LMucko/crystallography-open-database huggingface dataset:
Iodine pentafluoride-hydrogen fluoride co-crystallisates, directed weak interactions
Mahjoub, A.R.; Leopold, D.; Seppelt, K.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 635–647; doi:

data_4030433
_publ_section_title
;
 Iodine pentafluoride-hydrogen fluoride co-crystallisates, directed weak
 interactions
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              635
_journal_page_last               647
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'F7 H I N O'
_chemical_formula_weight         290.92
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                112.34(2)
_cell_angle_beta                 94.56(3)
_cell_angle_gamma                102.76(3)
_cell_formula_units_Z            2
_cell_length_a                   4.942(1)
_cell_length_b                   7.923(1)
_cell_length_c                   8.163(2)
_cell_volume                     283.56(12)
_diffrn_ambient_temperature      120
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    5.744
_exptl_crystal_density_diffrn    3.407
_exptl_crystal_F_000             264
_refine_ls_number_parameters     91
_refine_ls_number_reflns         1622
_refine_ls_R_factor_gt           0.024
_refine_ls_wR_factor_gt          0.022
_cod_data_source_file            EJSSIC-1992-29-635-647-2.cif
_cod_data_source_block           2
_cod_original_formula_sum        'H F7 I N O'
_cod_database_code               4030433
Iodine pentafluoride-hydrogen fluoride co-crystallisates, directed weak interactions
Mahjoub, A.R.; Leopold, D.; Seppelt, K.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 635–647; doi:

data_4030434
_publ_section_title
;
 Iodine pentafluoride-hydrogen fluoride co-crystallisates, directed weak
 interactions
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              635
_journal_page_last               647
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'F12 H I2 K'
_chemical_formula_weight         521.91
_space_group_IT_number           140
_symmetry_cell_setting           tetragonal
_symmetry_Int_Tables_number      140
_symmetry_space_group_name_Hall  '-I 4 2c'
_symmetry_space_group_name_H-M   'I 4/m c m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.706(4)
_cell_length_b                   9.706(4)
_cell_length_c                   10.548(4)
_cell_volume                     993.7(7)
_diffrn_ambient_temperature      113
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    6.895
_exptl_crystal_density_diffrn    3.489
_exptl_crystal_F_000             936
_refine_ls_number_parameters     25
_refine_ls_number_reflns         418
_refine_ls_R_factor_gt           0.025
_refine_ls_wR_factor_gt          0.025
_cod_data_source_file            EJSSIC-1992-29-635-647-3.cif
_cod_data_source_block           3
_cod_original_cell_volume        993.7(9)
_cod_original_formula_sum        'H F12 I2 K'
_cod_database_code               4030434
Iodine pentafluoride-hydrogen fluoride co-crystallisates, directed weak interactions
Mahjoub, A.R.; Leopold, D.; Seppelt, K.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 635–647; doi:

data_4030435
_publ_section_title
;
 Iodine pentafluoride-hydrogen fluoride co-crystallisates, directed weak
 interactions
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              635
_journal_page_last               647
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'Cs F19 H13 I3'
_chemical_formula_weight         887.69
_space_group_IT_number           62
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      62
_symmetry_space_group_name_Hall  '-P 2n 2a'
_symmetry_space_group_name_H-M   'P m c n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   7.276(4)
_cell_length_b                   22.114(7)
_cell_length_c                   9.404(5)
_cell_volume                     1513.1(13)
_diffrn_ambient_temperature      117
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_refine_ls_number_parameters     105
_refine_ls_number_reflns         1752
_refine_ls_R_factor_gt           0.096
_refine_ls_wR_factor_gt          0.078
_cod_data_source_file            EJSSIC-1992-29-635-647-4.cif
_cod_data_source_block           4
_cod_original_cell_volume        1512.9
_cod_original_formula_sum        'H13 Cs F19 I3'
_cod_database_code               4030435
Two new compounds of the SmZrF7-type: EuSnF7 and YSnF7
Benner, G.; Hoppe, R.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 659–677; doi:

