Entangled coordination polymers with mixed N- and O-donor organic linkers: A case of module-matching priority.
Han, Li-Wei; Gong, Yun; Lin, Zu-Jin; Lü, Jian; Cao, Rong; Dalton transactions (Cambridge, England : 2003) 41 (2012) 4146–4152; doi:10.1039/c2dt11899h

data_7018382
_publ_section_title
;
 Entangled coordination polymers with mixed N- and O-donor organic
 linkers: A case of module-matching priority.
;
_journal_issue                   14
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              4146
_journal_page_last               4152
_journal_paper_doi               10.1039/c2dt11899h
_journal_volume                  41
_journal_year                    2012
_chemical_formula_sum            'C36 H34 Co N6 O8'
_chemical_formula_weight         737.62
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                108.865(4)
_cell_angle_beta                 107.898(4)
_cell_angle_gamma                99.825(4)
_cell_formula_units_Z            2
_cell_length_a                   10.5853(5)
_cell_length_b                   12.8836(5)
_cell_length_c                   14.6733(6)
_cell_measurement_temperature    293(2)
_cell_volume                     1719.05(16)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.826
_diffrn_measured_fraction_theta_max 0.826
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0309
_diffrn_reflns_av_sigmaI/netI    0.0823
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       10
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            12388
_diffrn_reflns_theta_full        26.74
_diffrn_reflns_theta_max         26.74
_diffrn_reflns_theta_min         2.31
_exptl_absorpt_coefficient_mu    0.561
_exptl_crystal_density_diffrn    1.425
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             766
_refine_diff_density_max         0.588
_refine_diff_density_min         -0.479
_refine_diff_density_rms         0.070
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.025
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     435
_refine_ls_number_reflns         6055
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.025
_refine_ls_R_factor_all          0.0798
_refine_ls_R_factor_gt           0.0484
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0602P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1204
_refine_ls_wR_factor_ref         0.1257
_reflns_number_gt                3879
_reflns_number_total             6055
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c2dt11899h.txt
_cod_data_source_block           1010251
_cod_original_cell_volume        1719.05(13)
_cod_database_code               7018382