Solvent effect on the structure and topology of metal-organic frameworks with the rigid tripodal star ligand 1,3,5-tris(1-imidazolyl)benzene and lead(ii) nitrateElectronic supplementary information (ESI) available: crystal packing diagram of 1. See http://www.rsc.org/suppdata/nj/b3/b306876p/
Fan, Jian; Shu, Mou-Hai; Okamura, Taka-aki; Li, Yi-Zhi; Sun, Wei-Yin; Tang, Wen-Xia; Ueyama, Norikazu; New Journal of Chemistry 27 (2003) 1307–; doi:10.1039/b306876p

data_7050656
_publ_section_title
;
 Solvent effect on the structure and topology of metal-organic
 frameworks with the rigid tripodal star ligand
 1,3,5-tris(1-imidazolyl)benzene and lead(ii) nitrateElectronic
 supplementary information (ESI) available: crystal packing diagram of
 1. See http://www.rsc.org/suppdata/nj/b3/b306876p/
;
_journal_issue                   9
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              1307
_journal_paper_doi               10.1039/b306876p
_journal_volume                  27
_journal_year                    2003
_chemical_formula_moiety         'C15 H12 N8 O6 Pb '
_chemical_formula_sum            'C15 H12 N8 O6 Pb'
_chemical_formula_weight         607.52
_chemical_name_common            (Pb(tib))(NO3)2
_chemical_name_systematic
;
[Pb(tib)](NO3)2
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                84.345(4)
_cell_angle_beta                 84.226(5)
_cell_angle_gamma                75.040(4)
_cell_formula_units_Z            2
_cell_length_a                   8.6278(6)
_cell_length_b                   9.5870(7)
_cell_length_c                   11.5759(8)
_cell_measurement_reflns_used    2555
_cell_measurement_temperature    200
_cell_measurement_theta_max      27.3
_cell_measurement_theta_min      2.7
_cell_volume                     917.72(11)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-86 (Sheldrick, 1985)'
_diffrn_ambient_temperature      200
_diffrn_detector_area_resol_mean 10.00
_diffrn_measured_fraction_theta_full 0.985
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measurement_device_type  'Rigaku RAXIS-RAPID Imaging Plate'
_diffrn_measurement_method       \w
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0812
_diffrn_reflns_av_sigmaI/netI    0.0753
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            8649
_diffrn_reflns_theta_full        27.38
_diffrn_reflns_theta_max         27.38
_diffrn_reflns_theta_min         2.21
_exptl_absorpt_coefficient_mu    9.247
_exptl_absorpt_correction_T_max  0.757
_exptl_absorpt_correction_T_min  0.433
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(Higashi, 1995)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.198
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             576
_exptl_crystal_size_max          0.150
_exptl_crystal_size_mid          0.100
_exptl_crystal_size_min          0.030
_refine_diff_density_max         2.108
_refine_diff_density_min         -2.832
_refine_diff_density_rms         0.252
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.087
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     271
_refine_ls_number_reflns         4112
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.087
_refine_ls_R_factor_all          0.0606
_refine_ls_R_factor_gt           0.0538
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0827P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1340
_refine_ls_wR_factor_ref         0.1386
_reflns_number_gt                3373
_reflns_number_total             4112
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b306876p.txt
_cod_data_source_block           2
_cod_original_cell_volume        917.73(11)
_cod_original_sg_symbol_H-M      'P -1         '
_cod_database_code               7050656