data_4030437
_publ_section_title
;
 Two new compounds of the SmZrF7-type: EuSnF7 and YSnF7
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              659
_journal_page_last               677
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'Eu F7 Sn'
_chemical_formula_weight         403.67
_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      4
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90
_cell_angle_beta                 103.09(2)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   6.056(1)
_cell_length_b                   5.628(1)
_cell_length_c                   8.175(1)
_cell_volume                     271.39(8)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    13.16
_exptl_crystal_density_diffrn    4.94
_exptl_crystal_F_000             176
_refine_ls_number_parameters     82
_refine_ls_number_reflns         2039
_refine_ls_R_factor_gt           0.0419
_refine_ls_wR_factor_gt          0.0366
_cod_data_source_file            EJSSIC-1992-29-659-677-1.cif
_cod_data_source_block           EuSnF7
_cod_original_sg_symbol_H-M      'P 21'
_cod_database_code               4030437
Two new compounds of the SmZrF7-type: EuSnF7 and YSnF7
Benner, G.; Hoppe, R.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 659–677; doi:

data_4030438
_publ_section_title
;
 Two new compounds of the SmZrF7-type: EuSnF7 and YSnF7
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              659
_journal_page_last               677
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'F7 Sn Y'
_chemical_formula_weight         340.62
_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      4
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90
_cell_angle_beta                 103.32(1)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   5.9540(9)
_cell_length_b                   5.5646(7)
_cell_length_c                   8.057(1)
_cell_volume                     259.76(6)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    15.48
_exptl_crystal_density_diffrn    4.35
_exptl_crystal_F_000             304
_refine_ls_number_parameters     82
_refine_ls_number_reflns         1476
_refine_ls_R_factor_gt           0.0345
_refine_ls_wR_factor_gt          0.0328
_cod_data_source_file            EJSSIC-1992-29-659-677-2.cif
_cod_data_source_block           YSnF7
_cod_original_sg_symbol_H-M      'P 21'
_cod_original_formula_sum        'F7 Sn  Y'
_cod_database_code               4030438
Structures of cesium containing fluorides, X : crystal structure refinements of the ternary fluorides Cs4M3F10 (M = Mg, Co, Ni, Zn= and magnetism of Cs4Ni3F10
Schmidt, R.E.; Pebler, J.; Babel, D.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 679–690; doi:

data_4030439
_publ_section_title
;
 Structures of cesium containing fluorides, X : crystal structure
 refinements of the ternary fluorides Cs4M3F10 (M = Mg, Co, Ni, Zn= and
 magnetism of Cs4Ni3F10
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              679
_journal_page_last               690
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'Cs4 F10 Mg3'
_chemical_formula_weight         794.57
_space_group_IT_number           64
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      64
_symmetry_space_group_name_Hall  '-C 2ac 2'
_symmetry_space_group_name_H-M   'C m c a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   6.143(1)
_cell_length_b                   14.576(4)
_cell_length_c                   13.650(3)
_cell_volume                     1222.2(5)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    12.086
_exptl_crystal_density_diffrn    4.318
_exptl_crystal_density_meas      4.33
_exptl_crystal_F_000             1384
_refine_ls_number_reflns         1347
_refine_ls_R_factor_gt           0.043
_refine_ls_wR_factor_gt          0.042
_cod_data_source_file            EJSSIC-1992-29-679-690-1.cif
_cod_data_source_block           Cs4Mg3F10
_cod_original_sg_symbol_Hall     '-C 2bc 2'
_cod_database_code               4030439
Structures of cesium containing fluorides, X : crystal structure refinements of the ternary fluorides Cs4M3F10 (M = Mg, Co, Ni, Zn= and magnetism of Cs4Ni3F10
Schmidt, R.E.; Pebler, J.; Babel, D.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 679–690; doi:

