Redox-induced dimerisations of a phosphacyclic biradicaloid.
Zuber, David; Storcheva, Oksana; Lüdtke, Karsten Paul; Brunk, Leonidas; Coburger, Peter; Chemical communications (Cambridge, England) 61 (2025) 2798–2801; doi:10.1039/d4cc05656f

data_7134103
_publ_section_title
;
 Redox-induced dimerisations of a phosphacyclic biradicaloid.
;
_journal_issue                   13
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              2798
_journal_page_last               2801
_journal_paper_doi               10.1039/d4cc05656f
_journal_volume                  61
_journal_year                    2025
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;
2024-12-03 deposited with the CCDC.	2024-12-29 downloaded from the CCDC.
;
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_computing_cell_refinement
; 
   STOE & CIE GmbH 
   Hilpertstr. 10 
   D-64295 Darmstadt 
   Germany 
;
_computing_data_collection
; 
   STOE & CIE GmbH 
   Hilpertstr. 10 
   D-64295 Darmstadt 
   Germany 
;
_computing_data_reduction
; 
   STOE & CIE GmbH 
   Hilpertstr. 10 
   D-64295 Darmstadt 
   Germany 
;
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; 
   STOE & CIE GmbH 
   Hilpertstr. 10 
   D-64295 Darmstadt 
   Germany 
;
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_diffrn_measurement_method       'rotation method, \w scans'
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_av_R_equivalents  0.0156
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_diffrn_reflns_point_group_measured_fraction_full 0.996
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_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         25.350
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_diffrn_source                   'Genix 3D HF Mo'
_exptl_absorpt_coefficient_mu    0.261
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_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
; 
   STOE & CIE GmbH 
   Hilpertstr. 10 
   D-64295 Darmstadt 
   Germany 
;
_exptl_crystal_colour            yellow
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_exptl_crystal_description       prism
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0444P)^2^+0.3025P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_data_source_block           DZ-PPIPh-precise-cell_a_sq
_cod_depositor_comments
'Adding full bibliography for 7134102--7134104.cif.'
_cod_original_cell_volume        1170.6(5)
_cod_database_code               7134103
_shelx_shelxl_version_number     2018/3
_shelx_res_checksum              83995
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