New three-dimensional inorganic frameworks based on the uranophane-type sheet in monoamine templated uranyl-vanadates
Jouffret, Laurent; Shao, Zhenmian; Rivenet, Murielle; Abraham, Francis; Journal of Solid State Chemistry 183 (2010) 2290–2297; doi:10.1016/j.jssc.2010.07.035

data_1563493
_publ_section_title
;
 New three-dimensional inorganic frameworks based on the uranophane-type
 sheet in monoamine templated uranyl-vanadates
;
_journal_issue                   10
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              2290
_journal_page_last               2297
_journal_paper_doi               10.1016/j.jssc.2010.07.035
_journal_volume                  183
_journal_year                    2010
_chemical_absolute_configuration .
_chemical_formula_sum            'C2 H14 N O23 U4 V3'
_chemical_formula_weight         1525.1
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 96.966(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   10.2312(4)
_cell_length_b                   13.5661(7)
_cell_length_c                   17.5291(7)
_cell_measurement_temperature    100
_cell_volume                     2415.04(18)
_computing_publication_material
'Jana2000 (Petricek, Dusek & Palatinus, 2000)'
_computing_structure_refinement
'Jana2000 (Petricek, Dusek & Palatinus, 2000)'
_diffrn_ambient_temperature      100
_diffrn_measured_fraction_theta_full 0.99
_diffrn_measured_fraction_theta_max 0.94
_diffrn_measurement_device_type  SMART-1K-CCD
_diffrn_measurement_method       'omega scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0493
_diffrn_reflns_av_sigmaI/netI    0.0570
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       7
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            29217
_diffrn_reflns_theta_full        26.73
_diffrn_reflns_theta_max         33.96
_diffrn_reflns_theta_min         1.90
_exptl_absorpt_coefficient_mu    27.925
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.380
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            'pale yellow'
_exptl_crystal_density_diffrn    4.1931
_exptl_crystal_description       plate
_exptl_crystal_F_000             2559
_exptl_crystal_size_max          0.164
_exptl_crystal_size_mid          0.100
_exptl_crystal_size_min          0.010
_refine_diff_density_max         3.51
_refine_diff_density_min         -2.14
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_gt    1.39
_refine_ls_goodness_of_fit_ref   1.28
_refine_ls_hydrogen_treatment    undef
_refine_ls_number_parameters     168
_refine_ls_number_reflns         9185
_refine_ls_R_factor_all          0.0589
_refine_ls_R_factor_gt           0.0346
_refine_ls_shift/su_max          0.0310
_refine_ls_shift/su_mean         0.0021
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w=1/\s^2^(F)
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.0316
_refine_ls_wR_factor_ref         0.0343
_reflns_number_gt                6638
_reflns_number_total             9185
_reflns_threshold_expression     I>3\s(I)
_cod_data_source_file            JSSC-2010-183-2290.cif
_cod_data_source_block           3
_cod_original_sg_symbol_Hall     '-P 2yabc'
_cod_original_formula_sum        'C2 H14 N1 O23 U4 V3'
_cod_database_code               1563493