data_4030440
_publ_section_title
;
 Structures of cesium containing fluorides, X : crystal structure
 refinements of the ternary fluorides Cs4M3F10 (M = Mg, Co, Ni, Zn= and
 magnetism of Cs4Ni3F10
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              679
_journal_page_last               690
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'Cs4 F10 Ni3'
_chemical_formula_weight         897.71
_space_group_IT_number           64
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      64
_symmetry_space_group_name_Hall  '-C 2ac 2'
_symmetry_space_group_name_H-M   'C m c a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   6.158(1)
_cell_length_b                   14.514(1)
_cell_length_c                   13.736(1)
_cell_volume                     1227.7(2)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    15.52
_exptl_crystal_density_diffrn    4.857
_exptl_crystal_density_meas      4.87
_exptl_crystal_F_000             1576
_refine_ls_number_reflns         1302
_refine_ls_R_factor_gt           0.030
_refine_ls_wR_factor_gt          0.027
_cod_data_source_file            EJSSIC-1992-29-679-690-2.cif
_cod_data_source_block           Cs4Ni3F10
_cod_original_cell_volume        1227.7
_cod_original_sg_symbol_Hall     '-C 2bc 2'
_cod_database_code               4030440
Structures of cesium containing fluorides, X : crystal structure refinements of the ternary fluorides Cs4M3F10 (M = Mg, Co, Ni, Zn= and magnetism of Cs4Ni3F10
Schmidt, R.E.; Pebler, J.; Babel, D.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 679–690; doi:

data_4030441
_publ_section_title
;
 Structures of cesium containing fluorides, X : crystal structure
 refinements of the ternary fluorides Cs4M3F10 (M = Mg, Co, Ni, Zn= and
 magnetism of Cs4Ni3F10
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              679
_journal_page_last               690
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'Cs4 F10 Zn3'
_chemical_formula_weight         917.81
_space_group_IT_number           64
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      64
_symmetry_space_group_name_Hall  '-C 2ac 2'
_symmetry_space_group_name_H-M   'C m c a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   6.205(1)
_cell_length_b                   14.547(2)
_cell_length_c                   13.827(2)
_cell_volume                     1248.1(3)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    16.50
_exptl_crystal_density_diffrn    4.885
_exptl_crystal_density_meas      4.86
_exptl_crystal_F_000             1600
_refine_ls_number_reflns         1172
_refine_ls_R_factor_gt           0.029
_refine_ls_wR_factor_gt          0.026
_cod_data_source_file            EJSSIC-1992-29-679-690-3.cif
_cod_data_source_block           Cs4Zn3F10
_cod_original_sg_symbol_Hall     '-C 2bc 2'
_cod_database_code               4030441
Structures of cesium containing fluorides, X : crystal structure refinements of the ternary fluorides Cs4M3F10 (M = Mg, Co, Ni, Zn= and magnetism of Cs4Ni3F10
Schmidt, R.E.; Pebler, J.; Babel, D.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 679–690; doi:

data_4030442
_publ_section_title
;
 Structures of cesium containing fluorides, X : crystal structure
 refinements of the ternary fluorides Cs4M3F10 (M = Mg, Co, Ni, Zn= and
 magnetism of Cs4Ni3F10
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              679
_journal_page_last               690
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'Co3 Cs4 F10'
_chemical_formula_weight         898.43
_space_group_IT_number           64
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      64
_symmetry_space_group_name_Hall  '-C 2ac 2'
_symmetry_space_group_name_H-M   'C m c a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   6.214(1)
_cell_length_b                   14.513(2)
_cell_length_c                   13.892(1)
_cell_volume                     1252.8(3)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    14.68
_exptl_crystal_density_diffrn    4.76
_exptl_crystal_density_meas      4.73
_exptl_crystal_F_000             1564
_refine_ls_number_reflns         1411
_refine_ls_R_factor_gt           0.034
_refine_ls_wR_factor_gt          0.034
_cod_data_source_file            EJSSIC-1992-29-679-690-4.cif
_cod_data_source_block           Cs4Co3F10
_cod_original_sg_symbol_Hall     '-C 2bc 2'
_cod_database_code               4030442
XeF2.CrF4 and (XeF5+CrF5-)4.XeF4: Syntheses, crystal structures and some properties
Lutar, K.; Leban, I.; Ogrin, T.; Zemva, B.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 713–727; doi:

