data_5000334
_chemical_formula_moiety         'C25 H46 F2 O1 Os1 P2'
_chemical_formula_sum            'C25 H46 F2 O Os P2'
_chemical_formula_weight         652.814
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                97.840(7)
_cell_angle_beta                 93.437(7)
_cell_angle_gamma                87.191(7)
_cell_formula_units_Z            4
_cell_length_a                   14.3306(18)
_cell_length_b                   18.409(2)
_cell_length_c                   10.6652(15)
_cell_measurement_reflns_used    152
_cell_measurement_temperature    113
_cell_measurement_theta_max      15.94
_cell_measurement_theta_min      10.27
_cell_volume                     2779.9(6)
_diffrn_ambient_temperature      113
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0
_diffrn_measured_fraction_theta_max 1
_diffrn_measurement_device_type  'refurbished Picker diffractometer'
_diffrn_measurement_method       '\q/2\q scans'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.035
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       4
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            14452
_diffrn_reflns_theta_full        0
_diffrn_reflns_theta_max         25.0621
_diffrn_reflns_theta_min         3.00702
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 300
_diffrn_standards_number         4
_exptl_absorpt_coefficient_mu    4.7288
_exptl_absorpt_correction_T_max  0.663
_exptl_absorpt_correction_T_min  0.401
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details   Tompa
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.56
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       'irregular prism'
_exptl_crystal_F_000             1312
_exptl_crystal_size_max          .25
_exptl_crystal_size_mid          .175
_exptl_crystal_size_min          .10
_refine_diff_density_max         2.1
_refine_diff_density_min         -1.62
_refine_ls_abs_structure_details none
_refine_ls_abs_structure_Flack   ?
_refine_ls_extinction_coef       -0.00000017(2)
_refine_ls_extinction_expression
;
Larson, A. C. (1967).  Acta Cryst. 23, p. 664.  Eq. (3)
;
_refine_ls_extinction_method     Zachariasen
_refine_ls_goodness_of_fit_ref   0.8791
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_parameters     560
_refine_ls_number_reflns         7236
_refine_ls_R_factor_gt           0.0425
_refine_ls_shift/su_max          0.0195
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w^-1^=\s^2^(F)+(.07F)^2^
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.0388
_reflns_number_gt                7235
_reflns_number_total             9847
_reflns_threshold_expression     F>3.0\s(F)
_cod_original_formula_sum        'C25 H46 F2 O1 Os1 P2'
_cod_database_code               5000334