N-bromosuccinimide initiated one-pot synthesis of imidazoline.
Zhou, Ling; Zhou, Jing; Tan, Chong Kiat; Chen, Jie; Yeung, Ying-Yeung; Organic letters 13 (2011) 2448–2451; doi:10.1021/ol2006902

data_1502149
_publ_section_title
;
 N-bromosuccinimide initiated one-pot synthesis of imidazoline.
;
_journal_issue                   9
_journal_name_full               'Organic letters'
_journal_page_first              2448
_journal_page_last               2451
_journal_paper_doi               10.1021/ol2006902
_journal_volume                  13
_journal_year                    2011
_chemical_formula_sum            'C15 H21 Br N2 O2 S'
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_cell_angle_beta                 90.00
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_cell_measurement_temperature    223(2)
_cell_measurement_theta_max      22.24
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_computing_cell_refinement       'Bruker SMART'
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_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      223(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'CCD area detector'
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_exptl_crystal_colour            Colourless
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_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0459P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_data_source_file            ol2006902_si_001.cif
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_cod_depositor_comments
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The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Orthorhombic' changed to
'orthorhombic' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan'
changed to 'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'Not Measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        1712.6(5)
_cod_original_sg_symbol_H-M      Pna2(1)
_cod_database_code               1502149