LMucko/crystallography-open-database huggingface dataset:
Crystal structure evolution and luminescence properties of color tunable solid solution phosphors Ca2+xLa8-x(SiO4)6-x(PO4)xO2:Eu2+
Yufei Xia; Jian Chen; Yan-gai Liu; Maxim S. Molokeev; Ming Guan; Zhaohui Huang; Minghao Fang; Dalton Transactions 45 (2016) 1007–1015; doi:10.1039/C5DT03786G

data_7038851
_publ_section_title
;
 Crystal structure evolution and luminescence properties of color tunable
 solid solution phosphors Ca2+xLa8-x(SiO4)6-x(PO4)xO2:Eu2+
;
_journal_issue                   3
_journal_name_full               'Dalton Transactions'
_journal_page_first              1007
_journal_page_last               1015
_journal_paper_doi               10.1039/C5DT03786G
_journal_volume                  45
_journal_year                    2016
_chemical_formula_moiety         'La7.13 O26 Si6, 2.868(Ca)'
_chemical_formula_sum            'Ca2.87 La7.13 O26 Si6'
_chemical_formula_weight         1690.20
_space_group_IT_number           176
_symmetry_cell_setting           hexagonal
_symmetry_space_group_name_Hall  '-P 6c'
_symmetry_space_group_name_H-M   'P 63/m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            1
_cell_length_a                   9.65586(14)
_cell_length_b                   9.65586(14)
_cell_length_c                   7.15289(12)
_cell_measurement_temperature    300
_cell_volume                     577.556(15)
_diffrn_ambient_temperature      300
_diffrn_measurement_device_type
;
D8 ADVANCE Bruker
;
_diffrn_radiation_monochromator  none
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type
;
 Cu K\a~1~~2~
;
_exptl_absorpt_coefficient_mu    108.624
_exptl_crystal_density_diffrn    4.859293
_pd_char_colour
;
colourless
;
_pd_meas_2theta_range_inc        0.02
_pd_meas_2theta_range_max        110
_pd_meas_2theta_range_min        9
_pd_meas_scan_method             step
_pd_proc_ls_pref_orient_corr
;
Anisotropic model of PO. Spherical harmonics 6 ordrer.
 Jarvinen (1993). Application of symmetrized harmonics expansion to correction
of the preferred orientation effect. - J. Appl. Cryst. 26 p525-531.
;
_pd_proc_ls_profile_function     PearsonVII
_pd_proc_ls_prof_R_factor        7.337
_pd_proc_ls_prof_wR_expected     1.311
_pd_proc_ls_prof_wR_factor       10.038
_pd_proc_number_of_points        5050
_pd_spec_mount_mode              reflection
_refine_ls_goodness_of_fit_all   7.655
_refine_ls_R_I_factor            2.27
_refine_ls_shift/su_max          0.01000
_cod_data_source_file            Ca2La8SiO46O2_Eu.cif
_cod_data_source_block           a
_cod_original_cell_volume        577.556(20)
_cod_original_sg_symbol_Hall
;
-P 6c
;
_cod_original_sg_symbol_H-M      P63/m
_cod_original_formula_sum
;
Ca2.87 La7.13 O26 Si6
;
_cod_database_code               7038851
_cod_database_fobs_code          7038851
Crystal structure evolution and luminescence properties of color tunable solid solution phosphors Ca2+xLa8-x(SiO4)6-x(PO4)xO2:Eu2+
Yufei Xia; Jian Chen; Yan-gai Liu; Maxim S. Molokeev; Ming Guan; Zhaohui Huang; Minghao Fang; Dalton Transactions 45 (2016) 1007–1015; doi:10.1039/C5DT03786G

data_7038852
_publ_section_title
;
 Crystal structure evolution and luminescence properties of color tunable
 solid solution phosphors Ca2+xLa8-x(SiO4)6-x(PO4)xO2:Eu2+
;
_journal_issue                   3
_journal_name_full               'Dalton Transactions'
_journal_page_first              1007
_journal_page_last               1015
_journal_paper_doi               10.1039/C5DT03786G
_journal_volume                  45
_journal_year                    2016
_chemical_formula_moiety         'La5.53 O26 P2.47 Si3.53, 4.466(Ca)'
_chemical_formula_sum            'Ca4.47 La5.53 O26 P2.47 Si3.53'
_chemical_formula_weight         1539.38
_space_group_IT_number           176
_symmetry_cell_setting           hexagonal
_symmetry_space_group_name_Hall  '-P 6c'
_symmetry_space_group_name_H-M   'P 63/m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            1
_cell_length_a                   9.59484(58)
_cell_length_b                   9.59484(58)
_cell_length_c                   7.08819(46)
_cell_measurement_temperature    300
_cell_volume                     565.12(6)
_diffrn_ambient_temperature      300
_diffrn_measurement_device_type
;
D8 ADVANCE Bruker
;
_diffrn_radiation_monochromator  none
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type
;
 Cu K\a~1~~2~
;
_exptl_absorpt_coefficient_mu    92.031
_exptl_crystal_density_diffrn    4.521925
_pd_char_colour
;
colourless
;
_pd_meas_2theta_range_inc        0.02
_pd_meas_2theta_range_max        110
_pd_meas_2theta_range_min        9
_pd_meas_scan_method             step
_pd_proc_ls_pref_orient_corr
;
Anisotropic model of PO. Spherical harmonics 6 ordrer.
