Structural investigations of 1,2,3,4-tetrahydrocarbazole derivatives. I. 2,3-Dihydro-9-(phenylsulfonyl)carbazole-4(1<i>H</i>)-one and 1,2,3,4-tetrahydrocarbazole-1-spiro-2'-[1,3]dithiolane
Hökelek, T.; Patir, S.; Gülce, A.; Okay, G.; Acta Crystallographica Section C 50 (1994) 450–453; doi:10.1107/S0108270193007516

data_2009506
_publ_section_title
;
 Structural investigations of 1,2,3,4-tetrahydrocarbazole derivatives.
 I. 2,3-Dihydro-9-(phenylsulfonyl)carbazole-4(1<i>H</i>)-one and
 1,2,3,4-tetrahydrocarbazole-1-spiro-2'-[1,3]dithiolane
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              450
_journal_page_last               453
_journal_paper_doi               10.1107/S0108270193007516
_journal_volume                  50
_journal_year                    1994
_chemical_formula_sum            'C14 H15 N S2'
_chemical_formula_weight         261.4
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.
_cell_angle_beta                 91.29(3)
_cell_angle_gamma                90.
_cell_formula_units_Z            4
_cell_length_a                   9.715(2)
_cell_length_b                   6.721(2)
_cell_length_c                   19.854(8)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293
_cell_measurement_theta_max      14
_cell_measurement_theta_min      6
_cell_volume                     1296.0(7)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54180
_diffrn_reflns_av_R_equivalents  'not calculated'
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       8
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            3986
_diffrn_reflns_theta_max         75
_diffrn_standards_decay_%        1
_diffrn_standards_interval_time  180
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    3.46
_exptl_absorpt_correction_T_max  0.855
_exptl_absorpt_correction_T_min  0.341
_exptl_absorpt_correction_type   semi-empirical
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.340
_exptl_crystal_description       plate
_exptl_crystal_size_max          0.52
_exptl_crystal_size_mid          0.32
_exptl_crystal_size_min          0.06
_refine_diff_density_max         0.04
_refine_diff_density_min         -0.64
_refine_ls_goodness_of_fit_obs   'not calculated'
_refine_ls_hydrogen_treatment    refall
_refine_ls_number_parameters     214
_refine_ls_number_reflns         1616
_refine_ls_R_factor_obs          0.054
_refine_ls_shift/esd_max         0.01
_refine_ls_structure_factor_coef F
_refine_ls_wR_factor_obs         0.067
_reflns_number_observed          1847
_reflns_number_total             2486
_reflns_observed_criterion       F>=3\s(F)
_cod_data_source_file            ab1076.cif
_cod_data_source_block           ab1076_structure_2_of_2
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C14 H15 N1 S2'
_cod_database_code               2009506