The Solid Solution Series (GeTe)x(LiSbTe2)2 (1 <=x<= 11) and the Thermoelectric Properties of (GeTe)11(LiSbTe2)2
Thorsten Schröder; Stefan Schwarzmüller; Christian Stiewe; Johannes de Boor; Markus Hölzel; Oliver Oeckler; Inorganic Chemistry 52 (2013) 11288–11294; doi:10.1021/ic401516m

data_4336234
_publ_contact_author_address
;
Institut f\"ur Mineralogie, Kristallographie und Materialwissenschaft
Universit\"at Leipzig
Scharnhorststr. 20
04275 Leipzig, Germany
;
_publ_contact_author_email       oliver.oeckler@gmx.de
_publ_contact_author_fax         +49/341/97-36299
_publ_contact_author_name
;
Prof. Dr. Oliver Oeckler
;
_publ_contact_author_phone       +49/341/97-36251
_publ_section_title
;
 The Solid Solution Series (GeTe)x(LiSbTe2)2 (1 <=x<= 11) and the
 Thermoelectric Properties of (GeTe)11(LiSbTe2)2
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              11288
_journal_page_last               11294
_journal_paper_doi               10.1021/ic401516m
_journal_volume                  52
_journal_year                    2013
_chemical_formula_moiety         'Ge0.429 Li0.286 Sb0.286 Te'
_chemical_formula_sum            'Ge0.429 Li0.286 Sb0.286 Te'
_chemical_formula_weight         195.5
_chemical_name_common            'germanium lithium antimony telluride'
_chemical_name_systematic
; 
germanium lithium antimony telluride
;
_space_group_IT_number           225
_symmetry_cell_setting           cubic
_symmetry_Int_Tables_number      225
_symmetry_space_group_name_Hall  '-F 4 2 3'
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_audit_creation_method           'TOPAS ACADEMIC 4.1 + PLATON'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   6.03207(6)
_cell_length_b                   6.03207(6)
_cell_length_c                   6.03207(6)
_cell_measurement_temperature    293(2)
_cell_volume                     219.482(4)
_computing_molecular_graphics    'Diamond 3.1b'
_computing_publication_material  'TOPAS ACADEMIC 4.1'
_computing_structure_refinement  'TOPAS ACADEMIC 4.1'
_computing_structure_solution    model
_diffrn_ambient_temperature      293(2)
_diffrn_measurement_device_type  'Huber G670'
_diffrn_radiation_monochromator  Ge-111
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Cu K\a~1~'
_diffrn_radiation_wavelength     1.54051
_exptl_absorpt_coefficient_mu    136.71
_exptl_absorpt_correction_type   none
_exptl_absorpt_process_details
;
none
;
_exptl_crystal_density_diffrn    5.914
_exptl_crystal_F_000             324.4
_pd_calc_method                  'Rietveld Refinement'
_pd_char_colour                  metallic_light_grey
_pd_char_particle_morphology     powder
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_pd_proc_ls_prof_wR_factor       0.03589
_pd_proc_number_of_points        15601
_refine_ls_goodness_of_fit_all   1.375
_refine_ls_matrix_type           full
_refine_ls_number_constraints    4
_refine_ls_number_parameters     29
_refine_ls_number_restraints     0
_refine_ls_R_Fsqd_factor         0.03465
_refine_ls_shift/su_max          0.00
_refine_ls_shift/su_mean         0.00
_reflns_d_resolution_high        3.48262
_reflns_d_resolution_low         1.00535
_reflns_limit_h_max              5
_reflns_limit_h_min              0
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_reflns_limit_k_min              0
_reflns_limit_l_max              6
_reflns_limit_l_min              1
_reflns_number_total             15
_cod_data_source_file            ic401516m_si_005.cif
_cod_data_source_block           TSSS67
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_cod_database_code               4336234
_pd_proc_ls_prof_r_expected      0.02611