Synthesis and Crystallization Behavior of Surfactants with Hexamolybdate as the Polar Headgroup.
Zhu, Li; Chen, Kun; Hao, Jian; Wei, Zheyu; Zhang, Haocheng; Yin, Panchao; Wei, Yongge; Inorganic chemistry 54 (2015) 6075–6077; doi:10.1021/acs.inorgchem.5b00903

data_4343326
_publ_section_title
;
 Synthesis and Crystallization Behavior of Surfactants with Hexamolybdate
 as the Polar Headgroup.
;
_journal_issue                   13
_journal_name_full               'Inorganic chemistry'
_journal_page_first              6075
_journal_page_last               6077
_journal_paper_doi               10.1021/acs.inorgchem.5b00903
_journal_volume                  54
_journal_year                    2015
_chemical_formula_sum            'C52 H105 Mo6 N3 O22'
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_space_group_name_Hall           '-P 2ybc'
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_symmetry_space_group_name_H-M   'P 1 21/c 1'
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_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      296(2)
_diffrn_detector_area_resol_mean 28.5714
_diffrn_measured_fraction_theta_full 0.984
_diffrn_measured_fraction_theta_max 0.984
_diffrn_measurement_device_type  'Saturn724+ (4x4 bin mode)'
_diffrn_measurement_method       dtprofit.ref
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_diffrn_reflns_av_R_equivalents  0.0571
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_diffrn_reflns_point_group_measured_fraction_full 0.984
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_diffrn_reflns_theta_max         25.000
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_diffrn_source                   'Rotating Anode'
_exptl_absorpt_coefficient_mu    1.106
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_exptl_absorpt_correction_T_min  0.594
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    1.607
_exptl_crystal_description       block
_exptl_crystal_F_000             3464
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_exptl_crystal_size_mid          0.400
_exptl_crystal_size_min          0.300
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_refine_ls_extinction_method     none
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0536P)^2^+91.2856P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.1814
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_reflns_number_gt                9991
_reflns_number_total             12188
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            ic5b00903_si_002.cif
_cod_data_source_block           C6
_cod_depositor_comments
'Adding full bibliography for 4343325--4343327.cif.'
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_shelx_res_checksum              51117
_shelx_hkl_checksum              2250