.666
_cod_duplicate_entry             4074778
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4060864
Thulium Alkylidene Complexes: Synthesis, X-ray Structures, and Reactivity
Cantat, Thibault; Jaroschik, Florian; Ricard, Louis; Le Floch, Pascal; Nief, François; Mézailles, Nicolas; Organometallics 25 (2006) 1329–1332; doi:10.1021/om050877c

data_4060865
_publ_section_title
;
 Thulium Alkylidene Complexes: Synthesis, X-ray Structures, and Reactivity
;
_journal_coden_ASTM              ORGND7
_journal_issue                   5
_journal_name_full               Organometallics
_journal_page_first              1329
_journal_page_last               1332
_journal_paper_doi               10.1021/om050877c
_journal_volume                  25
_journal_year                    2006
_chemical_formula_sum            'C66 H72 Li O4 P4 S4 Tm'
_chemical_formula_weight         1357.23
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                74.5200(10)
_cell_angle_beta                 79.5400(10)
_cell_angle_gamma                76.4200(10)
_cell_formula_units_Z            4
_cell_length_a                   14.8860(10)
_cell_length_b                   20.6060(10)
_cell_length_c                   22.2730(10)
_cell_measurement_temperature    150.0(1)
_cell_volume                     6348.4(6)
_diffrn_ambient_temperature      150.0(1)
_exptl_crystal_density_diffrn    1.420
_cod_duplicate_entry             4074779
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4060865
Thulium Alkylidene Complexes: Synthesis, X-ray Structures, and Reactivity
Cantat, Thibault; Jaroschik, Florian; Ricard, Louis; Le Floch, Pascal; Nief, François; Mézailles, Nicolas; Organometallics 25 (2006) 1329–1332; doi:10.1021/om050877c

data_4060866
_publ_section_title
;
 Thulium Alkylidene Complexes: Synthesis, X-ray Structures, and Reactivity
;
_journal_coden_ASTM              ORGND7
_journal_issue                   5
_journal_name_full               Organometallics
_journal_page_first              1329
_journal_page_last               1332
_journal_paper_doi               10.1021/om050877c
_journal_volume                  25
_journal_year                    2006
_chemical_formula_sum            'C66 H72 Li O4 P4 S4 Tm'
_chemical_formula_weight         1357.23
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 98.6800(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   26.4430(10)
_cell_length_b                   14.6880(10)
_cell_length_c                   17.0920(10)
_cell_measurement_temperature    230.0(1)
_cell_volume                     6562.4(6)
_diffrn_ambient_temperature      230.0(1)
_exptl_crystal_density_diffrn    1.374
_cod_duplicate_entry             4074780
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4060866
Thulium Alkylidene Complexes: Synthesis, X-ray Structures, and Reactivity
Cantat, Thibault; Jaroschik, Florian; Ricard, Louis; Le Floch, Pascal; Nief, François; Mézailles, Nicolas; Organometallics 25 (2006) 1329–1332; doi:10.1021/om050877c

data_4060867
_publ_section_title
;
 Thulium Alkylidene Complexes: Synthesis, X-ray Structures, and Reactivity
;
_journal_coden_ASTM              ORGND7
_journal_issue                   5
_journal_name_full               Organometallics
_journal_page_first              1329
_journal_page_last               1332
_journal_paper_doi               10.1021/om050877c
_journal_volume                  25
_journal_year                    2006
_chemical_formula_sum            'C80 H68 Li O3 P4 S4 Tm'
_chemical_formula_weight         1505.37
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 108.3510(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   20.0750(10)
_cell_length_b                   11.6070(10)
_cell_length_c                   29.6480(10)
_cell_measurement_temperature    150.0(1)
_cell_volume                     6557.0(7)
_diffrn_ambient_temperature      150.0(1)
_exptl_crystal_density_diffrn    1.525
_cod_duplicate_entry             4074781
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4060867
Deprotonation of N-Heterocyclic Carbenes to Afford Heterobimetallic Organolanthanide Complexes
Arnold, Polly L.; Liddle, Stephen T.; Organometallics 25 (2006) 1485–1491; doi:10.1021/om050895u

