Synthesis and characterisation of boranediyl- and diboranediyl-bridged diplatinum A-frame complexes.
Brunecker, Carina; Arrowsmith, Merle; Müssig, Jonas H; Böhnke, Julian; Stoy, Andreas; Heß, Merlin; Hofmann, Alexander; Lenczyk, Carsten; Lichtenberg, Crispin; Ramler, Jacqueline; Rempel, Anna; Braunschweig, Holger; Dalton transactions (Cambridge, England : 2003) 50 (2021) 3506–3515; doi:10.1039/d0dt03855e

data_7706357
_publ_section_title
;
 Synthesis and characterisation of boranediyl- and diboranediyl-bridged
 diplatinum A-frame complexes.
;
_journal_issue                   10
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              3506
_journal_page_last               3515
_journal_paper_doi               10.1039/d0dt03855e
_journal_volume                  50
_journal_year                    2021
_chemical_formula_moiety         'C10 H28 I4 P4 Pt2, C6 H6'
_chemical_formula_sum            'C16 H34 I4 P4 Pt2'
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_space_group_name_Hall           '-P 1'
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_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2020-11-06 deposited with the CCDC.	2021-01-08 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'Bruker D8 Quest'
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_diffrn_reflns_point_group_measured_fraction_full 0.993
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_exptl_crystal_recrystallization_method
'Re-crystallisation from solvent: CH2Cl2/pentane'
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_refine_ls_extinction_method     none
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_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+0.6595P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0340
_refine_ls_wR_factor_ref         0.0340
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_reflns_number_total             2772
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           test_a
_cod_depositor_comments
'Adding full bibliography for 7706356--7706368.cif.'
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_shelx_shelxl_version_number     2018/3
_shelx_estimated_absorpt_t_min   0.118
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_shelx_res_checksum              93513