Thiophene-substituted nickel dithiolene complexes. Precursors for low band gap conjugated metallopolymers
Kean, Christopher L.; Miller, David O.; Pickup, Peter G.; Journal of Materials Chemistry 12 (2002) 2949–; doi:10.1039/b204090e

data_7204439
_publ_section_title
;
 Thiophene-substituted nickel dithiolene complexes. Precursors for low
 band gap conjugated metallopolymers
;
_journal_issue                   10
_journal_name_full               'Journal of Materials Chemistry'
_journal_page_first              2949
_journal_paper_doi               10.1039/b204090e
_journal_volume                  12
_journal_year                    2002
_chemical_formula_sum            'C42 H48 N1.5 Ni1.5 S12'
_chemical_formula_weight         1046.62
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_symmetry_cell_setting           triclinic
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_symmetry_space_group_name_Hall  '-P 1'
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;
?
;
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_cell_length_a                   14.522(2)
_cell_length_b                   19.507(2)
_cell_length_c                   8.667(1)
_cell_measurement_reflns_used    22
_cell_measurement_temperature    299.2
_cell_measurement_theta_max      15.8
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'teXsan for Windows version 1.06 (MSC, 1997-1999)'
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'teXsan for Windows version 1.06 (MSC, 1997-1999)'
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'teXsan for Windows version 1.06 (MSC, 1997-1999)'
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;
SIR92 (Altomare, et. al. 1994)
;
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_diffrn_radiation_detector       'scintillation counter'
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;
\y scans (North,Phillips & Matthews, 1968)
;
_exptl_crystal_colour            Black
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo) + 0.00001|Fo|^2^]'
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_reflns_threshold_expression     I>2.00\s(I)
_cod_data_source_file            b204090e.txt
_cod_data_source_block           '_CLKb95a'
_cod_original_sg_symbol_H-M      'P -1       '
_cod_original_formula_sum        'C42 H48 N1.50 Ni1.50 S12 '
_cod_database_code               7204439