Multifunctional sensing ability of a new Pt/Zn-based luminescent coordination polymer.
Kobayashi, Atsushi; Hara, Hirofumi; Noro, Shin-Ichiro; Kato, Masako; Dalton transactions (Cambridge, England : 2003) 39 (2010) 3400–3406; doi:10.1039/b917693d

data_7024481
_publ_section_title
;
 Multifunctional sensing ability of a new Pt/Zn-based luminescent
 coordination polymer.
;
_journal_issue                   14
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              3400
_journal_page_last               3406
_journal_paper_doi               10.1039/b917693d
_journal_volume                  39
_journal_year                    2010
_chemical_formula_moiety         'C14 H14 N4 O8 Pt Zn '
_chemical_formula_sum            'C14 H14 N4 O8 Pt Zn'
_chemical_formula_weight         626.76
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      11
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_cell_angle_alpha                90.0000
_cell_angle_beta                 101.38(3)
_cell_angle_gamma                90.0000
_cell_formula_units_Z            2
_cell_length_a                   9.495(17)
_cell_length_b                   6.577(11)
_cell_length_c                   14.10(2)
_cell_measurement_reflns_used    2301
_cell_measurement_temperature    90.1
_cell_measurement_theta_max      31.4
_cell_measurement_theta_min      1.4
_cell_volume                     863(2)
_computing_cell_refinement       CrystalClear
_computing_data_collection       CrystalClear
_computing_data_reduction        CrystalStructure
_computing_publication_material  'CrystalStructure 3.8'
_computing_structure_refinement  SHELXL
_computing_structure_solution    SIR2004
_diffrn_detector_area_resol_mean 7.31
_diffrn_measured_fraction_theta_full 0.895
_diffrn_measured_fraction_theta_max 0.895
_diffrn_measurement_device_type  'Rigaku Mercury'
_diffrn_measurement_method       \w
_diffrn_radiation_type           synchrotron
_diffrn_radiation_wavelength     0.68900
_diffrn_reflns_av_R_equivalents  0.112
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       -9
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            9503
_diffrn_reflns_theta_full        31.57
_diffrn_reflns_theta_max         31.57
_exptl_absorpt_coefficient_mu    9.419
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.025
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details
;
Higashi, T. (1999). Program for Absorption Correction.
Rigaku Corporation, Tokyo, Japan.
;
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    2.410
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       platelet
_exptl_crystal_F_000             596.00
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.02
_refine_diff_density_max         10.28
_refine_diff_density_min         -6.69
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.056
_refine_ls_hydrogen_treatment    refall
_refine_ls_number_parameters     168
_refine_ls_number_reflns         3055
_refine_ls_R_factor_gt           0.0771
_refine_ls_shift/su_max          0.0010
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s2^(Fo2^)+(0.1445P)2^+3.5307P] where P=(Fo2^+2Fc2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.2292
_reflns_number_gt                2470
_reflns_number_total             3055
_reflns_threshold_expression     F2^>2.0\s(F2^)
_cod_data_source_file            b917693d.txt
_cod_data_source_block           HH03-124Zn-a
_cod_original_cell_volume        864(3)
_cod_original_formula_sum        'C14 H14 N4 O8 Pt Zn '
_cod_database_code               7024481