Tuning the redox profiles of polyoxovanadate-alkoxide clusters via heterometal installation: toward designer redox Reagents.
VanGelder, L. E.; Brennessel, W. W.; Matson, E. M.; Dalton transactions (Cambridge, England : 2003) 47 (2018) 3698–3704; doi:10.1039/c7dt04455k

data_7045080
_publ_section_title
;
 Tuning the redox profiles of polyoxovanadate-alkoxide clusters via
 heterometal installation: toward designer redox Reagents.
;
_journal_issue                   11
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              3698
_journal_page_last               3704
_journal_paper_doi               10.1039/c7dt04455k
_journal_volume                  47
_journal_year                    2018
_chemical_formula_moiety         'C16 H36 N, C13 H39 O19 V5 Zr'
_chemical_formula_sum            'C29 H75 N O19 V5 Zr'
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_space_group_name_Hall           'P 2c -2n'
_space_group_name_H-M_alt        'P n a 21'
_symmetry_space_group_name_Hall  'P 2c -2n'
_symmetry_space_group_name_H-M   'P n a 21'
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_audit_update_record
;
2017-11-24 deposited with the CCDC.
2017-12-18 downloaded from the CCDC.
;
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_diffrn_measurement_method       '\w scans'
_diffrn_radiation_type           MoK\a
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; 
 Refined as an inversion twin. 
;
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0477P)^2^+2.0027P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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'Adding full bibliography for 7045078--7045080.cif.'
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