Supramolecular insulating networks sheathing conducting nanowires based on organic radical cations.
Yamamoto, Hiroshi M.; Kosaka, Yosuke; Maeda, Ryoko; Yamaura, Jun-ichi; Nakao, Akiko; Nakamura, Toshikazu; Kato, Reizo; ACS nano 2 (2008) 143–155; doi:10.1021/nn700035t

data_4503884
_publ_section_title
;
 Supramolecular insulating networks sheathing conducting nanowires based
 on organic radical cations.
;
_journal_issue                   1
_journal_name_full               'ACS nano'
_journal_page_first              143
_journal_page_last               155
_journal_paper_doi               10.1021/nn700035t
_journal_volume                  2
_journal_year                    2008
_chemical_formula_moiety         '2(C6 H6 Se2), 3(C I2), Cl '
_chemical_formula_sum            'C15 H12 Cl I6 Se4'
_chemical_formula_weight         1304.98
_space_group_IT_number           55
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      55
_symmetry_space_group_name_Hall  '-P 2 2ab'
_symmetry_space_group_name_H-M   'P b a m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   14.322(1)
_cell_length_b                   22.811(2)
_cell_length_c                   7.9230(7)
_cell_measurement_temperature    293
_cell_volume                     2588.4(4)
_computing_data_reduction        'teXsan Ver. 2.0'
_computing_publication_material  'teXsan Ver. 2.0'
_computing_structure_refinement  'teXsan Ver. 2.0'
_computing_structure_solution    SHELXS97
_diffrn_measured_fraction_theta_full 1.0038
_diffrn_measured_fraction_theta_max 1.0038
_diffrn_measurement_device_type  'RIGAKU AFC6S'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.041
_diffrn_reflns_limit_h_max       0
_diffrn_reflns_limit_h_min       -23
_diffrn_reflns_limit_k_max       36
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            6568
_diffrn_reflns_theta_full        34.99
_diffrn_reflns_theta_max         34.99
_exptl_absorpt_coefficient_mu    12.94
_exptl_absorpt_correction_T_max  0.999
_exptl_absorpt_correction_T_min  0.736
_exptl_absorpt_correction_type   psi-scan
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    3.348
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2292.00
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.200
_refine_diff_density_max         3.80
_refine_diff_density_min         -4.20
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.468
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     0
_refine_ls_number_reflns         2130
_refine_ls_R_factor_gt           0.0636
_refine_ls_shift/su_max          0.0000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^) + (0.05000(Max(Fo^2^,0) + 2Fc^2^)/3)^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1580
_reflns_number_gt                2130
_reflns_number_total             6251
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
_cod_data_source_file            nn700035t-file024.cif
_cod_data_source_block           (HMTSF)2Cl.TIE
_cod_original_sg_symbol_H-M      'P b a m      '
_cod_original_formula_sum        'C15 H12 Cl I6 Se4 '
_cod_database_code               4503884