Oligomeric pentafluorophenylboron azides
Fraenk, Wolfgang; Klapötke, Thomas M.; Krumm, Burkhard; Nöth, Heinrich; Suter, Max; Warchhold, Marcus; Journal of the Chemical Society, Dalton Transactions  (2000) 4635–; doi:10.1039/b007626k

data_7010276
_publ_contact_author
;
      Heinrich N\"oth
      Institut f\"ur anorganische Chemie
      Universit\"at M\"unchen
      Butenandtstr. 5-13 (Haus D)
      81377 M\"unchen
      Bundesrepublik Deutschland
;
_publ_section_title
;
 Oligomeric pentafluorophenylboron azides
;
_journal_issue                   24
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              4635
_journal_paper_doi               10.1039/b007626k
_journal_year                    2000
_chemical_formula_sum            'C18 B3 F15 N18'
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_cell_angle_alpha                90
_cell_angle_beta                 97.463(1)
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_cell_measurement_temperature    193(2)
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_computing_molecular_graphics    'XP (SHELXTL-Ver.5)'
_computing_publication_material  'SHELXL (Sheldrick 1997)'
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_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      193(2)
_diffrn_measured_fraction_theta_full 0.739
_diffrn_measured_fraction_theta_max 0.739
_diffrn_measurement_device_type  'Siemens SMART Area-detector'
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_diffrn_standards_interval_time  0
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_exptl_crystal_colour            colourless
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'calc w=1/[\s^2^(Fo^2^)+(0.0536P)^2^+3.1621P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_refine_ls_hydrogen_treatment' value 'mixed ' changed to
'mixed' according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_atom_sites_solution_primary' value 'direct methods' was changed to
'direct'.

'_atom_sites_solution_hydrogens' value 'geometrically' was changed to
'geom'.

Automatic conversion script
Id: cif_fix_values 6452 2018-10-05 10:23:21Z andrius 
;
_cod_original_cell_volume        5552.0(8)
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               7010276