Exploring supramolecular assembly and luminescent behavior in a series of RE-p-chlorobenzoic acid-1,10-phenanthroline complexes
Carter, Korey P.; Zulato, Cecília H. F.; Cahill, Christopher L.; CrystEngComm 16 (2014) 10189–; doi:10.1039/C4CE01806K

data_7218281
_publ_section_title
;
 Exploring supramolecular assembly and luminescent behavior in a series of
 RE-p-chlorobenzoic acid-1,10-phenanthroline complexes
;
_journal_issue                   44
_journal_name_full               CrystEngComm
_journal_page_first              10189
_journal_paper_doi               10.1039/C4CE01806K
_journal_volume                  16
_journal_year                    2014
_chemical_formula_sum            'C66 H40 Cl6 N4 O12 Yb2'
_chemical_formula_weight         1639.80
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_symmetry_cell_setting           triclinic
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_symmetry_space_group_name_Hall  '-P 1'
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_cell_measurement_theta_min      4.708
_cell_volume                     1519.4(2)
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_computing_structure_solution    'SIR92 (Gualardi, 1994)'
_diffrn_ambient_temperature      293(2)
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_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Bruker APEX II CCD'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_av_unetI/netI     0.0453
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_diffrn_reflns_limit_l_min       -19
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_diffrn_reflns_theta_min         1.567
_diffrn_source                   'fine-focus sealed tube'
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_exptl_absorpt_correction_T_min  0.6707
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_refine_ls_extinction_method     none
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_refine_ls_restrained_S_all      0.995
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0263P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_total             7640
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c4ce01806k2.cif
_cod_data_source_block           Compound_9
_cod_depositor_comments
'Adding full bibliography for 7218273--7218283.cif.'
_cod_database_code               7218281
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