One-dimensional nickel(II) coordination polymers of 9-anthracenyl-4'-benzoate and bispyridyl linkers as efficient electrocatalysts for hydrogen and oxygen evolution reactions.
Baig, K. Mohamed Yusuf; Marimuthu, Sundaramoorthy; Maduraiveeran, Govindhan; Kole, Goutam Kumar; Dalton transactions (Cambridge, England : 2003) 54 (2025) 11025–11035; doi:10.1039/d5dt00760g

data_7718970
_publ_section_title
;
 One-dimensional nickel(II) coordination polymers of
 9-anthracenyl-4'-benzoate and bispyridyl linkers as efficient
 electrocatalysts for hydrogen and oxygen evolution reactions.
;
_journal_issue                   28
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              11025
_journal_page_last               11035
_journal_paper_doi               10.1039/d5dt00760g
_journal_volume                  54
_journal_year                    2025
_chemical_formula_sum            'C108 H81 N4 Ni2 O12'
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_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
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_atom_sites_solution_primary     difmap
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_audit_update_record
;
2025-02-18 deposited with the CCDC.	2025-06-13 downloaded from the CCDC.
;
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_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
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_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker D8 Quest diffractometer'
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_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.998
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_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SadAbs 2016/2 (Bruker AXS)'
_exptl_crystal_colour            green
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_exptl_crystal_description       block
_exptl_crystal_F_000             1818
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_exptl_crystal_size_mid          0.308
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_refine_ls_extinction_method     none
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_refine_ls_matrix_type           full
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_refine_ls_number_reflns         15447
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_refine_ls_R_factor_all          0.1025
_refine_ls_R_factor_gt           0.0698
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0908P)^2^+8.2086P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1820
_refine_ls_wR_factor_ref         0.2223
_reflns_Friedel_coverage         0.000
_reflns_number_gt                11457
_reflns_number_total             15447
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d5dt00760g2.cif
_cod_data_source_block           BKYB78L
_cod_depositor_comments
'Adding full bibliography for 7718970--7718972.cif.'
_cod_database_code               7718970
_shelx_shelxl_version_number     2018/3
_shelx_estimated_absorpt_t_min   0.827
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_shelx_res_checksum              46147
_shelx_hkl_checksum              70632