LMucko/crystallography-open-database huggingface dataset:
Screening for Crystalline Salts via Mechanochemistry
W. Jones; Delia A. Haynes; W. Motherwell; Andrew Trask; Chemical Communications  (2006) –; doi:10.1039/b512626f

data_7100655
_publ_section_title
;
Screening for Crystalline Salts via Mechanochemistry
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b512626f
_journal_year                    2006
_chemical_formula_moiety         'C14 H19 N4 O3, 0.5(C4 H4 O4)'
_chemical_formula_sum            'C16 H21 N4 O5'
_chemical_formula_weight         349.37
_chemical_name_common            'trimethoprim succinate'
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 91.95(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   17.343(4)
_cell_length_b                   11.672(2)
_cell_length_c                   16.835(3)
_cell_measurement_temperature    180(2)
_cell_volume                     3405.8(12)
_diffrn_ambient_temperature      180(2)
_exptl_crystal_density_diffrn    1.363
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               7100655
Stabilisation of a paramagnetic dinickel borohydride complex by a macrodinucleating hexaaza-dithiophenolate ligand macrocycles
Berthold Kersting; Julia Hausmann; Yves Journaux; Vasile Lozan; Chemical Communications  (2006) –; doi:10.1039/b512744k

data_7100656
_publ_section_title
;
Stabilisation of a paramagnetic dinickel borohydride complex by a
macrodinucleating hexaaza-dithiophenolate ligand
macrocycles
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b512744k
_journal_year                    2006
_chemical_formula_structural
;
[(L)Ni2(u1,3-BH4)]BPh4(MeCN)2
;
_chemical_formula_sum            'C66 H94 B2 N8 Ni2 S2'
_chemical_formula_weight         1202.65
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                63.82(3)
_cell_angle_beta                 70.97(3)
_cell_angle_gamma                66.47(3)
_cell_formula_units_Z            2
_cell_length_a                   15.992(3)
_cell_length_b                   16.080(3)
_cell_length_c                   16.515(3)
_cell_measurement_temperature    210(2)
_cell_volume                     3435.8(12)
_diffrn_ambient_temperature      210(2)
_exptl_crystal_density_diffrn    1.162
_refine_diff_density_rms         0.113
_cod_database_code               7100656
Stabilisation of a paramagnetic dinickel borohydride complex by a macrodinucleating hexaaza-dithiophenolate ligand macrocycles
Berthold Kersting; Julia Hausmann; Yves Journaux; Vasile Lozan; Chemical Communications  (2006) –; doi:10.1039/b512744k

data_7100657
_publ_section_title
;
Stabilisation of a paramagnetic dinickel borohydride complex by a
macrodinucleating hexaaza-dithiophenolate ligand
macrocycles
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b512744k
_journal_year                    2006
_chemical_formula_structural
;
[(L)Ni2(u-O2CH)]BPh4
;
_chemical_formula_sum            'C63 H85 B N6 Ni2 O2 S2'
_chemical_formula_weight         1150.72
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 92.22(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   18.452(4)
_cell_length_b                   34.531(7)
_cell_length_c                   18.452(4)
_cell_measurement_temperature    210(2)
_cell_volume                     11748(4)
_diffrn_ambient_temperature      210(2)
_exptl_crystal_density_diffrn    1.301
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               7100657
Group 6 metal xantsil complexes with a labile oxygen coordination and insertion of tBuCN into a W-Si bond [xantsil = (9,9-dimethylxantene- 4,5-diyl)bis(dimethylsilyl)]
Rockshana Begum; Takashi Komuro; Hiromi Tobita; Chemical Communications  (2006) –; doi:10.1039/b512759a

data_7100658
_publ_section_title
;
Group 6 metal xantsil complexes with a labile oxygen coordination and
insertion of tBuCN into a W-Si bond [xantsil = (9,9-dimethylxantene-
4,5-diyl)bis(dimethylsilyl)]
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b512759a
_journal_year                    2006
_chemical_formula_sum            'C30 H40 O2 Si2 W'
_chemical_formula_weight         672.65
_space_group_IT_number           29
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      29
_symmetry_space_group_name_Hall  'P 2c -2ac'
_symmetry_space_group_name_H-M   'P c a 21'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   9.5123(3)
_cell_length_b                   18.0026(6)
_cell_length_c                   16.9940(7)
_cell_measurement_temperature    150(2)
_cell_volume                     2910.16(18)
_diffrn_ambient_temperature      150(2)
_exptl_crystal_density_diffrn    1.535
_cod_database_code               7100658
Group 6 metal xantsil complexes with a labile oxygen coordination and insertion of tBuCN into a W-Si bond [xantsil = (9,9-dimethylxantene- 4,5-diyl)bis(dimethylsilyl)]
Rockshana Begum; Takashi Komuro; Hiromi Tobita; Chemical Communications  (2006) –; doi:10.1039/b512759a

