Polyatomic Clusters of the Triel Elements. Palladium-Centered Clusters of Thallium in A8Tl11Pd, A = Cs, Rb, K
Stefan Kaskel; Michael T. Klem; John D. Corbett; Inorganic Chemistry 41 (2002) 3457–3462; doi:10.1021/ic020078b

data_4318182
_publ_contact_author_email       jdc@ameslab.gov
_publ_contact_author_name        'J.D. Corbett'
_publ_contact_author_phone       '515  294-3086 '
_publ_section_title
;
 Polyatomic Clusters of the Triel Elements. Palladium-Centered Clusters of
 Thallium in A8Tl11Pd, A = Cs, Rb, K
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              3457
_journal_page_last               3462
_journal_paper_doi               10.1021/ic020078b
_journal_volume                  41
_journal_year                    2002
_chemical_formula_moiety         'Cs8 Pd Tl11 '
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_symmetry_Int_Tables_number      167
_symmetry_space_group_name_Hall  '-R 3 2"c'
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_cell_angle_gamma                120
_cell_formula_units_Z            6
_cell_length_a                   10.610(1)
_cell_length_b                   10.610(1)
_cell_length_c                   54.683(8)
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_computing_cell_refinement       'MSC/AFC Diffractometer Control'
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_computing_data_reduction        'teXsan for Windows (MSC, 1997)'
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;
SHELX97 (Sheldrick, 1997)
;
_diffrn_ambient_temperature      296.2
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_diffrn_reflns_limit_l_max       70
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;
\y scans (North,Phillips & Matthews, 1968)
;
_exptl_crystal_colour            -------------------
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo) + 0.00000|Fo|^2^]'
_refine_ls_weighting_scheme      sigma
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_reflns_number_gt                420
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_reflns_threshold_expression     I>3.00\s(I)
_cod_data_source_file            ic020078b.cif
_cod_data_source_block           '_afc6r.xtl_master_file____'
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        5331.1(9)
_cod_original_sg_symbol_H-M      'R -3 c '
_cod_original_formula_sum        'Cs8 Pd Tl11 '
_cod_database_code               4318182