Cu(II), Mn(II) and Zn(II) complexes of hydrazones with a quaternary ammonium moiety: synthesis, experimental and theoretical characterization and cytotoxic activity.
Stevanović, Nevena; Zlatar, Matija; Novaković, Irena; Pevec, Andrej; Radanović, Dušanka; Matić, Ivana Z; Đorđić Crnogorac, Marija; Stanojković, Tatjana; Vujčić, Miroslava; Gruden, Maja; Sladić, Dušan; Anđelković, Katarina; Turel, Iztok; Čobeljić, Božidar; Dalton transactions (Cambridge, England : 2003) 51 (2021) 185–196; doi:10.1039/d1dt03169d

data_7709050
_publ_section_title
;
 Cu(II), Mn(II) and Zn(II) complexes of hydrazones with a quaternary
 ammonium moiety: synthesis, experimental and theoretical characterization
 and cytotoxic activity.
;
_journal_issue                   1
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              185
_journal_page_last               196
_journal_paper_doi               10.1039/d1dt03169d
_journal_volume                  51
_journal_year                    2021
_chemical_formula_sum            'C11 H20 B Cu F4 N7 O2 S'
_chemical_formula_weight         464.75
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2021-11-08 deposited with the CCDC.	2021-11-22 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 97.242(4)
_cell_angle_gamma                90
_cell_formula_units_Z            4
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_cell_length_b                   10.8941(3)
_cell_length_c                   25.6059(9)
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_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      30.1670
_cell_measurement_theta_min      3.4380
_cell_volume                     1938.01(12)
_computing_cell_refinement       'CrysAlis PRO (Agilent, 2011)'
_computing_data_collection       'CrysAlis PRO (Agilent, 2011)'
_computing_data_reduction        'CrysAlis PRO (Agilent, 2011)'
_computing_molecular_graphics    'ORTEP-3 for Windows (Farrugia, 2012)'
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_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_type           MoK\a
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_refine_ls_R_factor_all          0.0471
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_refine_ls_shift/su_max          0.0001
_refine_ls_shift/su_mean         0.0001
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0500P)^2^+0.9688P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_gt                3789
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_reflns_threshold_expression     'I > 2\s(I)'
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'Adding full bibliography for 7709050--7709052.cif.'
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