data_4030443
_publ_section_title
;
 XeF2.CrF4 and (XeF5+CrF5-)4.XeF4: Syntheses, crystal structures and some
 properties
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              713
_journal_page_last               727
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'Cr F6 Xe'
_chemical_formula_weight         297.29
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 91.25(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   7.666(2)
_cell_length_b                   7.268(5)
_cell_length_c                   9.901(3)
_cell_volume                     551.5(4)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    8.144
_exptl_crystal_density_diffrn    3.581
_exptl_crystal_F_000             528
_refine_ls_number_reflns         741
_refine_ls_R_factor_gt           0.068
_refine_ls_wR_factor_gt          0.076
_cod_data_source_file            EJSSIC-1992-29-713-727-1.cif
_cod_data_source_block           XeCrF6
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4030443
XeF2.CrF4 and (XeF5+CrF5-)4.XeF4: Syntheses, crystal structures and some properties
Lutar, K.; Leban, I.; Ogrin, T.; Zemva, B.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 713–727; doi:

data_4030444
_publ_section_title
;
 XeF2.CrF4 and (XeF5+CrF5-)4.XeF4: Syntheses, crystal structures and some
 properties
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              713
_journal_page_last               727
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'Cr4 F44 Xe5'
_chemical_formula_weight         1700.45
_space_group_IT_number           61
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      61
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   11.988(6)
_cell_length_b                   15.862(2)
_cell_length_c                   16.538(2)
_cell_volume                     3144.8(17)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    6.905
_exptl_crystal_density_diffrn    3.592
_refine_ls_number_reflns         2850
_refine_ls_R_factor_gt           0.052
_refine_ls_wR_factor_gt          0.0587
_cod_data_source_file            EJSSIC-1992-29-713-727-2.cif
_cod_data_source_block           Xe5Cr4F44
_cod_database_code               4030444
Preparation and structure characterization of the bis[tertbutyl(trimethylsilyl)amino]chalcogenides of selenium and tellurium
Bjorgvinsson, M.; Roesky, H.W.; Pauer, F.; Stalke, D.; Sheldrick, G.M.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 759–776; doi:

data_4030445
_publ_section_title
;
 Preparation and structure characterization of the
 bis[tertbutyl(trimethylsilyl)amino]chalcogenides of selenium and
 tellurium
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              759
_journal_page_last               776
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'C14 H36 N2 Se Si2'
_chemical_formula_weight         367.6
_space_group_IT_number           61
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      61
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   14.488(1)
_cell_length_b                   12.504(2)
_cell_length_c                   22.131(2)
_cell_volume                     4009.2(8)
_diffrn_ambient_temperature      153
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    1.80
_exptl_crystal_density_diffrn    1.218
_exptl_crystal_F_000             1568
_refine_ls_number_parameters     280
_refine_ls_number_reflns         2977
_refine_ls_R_factor_gt           0.0267
_refine_ls_wR_factor_gt          0.0246
_cod_data_source_file            EJSSIC-1992-29-759-776-1.cif
_cod_data_source_block           1
_cod_original_formula_sum        'C14 H36 N2 Si2 Se'
_cod_database_code               4030445
Preparation and structure characterization of the bis[tertbutyl(trimethylsilyl)amino]chalcogenides of selenium and tellurium
Bjorgvinsson, M.; Roesky, H.W.; Pauer, F.; Stalke, D.; Sheldrick, G.M.; European Journal of Solid State and Inorganic Chemistry 29 (1992) 759–776; doi:

data_4030446
_publ_section_title
;
 Preparation and structure characterization of the
 bis[tertbutyl(trimethylsilyl)amino]chalcogenides of selenium and
 tellurium
;
_journal_name_full
'European Journal of Solid State and Inorganic Chemistry'
_journal_page_first              759
_journal_page_last               776
_journal_volume                  29
_journal_year                    1992
_chemical_formula_sum            'C14 H36 N2 Si2 Te'
_chemical_formula_weight         416.2
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 111.89(1)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   13.161(3)
_cell_length_b                   10.560(3)
_cell_length_c                   15.961(3)
_cell_volume                     2058.3(9)
_diffrn_ambient_temperature      153
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    1.56
_exptl_crystal_density_diffrn    1.343
_exptl_crystal_F_000             856
_refine_ls_number_parameters     280
_refine_ls_number_reflns         4309
_refine_ls_R_factor_gt           0.0205
_refine_ls_wR_factor_gt          0.0209
_cod_data_source_file            EJSSIC-1992-29-759-776-2.cif
_cod_data_source_block           2
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4030446