Magnetic remanence in Yb14−RE MnSb11 (RE=Tb, Dy, Ho) single crystals
Grebenkemper, Jason H.; Hu, Yufei; Abdusalyamova, M.N.; Makhmudov, F.A.; Kauzlarich, Susan M.; Journal of Solid State Chemistry 238 (2016) 321–326; doi:10.1016/j.jssc.2016.03.037

data_1561540
_publ_section_title
;
 Magnetic remanence in Yb14&#x2212;RE MnSb11 (RE=Tb, Dy, Ho) single
 crystals
;
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              321
_journal_page_last               326
_journal_paper_doi               10.1016/j.jssc.2016.03.037
_journal_volume                  238
_journal_year                    2016
_chemical_formula_sum            'Mn Sb11 Tb0.4 Yb13.6'
_chemical_formula_weight         3811.10
_space_group_crystal_system      tetragonal
_space_group_IT_number           142
_space_group_name_Hall           '-I 4bd 2c'
_space_group_name_H-M_alt        'I 41/a c d :2'
_atom_sites_solution_hydrogens   .
_audit_creation_method           SHELXL-2014
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   16.5997(19)
_cell_length_b                   16.5997(19)
_cell_length_c                   21.963(3)
_cell_measurement_reflns_used    2349
_cell_measurement_temperature    90
_cell_measurement_theta_max      30.656
_cell_measurement_theta_min      2.454
_cell_volume                     6051.9(13)
_computing_structure_refinement  'SHELXL-2014 (Sheldrick, 2014)'
_diffrn_ambient_temperature      90
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker APEX II'
_diffrn_measurement_method       CCD
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0423
_diffrn_reflns_av_unetI/netI     0.0127
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -23
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -31
_diffrn_reflns_number            45629
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.656
_diffrn_reflns_theta_min         2.454
_exptl_absorpt_coefficient_mu    52.474
_exptl_absorpt_correction_T_max  0.0489
_exptl_absorpt_correction_T_min  0.0160
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            silver
_exptl_crystal_density_diffrn    8.366
_exptl_crystal_description       shard
_exptl_crystal_F_000             12512
_exptl_crystal_size_max          0.146
_exptl_crystal_size_mid          0.115
_exptl_crystal_size_min          0.094
_refine_diff_density_max         1.161
_refine_diff_density_min         -1.177
_refine_diff_density_rms         0.275
_refine_ls_extinction_coef       0.0000458(11)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.486
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     63
_refine_ls_number_reflns         2349
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.486
_refine_ls_R_factor_all          0.0175
_refine_ls_R_factor_gt           0.0173
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+134.2432P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0354
_refine_ls_wR_factor_ref         0.0354
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                2340
_reflns_number_total             2349
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            mmc5.cif
_cod_data_source_block           jhg55
_cod_original_cell_volume        6051.9(16)
_cod_original_sg_symbol_H-M      'I 41/a c d'
_cod_original_formula_sum        'Mn Sb11 Tb0.40 Yb13.60'
_cod_database_code               1561540
_shelx_estimated_absorpt_t_min   0.049
_shelx_estimated_absorpt_t_max   0.083
_shelxl_version_number           2014-3
_shelx_res_checksum              91241
_shelx_hkl_checksum              2436