Amidinatogermylene Metal Complexes as Homogeneous Catalysts in Alcoholic Media
Álvarez-Rodríguez, Lucía; Cabeza, Javier A.; Fernández-Colinas, José M.; García-Álvarez, Pablo; Polo, Diego; Organometallics 35 (2016) 2516–; doi:10.1021/acs.organomet.6b00426

data_4086678
_publ_section_title
;
 Amidinatogermylene Metal Complexes as Homogeneous Catalysts in Alcoholic
 Media
;
_journal_issue                   15
_journal_name_full               Organometallics
_journal_page_first              2516
_journal_paper_doi               10.1021/acs.organomet.6b00426
_journal_volume                  35
_journal_year                    2016
_chemical_formula_moiety         'C29 H46 Cl2 Ge N2 Ru'
_chemical_formula_sum            'C29 H46 Cl2 Ge N2 Ru'
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 ?
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET)
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET)
(compiled Aug 13 2014,18:06:01)
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_computing_data_reduction
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET)
(compiled Aug 13 2014,18:06:01)
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_computing_molecular_graphics    'X-SEED (Barbour, 1999)'
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_diffrn_reflns_theta_full        69.000
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_diffrn_source                   'Nova (Cu) X-ray Source'
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET)
(compiled Aug 13 2014,18:06:01)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
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_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.438
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_exptl_crystal_size_mid          0.100
_exptl_crystal_size_min          0.081
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_refine_ls_extinction_method     none
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0453P)^2^+7.4124P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_Friedel_coverage         0.000
_reflns_number_gt                5094
_reflns_number_total             5640
_reflns_threshold_expression     'I > 2\s(I)'
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