Crystal structure of dibenzyldimethylsilane
Knauer, Lena; Golz, Christopher; Kroesen, Ulrike; Koller, Stephan G.; Strohmann, Carsten; Acta Crystallographica Section E 71 (2015) o391–o392; doi:10.1107/S2056989015008713

data_2240583
_publ_section_title
;
 Crystal structure of dibenzyldimethylsilane
;
_journal_coeditor_code           FK2087
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o391
_journal_page_last               o392
_journal_paper_doi               10.1107/S2056989015008713
_journal_volume                  71
_journal_year                    2015
_chemical_formula_iupac          'C16 H20 Si'
_chemical_formula_moiety         'C16 H20 Si'
_chemical_formula_sum            'C16 H20 Si'
_chemical_formula_weight         240.41
_chemical_name_systematic
;
Dibenzyldimethylsilane
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
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Olex2 1.2
(compiled 2014.11.20 svn.r3092 for OlexSys, GUI svn.r4949)
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_cell_volume                     1420.54(7)
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CrysAlis PRO (Oxford Diffraction, 2010)
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CrysAlis PRO (Oxford Diffraction, 2010)
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CrysAlis PRO (Oxford Diffraction, 2010)
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OLEX2 (Dolomanov <i>et al.</i>,  2009)
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OLEX2 (Dolomanov <i>et al.</i>,  2009)
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SHELXL2014 (Sheldrick, 2015)
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SHELXS97 (Sheldrick, 2008)
;
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_diffrn_measurement_method       '\w scans'
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_diffrn_reflns_limit_k_min       -24
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_diffrn_reflns_limit_l_min       -14
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_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         25.997
_diffrn_reflns_theta_min         2.689
_exptl_absorpt_coefficient_mu    0.143
_exptl_absorpt_correction_T_max  1.00000
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;
(CrysAlis PRO; Oxford Diffraction, 2010)
;
_exptl_crystal_colour            colourless
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_exptl_crystal_size_min          0.1
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_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.063
_refine_ls_R_factor_all          0.0422
_refine_ls_R_factor_gt           0.0327
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0528P)^2^+0.0485P] where P=(Fo^2^+2Fc^2^)/3'
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