data_7100659
_publ_section_title
;
Group 6 metal xantsil complexes with a labile oxygen coordination and
insertion of tBuCN into a W-Si bond [xantsil = (9,9-dimethylxantene-
4,5-diyl)bis(dimethylsilyl)]
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b512759a
_journal_year                    2006
_chemical_formula_sum            'C35 H49 N O2 Si2 W'
_chemical_formula_weight         755.78
_space_group_IT_number           19
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      19
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   11.3139(5)
_cell_length_b                   14.8370(5)
_cell_length_c                   20.5961(7)
_cell_measurement_temperature    150(2)
_cell_volume                     3457.4(2)
_diffrn_ambient_temperature      150(2)
_exptl_crystal_density_diffrn    1.452
_cod_database_code               7100659
; Chemical Communications  (2006) –; doi:10.1039/b512884f

data_7100660
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b512884f
_journal_year                    2006
_chemical_formula_moiety         'C33 H42 Ag Cl6 F6 N8 P'
_chemical_formula_sum            'C33 H42 Ag Cl6 F6 N8 P'
_chemical_formula_weight         1016.29
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                89.293(5)
_cell_angle_beta                 78.318(4)
_cell_angle_gamma                88.874(4)
_cell_formula_units_Z            2
_cell_length_a                   9.550(1)
_cell_length_b                   14.096(2)
_cell_length_c                   16.484(2)
_cell_measurement_temperature    293(2)
_cell_volume                     2172.6(4)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.554
_cod_database_code               7100660
; Chemical Communications  (2006) –; doi:10.1039/b512884f

data_7100661
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b512884f
_journal_year                    2006
_chemical_formula_moiety         'C27 H37 Cl N4 Rh'
_chemical_formula_sum            'C27 H37 Cl N4 Rh'
_chemical_formula_weight         555.97
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                83.42(3)
_cell_angle_beta                 83.12(3)
_cell_angle_gamma                82.76(3)
_cell_formula_units_Z            2
_cell_length_a                   8.273(2)
_cell_length_b                   12.672(3)
_cell_length_c                   13.085(3)
_cell_measurement_temperature    293(2)
_cell_volume                     1344.2(5)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.374
_cod_database_code               7100661
Regioselective and enantiospecific rhodium-catalyzed allylic amination with thymine: synthesis of a new conformationally rigid nucleoside
Evans, P. Andrew; Lai, Kwong Wah; Zhang, Hai-Ren; Huffman, John C.; Chemical Communications  (2006) –; doi:10.1039/b513083b

data_7100662
_publ_section_title
;
Regioselective and enantiospecific rhodium-catalyzed allylic amination with
thymine: synthesis of a new conformationally rigid nucleoside
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b513083b
_journal_year                    2006
_chemical_formula_sum            'C16 H18 N2 O5'
_chemical_formula_weight         318.32
_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 98.717(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   6.2583(7)
_cell_length_b                   7.3007(8)
_cell_length_c                   16.5882(16)
_cell_measurement_temperature    118(2)
_cell_volume                     749.16(14)
_diffrn_ambient_temperature      118(2)
_exptl_crystal_density_diffrn    1.411
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21'
_cod_database_code               7100662
Sterically non Hindering Endocyclic Ligands of the Bi-isoquinoline Family
J. Sauvage; Fabien Durola; Oliver S. Wenger; Chemical Communications  (2006) –; doi:10.1039/b513222c

data_7100663
_publ_section_title
;
Sterically non Hindering Endocyclic Ligands of the
Bi-isoquinoline Family
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b513222c
_journal_year                    2006
_chemical_formula_moiety         'C96 H72 F12 Fe N6 O6 P2'
_chemical_formula_sum            'C96 H72 F12 Fe N6 O6 P2'
_chemical_formula_weight         1751.39
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 116.3621(8)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   15.4180(3)
_cell_length_b                   34.4150(6)
_cell_length_c                   17.0120(4)
_cell_measurement_temperature    173(2)
_cell_volume                     8088.0(3)
_diffrn_ambient_temperature      173(2)
_exptl_crystal_density_diffrn    1.438
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               7100663
poly-N-Methylated ?-Peptides: Synthesis and X-Ray Structure Determination of ?-Strand Forming Foldamers
Per Arvidsson; Palangpon Kongsaeree; Samran Prabpai; Suode Zhang; Chemical Communications  (2006) –; doi:10.1039/b513277k

