Unusual seeding effect in the liquid-assisted high-pressure polymorphism of chlorpropamide
Zakharov, B. A.; Goryainov, S. V.; Boldyreva, E. V.; CrystEngComm 18 (2016) 5423–; doi:10.1039/C6CE00711B

data_7225442
_publ_section_title
;
 Unusual seeding effect in the liquid-assisted high-pressure polymorphism
 of chlorpropamide
;
_journal_issue                   29
_journal_name_full               CrystEngComm
_journal_page_first              5423
_journal_paper_doi               10.1039/C6CE00711B
_journal_volume                  18
_journal_year                    2016
_chemical_absolute_configuration unk
_chemical_formula_sum            'C10 H13 Cl N2 O3 S'
_chemical_formula_weight         276.73
_chemical_name_common            chlorpropamide
_chemical_name_systematic
;
 4-chloro-N-((propylaminocarbonyl)benzenesulfonamide
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           4
_space_group_name_Hall           'P 2yb'
_space_group_name_H-M_alt        'P 1 21 1'
_symmetry_space_group_name_Hall  'P 2yb'
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_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2015-11-18 deposited with the CCDC.
2016-06-06 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_cell_measurement_reflns_used    182
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      21.5690
_cell_measurement_theta_min      3.2890
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_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET)
(compiled Aug 13 2014,18:06:01)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET)
(compiled Aug 13 2014,18:06:01)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET)
(compiled Aug 13 2014,18:06:01)
;
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      293(2)
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_diffrn_measured_fraction_theta_max 0.619
_diffrn_measurement_device_type
;
one-circle diffractometer
;
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_diffrn_reflns_Laue_measured_fraction_full 0.619
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_diffrn_reflns_limit_h_min       -1
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_diffrn_reflns_theta_max         25.639
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_diffrn_source                   synchrotron
_exptl_absorpt_coefficient_mu    0.455
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.422
_exptl_crystal_description       needle
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_refine_ls_R_factor_all          0.1033
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_refine_ls_shift/su_mean         0.000
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'w=1/[\s^2^(Fo^2^)+(0.1121P)^2^+0.0453P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.2044
_reflns_number_gt                480
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c6ce00711b4.cif
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_cod_depositor_comments          'Adding full bibliography for 7225442.cif.'
_cod_original_cell_volume        646.32(11)
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_shelx_res_checksum              78015