Formation of a molecular spin ladder induced by a supramolecular cation structure
Nishihara, Sadafumi; Akutagawa, Tomoyuki; Hasegawa, Tatsuo; Nakamura, Takayoshi; Chemical Communications  (2002) 408–; doi:10.1039/b110368g

data_7114334
_publ_section_title
;
 Formation of a molecular spin ladder induced by a supramolecular cation
 structure
;
_journal_issue                   5
_journal_name_full               'Chemical Communications'
_journal_page_first              408
_journal_paper_doi               10.1039/b110368g
_journal_year                    2002
_chemical_compound_source        'synthesized by the authors, see text'
_chemical_formula_sum            'C24 H32 N Ni O6 S10'
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_audit_creation_date             'Thu Mar 22 21:02:01 2001'
_audit_creation_method           'by teXsan'
_cell_angle_alpha                97.120(2)
_cell_angle_beta                 92.599(3)
_cell_angle_gamma                112.846(2)
_cell_formula_units_Z            2
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_cell_length_b                   16.666(2)
_cell_length_c                   8.1271(6)
_cell_measurement_reflns_used    9986
_cell_measurement_temperature    296.2
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      1.6
_cell_volume                     1751.7(3)
_computing_cell_refinement       PROCESS-AUTO
_computing_data_collection       PROCESS-AUTO
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_computing_publication_material  'teXsan Ver. 1.10'
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_diffrn_ambient_temperature      296.2
_diffrn_measurement_device_type  Rigaku
_diffrn_measurement_method       \w-scan
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_diffrn_orient_matrix_UB_33      0.00000
_diffrn_radiation_detector       'Imaging Plate'
_diffrn_radiation_monochromator  graphite
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_diffrn_radiation_type           'Mo K\a'
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_diffrn_reflns_reduction_process 'Lp corrections applied'
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_scheme      calc
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_reflns_observed_criterion       F^2^>3.0\s(F^2^)
_cod_data_source_file            b110368g.txt
_cod_data_source_block           1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        1751.6(3)
_cod_original_sg_symbol_H-M      'P -1         '
_cod_original_formula_sum        'C24 H32 N Ni O6 S10 '
_cod_database_code               7114334