Metal-free photocatalytic trifluoromethylative pyridylation of unactivated alkenes
He, Yu-Tao; Kang, Dahye; Kim, Inwon; Hong, Sungwoo; Green Chemistry 20 (2018) 5209–; doi:10.1039/C8GC02782J

data_7231651
_publ_section_title
;
 Metal-free photocatalytic trifluoromethylative pyridylation of
 unactivated alkenes
;
_journal_issue                   22
_journal_name_full               'Green Chemistry'
_journal_page_first              5209
_journal_paper_doi               10.1039/C8GC02782J
_journal_volume                  20
_journal_year                    2018
_chemical_formula_sum            'C20 H22 F3 N O3'
_chemical_formula_weight         381.38
_space_group_crystal_system      triclinic
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_space_group_name_Hall           '-P 1'
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_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2018-08-28 deposited with the CCDC.
2018-10-08 downloaded from the CCDC.
;
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_computing_structure_solution    SHELXS
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_diffrn_measured_fraction_theta_max 0.969
_diffrn_measurement_device_type  'Rayonix MX225HS CCD area detector'
_diffrn_measurement_method       'omega scan'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1208P)^2^+0.1221P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           P027_002M
_cod_depositor_comments          'Adding full bibliography for 7231651.cif.'
_cod_database_code               7231651
_shelx_shelxl_version_number     2018/3
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