Synthesis of the tricyclic skeleton of aberrarone.
Sui, Guoqing; Song, Xiaoqing; Guo, Huihui; Xie, Xiaolan; Ren, Li; Zhou, Wenming; Hao, Hong-Dong; Organic & biomolecular chemistry 23 (2025) 5763–5766; doi:10.1039/d5ob00644a

data_7160562
_publ_section_title
;
 Synthesis of the tricyclic skeleton of aberrarone.
;
_journal_issue                   24
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              5763
_journal_page_last               5766
_journal_paper_doi               10.1039/d5ob00644a
_journal_volume                  23
_journal_year                    2025
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_audit_update_record
;
2020-07-11 deposited with the CCDC.	2025-05-21 downloaded from the CCDC.
;
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_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      296(2)
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0732P)^2^+0.7268P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1663
_refine_ls_wR_factor_ref         0.2144
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_reflns_number_gt                2320
_reflns_number_total             5819
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d5ob00644a2.cif
_cod_data_source_block           sf190606-1_a
_cod_depositor_comments
'Adding full bibliography for 7160561--7160562.cif.'
_cod_database_code               7160562
_shelx_shelxl_version_number     2018/3
_shelx_estimated_absorpt_t_min   0.962
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_shelx_res_checksum              60155