Water-Soluble Iron(IV)-Oxo Complexes Supported by Pentapyridine Ligands: Axial Ligand Effects on Hydrogen Atom and Oxygen Atom Transfer Reactivity.
Chantarojsiri, Teera; Sun, Yujie; Long, Jeffrey R.; Chang, Christopher J.; Inorganic chemistry 54 (2015) 5879–5887; doi:10.1021/acs.inorgchem.5b00658

data_4343256
_publ_section_title
;
 Water-Soluble Iron(IV)-Oxo Complexes Supported by Pentapyridine Ligands:
 Axial Ligand Effects on Hydrogen Atom and Oxygen Atom Transfer
 Reactivity.
;
_journal_issue                   12
_journal_name_full               'Inorganic chemistry'
_journal_page_first              5879
_journal_page_last               5887
_journal_paper_doi               10.1021/acs.inorgchem.5b00658
_journal_volume                  54
_journal_year                    2015
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_space_group_name_Hall           '-P 2yb'
_space_group_name_H-M_alt        'P 1 21/m 1'
_symmetry_space_group_name_Hall  '-P 2yb'
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_cell_length_c                   12.4320(10)
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_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            orange
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_exptl_crystal_description       needles
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0485P)^2^+3.9401P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 4343251--4343257.cif.'
_cod_original_formula_sum        'C15 H17.50 B F4 Fe0.50 N2.50 O2'
_cod_database_code               4343256
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_shelx_hkl_checksum              43596