data_4060868
_publ_section_title
;
 Deprotonation of N-Heterocyclic Carbenes to Afford Heterobimetallic
 Organolanthanide Complexes
;
_journal_coden_ASTM              ORGND7
_journal_issue                   6
_journal_name_full               Organometallics
_journal_page_first              1485
_journal_page_last               1491
_journal_paper_doi               10.1021/om050895u
_journal_volume                  25
_journal_year                    2006
_chemical_formula_moiety         'C58 H138 K2 N10 O4 Si8 Y2'
_chemical_formula_sum            'C58 H138 K2 N10 O4 Si8 Y2'
_chemical_formula_weight         1520.52
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 96.674(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   12.8586(12)
_cell_length_b                   17.7064(17)
_cell_length_c                   19.2653(18)
_cell_measurement_temperature    150(2)
_cell_volume                     4356.6(7)
_diffrn_ambient_temperature      150(2)
_exptl_crystal_density_diffrn    1.159
_cod_duplicate_entry             4074797
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4060868
Deprotonation of N-Heterocyclic Carbenes to Afford Heterobimetallic Organolanthanide Complexes
Arnold, Polly L.; Liddle, Stephen T.; Organometallics 25 (2006) 1485–1491; doi:10.1021/om050895u

data_4060869
_publ_section_title
;
 Deprotonation of N-Heterocyclic Carbenes to Afford Heterobimetallic
 Organolanthanide Complexes
;
_journal_coden_ASTM              ORGND7
_journal_issue                   6
_journal_name_full               Organometallics
_journal_page_first              1485
_journal_page_last               1491
_journal_paper_doi               10.1021/om050895u
_journal_volume                  25
_journal_year                    2006
_chemical_formula_moiety         'C58 H138 K2 N10 O4 Si8 Sm2'
_chemical_formula_sum            'C58 H138 K2 N10 O4 Si8 Sm2'
_chemical_formula_weight         1643.40
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 96.474(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   12.897(2)
_cell_length_b                   17.735(3)
_cell_length_c                   19.302(3)
_cell_measurement_temperature    150(2)
_cell_volume                     4386.8(12)
_diffrn_ambient_temperature      150(2)
_exptl_crystal_density_diffrn    1.244
_cod_duplicate_entry             4074798
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4060869
Deprotonation of N-Heterocyclic Carbenes to Afford Heterobimetallic Organolanthanide Complexes
Arnold, Polly L.; Liddle, Stephen T.; Organometallics 25 (2006) 1485–1491; doi:10.1021/om050895u

data_4060870
_publ_section_title
;
 Deprotonation of N-Heterocyclic Carbenes to Afford Heterobimetallic
 Organolanthanide Complexes
;
_journal_coden_ASTM              ORGND7
_journal_issue                   6
_journal_name_full               Organometallics
_journal_page_first              1485
_journal_page_last               1491
_journal_paper_doi               10.1021/om050895u
_journal_volume                  25
_journal_year                    2006
_chemical_formula_moiety         'C40 H90 N8 O2 Si4 Sm2, 0.5(C6 H14)'
_chemical_formula_sum            'C43 H97 N8 O2 Si4 Sm2'
_chemical_formula_weight         1171.35
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 112.692(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   26.899(7)
_cell_length_b                   11.136(3)
_cell_length_c                   21.979(6)
_cell_measurement_temperature    150(2)
_cell_volume                     6074(3)
_diffrn_ambient_temperature      150(2)
_exptl_crystal_density_diffrn    1.281
_cod_duplicate_entry             4074799
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4060870
Synthesis of a Library of Iridium-Containing Dinuclear Complexes with Bridging PNNN and PNNP Ligands (BL), [LM(μ-BL)M'L']BF4. 2. Preparation, Basic Coordination Properties, and Reactivity of the Carbonyl Complexes
Dubs, Christian; Yamamoto, Toshiki; Inagaki, Akiko; Akita, Munetaka; Organometallics 25 (2006) 1359–1367; doi:10.1021/om050897e

