Chlorure de triamminetrichloroplatine(IV) chlorure d'ammonium monohydrate
Balde, L.; Khodadad, P.; Rodier, N.; Julien, R.; Acta Crystallographica Section C 49 (1993) 2064–2065; doi:10.1107/S0108270193005165

data_2001133
_publ_section_title
;
 Chlorure de triamminetrichloroplatine(IV) chlorure d'ammonium
 monohydrate
;
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              2064
_journal_page_last               2065
_journal_paper_doi               10.1107/S0108270193005165
_journal_volume                  49
_journal_year                    1993
_chemical_formula_sum            'Cl5 H15 N4 O Pt'
_chemical_formula_weight         459.5
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.0
_cell_angle_beta                 103.72(3)
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   11.485(3)
_cell_length_b                   6.549(2)
_cell_length_c                   15.774(7)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293
_cell_measurement_theta_max      23.47
_cell_measurement_theta_min      10.03
_cell_volume                     1152.6(7)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \q/2\q
_diffrn_radiation_type           MoK\=\a
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       5
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            1612
_diffrn_reflns_theta_max         27.0
_diffrn_standards_decay_%        1.2
_diffrn_standards_interval_time  120
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    13.44
_exptl_absorpt_correction_T_max  1.62
_exptl_absorpt_correction_T_min  0.56
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            'Jaune tr\`es p\^ale'
_exptl_crystal_density_diffrn    2.648
_exptl_crystal_density_meas      2.60
_exptl_crystal_description       Plaquette
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.06
_refine_diff_density_max         1.9(4)
_refine_diff_density_min         -1.5(4)
_refine_ls_goodness_of_fit_obs   1.87
_refine_ls_number_parameters     100
_refine_ls_number_reflns         1179
_refine_ls_R_factor_obs          0.048
_refine_ls_shift/esd_max         0.01
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w=1/\s^2^(F)
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.057
_reflns_number_observed          1179
_reflns_number_total             1612
_reflns_observed_criterion       I>3\s(I)
_cod_data_source_file            pa1046.cif
_cod_data_source_block           pa1046_structure_1_of_1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' tag value 'empirique' was replaced
with 'empirical' value.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'w=1/\s^2^(F)' was changed to
'calc'. New tag '_refine_ls_weighting_details' was created. The value
of the new tag was set to 'w=1/\s^2^(F)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        1153.0(10)
_cod_original_formula_sum        'H15 Cl5 N4 O Pt'
_cod_database_code               2001133