A study on the synthesis, pair distribution function and diverse properties of cobalt doped ZnS nanowires
Gawai, U. P.; Khawal, H. A.; Shripathi, T.; Dole, B. N.; CrystEngComm 18 (2016) 1439–; doi:10.1039/C5CE02253C

data_7223926
_publ_section_title
;
 A study on the synthesis, pair distribution function and diverse
 properties of cobalt doped ZnS nanowires
;
_journal_issue                   8
_journal_name_full               CrystEngComm
_journal_page_first              1439
_journal_paper_doi               10.1039/C5CE02253C
_journal_volume                  18
_journal_year                    2016
_chemical_formula_sum            'C28 H28 Cu2 Dy N5 O20'
_chemical_formula_weight         1044.14
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_audit_update_record
;
2003-08-19 deposited with the CCDC.
2016-01-15 downloaded from the CCDC.
;
_cell_angle_alpha                94.881(4)
_cell_angle_beta                 102.916(3)
_cell_angle_gamma                101.498(3)
_cell_formula_units_Z            2
_cell_length_a                   9.6720(9)
_cell_length_b                   13.729(1)
_cell_length_c                   13.997(1)
_cell_measurement_reflns_used    5545
_cell_measurement_temperature    183.1
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      3.0
_cell_volume                     1758.8(2)
_computing_cell_refinement       CRYSTALCLEAR
_computing_data_collection       CRYSTALCLEAR
_computing_data_reduction        'teXsan Ver. 1.11'
_computing_publication_material  'teXsan Ver. 1.11'
_computing_structure_refinement  'teXsan Ver. 1.10'
_computing_structure_solution    SAPI91
_diffrn_detector_area_resol_mean 14.62
_diffrn_measured_fraction_theta_full 0.9620
_diffrn_measured_fraction_theta_max 0.9620
_diffrn_measurement_device_type  'Rigaku/MSC Mercury CCD'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.036
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            13964
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_exptl_absorpt_coefficient_mu    3.397
_exptl_absorpt_correction_T_max  0.712
_exptl_absorpt_correction_T_min  0.712
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            Green
_exptl_crystal_density_diffrn    1.971
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Platelet
_exptl_crystal_size_max          0.340
_exptl_crystal_size_mid          0.230
_exptl_crystal_size_min          0.100
_refine_diff_density_max         1.30
_refine_diff_density_min         -1.08
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.001
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     514
_refine_ls_number_reflns         7716
_refine_ls_R_factor_gt           0.0321
_refine_ls_shift/su_max          0.0008
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^) + (0.06500(Max(Fo^2^,0) + 2Fc^2^)/3)^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.0957
_reflns_number_gt                6950
_reflns_number_total             7716
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
_cod_data_source_file            c5ce02253c2.cif
_cod_data_source_block           '_Cu2Dy(9")'
_cod_depositor_comments          'Adding full bibliography for 7223926.cif.'
_cod_original_cell_volume        1758.8148
_cod_original_sg_symbol_H-M      'P -1         '
_cod_original_formula_sum        'C28 H28 Cu2 Dy N5 O20 '
_cod_database_code               7223926
_audit_block_doi                 10.5517/cc79m26