Assembly of discrete and oligomeric structures of organotin double-decker silsesquioxanes: inherent stability studies
Loganathan, Pushparaj; Pillai, Renjith S.; Jeevananthan, Velusamy; David, Ezhumalai; Palanisami, Nallasamy; Bhuvanesh, Nattamai S. P.; Shanmugan, Swaminathan; New Journal of Chemistry 45 (2021) 20144–20154; doi:10.1039/D1NJ03128G

data_7060974
_publ_section_title
;
 Assembly of discrete and oligomeric structures of organotin double-decker
 silsesquioxanes: inherent stability studies
;
_journal_issue                   43
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              20144
_journal_page_last               20154
_journal_paper_doi               10.1039/D1NJ03128G
_journal_volume                  45
_journal_year                    2021
_chemical_formula_moiety         'C32 H38 O7 Si4 Sn'
_chemical_formula_sum            'C32 H38 O7 Si4 Sn'
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_audit_update_record
;
2021-09-25 deposited with the CCDC.	2021-09-29 downloaded from the CCDC.
;
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'ORTEP3 (Farrugia, 1997) and Mercury (Bruno et al., 2002)'
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_diffrn_measured_fraction_theta_full 0.987
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type  'Bruker axs kappa apex2 CCD Diffractometer'
_diffrn_measurement_method       '\w and \f scan'
_diffrn_radiation_type           MoK\a
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_refine_ls_matrix_type           full
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_refine_ls_R_factor_all          0.0666
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_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0876P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.1430
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_reflns_number_gt                4914
_reflns_number_total             6322
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7060973--7060974.cif.'
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