A three-dimensional framework aluminophosphate (CH~3~NH~3~)^+^[Al~3~P~3~O~13~H]^{-^}
Chippindale, A.M.; Powell, A.V.; Jones, R.H.; Thomas, J.M.; Cheetham, A.K.; Huo, Q.; Xu, R.; Acta Crystallographica Section C 50 (1994) 1537–1540; doi:10.1107/S0108270194003537

data_2010097
_publ_section_title
;
 A three-dimensional framework aluminophosphate
 (CH~3~NH~3~)^+^[Al~3~P~3~O~13~H]^{-^}
;
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1537
_journal_page_last               1540
_journal_paper_doi               10.1107/S0108270194003537
_journal_volume                  50
_journal_year                    1994
_chemical_formula_moiety         'C1 H7 Al3 N1 O13 P3'
_chemical_formula_sum            'C H7 Al3 N O13 P3'
_chemical_formula_weight         414.93
_space_group_IT_number           61
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2bc 2ac'
_symmetry_space_group_name_H-M   'P c a b'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.
_cell_angle_beta                 90.
_cell_angle_gamma                90.
_cell_formula_units_Z            8
_cell_length_a                   10.281(2)
_cell_length_b                   13.844(3)
_cell_length_c                   17.064(5)
_cell_measurement_reflns_used    20
_cell_measurement_temperature    293
_cell_measurement_theta_max      16.5
_cell_measurement_theta_min      15.1
_cell_volume                     2428.7(10)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0279
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -1
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -1
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -1
_diffrn_reflns_number            2803
_diffrn_reflns_theta_max         23
_diffrn_standards_decay_%        none
_diffrn_standards_interval_time  60
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    76.48
_exptl_absorpt_correction_T_max  1.00
_exptl_absorpt_correction_T_min  .89
_exptl_absorpt_correction_type   sphere
_exptl_crystal_colour            transparent
_exptl_crystal_density_diffrn    2.270
_exptl_crystal_description       plate
_exptl_crystal_size_max          0.23
_exptl_crystal_size_mid          0.09
_exptl_crystal_size_min          0.05
_refine_diff_density_max         0.55
_refine_diff_density_min         -0.48
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   1.38
_refine_ls_number_parameters     190
_refine_ls_number_reflns         1343
_refine_ls_R_factor_obs          0.0476
_refine_ls_shift/esd_max         0.004
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      'Chebyshev, three term polynomial'
_refine_ls_wR_factor_obs         0.0456
_reflns_number_observed          1343
_reflns_number_total             1683
_reflns_observed_criterion       I>1.5\s(I)
_cod_data_source_file            du1073.cif
_cod_data_source_block           du1073_structure_1_of_1
_cod_depositor_comments
;
 Changing the _atom_site_occupancy data item value from '?' to '1'
 for all fully occupied atom sites.

 Antanas Vaitkus,
 2017-02-13
;
_cod_original_cell_volume        2428.72
_cod_original_sg_symbol_Hall     '-P 2bc -2ac'
_cod_original_formula_sum        'C1 H7 Al3 N1 O13 P3'
_cod_database_code               2010097