 Jarvinen (1993). Application of symmetrized harmonics expansion to correction
of the preferred orientation effect. - J. Appl. Cryst. 26 p525-531.
;
_pd_proc_ls_profile_function     PearsonVII
_pd_proc_ls_prof_R_factor        8.063
_pd_proc_ls_prof_wR_expected     1.299
_pd_proc_ls_prof_wR_factor       11.012
_pd_proc_number_of_points        5050
_pd_spec_mount_mode              reflection
_refine_ls_goodness_of_fit_all   8.474
_refine_ls_R_I_factor            2.17
_refine_ls_shift/su_max          0.01000
_cod_data_source_file            Ca4La6SiO44PO42O2_Eu.cif
_cod_data_source_block           a
_cod_original_cell_volume        565.121(78)
_cod_original_sg_symbol_Hall
;
-P 6c
;
_cod_original_sg_symbol_H-M      P63/m
_cod_original_formula_sum
;
Ca4.47 La5.53 O26 P2.47 Si3.53
;
_cod_database_code               7038852
_cod_database_fobs_code          7038852
Crystal structure evolution and luminescence properties of color tunable solid solution phosphors Ca2+xLa8-x(SiO4)6-x(PO4)xO2:Eu2+
Yufei Xia; Jian Chen; Yan-gai Liu; Maxim S. Molokeev; Ming Guan; Zhaohui Huang; Minghao Fang; Dalton Transactions 45 (2016) 1007–1015; doi:10.1039/C5DT03786G

data_7038853
_publ_section_title
;
 Crystal structure evolution and luminescence properties of color tunable
 solid solution phosphors Ca2+xLa8-x(SiO4)6-x(PO4)xO2:Eu2+
;
_journal_issue                   3
_journal_name_full               'Dalton Transactions'
_journal_page_first              1007
_journal_page_last               1015
_journal_paper_doi               10.1039/C5DT03786G
_journal_volume                  45
_journal_year                    2016
_chemical_formula_moiety         'La3.48 O26 P4.52 Si1.48, 6.524(Ca)'
_chemical_formula_sum            'Ca6.52 La3.48 O26 P4.52 Si1.48'
_chemical_formula_weight         1341.90
_space_group_IT_number           176
_symmetry_cell_setting           hexagonal
_symmetry_space_group_name_Hall  '-P 6c'
_symmetry_space_group_name_H-M   'P 63/m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            1
_cell_length_a                   9.53251(43)
_cell_length_b                   9.53251(43)
_cell_length_c                   7.02062(36)
_cell_measurement_temperature    300
_cell_volume                     552.49(5)
_diffrn_ambient_temperature      300
_diffrn_measurement_device_type
;
D8 ADVANCE Bruker
;
_diffrn_radiation_monochromator  none
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type
;
 Cu K\a~1~~2~
;
_exptl_absorpt_coefficient_mu    68.939
_exptl_crystal_density_diffrn    4.032758
_pd_char_colour
;
colourless
;
_pd_meas_2theta_range_inc        0.02
_pd_meas_2theta_range_max        110
_pd_meas_2theta_range_min        9
_pd_meas_scan_method             step
_pd_proc_ls_pref_orient_corr
;
Anisotropic model of PO. Spherical harmonics 6 ordrer.
