TaS3 Nanofibers: Layered Trichalcogenide for High-Performance Electronic and Sensing Devices.
Mayorga-Martinez, Carmen C; Sofer, Zdeněk; Luxa, Jan; Huber, Štěpán; Sedmidubský, David; Brázda, Petr; Palatinus, Lukáš; Mikulics, Martin; Lazar, Petr; Medlín, Rostislav; Pumera, Martin; ACS nano 12 (2018) 464–473; doi:10.1021/acsnano.7b06853

data_4514335
_publ_section_title
;
 TaS3 Nanofibers: Layered Trichalcogenide for High-Performance Electronic
 and Sensing Devices.
;
_journal_issue                   1
_journal_name_full               'ACS nano'
_journal_page_first              464
_journal_page_last               473
_journal_paper_doi               10.1021/acsnano.7b06853
_journal_volume                  12
_journal_year                    2018
_chemical_formula_analytical     'Ta1 S3'
_chemical_formula_moiety         'Ta1 S3'
_chemical_formula_structural     'Ta1 S3'
_chemical_formula_sum            'S3 Ta'
_chemical_formula_weight         277.14
_chemical_name_systematic        'Tantalum trisufide'
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      11
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 110.0
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.52
_cell_length_b                   3.34
_cell_length_c                   14.9
_cell_measurement_temperature    293
_cell_volume                     445.200
_computing_cell_refinement
;
Jana2006 (Petricek et al., 2014).
;
_computing_data_collection
;
PETS (Palatinus, L., 2011).
;
_computing_data_reduction
;
PETS (Palatinus, L., 2011).
;
_computing_structure_refinement
;
Jana2006 (Petricek et al., 2014). Dynamical refinement (Palatinus, L. et al.
 2015).
;
_computing_structure_solution
;
Superflip (Palatinus et al., 2007).
;
_diffrn_ambient_temperature      293
_diffrn_detector                 ';CCD camera Olympus SIS Veleta;'
_diffrn_detector_area_resol_mean 2048.2048
_diffrn_measured_fraction_theta_full 0.68
_diffrn_measured_fraction_theta_max 0.66
_diffrn_measurement_device       ';Transmission electron microscope;'
_diffrn_measurement_device_type  ';Philips CM120;'
_diffrn_measurement_method       PEDT
_diffrn_measurement_specimen_support ';Cu grid with carbon foil;'
_diffrn_radiation_probe          electron
_diffrn_radiation_source         LaB6
_diffrn_radiation_type           electron
_diffrn_radiation_wavelength     0.0335
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       4
_diffrn_reflns_limit_k_min       -4
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            15484
_diffrn_reflns_reduction_process 'data integration with PETS'
_diffrn_reflns_theta_full        0.66
_diffrn_reflns_theta_max         1.34
_diffrn_reflns_theta_min         0.07
_diffrn_source                   'electron microscope'
_diffrn_source_voltage           120
_exptl_absorpt_correction_type   none
_exptl_crystal_density_diffrn    3.1757
_exptl_crystal_description
;
piece of nano-ribbon
;
_exptl_crystal_F_000             726
_exptl_crystal_size_max          0.0003
_exptl_crystal_size_mid          0.0001
_exptl_crystal_size_min          0.00005
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_gt    2.76
_refine_ls_goodness_of_fit_ref   2.10
_refine_ls_number_constraints    0
_refine_ls_number_parameters     147
_refine_ls_number_reflns         4056
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.1358
_refine_ls_R_factor_gt           0.0705
_refine_ls_shift/su_max          0.0000
_refine_ls_shift/su_mean         0.0000
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     ;w=1/(\s^2^(F)+0.0001F^2^);
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.0766
_refine_ls_wR_factor_ref         0.0785
_reflns_number_gt                2250
_reflns_number_total             4056
_reflns_threshold_expression     I>3\s(I)
_cod_data_source_file            nn7b06853_si_003.cif
_cod_data_source_block           I
_cod_depositor_comments
'Adding full bibliography for 4514334--4514335.cif.'
_cod_original_cell_volume        446
_cod_original_formula_sum        'Ta1 S3'
_cod_database_code               4514335