A copper-amidocarboxylate based metal organic macrocycle and framework: synthesis, structure and catalytic activities towards microwave assisted alcohol oxidation and Knoevenagel reactions
Karmakar, Anirban; Soliman, Mohamed M. A.; Alegria, Elisabete C. B. A.; Rúbio, Guilherme M. D. M.; Guedes da Silva, M. Fátima C.; Pombeiro, Armando J. L.; New Journal of Chemistry 43 (2019) 9843–; doi:10.1039/C9NJ02064K

data_7058396
_publ_section_title
;
 A copper-amidocarboxylate based metal organic macrocycle and framework:
 synthesis, structure and catalytic activities towards microwave assisted
 alcohol oxidation and Knoevenagel reactions
;
_journal_issue                   25
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              9843
_journal_paper_doi               10.1039/C9NJ02064K
_journal_volume                  43
_journal_year                    2019
_chemical_formula_sum            'C27 H27 Cu N5 O8'
_chemical_formula_weight         613.07
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2yn'
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_symmetry_space_group_name_Hall  '-P 2yn'
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_atom_sites_solution_hydrogens   mixed
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_audit_update_record
;
2018-10-15 deposited with the CCDC.    2019-05-20 downloaded from the CCDC.
;
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_computing_cell_refinement       'Bruker SAINT'
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_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0459P)^2^+4.5128P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_Friedel_coverage         0.000
_reflns_number_gt                3161
_reflns_number_total             5202
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           2
_cod_depositor_comments
'Adding full bibliography for 7058395--7058396.cif.'
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_shelx_res_checksum              29162
_shelx_fab_checksum              50240