Poly[(μ~2~-2,2-dimethylpropane-1,3-diyl diisocyanide)-μ~2~-nitrato-silver(I)]: a powder study
Rukiah, Mwaffak; Al-Ktaifani, Mahmoud; Acta Crystallographica Section C 64 (2008) m170–m172; doi:10.1107/S0108270108005143

data_2016565
_publ_section_title
;
 Poly[(\m~2~-2,2-dimethylpropane-1,3-diyl
 diisocyanide)-\m~2~-nitrato-silver(I)]: a powder study
;
_journal_coeditor_code           SK3191
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m170
_journal_page_last               m172
_journal_paper_doi               10.1107/S0108270108005143
_journal_volume                  64
_journal_year                    2008
_chemical_formula_iupac          '[Ag (N O3) (C7 H10 N2)]'
_chemical_formula_moiety         'C7 H10 Ag1 N3 O3'
_chemical_formula_sum            'C7 H10 Ag N3 O3'
_chemical_formula_weight         292
_chemical_name_systematic
;Poly[(\m~2~-2,2-dimethylpropane-1,3-diyl
 diisocyanide)-\m~2~-nitrato-silver(I)]
;
_space_group_IT_number           61
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   16.8649(8)
_cell_length_b                   16.5864(9)
_cell_length_c                   7.4838(4)
_cell_measurement_temperature    295
_cell_volume                     2093.43(19)
_computing_cell_refinement
'JANA2000 (Pet\<r\'i\<cek <i>et al.</i>,  2000)'
_computing_data_collection       'WinXpow (Stoe & Cie, 1999)'
_computing_data_reduction        'WinXpow (Stoe & Cie, 1999)'
_computing_molecular_graphics    'PLATON (Spek, 2003)'
_computing_publication_material
'JANA2000 (Pet\<r\'i\<cek <i>et al.</i>,  2000)'
_computing_structure_refinement
'JANA2000 (Pet\<r\'i\<cek <i>et al.</i>,  2000)'
_computing_structure_solution    'FOX (Favre-Nicolin & \<Cern\'y, 2002)'
_diffrn_ambient_temperature      295
_diffrn_measurement_device_type  'Stoe STADI P transmission'
_diffrn_radiation_monochromator  'Curved Ge 111'
_diffrn_radiation_type           'Cu K\a1'
_diffrn_radiation_wavelength     1.5406
_exptl_absorpt_coefficient_mu    15.388
_exptl_absorpt_correction_T_max  0.3999
_exptl_absorpt_correction_T_min  0.3702
_exptl_absorpt_correction_type   cylinder
_exptl_absorpt_process_details
'(JANA2000; Pet\<r\'i\<cek <i>et al.</i>,  2000)'
_exptl_crystal_density_diffrn    1.8526
_exptl_crystal_F_000             1152
_refine_diff_density_max         0.18
_refine_diff_density_min         -0.22
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   1.27
_refine_ls_hydrogen_treatment    constr
_refine_ls_number_parameters     92
_refine_ls_number_restraints     18
_refine_ls_R_factor_all          0.0252
_refine_ls_R_factor_gt           0.0251
_refine_ls_shift/su_max          0.0477
_refine_ls_shift/su_mean         0.0038
_refine_ls_structure_factor_coef Inet
_refine_ls_weighting_details     mesur
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.0164
_refine_ls_wR_factor_ref         0.0164
_cod_data_source_file            sk3191.cif
_cod_data_source_block           I
_cod_original_formula_sum        'C7 H10 Ag1 N3 O3'
_cod_database_code               2016565