Co-organizing synthesis of heterogeneous nanostructures through the photo-cleavage of pre-stabilized self-assemblies.
Ji, Wei; Zhang, Shijin; Filonenko, Georgy A.; Li, Guanying; Sasaki, Toshio; Feng, Chuanliang; Zhang, Ye; Chemical communications (Cambridge, England) 53 (2017) 4702–4705; doi:10.1039/c7cc01912b

data_7119884
_publ_section_title
;
 Co-organizing synthesis of heterogeneous nanostructures through the
 photo-cleavage of pre-stabilized self-assemblies.
;
_journal_issue                   34
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              4702
_journal_page_last               4705
_journal_paper_doi               10.1039/c7cc01912b
_journal_volume                  53
_journal_year                    2017
_chemical_formula_moiety         'C17 H12 O5'
_chemical_formula_sum            'C17 H12 O5'
_chemical_formula_weight         296.27
_chemical_name_systematic        '4-(hydroxymethyl)coumarin 7-benzoate'
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_space_group_name_Hall           '-P 1'
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_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   mixed
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;
2017-02-08 deposited with the CCDC.
2017-04-03 downloaded from the CCDC.
;
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_cell_measurement_temperature    93(2)
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_cell_volume                     655.52(6)
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_computing_data_reduction        'CrysAlisPro 1.171.39.7b (Rigaku OD, 2015)'
_computing_molecular_graphics
'WinGX (Farrugia, 2012); ORTEP-3 (Farrugia, 2012); PLATON (Spek, 2009)'
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_computing_structure_solution    'SHELXT-2014/5 (Sheldrick, 2015)'
_diffrn_ambient_temperature      93(2)
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_diffrn_measured_fraction_theta_max 0.913
_diffrn_measurement_device       'four-circle diffractometer'
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_diffrn_reflns_av_unetI/netI     0.0735
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.913
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_diffrn_reflns_limit_l_min       -13
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_diffrn_source                   'microfocus sealed X-ray tube'
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;
CrysAlisPro 1.171.39.7b (Rigaku Oxford Diffraction, 2015).
Numerical absorption correction based on gaussian integration over 
a multifaceted crystal model. Empirical absorption correction using 
spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.501
_exptl_crystal_description       plate
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_exptl_crystal_recrystallization_method
'slow evaporation from hexane/methylene chloride'
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_refine_ls_extinction_method     none
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_refine_ls_number_restraints     0
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0840P)^2^+0.0190P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.1434
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2365
_reflns_number_total             2901
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c7cc01912b2.cif
_cod_data_source_block           jk093
_cod_depositor_comments          'Adding full bibliography for 7119884.cif.'
_cod_database_code               7119884
_shelx_shelxl_version_number     2016/6
_shelx_estimated_absorpt_t_min   0.976
_shelx_estimated_absorpt_t_max   0.995
_shelx_res_checksum              21822
_shelx_hkl_checksum              31933