Leveraging cascade annulation of 2-alkynylcyclopropanes with substituted azides to access fused N-heterocyclic scaffolds
Saikia, Anil Kumar; Arandhara, Pallav Jyoti; Chutia, Archana; Chemical Communications  (2025) –; doi:10.1039/D5CC04317D

data_7135165
_publ_section_title
;
 Leveraging cascade annulation of 2-alkynylcyclopropanes with substituted
 azides to access fused N-heterocyclic scaffolds
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/D5CC04317D
_journal_year                    2025
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_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2025-05-18 deposited with the CCDC.	2025-11-10 downloaded from the CCDC.
;
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_cell_measurement_temperature    295(2)
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_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_diffrn_ambient_temperature      295(2)
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_diffrn_radiation_type           MoK\a
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_diffrn_reflns_av_unetI/netI     0.0242
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_diffrn_reflns_limit_k_max       13
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_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_database_code               7135165
_shelx_shelxl_version_number     2018/3
_shelx_res_checksum              8900