Direct methylation and carbonylation of in situ generated arynes via HDDA-Wittig coupling
Liu, Baohua; Mao, Chunyan; Hu, Qiong; Yao, Liangliang; Hu, Yimin; Organic Chemistry Frontiers 6 (2019) 2788–; doi:10.1039/C9QO00621D

data_1554980
_publ_section_title
;
 Direct methylation and carbonylation of in situ generated arynes via
 HDDA-Wittig coupling
;
_journal_issue                   15
_journal_name_full               'Organic Chemistry Frontiers'
_journal_page_first              2788
_journal_paper_doi               10.1039/C9QO00621D
_journal_volume                  6
_journal_year                    2019
_chemical_formula_sum            'C15 H12 F O3'
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_audit_update_record
;
2019-03-14 deposited with the CCDC.	2019-06-13 downloaded from the CCDC.
;
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_diffrn_ambient_temperature      273(2)
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
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_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.1359P)^2^+0.4109P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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