Redox-induced dimerisations of a phosphacyclic biradicaloid.
Zuber, David; Storcheva, Oksana; Lüdtke, Karsten Paul; Brunk, Leonidas; Coburger, Peter; Chemical communications (Cambridge, England) 61 (2025) 2798–2801; doi:10.1039/d4cc05656f

data_7134104
_publ_section_title
;
 Redox-induced dimerisations of a phosphacyclic biradicaloid.
;
_journal_issue                   13
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              2798
_journal_page_last               2801
_journal_paper_doi               10.1039/d4cc05656f
_journal_volume                  61
_journal_year                    2025
_chemical_formula_sum            'C52 H42 B2 Cl4 F8 P6'
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;
2024-12-03 deposited with the CCDC.	2024-12-29 downloaded from the CCDC.
;
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_computing_cell_refinement
; 
   STOE & CIE GmbH 
   Hilpertstr. 10 
   D-64295 Darmstadt 
   Germany 
;
_computing_data_collection
; 
   STOE & CIE GmbH 
   Hilpertstr. 10 
   D-64295 Darmstadt 
   Germany 
;
_computing_data_reduction
; 
   STOE & CIE GmbH 
   Hilpertstr. 10 
   D-64295 Darmstadt 
   Germany 
;
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; 
   STOE & CIE GmbH 
   Hilpertstr. 10 
   D-64295 Darmstadt 
   Germany 
;
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_diffrn_radiation_type           MoK\a
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_diffrn_reflns_point_group_measured_fraction_full 0.998
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_diffrn_reflns_theta_min         2.220
_diffrn_source                   'Genix 3D HF Mo'
_exptl_absorpt_coefficient_mu    0.444
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_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
; 
   STOE & CIE GmbH 
   Hilpertstr. 10 
   D-64295 Darmstadt 
   Germany 
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.386
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_exptl_crystal_description       prism
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0521P)^2^+1.4197P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_depositor_comments
'Adding full bibliography for 7134102--7134104.cif.'
_cod_original_cell_volume        2801.0(11)
_cod_database_code               7134104
_shelx_shelxl_version_number     2018/3
_shelx_res_checksum              45448
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