 Jarvinen (1993). Application of symmetrized harmonics expansion to correction
of the preferred orientation effect. - J. Appl. Cryst. 26 p525-531.
;
_pd_proc_ls_profile_function     PearsonVII
_pd_proc_ls_prof_R_factor        7.634
_pd_proc_ls_prof_wR_expected     1.287
_pd_proc_ls_prof_wR_factor       10.135
_pd_proc_number_of_points        5050
_pd_spec_mount_mode              reflection
_refine_ls_goodness_of_fit_all   7.874
_refine_ls_R_I_factor            1.79
_refine_ls_shift/su_max          0.01000
_cod_data_source_file            Ca6La4SiO42PO44O2_Eu.cif
_cod_data_source_block           a
_cod_original_cell_volume        552.485(58)
_cod_original_sg_symbol_Hall
;
-P 6c
;
_cod_original_sg_symbol_H-M      P63/m
_cod_original_formula_sum
;
Ca6.52 La3.48 O26 P4.52 Si1.48
;
_cod_database_code               7038853
_cod_database_fobs_code          7038853
Crystal structure evolution and luminescence properties of color tunable solid solution phosphors Ca2+xLa8-x(SiO4)6-x(PO4)xO2:Eu2+
Yufei Xia; Jian Chen; Yan-gai Liu; Maxim S. Molokeev; Ming Guan; Zhaohui Huang; Minghao Fang; Dalton Transactions 45 (2016) 1007–1015; doi:10.1039/C5DT03786G

data_7038854
_publ_section_title
;
 Crystal structure evolution and luminescence properties of color tunable
 solid solution phosphors Ca2+xLa8-x(SiO4)6-x(PO4)xO2:Eu2+
;
_journal_issue                   3
_journal_name_full               'Dalton Transactions'
_journal_page_first              1007
_journal_page_last               1015
_journal_paper_doi               10.1039/C5DT03786G
_journal_volume                  45
_journal_year                    2016
_chemical_formula_moiety         'La1.72 O26 P6, 8.284(Ca)'
_chemical_formula_sum            'Ca8.28 La1.72 O26 P6'
_chemical_formula_weight         1173.05
_space_group_IT_number           176
_symmetry_cell_setting           hexagonal
_symmetry_space_group_name_Hall  '-P 6c'
_symmetry_space_group_name_H-M   'P 63/m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            1
_cell_length_a                   9.46060(18)
_cell_length_b                   9.46060(18)
_cell_length_c                   6.93560(13)
_cell_measurement_temperature    300
_cell_volume                     537.591(18)
_diffrn_ambient_temperature      300
_diffrn_measurement_device_type
;
D8 ADVANCE Bruker
;
_diffrn_radiation_monochromator  none
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type
;
 Cu K\a~1~~2~
;
_exptl_absorpt_coefficient_mu    48.747
_exptl_crystal_density_diffrn    3.623
_pd_char_colour
;
colourless
;
_pd_meas_2theta_range_inc        0.02
_pd_meas_2theta_range_max        110
_pd_meas_2theta_range_min        9
_pd_meas_scan_method             step
_pd_proc_ls_pref_orient_corr
;
Anisotropic model of PO. Spherical harmonics 6 ordrer.
 Jarvinen (1993). Application of symmetrized harmonics expansion to correction
of the preferred orientation effect. - J. Appl. Cryst. 26 p525-531.
