π-Rich σ(2)P-Heterocycles: Bent η(1)-P- and μ(2)-P-Coordinated 1,3-Benzazaphosphole Copper(I) Halide Complexes.
Ghalib, Mohammed; Jones, Peter G.; Schulzke, Carola; Sziebert, Dénes; Nyulászi, László; Heinicke, Joachim W.; Inorganic chemistry 54 (2015) 2117–; doi:10.1021/ic502367d

data_4342364
_publ_section_title
;
 \p-Rich \s(2)P-Heterocycles: Bent \h(1)-P- and \m(2)-P-Coordinated
 1,3-Benzazaphosphole Copper(I) Halide Complexes.
;
_journal_issue                   5
_journal_name_full               'Inorganic chemistry'
_journal_page_first              2117
_journal_paper_doi               10.1021/ic502367d
_journal_volume                  54
_journal_year                    2015
_chemical_formula_sum            'C88 H128 Cl9 Cu9 N6 O4 P6'
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_diffrn_measured_fraction_theta_max 0.978
_diffrn_measurement_device_type  'STOE IPDS2T'
_diffrn_measurement_method       \w
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_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'face indexed'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.600
_exptl_crystal_description       block
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0643P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_gt                4693
_reflns_number_total             13416
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 4342364--4342369.cif.'
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