Structural Variation of Dinuclear Transition Metal Compounds with a Common Type of Ligand: Solid State and Solution Structures and Model Studies
Peter Comba; Sergey P. Gavrish; Robert W. Hay; Peter Hilfenhaus; Yaroslaw D. Lampeka; Philip Lightfoot; Alexander Peters; Inorganic Chemistry 38 (1999) 1416–1421; doi:10.1021/ic9807184

data_4321861
_publ_section_title
;
 Structural Variation of Dinuclear Transition Metal Compounds with a
 Common Type of Ligand: Solid State and Solution Structures and Model
 Studies
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1416
_journal_page_last               1421
_journal_paper_doi               10.1021/ic9807184
_journal_volume                  38
_journal_year                    1999
_chemical_formula_sum            'C18 H58 Cu2 N8 O18'
_chemical_formula_weight         801.79
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_audit_creation_date             'Thu Jul  9 10:54:34 1998'
_audit_creation_method           'from TEXRAY.INF file'
_cell_angle_alpha                90
_cell_angle_beta                 103.91(3)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   8.739(4)
_cell_length_b                   12.140(4)
_cell_length_c                   17.207(6)
_cell_measurement_reflns_used    20
_cell_measurement_temperature    566.2
_cell_measurement_theta_max      15.0
_cell_measurement_theta_min      6.0
_cell_volume                     1772.0(12)
_computing_cell_refinement       'MSC/AFC Diffractometer Control'
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_computing_data_reduction        teXsan
_computing_publication_material  teXsan
_computing_structure_refinement  teXsan
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_diffrn_measurement_device       AFC7S
_diffrn_measurement_method       'omega/2-theta scans'
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_diffrn_orient_matrix_UB_33      -0.05361
_diffrn_radiation_monochromator  graphite
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_diffrn_reflns_limit_h_max       9
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_diffrn_reflns_limit_k_min       -8
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_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    1.281
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            blue
_exptl_crystal_density_diffrn    1.503
_exptl_crystal_description       block
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_refine_ls_structure_factor_coef F
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_cod_data_source_file            ic9807184_1.cif
_cod_data_source_block           IC9807184-1
_cod_original_cell_volume        1771(1)
_cod_original_sg_symbol_H-M      'P 21/n '
_cod_original_formula_sum        'C18 H58 Cu2 N8 O18 '
_cod_database_code               4321861
_cod_database_fobs_code          4321861