Crystal chemistry of layered structures formed by linear rigid silyl-capped molecules.
Lumpi, Daniel; Kautny, Paul; Stöger, Berthold; Fröhlich, Johannes; IUCrJ 2 (2015) 584–600; doi:10.1107/S2052252515011665

data_1556741
_publ_section_title
;
 Crystal chemistry of layered structures formed by linear rigid
 silyl-capped molecules.
;
_journal_issue                   'Pt 5'
_journal_name_full               IUCrJ
_journal_page_first              584
_journal_page_last               600
_journal_paper_doi               10.1107/S2052252515011665
_journal_volume                  2
_journal_year                    2015
_chemical_formula_sum            'C22 H32 O2 S3 Si2'
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_space_group_name_H-M_alt        'C 1 2/c 1'
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_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
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_diffrn_measured_fraction_theta_full 0.99
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_diffrn_measurement_device       'four-circle diffractometer'
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_diffrn_measurement_method       '\w- and \f-scans'
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_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_type           'Mo K\a'
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_diffrn_reflns_av_sigmaI/netI    0.0185
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_diffrn_reflns_limit_h_min       -44
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_diffrn_reflns_theta_max         27.61
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_exptl_absorpt_coefficient_mu    0.369
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_exptl_absorpt_correction_T_min  0.74
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            'clear yellow'
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_exptl_crystal_description       'rhombic prism'
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_refine_ls_shift/su_max          0.0303
_refine_ls_shift/su_mean         0.0010
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w=1/(\s^2^(F)+0.0001F^2^)
_refine_ls_weighting_scheme      sigma
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_refine_ls_wR_factor_ref         0.0588
_reflns_number_gt                4903
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_publcif_datablock.id            {d6b6d973-fc2a-4196-8550-5f6f0e7a4ba6}
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_cod_depositor_comments
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The following automatic conversions were performed:

data item '_diffrn_radiation_probe' value 'X-ray' was changed to
'x-ray' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/IUCr/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas 
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_cod_database_code               1556741