Investigation of benzoyloximes as benzoylating reagents: benzoyl-Oxyma as a selective benzoylating reagent.
Burugupalli, Satvika; Shah, Sayali; van der Peet, Phillip L.; Arora, Seep; White, Jonathan M.; Williams, Spencer J.; Organic & biomolecular chemistry 14 (2016) 97–104; doi:10.1039/c5ob02092a

data_7154769
_publ_section_title
;
 Investigation of benzoyloximes as benzoylating reagents: benzoyl-Oxyma as
 a selective benzoylating reagent.
;
_journal_issue                   1
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              97
_journal_page_last               104
_journal_paper_doi               10.1039/c5ob02092a
_journal_volume                  14
_journal_year                    2016
_chemical_formula_sum            'C12 H10 N2 O4'
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_chemical_name_common            Benzoyl-Oxyma
_space_group_crystal_system      monoclinic
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2015-06-11 deposited with the CCDC.
2015-10-28 downloaded from the CCDC.
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
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Empirical absorption correction using spherical harmonics,
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_exptl_crystal_colour            colourless
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_exptl_crystal_description       block
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_exptl_crystal_recrystallization_method 'Re-crystallisation from solvent: '
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_refine_ls_extinction_method     'SHELXL-2014/7 (Sheldrick 2014'
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_refine_ls_restrained_S_all      1.065
_refine_ls_R_factor_all          0.0355
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0555P)^2^+0.2682P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0955
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_reflns_number_gt                2347
_reflns_number_total             2434
_reflns_threshold_expression     'I > 2\s(I)'
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'Adding full bibliography for 7154769--7154770.cif.'
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