Cyclopalladation of a ferrocene acylphosphine and the reactivity of the C-H activated products.
Vosáhlo, Petr; Schulz, Jiří; Císařová, Ivana; Štěpnička, Petr; Dalton transactions (Cambridge, England : 2003) 50 (2021) 6232–6244; doi:10.1039/d1dt00668a

data_7706943
_publ_section_title
;
 Cyclopalladation of a ferrocene acylphosphine and the reactivity of the
 C-H activated products.
;
_journal_issue                   18
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              6232
_journal_page_last               6244
_journal_paper_doi               10.1039/d1dt00668a
_journal_volume                  50
_journal_year                    2021
_chemical_formula_moiety         'C30 H28 Cl Fe N2 O P Pd'
_chemical_formula_sum            'C30 H28 Cl Fe N2 O P Pd'
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_audit_update_record
;
2021-02-17 deposited with the CCDC.	2021-03-23 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_cell_measurement_temperature    150(2)
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_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_monochromator  'Quazar Mo multilayer optic'
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_exptl_absorpt_process_details   'SADABS-2016/2 - Bruker AXS'
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_refine_ls_number_reflns         5974
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_refine_ls_R_factor_all          0.0240
_refine_ls_R_factor_gt           0.0232
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0285P)^2^+2.5565P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                5772
_reflns_number_total             5974
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           pv440
_cod_depositor_comments
'Adding full bibliography for 7706929--7706948.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7706943
_shelx_shelxl_version_number     2017/1
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