Chlorure de <i>cis</i>-Chloro(diméthyl sulfoxyde)(metformine)platine(II)
Viossat, B.; Nguyen-Huy Dung; Rodier, N.; Bentefrit, F.; Acta Crystallographica Section C 51 (1995) 878–880; doi:10.1107/S0108270194009674

data_2003499
_publ_section_title
;
 Chlorure de <i>cis</i>-Chloro(dim\'ethyl
 sulfoxyde)(metformine)platine(II)
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              878
_journal_page_last               880
_journal_paper_doi               10.1107/S0108270194009674
_journal_volume                  51
_journal_year                    1995
_chemical_compound_source        '\'evaporation d'une solution m\'ethanolique'
_chemical_formula_sum            'C6 H17 Cl2 N5 O Pt S'
_chemical_formula_weight         473.30
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90
_cell_angle_beta                 117.17(2)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   18.169(3)
_cell_length_b                   10.932(3)
_cell_length_c                   16.120(3)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293
_cell_measurement_theta_max      13.38
_cell_measurement_theta_min      8.79
_cell_volume                     2848.5(12)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            2877
_diffrn_reflns_theta_max         26
_diffrn_standards_decay_%        'non significatives'
_diffrn_standards_interval_time  120
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    10.47
_exptl_absorpt_correction_T_max  1.330
_exptl_absorpt_correction_T_min  0.668
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            'jaune p\^ale'
_exptl_crystal_density_diffrn    2.21
_exptl_crystal_density_meas      2.20
_exptl_crystal_description       parall\'el\'epip\`ede
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.9(2)
_refine_diff_density_min         -0.9(2)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   1.20
_refine_ls_number_parameters     145
_refine_ls_number_reflns         1816
_refine_ls_R_factor_obs          0.032
_refine_ls_shift/esd_max         0.01
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/\s^2^(F~o~)'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.038
_reflns_number_observed          1816
_reflns_number_total             2877
_reflns_observed_criterion       'I >= 3\s(I)'
_cod_data_source_file            pa1121.cif
_cod_data_source_block           pa1121a
_cod_depositor_comments
;
 Marking attached hydrogen atoms.

 Antanas Vaitkus,
 2017-08-09

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value '1/\s^2^(F~o~)' was changed to
'calc'. New tag '_refine_ls_weighting_details' was created. The value
of the new tag was set to 'w = 1/\s^2^(F~o~)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        2842(8)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               2003499