Reductive Coupling of Metal Triangles in Sandwich Complexes
Tetsuro Murahashi; Yasuhiro Hashimoto; Koji Chiyoda; Mayu Fujimoto; Tomohito Uemura; Ryou Inoue; Sensuke Ogoshi; Hideo Kurosawa; Journal of the American Chemical Society 130 (2008) 8586–8587; doi:10.1021/ja802624p

data_4107987
_publ_section_title
;
 Reductive Coupling of Metal Triangles in Sandwich Complexes
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              8586
_journal_page_last               8587
_journal_paper_doi               10.1021/ja802624p
_journal_volume                  130
_journal_year                    2008
_chemical_formula_moiety         'C38 H43 B2 F8 N5 Pd6 '
_chemical_formula_sum            'C38 H43 B2 F8 N5 Pd6'
_chemical_formula_weight         1381.80
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_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
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_cell_angle_beta                 77.0220(13)
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_cell_length_b                   13.8401(6)
_cell_length_c                   14.3530(6)
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_cell_measurement_temperature    123.1
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      3.0
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_computing_cell_refinement       PROCESS-AUTO
_computing_data_collection       PROCESS-AUTO
_computing_data_reduction        CrystalStructure
_computing_publication_material  'CrystalStructure 3.8'
_computing_structure_refinement  CRYSTALS
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_diffrn_radiation_type           'Mo K\a'
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_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       17
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_diffrn_reflns_theta_full        27.46
_diffrn_reflns_theta_max         27.46
_exptl_absorpt_coefficient_mu    2.597
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    2.193
_exptl_crystal_description       block
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_exptl_crystal_size_mid          0.80
_exptl_crystal_size_min          0.60
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_refine_diff_density_min         -3.05
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_refine_ls_R_factor_gt           0.0720
_refine_ls_shift/su_max          0.0000
_refine_ls_structure_factor_coef F
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_reflns_threshold_expression     F^2^>2.0\s(F^2^)
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_cod_data_source_block           '_hashimoto'
_cod_original_cell_volume        2092.18(14)
_cod_original_formula_sum        'C38 H43 B2 F8 N5 Pd6 '
_cod_database_code               4107987