Crystal structure of an organic–inorganic hybrid compound based on morpholinium cations and a β-type Anderson polyanion
Lukianova, Tamara J.; Kinzhybalo, Vasyl; Pietraszko, Adam; Acta Crystallographica Section E 71 (2015) 1345–1348; doi:10.1107/S2056989015019246

data_2241247
_publ_section_title
;
 Crystal structure of an organic--inorganic hybrid compound based on
 morpholinium cations and a \b-type Anderson polyanion
;
_journal_coeditor_code           WM5221
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              1345
_journal_page_last               1348
_journal_paper_doi               10.1107/S2056989015019246
_journal_volume                  71
_journal_year                    2015
_chemical_formula_iupac
'(C4 H10 N O)5 [Fe (O H)6 Mo6 O18] (S O4), 3.5H2 O'
_chemical_formula_moiety
'5(C4 H10 N O +), Fe H6 Mo6 O24 3-, O4 S 2-, 3.5H2 O'
_chemical_formula_sum            'C20 H63 Fe Mo6 N5 O36.5 S'
_chemical_formula_weight         1621.30
_chemical_name_systematic
;
Pentamorpholinium hexahydrogen hexamolybdoferrate(III) sulfate 3.5-hydrate
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
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Olex2 1.2
(compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998)
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;
CrysAlis PRO (Rigaku Oxford Diffraction, 2015)
;
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CrysAlis PRO (Rigaku Oxford Diffraction, 2015)
;
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CrysAlis PRO (Rigaku Oxford Diffraction, 2015)
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DIAMOND (Brandenburg, 1997)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>,  2009)
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SHELXL2014 (Sheldrick, 2015)
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SHELXS97 (Sheldrick, 2008)
;
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;
(CrysAlisPro; Rigaku Oxford Diffraction, 2015)
;
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0601P)^2^+2.7906P] where P=(Fo^2^+2Fc^2^)/3'
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