data_7100664
_publ_section_title
;
poly-N-Methylated ?-Peptides: Synthesis and X-Ray
Structure Determination of ?-Strand Forming Foldamers
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b513277k
_journal_year                    2006
_chemical_absolute_configuration syn
_chemical_formula_moiety         'C20 H37 N5 O6, H2 O'
_chemical_formula_sum            'C20 H39 N5 O7'
_chemical_formula_weight         461.560
_space_group_IT_number           1
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      1
_symmetry_space_group_name_Hall  'P 1'
_symmetry_space_group_name_H-M   'P 1'
_cell_angle_alpha                97.127(4)
_cell_angle_beta                 92.392(6)
_cell_angle_gamma                99.132(6)
_cell_formula_units_Z            1
_cell_length_a                   5.9382(4)
_cell_length_b                   6.7703(7)
_cell_length_c                   15.524(2)
_cell_measurement_temperature    298
_cell_volume                     610.22(10)
_diffrn_ambient_temperature      298
_exptl_crystal_density_diffrn    1.256
_refine_diff_density_rms         0.032
_cod_database_code               7100664
; Chemical Communications  (2006) –; doi:10.1039/b513277k

data_7100665
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b513277k
_journal_year                    2006
_chemical_absolute_configuration syn
_chemical_formula_moiety         'C24 H44 N6 O7, 3(H2 O) '
_chemical_formula_sum            'C24 H50 N6 O10'
_chemical_formula_weight         582.696
_space_group_IT_number           1
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  'P 1'
_symmetry_space_group_name_H-M   'P 1'
_cell_angle_alpha                98.898(3)
_cell_angle_beta                 93.638(4)
_cell_angle_gamma                102.759(4)
_cell_formula_units_Z            1
_cell_length_a                   5.9757(3)
_cell_length_b                   9.9960(8)
_cell_length_c                   13.5831(10)
_cell_measurement_temperature    298
_cell_volume                     777.78(9)
_exptl_crystal_density_diffrn    1.244
_refine_diff_density_rms         0.036
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 1 '
_cod_original_formula_sum        'C24 H50 N6 O10 '
_cod_database_code               7100665
; Chemical Communications  (2006) –; doi:10.1039/b513277k

data_7100666
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b513277k
_journal_year                    2006
_chemical_formula_moiety         'C42 H64 N6 O9 '
_chemical_formula_sum            'C42 H64 N6 O9'
_chemical_formula_weight         797.007
_space_group_IT_number           19
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   6.1923(2)
_cell_length_b                   18.8230(8)
_cell_length_c                   38.868(2)
_cell_measurement_temperature    298
_cell_volume                     4530.4(3)
_exptl_crystal_density_diffrn    1.169
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21 21 21 '
_cod_original_formula_sum        'C42 H64 N6 O9 '
_cod_database_code               7100666
Unusual Carbon-Sulfur Bond Cleavage in the Reaction of a New Type of Bulky Hexathioether with a Zerovalent Palladium Complex
Norihiro Tokitoh; Daisuke Shimizu; Nobuhiro Takeda; Chemical Communications  (2006) –; doi:10.1039/b513339d

data_7100667
_publ_section_title
;
Unusual Carbon-Sulfur Bond Cleavage in the Reaction of
a New Type of Bulky Hexathioether with a Zerovalent Palladium Complex
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b513339d
_journal_year                    2006
_chemical_formula_moiety
'C114 H164 P2 Pd3 S6 Si12, 3.2(C6 H6), 0.8(C1 H1 Cl3)'
_chemical_formula_sum            'C134 H184 Cl2.4 P2 Pd3 S6 Si12'
_chemical_formula_weight         2790.47
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 130.2043(8)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   31.9316(5)
_cell_length_b                   24.7082(6)
_cell_length_c                   24.0157(5)
_cell_measurement_temperature    103(2)
_cell_volume                     14471.3(5)
_diffrn_ambient_temperature      103(2)
_exptl_crystal_density_diffrn    1.281
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_original_formula_sum        'C134 H184 Cl2.40 P2 Pd3 S6 Si12'
_cod_database_code               7100667
Unusual Carbon-Sulfur Bond Cleavage in the Reaction of a New Type of Bulky Hexathioether with a Zerovalent Palladium Complex
Norihiro Tokitoh; Daisuke Shimizu; Nobuhiro Takeda; Chemical Communications  (2006) –; doi:10.1039/b513339d

