<i>cis</i>-Amminedichloroisopropylamineplatinum(II) by X-ray powder diffraction analysis
Kirik, Sergei D.; Starkov, Aleksandr K.; Kozhuhovskay, Galina A.; Acta Crystallographica Section C 62 (2006) m249–m251; doi:10.1107/S0108270106013503

data_2015346
_publ_section_title
;
 <i>cis</i>-Amminedichloroisopropylamineplatinum(II) by X-ray powder
 diffraction analysis
;
_journal_coeditor_code           DN3009
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m249
_journal_page_last               m251
_journal_paper_doi               10.1107/S0108270106013503
_journal_volume                  62
_journal_year                    2006
_chemical_formula_analytical     'Pt (N H3) (N H2 C3 H7) Cl2'
_chemical_formula_iupac          '[Pt Cl2 (C3 H9 N1) (N H3)]'
_chemical_formula_moiety         'C3 H12 Cl2 N2 Pt'
_chemical_formula_structural     'cis-Pt (N H3) (N H2 C3 H7) Cl2'
_chemical_formula_sum            'C3 H12 Cl2 N2 Pt'
_chemical_formula_weight         342.14
_chemical_name_common
'cis-(isopropylamine) ammine dichloro platinum(II)'
_chemical_name_systematic
;
cis-Amminedichloroisopropylamineplatinum(II)
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yab'
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_cell_angle_alpha                90.000
_cell_angle_beta                 108.3860(10)
_cell_angle_gamma                90.000
_cell_formula_units_Z            4
_cell_length_a                   10.3661(2)
_cell_length_b                   9.5622(2)
_cell_length_c                   9.1261(2)
_cell_measurement_temperature    293
_cell_volume                     858.43(3)
_computing_cell_refinement       'POWDER (Kirik <i>et al.</i>,  1979)'
_computing_data_collection       'DRON-4 data collection software'
_computing_data_reduction        '[Please provide missing details]'
_computing_molecular_graphics    'XP (Siemens, 1989)'
_computing_publication_material  '[Please provide missing details]'
_computing_structure_refinement  'DBWM, modified'
_computing_structure_solution    'DBWM (Wiles & Young, 1981), modified'
_diffrn_ambient_temperature      293
_diffrn_measurement_device       'DRON-4 powder diffractometer'
_diffrn_measurement_method       \q/2\q
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'conventional sealed tube'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.5418
_diffrn_reflns_av_R_equivalents  0
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_diffrn_reflns_limit_h_min       0
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_diffrn_reflns_limit_l_min       -8
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_diffrn_reflns_theta_max         45.0
_diffrn_reflns_theta_min         2.5
_exptl_absorpt_coefficient_mu    35.648
_exptl_absorpt_correction_type   none
_exptl_absorpt_process_details   none
_exptl_crystal_density_diffrn    2.647
_exptl_crystal_F_000             624.0
_refine_ls_goodness_of_fit_all   1.29
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_constraints    0
_refine_ls_number_parameters     58
_refine_ls_number_restraints     0
_refine_ls_shift/su_max          0.1
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_scheme      sigma
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