Design of a flexible organometallic tecton: host-guest chemistry with picric acid and self-assembly of platinum macrocycles.
Jana, Achintya; Bhowmick, Sourav; Kaur, Supreet; Kashyap, Hemant K.; Das, Neeladri; Dalton transactions (Cambridge, England : 2003) 46 (2017) 1986–1995; doi:10.1039/c6dt03498e

data_7041606
_publ_section_title
;
 Design of a flexible organometallic tecton: host-guest chemistry with
 picric acid and self-assembly of platinum macrocycles.
;
_journal_issue                   6
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1986
_journal_page_last               1995
_journal_paper_doi               10.1039/c6dt03498e
_journal_volume                  46
_journal_year                    2017
_chemical_formula_moiety         'C44 H70 I2 N2 O2 P4 Pt2'
_chemical_formula_sum            'C44 H70 I2 N2 O2 P4 Pt2'
_chemical_formula_weight         1426.86
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2016-05-25 deposited with the CCDC.
2017-01-03 downloaded from the CCDC.
;
_cell_angle_alpha                107.089(6)
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_cell_measurement_temperature    150(2)
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_cell_measurement_theta_min      2.69
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_computing_cell_refinement       'Bruker SAINT'
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_type           MoK\a
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_refine_ls_extinction_method     'SHELXL-2014/7 (Sheldrick 2014'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0391P)^2^+32.5014P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1153
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_reflns_Friedel_coverage         0.000
_reflns_number_gt                10000
_reflns_number_total             12836
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments          'Adding full bibliography for 7041606.cif.'
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