Novel silver(i) cluster-based coordination polymers as efficient luminescent thermometers
Xue, Zhen-Zhen; Li, Xin-Yu; Xu, Lei; Han, Song-De; Pan, Jie; Wang, Guo-Ming; CrystEngComm 23 (2021) 56–63; doi:10.1039/D0CE01507E

data_7241435
_publ_section_title
;
 Novel silver(i) cluster-based coordination polymers as efficient
 luminescent thermometers
;
_journal_issue                   1
_journal_name_full               CrystEngComm
_journal_page_first              56
_journal_page_last               63
_journal_paper_doi               10.1039/D0CE01507E
_journal_volume                  23
_journal_year                    2021
_chemical_formula_sum            'C19 H11 Ag3 I N9'
_chemical_formula_weight         815.88
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_space_group_name_Hall           '-P 2ybc'
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_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2020-11-05 deposited with the CCDC.	2020-11-10 downloaded from the CCDC.
;
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_cell_angle_gamma                90
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_cell_length_c                   20.839(2)
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_computing_data_collection       'CrysAlisPro 1.171.39.16b (Rigaku OD, 2015)'
_computing_data_reduction        'CrysAlisPro 1.171.39.16b (Rigaku OD, 2015)'
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'XtaLAB Mini (ROW)'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
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_diffrn_reflns_av_unetI/netI     0.0919
_diffrn_reflns_Laue_measured_fraction_full 0.999
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_diffrn_reflns_limit_h_max       17
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_diffrn_reflns_limit_k_min       -8
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_diffrn_reflns_theta_full        25.193
_diffrn_reflns_theta_max         25.193
_diffrn_reflns_theta_min         2.829
_exptl_absorpt_coefficient_mu    4.490
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.74152
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.714
_exptl_crystal_description       strip-shaped
_exptl_crystal_F_000             1528
_exptl_crystal_size_max          0.18
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.15
_refine_diff_density_max         1.550
_refine_diff_density_min         -0.941
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_refine_ls_extinction_method     none
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_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
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_refine_ls_number_reflns         3587
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_refine_ls_restrained_S_all      0.992
_refine_ls_R_factor_all          0.0959
_refine_ls_R_factor_gt           0.0513
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0407P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1049
_refine_ls_wR_factor_ref         0.1334
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2203
_reflns_number_total             3587
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d0ce01507e2.cif
_cod_data_source_block           2
_cod_depositor_comments
'Adding full bibliography for 7241434--7241435.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7241435
_shelx_shelxl_version_number     2014/7
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