Dual structure evolution of a Ag(i) supramolecular framework triggered by anion-exchange: replacement of terminal ligand and switching of network interpenetration degree.
Li, Cheng-Peng; Wang, Si; Guo, Wei; Yan, Yan; Du, Miao; Chemical communications (Cambridge, England) 52 (2016) 11060–11063; doi:10.1039/c6cc05938d

data_7124972
_publ_section_title
;
 Dual structure evolution of a Ag(i) supramolecular framework triggered by
 anion-exchange: replacement of terminal ligand and switching of network
 interpenetration degree.
;
_journal_issue                   74
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              11060
_journal_page_last               11063
_journal_paper_doi               10.1039/c6cc05938d
_journal_volume                  52
_journal_year                    2016
_chemical_formula_sum            'C17 H15 Ag N7 O3.5'
_chemical_formula_weight         481.23
_space_group_IT_number           88
_space_group_name_Hall           '-I 4ad'
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_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_H-M   'I 41/a :2'
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_audit_update_record
;
2014-11-24 deposited with the CCDC.
2016-08-08 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
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_cell_length_b                   31.065(3)
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_computing_cell_refinement       'Bruker SMART'
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_computing_publication_material  'Bruker SHELXTL'
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_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'CCD area detector'
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_diffrn_radiation_monochromator  graphite
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0516P)^2^+6.0383P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_data_source_file            c6cc05938d3.cif
_cod_data_source_block           2
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'MULTI-SCAN' was
changed to 'multi-scan' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/RSC/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

data item '_symmetry_cell_setting' value 'Tetragonal' was changed to
'tetragonal' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/RSC/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

data item '_exptl_crystal_density_meas' value 'NONE' was changed to
'?' -- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_original_cell_volume        7720.4(17)
_cod_original_sg_symbol_H-M      I4(1)/a
_cod_original_formula_sum        'C17 H15 Ag N7 O3.50'
_cod_database_code               7124972