Spacer-Directed Selective Assembly of Copper Square or Hexagon and Ring-Stacks or Coordination Nanotubes.
Wu, Xialu; Ding, Nini; Zhang, Wenhua; Xue, Fei; Hor, T. S. Andy; Inorganic chemistry 54 (2015) 6680–6686; doi:10.1021/ic502552y

data_4343476
_publ_section_title
;
 Spacer-Directed Selective Assembly of Copper Square or Hexagon and
 Ring-Stacks or Coordination Nanotubes.
;
_journal_issue                   14
_journal_name_full               'Inorganic chemistry'
_journal_page_first              6680
_journal_page_last               6686
_journal_paper_doi               10.1021/ic502552y
_journal_volume                  54
_journal_year                    2015
_chemical_formula_moiety         'C120 H120 Cu6 N18 O18, 6(Cl O4), 6(H2 O)'
_chemical_formula_sum            'C120 H132 Cl6 Cu6 N18 O48'
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_space_group_name_Hall           '-R 3'
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_symmetry_space_group_name_Hall  '-R 3'
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;
2015-02-27 # Formatted by publCIF

;
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_diffrn_reflns_point_group_measured_fraction_full 0.995
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_refine_ls_R_factor_all          0.0591
_refine_ls_R_factor_gt           0.0522
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
 w=1/[\s^2^(Fo^2^)+(0.0983P)^2^+26.8924P]
 where P=(Fo^2^+2Fc^2^)/3
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1471
_refine_ls_wR_factor_ref         0.1518
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_reflns_number_gt                5070
_reflns_number_total             6010
_reflns_threshold_expression     'I > 2\s(I)'
_publcif_datablock.id            {809df57c-1251-4297-95c0-68495aa1e469}
_cod_data_source_file            ic502552y_si_005.cif
_cod_data_source_block           CU
_cod_depositor_comments
'Adding full bibliography for 4343476--4343480.cif.'
_cod_original_cell_volume        12320(4)
_cod_database_code               4343476
_shelx_estimated_absorpt_t_min   0.651
_shelx_estimated_absorpt_t_max   0.806
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_shelx_hkl_checksum              97730
_shelx_fab_checksum              30421