;
_pd_proc_ls_profile_function     PearsonVII
_pd_proc_ls_prof_R_factor        7.533
_pd_proc_ls_prof_wR_expected     1.325
_pd_proc_ls_prof_wR_factor       10.065
_pd_proc_number_of_points        5050
_pd_spec_mount_mode              reflection
_refine_ls_goodness_of_fit_all   7.598
_refine_ls_R_I_factor            2.78
_refine_ls_shift/su_max          0.01000
_cod_data_source_file            Ca8PO46O2_Eu.cif
_cod_data_source_block           a
_cod_original_cell_volume        537.591(23)
_cod_original_sg_symbol_Hall
;
-P 6c
;
_cod_original_sg_symbol_H-M      P63/m
_cod_original_formula_sum
;
Ca8.28 La1.72 O26 P6
;
_cod_database_code               7038854
_cod_database_fobs_code          7038854
Structure and luminescence properties of Eu2+ doped LuxSr2-xSiNxO4-x phosphors evolved from chemical unit cosubstitution
Zhiguo Xia; Shihai Miao; Maxim S. Molokeev; Mingyue Chen; Quanlin Liu; Journal of Materials Chemistry C 4 (2016) 1336–1344; doi:10.1039/C5TC04222D

data_7224682
_publ_section_title
;
 Structure and luminescence properties of Eu2+ doped LuxSr2-xSiNxO4-x
 phosphors evolved from chemical unit cosubstitution
;
_journal_issue                   0
_journal_name_full               'Journal of Materials Chemistry C'
_journal_page_first              1336
_journal_page_last               1344
_journal_paper_doi               10.1039/C5TC04222D
_journal_volume                  4
_journal_year                    2016
_chemical_formula_moiety         'Eu0.13 O16 Si4, 3.944(Sr2)'
_chemical_formula_sum            'Eu0.13 O16 Si4 Sr7.89'
_chemical_formula_weight         1078.96
_space_group_IT_number           62
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            1
_cell_length_a                   7.075148(88)
_cell_length_b                   5.664368(77)
_cell_length_c                   9.73139(13)
_cell_measurement_temperature    300
_cell_volume                     389.998(9)
_diffrn_ambient_temperature      300
_diffrn_measurement_device_type
;
D8 ADVANCE Bruker
;
_diffrn_radiation_monochromator  none
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type
;
 Cu K\a~1~~2~
;
_exptl_absorpt_coefficient_mu    41.341
_exptl_crystal_density_diffrn    4.585732
_pd_char_colour
;
colourless
;
_pd_meas_2theta_range_inc        0.02
_pd_meas_2theta_range_max        90
_pd_meas_2theta_range_min        5
_pd_meas_scan_method             step
_pd_proc_ls_pref_orient_corr
;
Anisotropic model of PO. Spherical harmonics 4 ordrer.
 Jarvinen (1993). Application of symmetrized harmonics expansion to correction
of the preferred orientation effect. - J. Appl. Cryst. 26 p525-531.
;
_pd_proc_ls_profile_function     PearsonVII
_pd_proc_ls_prof_R_factor        4.586
_pd_proc_ls_prof_wR_expected     4.269
_pd_proc_ls_prof_wR_factor       6.104
_pd_proc_number_of_points        4250
_pd_spec_mount_mode              reflection
_refine_ls_goodness_of_fit_all   1.430
_refine_ls_R_I_factor            1.88
_refine_ls_shift/su_max          0.01000
_cod_data_source_file            Sr1p97Eu0p03SiO4.cif
_cod_data_source_block           a
_cod_original_cell_volume        389.9977(88)
_cod_original_sg_symbol_Hall
;
-P 2ac 2n
;
_cod_original_sg_symbol_H-M      Pnma
_cod_original_formula_sum
;
Eu0.13 O16 Si4 Sr7.89
;
_cod_database_code               7224682
_cod_database_fobs_code          7224682
Structure and luminescence properties of Eu2+ doped LuxSr2-xSiNxO4-x phosphors evolved from chemical unit cosubstitution
Zhiguo Xia; Shihai Miao; Maxim S. Molokeev; Mingyue Chen; Quanlin Liu; Journal of Materials Chemistry C 4 (2016) 1336–1344; doi:10.1039/C5TC04222D

data_7224683
_publ_section_title
;
 Structure and luminescence properties of Eu2+ doped LuxSr2-xSiNxO4-x
 phosphors evolved from chemical unit cosubstitution
;
_journal_issue                   0
_journal_name_full               'Journal of Materials Chemistry C'
_journal_page_first              1336
_journal_page_last               1344
_journal_paper_doi               10.1039/C5TC04222D
_journal_volume                  4
_journal_year                    2016
_chemical_formula_moiety         'Eu0.12 Lu0.02 O16 Si4, 3.93(Sr2)'
_chemical_formula_sum            'Eu0.12 Lu0.02 O16 Si4 Sr7.86'
_chemical_formula_weight         1078.77
_space_group_IT_number           62
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            1
_cell_length_a                   7.073702(73)
_cell_length_b                   5.667776(61)
_cell_length_c                   9.73626(10)
_cell_measurement_temperature    300
_cell_volume                     390.348(7)
_diffrn_ambient_temperature      300
_diffrn_measurement_device_type
;
D8 ADVANCE Bruker
;
_diffrn_radiation_monochromator  none
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type
;
 Cu K\a~1~~2~
;
_exptl_absorpt_coefficient_mu    41.126
_exptl_crystal_density_diffrn    4.588072
_pd_char_colour
;
colourless
;
_pd_meas_2theta_range_inc        0.02
_pd_meas_2theta_range_max        120
_pd_meas_2theta_range_min        5
_pd_meas_scan_method             step
_pd_proc_ls_pref_orient_corr
;
Anisotropic model of PO. Spherical harmonics 4 ordrer.
