Synthesis and structural trends in a series of simple tetraalkylphosphonium salts
Gawraczyński, Jakub; Leszczyński, Piotr J.; Cyrański, Michał K.; Dobrzycki, Łukasz; Koźmiński, Wiktor; Fijałkowski, Karol J.; Grochala, Wojciech; Jaroń, Tomasz; CrystEngComm 26 (2024) 2673–2682; doi:10.1039/D4CE00210E

data_7248500
_publ_section_title
;
 Synthesis and structural trends in a series of simple
 tetraalkylphosphonium salts
;
_journal_issue                   20
_journal_name_full               CrystEngComm
_journal_page_first              2673
_journal_page_last               2682
_journal_paper_doi               10.1039/D4CE00210E
_journal_volume                  26
_journal_year                    2024
_chemical_formula_moiety         '2(C4 H12 P), O4 S'
_chemical_formula_sum            'C8 H24 O4 P2 S'
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_space_group_IT_number           137
_space_group_name_Hall           'P 4n 2n -1n'
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_symmetry_cell_setting           tetragonal
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_symmetry_space_group_name_Hall  'P 4n 2n -1n'
_symmetry_space_group_name_H-M   'P 42/n m c :1'
_audit_update_record
;
2024-02-27 deposited with the CCDC.	2024-04-15 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_cell_length_b                   7.62801(13)
_cell_length_c                   11.6300(3)
_cell_measurement_temperature    295
_cell_volume                     676.71(2)
_diffrn_ambient_temperature      295
_diffrn_measurement_device_type  'Panalytical X'Pert Pro'
_diffrn_radiation_monochromator  none
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Co K\a'
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_exptl_crystal_density_diffrn    1.3657
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_pd_instr_location               ' ?'
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_pd_meas_scan_method             cont
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_pd_spec_mounting                'quartz capillary'
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_refine_ls_shift/su_max          0.0395
_refine_ls_shift/su_mean         0.0081
_refine_ls_weighting_details     w=1/(\s^2^(I)+0.0016I^2^)
_refine_ls_weighting_scheme      sigma
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_refine_ls_wR_factor_gt          0.0423
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_cod_depositor_comments
'Adding full bibliography for 7248499--7248509.cif.'
_cod_original_sg_symbol_H-M      'P 42/n m c'
_cod_database_code               7248500