Synthesis and catalytic application of magnesium complexes bearing pendant indolyl ligands.
Peng, Kuo-Fu; Chen, Yun; Chen, Chi-Tien; Dalton transactions (Cambridge, England : 2003) 44 (2015) 9610–9619; doi:10.1039/c5dt01173f

data_7034958
_publ_section_title
;
 Synthesis and catalytic application of magnesium complexes bearing
 pendant indolyl ligands.
;
_journal_issue                   20
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              9610
_journal_page_last               9619
_journal_paper_doi               10.1039/c5dt01173f
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety         'C38 H40 Mg N2 O4'
_chemical_formula_sum            'C38 H40 Mg N2 O4'
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 ? 
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2015-01-21 deposited with the CCDC.
2015-04-16 downloaded from the CCDC.
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_cell_angle_alpha                90.00
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_computing_cell_refinement
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CrysAlis RED, Oxford Diffraction Ltd., 
Version 1.171.32.29 (release 10-06-2008 CrysAlis171 .NET) 
(compiled Jun 10 2008,16:49:55) 
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_computing_data_collection
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CrysAlis CCD, Oxford Diffraction Ltd., 
Version 1.171.32.29 (release 10-06-2008 CrysAlis171 .NET) 
(compiled Jun 10 2008,16:49:55) 
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_computing_data_reduction
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CrysAlis RED, Oxford Diffraction Ltd., 
Version 1.171.32.29 (release 10-06-2008 CrysAlis171 .NET) 
(compiled Jun 10 2008,16:49:55) 
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_computing_molecular_graphics    'Bruker SHELXTL'
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_diffrn_radiation_monochromator  graphite
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CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.66 (release 28-04-2010 CrysAlis171 .NET)
(compiled Apr 28 2010,14:27:37)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
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_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.366
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       parallelpied
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_exptl_crystal_size_min          0.19
_refine_diff_density_max         0.630
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_refine_ls_extinction_method     none
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_refine_ls_number_restraints     0
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_refine_ls_R_factor_all          0.0773
_refine_ls_R_factor_gt           0.0527
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0955P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1411
_refine_ls_wR_factor_ref         0.1489
_reflns_number_gt                2392
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_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c5dt01173f2.cif
_cod_data_source_block           Compound3a
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 3271 2015-04-21 07:52:19Z andrius 

 Adding full bibliography for 7034958--7034959.cif.
;
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7034958