Chloro(ethanedithioamide-<i>S</i>)bis(triphenylphosphine)silver(I)
Long, D.-L.; Xin, X.-Q.; Huang, X.-Y.; Kang, B.-S.; Acta Crystallographica Section C 52 (1996) 1161–1163; doi:10.1107/S0108270195013813

data_2004897
_publ_section_title
;
 Chloro(ethanedithioamide-<i>S</i>)bis(triphenylphosphine)silver(I)
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1161
_journal_page_last               1163
_journal_paper_doi               10.1107/S0108270195013813
_journal_volume                  52
_journal_year                    1996
_chemical_formula_sum            'C38 H34 Ag Cl N2 P2 S2'
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_cell_angle_beta                 92.58(2)
_cell_angle_gamma                90
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_cell_length_b                   19.572(4)
_cell_length_c                   20.017(6)
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_cell_measurement_temperature    300
_cell_measurement_theta_max      14.91
_cell_measurement_theta_min      11.42
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_computing_cell_refinement       'CAD-4 Software'
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'TEXSAN (Molecular Structure Corporation, 1987)'
_computing_molecular_graphics
'ORTEPII (Johnson, 1976) and PLUTO (Motherwell & Clegg, 1978)'
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_diffrn_radiation_type           MoK\a
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_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       0
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_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       23
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'empirical, \DF (Texsan; Molecular Structure Corporation, 1987)'
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_refine_ls_extinction_method     none
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_refine_ls_hydrogen_treatment    'H atoms refined isotropically'
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_refine_ls_R_factor_obs          0.037
_refine_ls_shift/esd_max         0.11
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w=1/\s^2^(F)
_refine_ls_weighting_scheme      calc
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_reflns_number_observed          5452
_reflns_number_total             6850
_reflns_observed_criterion       I>3\s(I)
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_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value ' w=1/\s^2^(F)' was changed to
'calc'. New tag '_refine_ls_weighting_details' was created. The value
of the new tag was set to 'w=1/\s^2^(F)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        3702(2)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2004897