[NO3[symbol: see text]{(en)Pt(2,2'-bpz)}3]NO3(SO4)2: snapshot of nitrate insertion into a cationic Pt3 metallacycle or simply a packing effect?
Galstyan, Anzhela; Sanz Miguel, Pablo J.; Lippert, Bernhard; Dalton transactions (Cambridge, England : 2003) 39 (2010) 6386–6388; doi:10.1039/C0DT00463D

data_7026487
_publ_section_title
;
 [NO3[symbol: see text]{(en)Pt(2,2'-bpz)}3]NO3(SO4)2: snapshot of nitrate
 insertion into a cationic Pt3 metallacycle or simply a packing effect?
;
_journal_issue                   28
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              6386
_journal_page_last               6388
_journal_paper_doi               10.1039/C0DT00463D
_journal_volume                  39
_journal_year                    2010
_chemical_formula_moiety         'C30 H42 N18 Pt3, 2(O4 S), 2(N O3), 13(H2 O)'
_chemical_formula_sum            'C30 H68 N20 O27 Pt3 S2'
_chemical_formula_weight         1790.43
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             2010-05-26T14:38:51-00:00
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                71.621(3)
_cell_angle_beta                 73.280(3)
_cell_angle_gamma                72.520(3)
_cell_formula_units_Z            2
_cell_length_a                   12.9984(4)
_cell_length_b                   14.1428(4)
_cell_length_c                   17.2839(5)
_cell_measurement_reflns_used    13792
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      29.342
_cell_measurement_theta_min      2.2397
_cell_volume                     2809.92(16)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.989
_diffrn_measured_fraction_theta_max 0.793
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0443
_diffrn_reflns_av_unetI/netI     0.0592
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            22029
_diffrn_reflns_theta_full        25
_diffrn_reflns_theta_max         29.37
_diffrn_reflns_theta_min         2.25
_exptl_absorpt_coefficient_mu    7.624
_exptl_absorpt_correction_T_max  0.683
_exptl_absorpt_correction_T_min  0.208
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    2.116
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plates
_exptl_crystal_F_000             1740
_exptl_crystal_size_max          0.3
_exptl_crystal_size_mid          0.2
_exptl_crystal_size_min          0.05
_refine_diff_density_max         3.071
_refine_diff_density_min         -2.066
_refine_diff_density_rms         0.265
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.995
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     710
_refine_ls_number_reflns         12267
_refine_ls_number_restraints     12
_refine_ls_restrained_S_all      0.997
_refine_ls_R_factor_all          0.0604
_refine_ls_R_factor_gt           0.0482
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0874P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1263
_refine_ls_wR_factor_ref         0.1296
_reflns_number_gt                9556
_reflns_number_total             12267
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c0dt00463d.txt
_cod_data_source_block           1
_cod_original_cell_volume        2809.94(15)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7026487