Exploration of fluorescent organotin compounds of α-amino acid Schiff bases for the detection of organophosphorous chemical warfare agents: quantification of diethylchlorophosphate
Singh, Navjot; Kumar, Keshav; Srivastav, Neha; Singh, Raghubir; Kaur, Varinder; Jasinski, Jerry P.; Butcher, Ray J.; New Journal of Chemistry 42 (2018) 8756–; doi:10.1039/C8NJ01153B

data_7057257
_publ_section_title
;
 Exploration of fluorescent organotin compounds of \a-amino acid Schiff
 bases for the detection of organophosphorous chemical warfare agents:
 quantification of diethylchlorophosphate
;
_journal_issue                   11
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              8756
_journal_paper_doi               10.1039/C8NJ01153B
_journal_volume                  42
_journal_year                    2018
_chemical_formula_moiety         'C36 H45 N3 O9 Sn3'
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_audit_update_record
;
2017-12-20 deposited with the CCDC.
2018-04-09 downloaded from the CCDC.
;
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_cell_measurement_temperature    173(2)
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_diffrn_ambient_temperature      173(2)
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;
CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015)
Analytical numeric absorption correction using a multifaceted crystal
                        model based on expressions derived by R.C. Clark & J.S. Reid.
(Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            'pale yellow'
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'Re-crystallisation from solvent: methanol:hexane '
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0535P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.1000
_reflns_Friedel_coverage         0.000
_reflns_number_gt                6634
_reflns_number_total             7496
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7057257--7057258.cif.'
_cod_database_code               7057257
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