 Jarvinen (1993). Application of symmetrized harmonics expansion to correction
of the preferred orientation effect. - J. Appl. Cryst. 26 p525-531.
;
_pd_proc_ls_profile_function     PearsonVII
_pd_proc_ls_prof_R_factor        5.315
_pd_proc_ls_prof_wR_expected     4.440
_pd_proc_ls_prof_wR_factor       7.143
_pd_proc_number_of_points        5750
_pd_spec_mount_mode              reflection
_refine_ls_goodness_of_fit_all   1.609
_refine_ls_R_I_factor            2.09
_refine_ls_shift/su_max          0.01000
_cod_data_source_file            Sr1p965Lu0p005Eu0p03SiO3p995N0p005.cif
_cod_data_source_block           a
_cod_original_cell_volume        390.3479(71)
_cod_original_sg_symbol_Hall
;
-P 2ac 2n
;
_cod_original_sg_symbol_H-M      Pnma
_cod_original_formula_sum
;
Eu0.12 Lu0.02 O16 Si4 Sr7.86
;
_cod_database_code               7224683
_cod_database_fobs_code          7224683
New garnet structure phosphors, Lu3-xYxMgAl3SiO12:Ce3+ (x = 0, 1, 2, 3), developed by solid solution design
Haipeng Ji; Le Wang; Maxim Molokeev; Naoto Hirosaki; Zhaohui Huang; Zhiguo Xia; Otmar Melvin ten Kate; Lihong Liu; Rong-Jun Xie; Journal of Materials Chemistry C 4 (2016) 2359–2366; doi:10.1039/c6tc00089d

data_7224684
_publ_section_title
;
 New garnet structure phosphors, Lu3-xYxMgAl3SiO12:Ce3+ (x = 0, 1, 2, 3),
 developed by solid solution design
;
_journal_issue                   12
_journal_name_full               'Journal of Materials Chemistry C'
_journal_page_first              2359
_journal_page_last               2366
_journal_paper_doi               10.1039/c6tc00089d
_journal_volume                  4
_journal_year                    2016
_chemical_formula_moiety         'Al24 Ce0.48 Mg8 O96 Si8 Y23.52'
_chemical_formula_sum            'Al24 Ce0.48 Mg8 O96 Si8 Y23.52'
_chemical_formula_weight         4761.14
_space_group_IT_number           230
_symmetry_cell_setting           cubic
_symmetry_space_group_name_Hall  '-I 4bd 2c 3'
_symmetry_space_group_name_H-M   'I a -3 d'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            1
_cell_length_a                   12.058912(96)
_cell_length_b                   12.058912(96)
_cell_length_c                   12.058912(96)
_cell_measurement_reflns_used    104
_cell_measurement_temperature    300
_cell_measurement_theta_max      60
_cell_measurement_theta_min      7.5
_cell_volume                     1753.58(2)
_diffrn_ambient_temperature      300
_diffrn_measurement_device_type
;
D8 ADVANCE Bruker
;
_diffrn_radiation_monochromator  none
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type
;
 Cu K\a~1~~2~
;
_exptl_absorpt_coefficient_mu    33.683
_exptl_crystal_density_diffrn    4.508717(17)
_pd_char_colour
;
colourless
;
_pd_meas_2theta_range_inc        0.02
_pd_meas_2theta_range_max        60
_pd_meas_2theta_range_min        7.5
_pd_meas_scan_method             step
_pd_proc_ls_pref_orient_corr
;
no preferred orientation
;
_pd_proc_ls_profile_function     PearsonVII
_pd_proc_ls_prof_R_factor        10.645
_pd_proc_ls_prof_wR_expected     8.764
_pd_proc_ls_prof_wR_factor       14.041
_pd_proc_number_of_points        5250
_pd_spec_mount_mode              reflection
_refine_ls_goodness_of_fit_all   1.602
