Crystal engineering with isosteric triether and triamine linked aromatic tri-carboxylic acids: iso-structurality and synthon interplay in their co-crystals and salts with bis(pyridyl) derivatives
Das, Debarati; Roy, Sandipan; Biradha, Kumar; New Journal of Chemistry 42 (2018) 19953–; doi:10.1039/C8NJ04600J

data_7057935
_publ_section_title
;
 Crystal engineering with isosteric triether and triamine linked aromatic
 tri-carboxylic acids: iso-structurality and synthon interplay in their
 co-crystals and salts with bis(pyridyl) derivatives
;
_journal_issue                   24
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              19953
_journal_paper_doi               10.1039/C8NJ04600J
_journal_volume                  42
_journal_year                    2018
_chemical_formula_sum            'C27 H18 O9'
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_symmetry_space_group_name_Hall  '-P 2yn'
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_audit_update_record
;
2018-09-10 deposited with the CCDC.
2018-11-06 downloaded from the CCDC.
;
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_diffrn_ambient_temperature      150(2)
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_exptl_absorpt_coefficient_mu    0.111
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_exptl_crystal_description       needle
_exptl_crystal_F_000             2016
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1876P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1776
_refine_ls_wR_factor_ref         0.2459
_reflns_Friedel_coverage         0.000
_reflns_number_gt                5627
_reflns_number_total             8280
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c8nj04600j2.cif
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_cod_depositor_comments
'Adding full bibliography for 7057935--7057944.cif.'
_cod_database_code               7057935
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