Synthesis, Characterization, and Reactivity of Arylpalladium Cyanoalkyl Complexes: Selection of Catalysts for the α-Arylation of Nitriles
Darcy A. Culkin; John F. Hartwig; Journal of the American Chemical Society 124 (2002) 9330–9331; doi:10.1021/ja026584h

data_4115034
_publ_section_title
;
 Synthesis, Characterization, and Reactivity of Arylpalladium Cyanoalkyl
 Complexes: Selection of Catalysts for the \a-Arylation of Nitriles
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              9330
_journal_page_last               9331
_journal_paper_doi               10.1021/ja026584h
_journal_volume                  124
_journal_year                    2002
_chemical_formula_sum            'C55 H53 N P2 Pd'
_chemical_formula_weight         896.38
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_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_audit_creation_date             'Fri Dec  1 10:24:00 2001'
_audit_creation_method           'from TEXRAY.INF file'
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_cell_angle_beta                 108.412(1)
_cell_angle_gamma                62.816(1)
_cell_formula_units_Z            2
_cell_length_a                   15.452(1)
_cell_length_b                   16.887(1)
_cell_length_c                   10.5491(3)
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_cell_measurement_theta_max      0.0
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_computing_data_reduction        teXsan
_computing_publication_material  teXsan
_computing_structure_refinement  teXsan
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_diffrn_measurement_device       unknown
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_diffrn_orient_matrix_UB_11      0.00000
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_diffrn_orient_matrix_UB_33      0.00000
_diffrn_radiation_monochromator  graphite
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_diffrn_standards_decay_%        0.00
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_exptl_absorpt_correction_type   none
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_exptl_crystal_description       prism
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_refine_ls_structure_factor_coef F
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_reflns_observed_criterion       5.00
_cod_data_source_file            ja026584h_s2_1.cif
_cod_data_source_block           X-ray_data_for_4.
_cod_original_sg_symbol_H-M      'P -1       '
_cod_original_formula_sum        'C55 H53 N P2 Pd '
_cod_database_code               4115034