_refine_ls_R_I_factor            1.96
_refine_ls_shift/su_max          0.01000
_cod_data_source_file            Y2.94Ce0.06MgAl3SiO12.cif
_cod_data_source_block           a
_cod_original_cell_volume        1753.575(42)
_cod_original_sg_symbol_Hall
;
-I 4bd 2c 3
;
_cod_original_sg_symbol_H-M      Ia-3d
_cod_original_formula_sum
;
Al24 Ce0.48 Mg8 O96 Si8 Y23.52
;
_cod_database_code               7224684
_cod_database_fobs_code          7224684
New garnet structure phosphors, Lu3-xYxMgAl3SiO12:Ce3+ (x = 0, 1, 2, 3), developed by solid solution design
Haipeng Ji; Le Wang; Maxim Molokeev; Naoto Hirosaki; Zhaohui Huang; Zhiguo Xia; Otmar Melvin ten Kate; Lihong Liu; Rong-Jun Xie; Journal of Materials Chemistry C 4 (2016) 2359–2366; doi:10.1039/c6tc00089d

data_7224685
_publ_section_title
;
 New garnet structure phosphors, Lu3-xYxMgAl3SiO12:Ce3+ (x = 0, 1, 2, 3),
 developed by solid solution design
;
_journal_issue                   12
_journal_name_full               'Journal of Materials Chemistry C'
_journal_page_first              2359
_journal_page_last               2366
_journal_paper_doi               10.1039/c6tc00089d
_journal_volume                  4
_journal_year                    2016
_chemical_formula_moiety         'Al24 Ce0.48 Lu7.84 Mg8 O96 Si8 Y15.68'
_chemical_formula_sum            'Al24 Ce0.48 Lu7.84 Mg8 O96 Si8 Y15.68'
_chemical_formula_weight         5435.92
_space_group_IT_number           230
_symmetry_cell_setting           cubic
_symmetry_space_group_name_Hall  '-I 4bd 2c 3'
_symmetry_space_group_name_H-M   'I a -3 d'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            1
_cell_length_a                   12.02572(11)
_cell_length_b                   12.02572(11)
_cell_length_c                   12.02572(11)
_cell_measurement_reflns_used    104
_cell_measurement_temperature    300
_cell_measurement_theta_max      60
_cell_measurement_theta_min      7.5
_cell_volume                     1739.13(3)
_diffrn_ambient_temperature      300
_diffrn_measurement_device_type
;
D8 ADVANCE Bruker
;
_diffrn_radiation_monochromator  none
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type
;
 Cu K\a~1~~2~
;
_exptl_absorpt_coefficient_mu    45.999
_exptl_crystal_density_diffrn    5.210(10)
_pd_char_colour
;
colourless
;
_pd_meas_2theta_range_inc        0.02
_pd_meas_2theta_range_max        60
_pd_meas_2theta_range_min        7.5
_pd_meas_scan_method             step
_pd_proc_ls_pref_orient_corr
;
no preferred orientation
;
_pd_proc_ls_profile_function     PearsonVII
_pd_proc_ls_prof_R_factor        8.749
_pd_proc_ls_prof_wR_expected     8.264
_pd_proc_ls_prof_wR_factor       11.811
_pd_proc_number_of_points        5250
_pd_spec_mount_mode              reflection
_refine_ls_goodness_of_fit_all   1.429
_refine_ls_R_I_factor            1.62
_refine_ls_shift/su_max          0.01000
_cod_data_source_file            Lu0.98Y1.96Ce0.06MgAl3SiO12.cif
_cod_data_source_block           a
_cod_original_cell_volume        1739.136(49)
_cod_original_sg_symbol_Hall
;
-I 4bd 2c 3
;
_cod_original_sg_symbol_H-M      Ia-3d
_cod_original_formula_sum
;
Al24 Ce0.48 Lu7.84 Mg8 O96 Si8 Y15.68
;
_cod_database_code               7224685
_cod_database_fobs_code          7224685