Reversibility in Reactions of Linker-Bridged Distannenes with Terminal Alkynes at Ambient Temperature.
Schneider, Julia; Henning, Jens; Edrich, Jessica; Schubert, Hartmut; Wesemann, Lars; Inorganic chemistry 54 (2015) 6020–6027; doi:10.1021/acs.inorgchem.5b00896

data_4343093
_publ_section_title
;
 Reversibility in Reactions of Linker-Bridged Distannenes with Terminal
 Alkynes at Ambient Temperature.
;
_journal_issue                   12
_journal_name_full               'Inorganic chemistry'
_journal_page_first              6020
_journal_page_last               6027
_journal_paper_doi               10.1021/acs.inorgchem.5b00896
_journal_volume                  54
_journal_year                    2015
_chemical_formula_moiety         'C68 H64 Sn2, 1.5(C6H6)'
_chemical_formula_sum            'C77 H73 Sn2'
_chemical_formula_weight         1235.73
_chemical_name_systematic
; 
 ? 
;
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_space_group_name_Hall           '-P 1'
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_symmetry_space_group_name_Hall  '-P 1'
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_diffrn_ambient_temperature      100(2)
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_exptl_crystal_colour            colorless
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_refine_ls_number_reflns         14374
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0245P)^2^+2.2153P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     >2sigma(I)
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_cod_depositor_comments
'Adding full bibliography for 4343090--4343095.cif.'
_cod_database_code               4343093
_computing_bruker_data_scaling   'SADABS V2008/1 (Bruker AXS)'