Supramolecular triangular and linear arrays of metal-radical solids using pyrazolato-silver(I) motifs.
Yamada, Susumu; Ishida, Takayuki; Nogami, Takashi; Dalton transactions (Cambridge, England : 2003)  (2004) 898–903; doi:10.1039/b312406a

data_7013696
_publ_section_title
;
 Supramolecular triangular and linear arrays of metal-radical solids
 using pyrazolato-silver(I) motifs.
;
_journal_issue                   6
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              898
_journal_page_last               903
_journal_paper_doi               10.1039/b312406a
_journal_year                    2004
_chemical_formula_moiety         'C10 H14 Ag N4 O '
_chemical_formula_sum            'C10 H14 Ag N4 O'
_chemical_formula_weight         314.11
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2yab'
_symmetry_space_group_name_H-M   'P 1 21/a 1'
_cell_angle_alpha                90
_cell_angle_beta                 115.497(3)
_cell_angle_gamma                90
_cell_formula_units_Z            12
_cell_length_a                   14.1412(7)
_cell_length_b                   18.504(1)
_cell_length_c                   15.1158(8)
_cell_measurement_reflns_used    24003
_cell_measurement_temperature    90.0
_cell_measurement_theta_max      25.0
_cell_measurement_theta_min      1.9
_cell_volume                     3570.1(3)
_computing_cell_refinement       PROCESS-AUTO
_computing_data_collection       PROCESS-AUTO
_computing_data_reduction        'teXsan Ver. 1.11'
_computing_publication_material  'teXsan Ver. 1.11'
_computing_structure_refinement  'teXsan Ver. 1.10'
_computing_structure_solution    SIR92
_diffrn_detector_area_resol_mean 10.00
_diffrn_measured_fraction_theta_full 0.9684
_diffrn_measured_fraction_theta_max 0.9684
_diffrn_measurement_device_type  'Rigaku RAXIS-RAPID Imaging Plate'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.065
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            21590
_diffrn_reflns_theta_full        26.25
_diffrn_reflns_theta_max         26.25
_exptl_absorpt_coefficient_mu    1.674
_exptl_absorpt_correction_T_max  0.946
_exptl_absorpt_correction_T_min  0.612
_exptl_absorpt_correction_type   integration
_exptl_absorpt_process_details   '(Higashi, 1999)'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.753
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       platelet
_exptl_crystal_size_max          0.400
_exptl_crystal_size_mid          0.300
_exptl_crystal_size_min          0.020
_refine_diff_density_max         1.87
_refine_diff_density_min         -2.01
_refine_ls_extinction_coef       0.0000(2)
_refine_ls_extinction_method     'Zachariasen(1967) type 2 Gaussian isotropic'
_refine_ls_goodness_of_fit_ref   1.438
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     434
_refine_ls_number_reflns         6963
_refine_ls_R_factor_gt           0.0699
_refine_ls_shift/su_max          0.0002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^) + (0.07300(Max(Fo^2^,0) + 2Fc^2^)/3)^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1706
_reflns_number_gt                5257
_reflns_number_total             6968
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
_cod_data_source_file            b312406a.txt
_cod_data_source_block           '[Ag(pzIN)]6_'
_cod_original_formula_sum        'C10 H14 Ag N4 O '
_cod_database_code               7013696