Probing Lewis acidity of Y(BH(4))(3)via its reactions with MBH(4) (M = Li, Na, K, NMe(4)).
Jaroń, Tomasz; Grochala, Wojciech; Dalton transactions (Cambridge, England : 2003) 40 (2011) 12808–12817; doi:10.1039/c1dt10955c

data_7017292
_publ_section_title
;
 Probing Lewis acidity of Y(BH(4))(3)via its reactions with MBH(4) (M =
 Li, Na, K, NMe(4)).
;
_journal_issue                   48
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              12808
_journal_page_last               12817
_journal_paper_doi               10.1039/c1dt10955c
_journal_volume                  40
_journal_year                    2011
_chemical_formula_moiety         'B4 H16 Y, C4 H12 N'
_chemical_formula_sum            'C4 H28 B4 N Y'
_chemical_formula_weight         222.42
_chemical_name_systematic        ' ?'
_space_group_IT_number           62
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      62
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   15.0290(10)
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_cell_length_c                   12.0811(7)
_cell_measurement_temperature    298
_cell_volume                     1546.30(17)
_diffrn_ambient_temperature      298
_diffrn_detector                 one-dimensional
_diffrn_detector_type            VANTEC
_diffrn_measurement_device_type  'Bruker D8 Discover'
_diffrn_radiation_monochromator  none
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.5418
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_pd_instr_location               ' ?'
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_pd_meas_2theta_range_min        5.000
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_pd_meas_scan_method             cont
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_pd_proc_2theta_range_inc        0.0183857
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_pd_proc_2theta_range_min        6.011
_pd_proc_ls_background_function  '20 Legendre polynoms'
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_pd_proc_ls_prof_wR_factor       0.0144
_pd_spec_mounting                'quartz capillary'
_pd_spec_mount_mode              transmission
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_refine_ls_hydrogen_treatment    refall
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_refine_ls_shift/su_max          0.0128
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_cod_data_source_file            c1dt10955c.txt
_cod_data_source_block           I
_cod_original_cell_volume        1546.29(17)
_cod_original_sg_symbol_Hall     '-P -2xabc;-2yb;-2zac'
_cod_original_formula_sum        'C4 H28 B4 N1 Y1'
_cod_database_code               7017292