<i>Pseudo</i>-<i>S</i><sub>6</sub> Complex Cations of a Hexakis-<i>N</i>-methylformamide Nickel(II) Complex
SAKIYAMA, Hiroshi; MITSUHASHI, Ryoji; MIKURIYA, Masahiro; X-ray Structure Analysis Online 31 (2015) 45–; doi:10.2116/xraystruct.31.45

data_1551626
_publ_section_title
;
 &lt;i&gt;Pseudo&lt;/i&gt;-&lt;i&gt;S&lt;/i&gt;&lt;sub&gt;6&lt;/sub&gt;
 Complex Cations of a Hexakis-&lt;i&gt;N&lt;/i&gt;-methylformamide
 Nickel(II) Complex
;
_journal_issue                   0
_journal_name_full               'X-ray Structure Analysis Online'
_journal_page_first              45
_journal_paper_doi               10.2116/xraystruct.31.45
_journal_volume                  31
_journal_year                    2015
_chemical_formula_sum            'C60 H70 B2 N6 Ni O6'
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_cell_length_b                   13.271(3)
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_diffrn_ambient_temperature      90(2)
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.870
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_diffrn_measurement_method       '\p and \w'
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_diffrn_reflns_theta_max         28.647
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_diffrn_source                   'fine-focus sealed tube'
_exptl_absorpt_coefficient_mu    0.401
_exptl_absorpt_correction_T_max  0.924
_exptl_absorpt_correction_T_min  0.906
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_exptl_absorpt_process_details   SADABS
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0343P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_original_cell_volume        2807.0(10)
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