Hydrogen-bonding directed, regioselective photocycloaddition reactions of cyanonaphthalenes with furanmethanols.
Maeda, Hajime; Chiyonobu, Kazuhiko; Mizuno, Kazuhiko; Photochemical & photobiological sciences : Official journal of the European Photochemistry Association and the European Society for Photobiology 10 (2011) 1445–1449; doi:10.1039/c1pp05060e

data_1515743
_publ_section_title
;
 Hydrogen-bonding directed, regioselective photocycloaddition reactions of
 cyanonaphthalenes with furanmethanols.
;
_journal_issue                   9
_journal_name_full
'Photochemical &amp; photobiological sciences : Official journal of the European Photochemistry Association and the European Society for Photobiology'
_journal_page_first              1445
_journal_page_last               1449
_journal_paper_doi               10.1039/c1pp05060e
_journal_volume                  10
_journal_year                    2011
_chemical_formula_moiety         'C16 H13 N O2 '
_chemical_formula_sum            'C16 H13 N O2'
_chemical_formula_weight         251.28
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2yab'
_symmetry_space_group_name_H-M   'P 1 21/a 1'
_audit_creation_date             2002-01-28
_audit_creation_method           'by CrystalStructure v2.00'
_cell_angle_alpha                90
_cell_angle_beta                 105.29(7)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   11.80(3)
_cell_length_b                   6.73(1)
_cell_length_c                   16.57(5)
_cell_measurement_reflns_used    96
_cell_measurement_temperature    296.1
_cell_measurement_theta_max      19.9
_cell_measurement_theta_min      3.5
_cell_volume                     1269(5)
_computing_cell_refinement       PROCESS-AUTO
_computing_data_collection       PROCESS-AUTO
_computing_data_reduction        CrystalStructure
_computing_publication_material  'CrystalStructure Ver. 2.00'
_computing_structure_refinement  CRYSTALS
_computing_structure_solution    SIR92
_diffrn_detector_area_resol_mean 10.00
_diffrn_measured_fraction_theta_full 0.9373
_diffrn_measured_fraction_theta_max 0.9373
_diffrn_measurement_device_type  'Rigaku RAXIS-RAPID'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.058
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       8
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -21
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_diffrn_reflns_theta_max         27.47
_exptl_absorpt_coefficient_mu    0.087
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.315
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.15
_refine_diff_density_max         0.50
_refine_diff_density_min         -0.43
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.991
_refine_ls_hydrogen_treatment    refall
_refine_ls_number_parameters     129
_refine_ls_number_reflns         1325
_refine_ls_R_factor_gt           0.0810
_refine_ls_shift/su_max          0.0000
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1.0'
_refine_ls_weighting_scheme      unit
_refine_ls_wR_factor_ref         0.0770
_reflns_number_gt                1325
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_reflns_threshold_expression     F^2^>2.0\s(F^2^)
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_cod_data_source_block           chiyo02
_cod_original_cell_volume        1269.6(5)
_cod_original_formula_sum        'C16 H13 N O2 '
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