Bulky 2,6-disubstituted aryl siloxanes and a disilanamine
Marszaukowski, Flavia; Wohnrath, Karen; Boeré, René T.; Acta Crystallographica Section E 76 (2020) 318–323; doi:10.1107/S2056989020001413

data_2243271
_publ_section_title
;
 Bulky 2,6-disubstituted aryl siloxanes and a disilanamine
;
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_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              318
_journal_page_last               323
_journal_paper_doi               10.1107/S2056989020001413
_journal_volume                  76
_journal_year                    2020
_chemical_formula_iupac          'C17 H29 Br O Si'
_chemical_formula_moiety         'C17 H29 Br O Si'
_chemical_formula_sum            'C17 H29 Br O Si'
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_chemical_name_systematic
;
5-Bromo-1,3-di-<i>tert</i>-butyl-2-[(trimethylsilyl)oxy]benzene
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Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
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CrysAlisPro (Rigaku OD, 2018)
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CrysAlisPro (Rigaku OD, 2018)
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CrysAlisPro (Rigaku OD, 2018)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>,  2009)
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publCIF (Westrip, 2010)
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ShelXL (Sheldrick, 2015b)
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ShelXT (Sheldrick, 2015a)
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'Rigaku Oxford Diffraction SuperNova, Dual, Cu at zero, Pilatus 200K'
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(CrysAlisPro; Rigaku OD, 2018)
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_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
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SHELXL-2018/3 (Sheldrick 2015b)
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0196P)^2^+3.6340P] where P=(Fo^2^+2Fc^2^)/3'
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_refine_ls_wR_factor_ref         0.0733
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