data_7100668
_publ_section_title
;
Unusual Carbon-Sulfur Bond Cleavage in the Reaction of
a New Type of Bulky Hexathioether with a Zerovalent Palladium Complex
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b513339d
_journal_year                    2006
_chemical_formula_moiety         'C78 H134 S6 Si12, 0.5(C1 H2 Cl2), 0.5(C6 H14)'
_chemical_formula_sum            'C81.5 H142 Cl S6 Si12'
_chemical_formula_weight         1686.84
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                71.290(7)
_cell_angle_beta                 83.335(10)
_cell_angle_gamma                83.675(11)
_cell_formula_units_Z            2
_cell_length_a                   10.920(2)
_cell_length_b                   20.424(5)
_cell_length_c                   23.068(5)
_cell_measurement_temperature    103(2)
_cell_volume                     4825.5(18)
_diffrn_ambient_temperature      103(2)
_exptl_crystal_density_diffrn    1.161
_cod_original_formula_sum        'C81.50 H142 Cl S6 Si12'
_cod_database_code               7100668
From Allene to Allene: A Palladium-Catalyzed Approach to b-Allenyl Butenolides and Their Application to the Synthesis of Polysubstituted Benzene Derivatives
Shengming Ma.; Youqian Deng.; Zhenhua Gu.; Chemical Communications  (2006) –; doi:10.1039/b513371h

data_7100669
_publ_section_title
;
From Allene to Allene: A Palladium-Catalyzed Approach
to b-Allenyl Butenolides and Their Application to the Synthesis of
Polysubstituted Benzene Derivatives
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b513371h
_journal_year                    2006
_chemical_formula_sum            'C16 H16 O2'
_chemical_formula_weight         240.29
_space_group_IT_number           61
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   11.592(2)
_cell_length_b                   14.568(3)
_cell_length_c                   16.342(3)
_cell_measurement_temperature    293(2)
_cell_volume                     2759.7(8)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.157
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Orthorhombic' changed to 'orthorhombic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               7100669
From Allene to Allene: A Palladium-Catalyzed Approach to b-Allenyl Butenolides and Their Application to the Synthesis of Polysubstituted Benzene Derivatives
Shengming Ma.; Youqian Deng.; Zhenhua Gu.; Chemical Communications  (2006) –; doi:10.1039/b513371h

data_7100670
_publ_section_title
;
From Allene to Allene: A Palladium-Catalyzed Approach
to b-Allenyl Butenolides and Their Application to the Synthesis of
Polysubstituted Benzene Derivatives
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b513371h
_journal_year                    2006
_chemical_formula_sum            'C26 H30 O6'
_chemical_formula_weight         438.50
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 99.356(4)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.0344(17)
_cell_length_b                   13.210(2)
_cell_length_c                   18.172(3)
_cell_measurement_temperature    293(2)
_cell_volume                     2376.7(7)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.225
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               7100670
Syntheses and structures of new diaryl lead(II) compounds PbR2 (1, R = 2,4,6-triphenylphenyl; 2, R = 2,6-bis(1'-napthyl)phenyl
G.Robinson; Brandon Quillian; Yuzhong Wang.; Pingrong Wei.; Xiao-Juan Yang.; Chemical Communications  (2006) –; doi:10.1039/b513401c

data_7100671
_publ_section_title
;
Syntheses and structures of new diaryl lead(II)
compounds PbR2 (1, R = 2,4,6-triphenylphenyl; 2, R =
2,6-bis(1'-napthyl)phenyl
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/b513401c
_journal_year                    2006
_chemical_formula_sum            'C52 H34 Pb'
_chemical_formula_weight         865.98
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 100.3270(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   11.4487(9)
_cell_length_b                   16.1126(13)
_cell_length_c                   21.3687(18)
_cell_measurement_temperature    273(2)
_cell_volume                     3878.0(5)
_diffrn_ambient_temperature      273(2)
_exptl_crystal_density_diffrn    1.483
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               7100671