Pd(II)/Ag(I)-Catalyzed Room-Temperature Reaction of γ-Hydroxy Lactams: Mechanism, Scope, and Antistaphylococcal Activity.
Dutta, Manali; Mandal, Santi M.; Pegu, Rupa; Pratihar, Sanjay; The Journal of organic chemistry 82 (2017) 2193–2198; doi:10.1021/acs.joc.6b02378

data_4032156
_publ_section_title
;
 Pd(II)/Ag(I)-Catalyzed Room-Temperature Reaction of \g-Hydroxy Lactams:
 Mechanism, Scope, and Antistaphylococcal Activity.
;
_journal_issue                   4
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              2193
_journal_page_last               2198
_journal_paper_doi               10.1021/acs.joc.6b02378
_journal_volume                  82
_journal_year                    2017
_chemical_formula_moiety         C14H12N2O2
_chemical_formula_sum            'C14 H12 N2 O2'
_chemical_formula_weight         240.26
_chemical_melting_point          205
_chemical_name_common            Isoindolehydroxylactam
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
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_cell_length_b                   14.6572(5)
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_diffrn_radiation_type           MoK\a
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_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -16
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_diffrn_reflns_number            10088
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.976
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.738
_diffrn_reflns_theta_min         2.291
_diffrn_source                   'fine-focous sealed tube'
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_refine_ls_number_reflns         2609
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.172
_refine_ls_R_factor_all          0.0551
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_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0640P)^2^+0.8643P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_total             2609
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 4032156--4032157.cif.'
_cod_database_code               4032156
_shelxl_version_number           2014-1
_shelx_res_checksum              34753
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