data_4060871
_publ_section_title
;
 Synthesis of a Library of Iridium-Containing Dinuclear Complexes with
 Bridging PNNN and PNNP Ligands (BL), [LM(\m-BL)M'L']BF4.
 2. Preparation, Basic Coordination Properties, and Reactivity of the
 Carbonyl Complexes
;
_journal_coden_ASTM              ORGND7
_journal_issue                   6
_journal_name_full               Organometallics
_journal_page_first              1359
_journal_page_last               1367
_journal_paper_doi               10.1021/om050897e
_journal_volume                  25
_journal_year                    2006
_chemical_formula_moiety         'C27 H27 B F4 N3 P Pd2 '
_chemical_formula_sum            'C27 H27 B F4 N3 P Pd2'
_chemical_formula_weight         724.11
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                97.89(2)
_cell_angle_beta                 110.574(8)
_cell_angle_gamma                91.28(2)
_cell_formula_units_Z            2
_cell_length_a                   10.638(4)
_cell_length_b                   11.351(3)
_cell_length_c                   12.251(4)
_cell_measurement_temperature    213.2
_cell_volume                     1367.9(8)
_diffrn_ambient_temperature      213
_exptl_crystal_density_diffrn    1.758
_cod_duplicate_entry             4074800
_cod_original_formula_sum        'C27 H27 B F4 N3 P Pd2 '
_cod_database_code               4060871
Synthesis of a Library of Iridium-Containing Dinuclear Complexes with Bridging PNNN and PNNP Ligands (BL), [LM(μ-BL)M'L']BF4. 2. Preparation, Basic Coordination Properties, and Reactivity of the Carbonyl Complexes
Dubs, Christian; Yamamoto, Toshiki; Inagaki, Akiko; Akita, Munetaka; Organometallics 25 (2006) 1359–1367; doi:10.1021/om050897e

data_4060872
_publ_section_title
;
 Synthesis of a Library of Iridium-Containing Dinuclear Complexes with
 Bridging PNNN and PNNP Ligands (BL), [LM(\m-BL)M'L']BF4.
 2. Preparation, Basic Coordination Properties, and Reactivity of the
 Carbonyl Complexes
;
_journal_coden_ASTM              ORGND7
_journal_issue                   6
_journal_name_full               Organometallics
_journal_page_first              1359
_journal_page_last               1367
_journal_paper_doi               10.1021/om050897e
_journal_volume                  25
_journal_year                    2006
_chemical_formula_moiety         'C39 H45 B Cl4 F4 Ir N3 P Rh '
_chemical_formula_sum            'C39 H45 B Cl4 F4 Ir N3 P Rh'
_chemical_formula_weight         1110.52
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                99.43(1)
_cell_angle_beta                 103.25(2)
_cell_angle_gamma                91.89(2)
_cell_formula_units_Z            2
_cell_length_a                   12.795(3)
_cell_length_b                   13.033(4)
_cell_length_c                   14.044(5)
_cell_measurement_temperature    213
_cell_volume                     2242(1)
_diffrn_ambient_temperature      213
_exptl_crystal_density_diffrn    1.644
_cod_duplicate_entry             4074801
_cod_original_formula_sum        'C39 H45 B Cl4 F4 Ir N3 P Rh '
_cod_database_code               4060872
Synthesis of a Library of Iridium-Containing Dinuclear Complexes with Bridging PNNN and PNNP Ligands (BL), [LM(μ-BL)M'L']BF4. 2. Preparation, Basic Coordination Properties, and Reactivity of the Carbonyl Complexes
Dubs, Christian; Yamamoto, Toshiki; Inagaki, Akiko; Akita, Munetaka; Organometallics 25 (2006) 1359–1367; doi:10.1021/om050897e

data_4060873
_publ_section_title
;
 Synthesis of a Library of Iridium-Containing Dinuclear Complexes with
 Bridging PNNN and PNNP Ligands (BL), [LM(\m-BL)M'L']BF4.
 2. Preparation, Basic Coordination Properties, and Reactivity of the
 Carbonyl Complexes
;
_journal_coden_ASTM              ORGND7
_journal_issue                   6
_journal_name_full               Organometallics
_journal_page_first              1359
_journal_page_last               1367
_journal_paper_doi               10.1021/om050897e
_journal_volume                  25
_journal_year                    2006
_chemical_formula_moiety         'C51 H36 B2 Cl2 F8 N6 O9 P2 Rh4 '
_chemical_formula_sum            'C51 H36 B2 Cl2 F8 N6 O9 P2 Rh4'
_chemical_formula_weight         1594.96
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                90.35(2)
_cell_angle_beta                 99.879(7)
_cell_angle_gamma                96.11(2)
_cell_formula_units_Z            2
_cell_length_a                   9.990(4)
_cell_length_b                   13.054(3)
_cell_length_c                   22.616(8)
_cell_measurement_temperature    213
_cell_volume                     2888(1)
_diffrn_ambient_temperature      213
_exptl_crystal_density_diffrn    1.834
_cod_duplicate_entry             4074802
_cod_original_formula_sum        'C51 H36 B2 Cl2 F8 N6 O9 P2 Rh4 '
_cod_database_code               4060873