Asymmetric three- and [2 + 1]-component conjugate addition reactions for the stereoselective synthesis of polysubstituted piperidinones.
Davies, Stephen G.; Roberts, Paul M.; Smith, Andrew D.; Organic & biomolecular chemistry 5 (2007) 1405–1415; doi:10.1039/b701226h

data_7151100
_publ_section_title
;
 Asymmetric three- and [2 + 1]-component conjugate addition reactions
 for the stereoselective synthesis of polysubstituted piperidinones.
;
_journal_issue                   9
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              1405
_journal_page_last               1415
_journal_paper_doi               10.1039/b701226h
_journal_volume                  5
_journal_year                    2007
_chemical_formula_moiety         'C38 H43 N1 O4'
_chemical_formula_sum            'C38 H43 N O4'
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_space_group_IT_number           19
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_symmetry_space_group_name_Hall  'P 2ac 2ab'
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_computing_cell_refinement
;
DIP2000 software 'DENZO' (Otwinowski & Minor, 1996)
;
_computing_data_collection
;
DIP2000 software 'Xpress' (MAC Science, 1989)
;
_computing_data_reduction
;
DIP2000 software 'DENZO' (Otwinowski & Minor, 1996)
;
_computing_molecular_graphics
;
CAMERON (Watkin, Prout & Pearce, 1996)
;
_computing_publication_material
;
CRYSTALS Issue 10 (Watkin, Prout, Carruthers & Betteridge, 1996)
;
_computing_structure_refinement
;
CRYSTALS Issue 10 (Watkin, Prout, Carruthers & Betteridge, 1996)
;
_computing_structure_solution    'SIR92 (Giacovazzo et al, 1992)'
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;
Enraf-nonius DIP2000
;
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_exptl_crystal_colour            ' colourless '
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_exptl_crystal_description       ' block '
_exptl_crystal_F_000             1240.29
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details
;
Chebychev polynomial with 3 parameters, Carruthers & Watkin , 1979,
2.43 0.858 1.59
;
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_cod_original_formula_sum        'C38 H43 N1 O4'
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