A diversity-oriented novel regioselective synthesis of sulfonamide–thiazolidinone hybrids
Preeti, Preeti; Singh, Krishna Nand; New Journal of Chemistry 43 (2019) 6288–; doi:10.1039/C9NJ00055K

data_7058263
_publ_section_title
;
 A diversity-oriented novel regioselective synthesis of
 sulfonamide--thiazolidinone hybrids
;
_journal_issue                   16
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              6288
_journal_paper_doi               10.1039/C9NJ00055K
_journal_volume                  43
_journal_year                    2019
_chemical_formula_moiety         'C19 H17 N3 O5 S2'
_chemical_formula_sum            'C19 H17 N3 O5 S2'
_chemical_formula_weight         431.48
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2018-05-18 deposited with the CCDC.    2019-03-21 downloaded from the CCDC.
;
_cell_angle_alpha                97.739(5)
_cell_angle_beta                 103.231(5)
_cell_angle_gamma                109.788(5)
_cell_formula_units_Z            2
_cell_length_a                   9.050(5)
_cell_length_b                   10.325(5)
_cell_length_c                   11.792(5)
_cell_measurement_reflns_used    4085
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      25.89
_cell_measurement_theta_min      2.29
_cell_volume                     981.8(8)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.982
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0372
_diffrn_reflns_av_sigmaI/netI    0.0325
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            15992
_diffrn_reflns_theta_full        28.34
_diffrn_reflns_theta_max         28.34
_diffrn_reflns_theta_min         1.82
_exptl_absorpt_coefficient_mu    0.308
_exptl_absorpt_correction_T_max  0.974
_exptl_absorpt_correction_T_min  0.965
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   (SADABS;Bruker,2000)
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.459
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             448
_exptl_crystal_size_max          0.46
_exptl_crystal_size_mid          0.43
_exptl_crystal_size_min          0.42
_refine_diff_density_max         0.567
_refine_diff_density_min         -0.368
_refine_diff_density_rms         0.082
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.085
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     270
_refine_ls_number_reflns         4805
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.085
_refine_ls_R_factor_all          0.0614
_refine_ls_R_factor_gt           0.0448
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0891P)^2^+0.2032P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1250
_refine_ls_wR_factor_ref         0.1530
_reflns_number_gt                3772
_reflns_number_total             4805
_reflns_threshold_expression     >2\s(I)
_cod_data_source_file            c9nj00055k2.cif
_cod_data_source_block           ups3310_kns_bhu_0m
_cod_depositor_comments          'Adding full bibliography for 7058263.cif.'
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7058263