Interesting supergene Pb-rich mineral association from the Rovnost mining field, Jachymov (St. Joachimsthal), Czech Republic
Jiri Sejkora; Jakub Plasil; Ivana Cisarova; Radek Skoda; Jan Hlousek; Frantisek Veselovsky; Ivana Jebava; Journal of GeoSciences 56 (2011) 257–271; doi:10.3190/jgeosci.100

data_1566330
_publ_section_title
;
 Interesting supergene Pb-rich mineral association from the Rovnost mining
 field, Jachymov (St. Joachimsthal), Czech Republic
;
_journal_name_full               'Journal of GeoSciences'
_journal_page_first              257
_journal_page_last               271
_journal_paper_doi               10.3190/jgeosci.100
_journal_volume                  56
_journal_year                    2011
_chemical_absolute_configuration .
_chemical_formula_sum            'As3 Cl O12 Pb5 Si0'
_chemical_formula_weight         1488.2
_space_group_IT_number           176
_space_group_name_Hall           '-P 6c'
_space_group_name_H-M_alt        'P 63/m'
_symmetry_cell_setting           hexagonal
_symmetry_space_group_name_Hall  '-P 6c'
_symmetry_space_group_name_H-M   'P 63/m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120.000
_cell_formula_units_Z            2
_cell_length_a                   10.237
_cell_length_b                   10.237
_cell_length_c                   7.426
_cell_measurement_temperature    293
_cell_volume                     673.955
_computing_cell_refinement       unknown
_computing_data_collection       unknown
_computing_data_reduction        unknown
_computing_molecular_graphics    unknown
_computing_structure_solution    unknown
_diffrn_ambient_temperature      293
_diffrn_measured_fraction_theta_full 0.99
_diffrn_measured_fraction_theta_max 0.99
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.2248
_diffrn_reflns_av_sigmaI/netI    0.0285
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       8
_diffrn_reflns_limit_l_min       -8
_diffrn_reflns_number            13490
_diffrn_reflns_theta_full        24.04
_diffrn_reflns_theta_max         24.04
_diffrn_reflns_theta_min         3.58
_exptl_absorpt_coefficient_mu    69.805
_exptl_crystal_density_diffrn    7.3309
_exptl_crystal_F_000             1244
_refine_diff_density_max         2.93
_refine_diff_density_min         -3.09
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_gt    2.50
_refine_ls_goodness_of_fit_ref   2.25
_refine_ls_number_constraints    0
_refine_ls_number_parameters     35
_refine_ls_number_reflns         390
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0646
_refine_ls_R_factor_gt           0.0381
_refine_ls_shift/su_max          0.0364
_refine_ls_shift/su_mean         0.0105
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     w=1/(\s^2^(I)+0.0004I^2^)
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.0866
_refine_ls_wR_factor_ref         0.0916
_reflns_number_gt                292
_reflns_number_total             390
_reflns_threshold_expression     I>3\s(I)
_cod_data_source_file            jgeosci.100_2011_3_sejkora_supplement.cif
_cod_data_source_block           I
_cod_original_cell_volume        673.9545
_cod_original_formula_sum        'As3 Cl1 O12 Pb5 Si0'
_cod_database_code               1566330