The facile and efficient synthesis of novel monocyclic cis-β-lactam conjugates with a 1-methyl-1H-imidazole-2-thiol nucleus
Singh, Vedeshwar Narayan; Sharma, Sitaram; New Journal of Chemistry 45 (2021) 19347–19357; doi:10.1039/D1NJ03566E

data_7060962
_publ_section_title
;
 The facile and efficient synthesis of novel monocyclic cis-\b-lactam
 conjugates with a 1-methyl-1H-imidazole-2-thiol nucleus
;
_journal_issue                   41
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              19347
_journal_page_last               19357
_journal_paper_doi               10.1039/D1NJ03566E
_journal_volume                  45
_journal_year                    2021
_chemical_formula_sum            'C30 H27 N3 O2 S'
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_audit_creation_method           SHELXL-2016/6
_audit_update_record
;
2021-03-01 deposited with the CCDC.	2021-09-20 downloaded from the CCDC.
;
_cell_angle_alpha                115.186(4)
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_cell_angle_gamma                92.280(6)
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_cell_volume                     1252.4(3)
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_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_diffrn_ambient_temperature      135(2)
_diffrn_measured_fraction_theta_full 0.980
_diffrn_measured_fraction_theta_max 0.980
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_av_unetI/netI     0.0734
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_refine_ls_extinction_method     none
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1699P)^2^+0.4889P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d1nj03566e2.cif
_cod_data_source_block           mo_NITPATNA6SN4A250221_0m_a
_cod_depositor_comments
;
Adding full bibliography for 7060962--7060963.cif.

2025-03-04
Z value and formula fixed to values more according to usual
chemical conventions.                 miguel
;
_cod_original_formula_sum            'C H N O S'
_cod_original_formula_weight         75.09
_cod_original_formula_units_Z            16
_cod_database_code               7060962
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