Effective Disruption of Phosphoprotein-Protein Surface Interaction Using Zn(II) Dipicolylamine-Based Artificial Receptors via Two-Point Interaction
Akio Ojida; Masa-aki Inoue; Yasuko Mito-oka; Hiroshi Tsutsumi; Kazuki Sada; Itaru Hamachi; Journal of the American Chemical Society 128 (2006) 2052–2058; doi:10.1021/ja056585k

data_4110411
_publ_section_title
;
 Effective Disruption of Phosphoprotein-Protein Surface Interaction Using
 Zn(II) Dipicolylamine-Based Artificial Receptors via Two-Point
 Interaction
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              2052
_journal_page_last               2058
_journal_paper_doi               10.1021/ja056585k
_journal_volume                  128
_journal_year                    2006
_chemical_formula_sum            'C42 H46 Cl4 N6 O Zn2'
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_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
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_cell_angle_gamma                90
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_cell_length_c                   24.167(2)
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_cell_measurement_temperature    123.2
_cell_measurement_theta_max      68.1
_cell_measurement_theta_min      3.3
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_computing_cell_refinement       PROCESS-AUTO
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_computing_publication_material  'teXsan Ver. 1.10'
_computing_structure_refinement  'teXsan Ver. 1.10'
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_diffrn_measured_fraction_theta_full 0.9550
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_diffrn_measurement_device_type  'Rigaku RAXIS-RAPID Imaging Plate'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Cu K\a'
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_diffrn_reflns_av_R_equivalents  0.093
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       0
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_diffrn_reflns_limit_k_min       0
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_diffrn_reflns_theta_max         68.25
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_exptl_absorpt_correction_T_max  0.810
_exptl_absorpt_correction_T_min  0.297
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(Higashi, 1995)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.565
_exptl_crystal_description       platelet
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_exptl_crystal_size_min          0.050
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^) + (0.05700(Max(Fo^2^,0) + 2Fc^2^)/3)^2^]'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     F^2^>2.0\s(F^2^)
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_cod_data_source_block           Inoue
_cod_original_cell_volume        4088.2(7)
_cod_original_formula_sum        'C42 H46 Cl4 N6 O Zn2 '
_cod_database_code               4110411