Structural Characteristics of Aryloxybismuthanes Stabilized by Hypervalent Bond Formation. Synthesis, Incorporation of 4-Methoxyphenol through Hydrogen Bonding, and Crystal Supramolecularity
Murafuji, Toshihiro; Nagasue, Masahiro; Tashiro, Yoshihiro; Sugihara, Yoshikazu; Azuma, Nagao; Organometallics 19 (2000) 1003–; doi:10.1021/om9908534

data_4077685
_publ_section_title
;
 Structural Characteristics of Aryloxybismuthanes Stabilized by
 Hypervalent Bond Formation. Synthesis, Incorporation of 4-Methoxyphenol
 through Hydrogen Bonding, and Crystal Supramolecularity
;
_journal_issue                   6
_journal_name_full               Organometallics
_journal_page_first              1003
_journal_paper_doi               10.1021/om9908534
_journal_volume                  19
_journal_year                    2000
_chemical_formula_moiety         'C26 H23 Bi O6 S '
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_symmetry_cell_setting           monoclinic
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_symmetry_space_group_name_Hall  '-P 2yn'
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_audit_creation_date             '16-MAY-98 21:05:50'
_audit_creation_method           'from TEXRAY.INF file'
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_cell_length_c                   18.232(5)
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_computing_cell_refinement       'MSC/AFC Diffractometer Control'
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_computing_molecular_graphics    TEXSAN
_computing_publication_material  TEXSAN
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_computing_structure_solution    TEXSAN
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_diffrn_measurement_method       \w-2\q
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_diffrn_standards_decay_%        0.22
_diffrn_standards_interval_count 150
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;
?
;
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_refine_ls_shift/esd_max         0.0018
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/\s^2^(Fo)'
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_ref         0.0406
_reflns_number_gt                3211
_reflns_number_total             5965
_reflns_threshold_expression     >2.0sigma(I)
_cod_data_source_file            om9908534.cif
_cod_data_source_block           Bi-Compound-3_(compound_3_in_the_manuscript)
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 

The following automatic conversions were performed:

data name '_exptl_crystal_color' was replaced with
'_exptl_crystal_colour' as specified in the replacement file
'data/replacement-values/replacement_tags.lst'.

Automatic conversion script
Id: cif_correct_tags 9268 2022-04-12 08:56:07Z antanas 
;
_cod_original_cell_volume        2428(1)
_cod_original_sg_symbol_H-M      'P 21/N '
_cod_original_formula_sum        'C26 H23 Bi O6 S '
_cod_database_code               4077685