Simultaneous Generation of a [2 × 2] Grid-Like Complex and a Linear Double Helicate: a Three-Level Self-Sorting Process.
Ayme, Jean-François; Lehn, Jean-Marie; Bailly, Corinne; Karmazin, Lydia; Journal of the American Chemical Society 142 (2020) 5819–5824; doi:10.1021/jacs.0c00896

data_4134429
_publ_section_title
;
 Simultaneous Generation of a [2 \\times 2] Grid-Like Complex and a Linear
 Double Helicate: a Three-Level Self-Sorting Process.
;
_journal_issue                   12
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              5819
_journal_page_last               5824
_journal_paper_doi               10.1021/jacs.0c00896
_journal_volume                  142
_journal_year                    2020
_chemical_formula_moiety         'C64 H52 Cu2 N8 O4, 2(Cl O4), 2(C H Cl3)'
_chemical_formula_sum            'C66 H54 Cl8 Cu2 N8 O12'
_chemical_formula_weight         1561.85
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_diffrn_measured_fraction_theta_max 0.999
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_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_theta_min         1.637
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_exptl_absorpt_process_details   sadabs
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_refine_ls_restrained_S_all      1.059
_refine_ls_R_factor_all          0.0801
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_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0641P)^2^+16.3199P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           jmljfa161207
_cod_depositor_comments
'Adding full bibliography for 4134428--4134431.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4134429
_shelx_estimated_absorpt_t_min   0.626
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_shelx_res_checksum              3308
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