Solid-State Synthesis and Characterization of σ-Alkane Complexes, [Rh(L2)(η(2),η(2)-C7H12)][BAr(F)4] (L2 = Bidentate Chelating Phosphine).
Pike, Sebastian D.; Chadwick, F. Mark; Rees, Nicholas H.; Scott, Mark P.; Weller, Andrew S.; Krämer, Tobias; Macgregor, Stuart A.; Journal of the American Chemical Society 137 (2015) 820–833; doi:10.1021/ja510437p

data_4123243
_publ_section_title
;
 Solid-State Synthesis and Characterization of \s-Alkane Complexes,
 [Rh(L2)(\h(2),\h(2)-C7H12)][BAr(F)4] (L2 = Bidentate Chelating
 Phosphine).
;
_journal_issue                   2
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              820
_journal_page_last               833
_journal_paper_doi               10.1021/ja510437p
_journal_volume                  137
_journal_year                    2015
_chemical_compound_source        'S10, CRL, Uni Oxford'
_chemical_formula_moiety         'C54 H54 B1 F24 P2 Rh1'
_chemical_formula_sum            'C54 H54 B F24 P2 Rh'
_chemical_formula_weight         1334.64
_chemical_melting_point          ?
_chemical_name_systematic        '[Rh(dippp)NBD][BArF4]'
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   difmap
_atom_sites_solution_primary     other
_audit_creation_date             2014-06-23
_audit_creation_method           CRYSTALS_ver_14.43
_cell_angle_alpha                90
_cell_angle_beta                 90.957(2)
_cell_angle_gamma                90
_cell_formula_units_Z            12
_cell_length_a                   17.8334(5)
_cell_length_b                   17.5483(4)
_cell_length_c                   55.0406(15)
_cell_measurement_reflns_used    10371
_cell_measurement_temperature    150
_cell_measurement_theta_max      76
_cell_measurement_theta_min      4
_cell_volume                     17222.3(8)
_computing_cell_refinement       'CrysAlis, (Oxford Diffraction, 2002)'
_computing_data_collection       'SuperNova, (Oxford Diffraction, 2010)'
_computing_data_reduction        'CrysAlis, (Oxford Diffraction, 2002)'
_computing_molecular_graphics    'CAMERON (Watkin et al., 1996)'
_computing_publication_material  'CRYSTALS (Betteridge et al., 2003)'
_computing_structure_refinement  'CRYSTALS (Betteridge et al., 2003)'
_computing_structure_solution    'Superflip (Palatinus & Chapuis, 2007)'
_diffrn_ambient_temperature      150
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.983
_diffrn_measurement_device       Area
_diffrn_measurement_device_type  'Oxford Diffraction SuperNova'
_diffrn_measurement_method       \w
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.54180
_diffrn_reflns_av_R_equivalents  0.233
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       68
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            17822
_diffrn_reflns_theta_full        74.249
_diffrn_reflns_theta_max         76.545
_diffrn_reflns_theta_min         3.534
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    3.968
_exptl_absorpt_correction_T_max  0.89
_exptl_absorpt_correction_T_min  0.43
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'CrysAlis, (Oxford Diffraction, 2002)'
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.544
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             8088
_exptl_crystal_size_max          0.070
_exptl_crystal_size_mid          0.050
_exptl_crystal_size_min          0.030
_refine_diff_density_max         2.35
_refine_diff_density_min         -1.81
_refine_ls_extinction_method     None
_refine_ls_goodness_of_fit_ref   0.9834
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1422
_refine_ls_number_reflns         12965
_refine_ls_number_restraints     2334
_refine_ls_R_factor_all          0.1346
_refine_ls_R_factor_gt           0.1033
_refine_ls_shift/su_max          0.0353889
_refine_ls_shift/su_mean         0.0006512
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
 Method= Modified Sheldrick 
 w=1/[\s^2^(F^2^) + ( 0.15P)^2^ +*****P] 
 ,where P=(max(Fo^2^,0) + 2Fc^2^)/3 
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.2996
_refine_ls_wR_factor_gt          0.2789
_refine_ls_wR_factor_ref         0.2993
_reflns_limit_h_max              22
_reflns_limit_h_min              -22
_reflns_limit_k_max              22
_reflns_limit_k_min              0
_reflns_limit_l_max              68
_reflns_limit_l_min              0
_reflns_number_gt                8547
_reflns_number_total             17822
_reflns_threshold_expression     I>2.0\s(I)
_oxford_diffrn_Wilson_B_factor   3.44
_oxford_diffrn_Wilson_scale      7.52
_oxford_refine_ls_r_factor_ref   0.1345
_oxford_refine_ls_scale          0.4220(11)
_oxford_reflns_number_all        12967
_oxford_reflns_threshold_expression_ref I>-3.0\s(I)
_oxford_structure_analysis_title 058SDP13
_cod_data_source_file            ja510437p_si_001.cif
_cod_data_source_block           '[4-NBD][BArF4]'
_cod_depositor_comments
;
The following automatic conversions were performed:

'_chemical_melting_point' value 'not measured' was changed to '?' -
the value is undefined or not given.

'_atom_sites_solution_primary'
value 'Other' changed to 'other' according to
/home/saulius/struct/COD-crude-data--automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2935 2014-11-11 08:27:57Z andrius 

 Adding full bibliography for 4123238--4123246.cif.
;
_cod_original_sg_symbol_H-M      'C 2/c '
_cod_original_formula_sum        'C54 H54 B1 F24 P2 Rh1'
_cod_database_code               4123243
_iucr_refine_instructions_details_constraints
;
BLOCK SCALE X'S, U'S 
RIDE C   (   1,X'S) H   (  11,X'S) 
RIDE C   (   2,X'S) H   (  21,X'S) 
RIDE C   (   3,X'S) H   (  31,X'S) 
RIDE C   (   4,X'S) H   (  41,X'S) 
RIDE C   (   5,X'S) H   (  51,X'S) 
RIDE C   (   6,X'S) H   (  61,X'S) 
RIDE C   (  10,X'S) H   ( 101,X'S) H   ( 102,X'S) 
RIDE C   (  14,X'S) H   ( 141,X'S) 
RIDE C   (  15,X'S) H   ( 151,X'S) H   ( 152,X'S) H   ( 153,X'S) 
RIDE C   (  16,X'S) H   ( 163,X'S) H   ( 162,X'S) H   ( 161,X'S) 
RIDE C   (  17,X'S) H   ( 171,X'S) 
RIDE C   (  18,X'S) H   ( 183,X'S) H   ( 182,X'S) H   ( 181,X'S) 
RIDE C   (  19,X'S) H   ( 191,X'S) H   ( 192,X'S) H   ( 193,X'S) 
RIDE C   (  20,X'S) H   ( 201,X'S) 
RIDE C   (  21,X'S) H   ( 213,X'S) H   ( 212,X'S) H   ( 211,X'S) 
RIDE C   (  22,X'S) H   ( 221,X'S) H   ( 222,X'S) H   ( 223,X'S) 
RIDE C   ( 101,X'S) H   (1011,X'S) 
RIDE C   ( 102,X'S) H   (1021,X'S) 
RIDE C   ( 103,X'S) H   (1031,X'S) 
RIDE C   ( 104,X'S) H   (1041,X'S) 
RIDE C   ( 107,X'S) H   (1071,X'S) 
RIDE C   ( 108,X'S) H   (1081,X'S) H   (1082,X'S) H   (1083,X'S) 
RIDE C   ( 109,X'S) H   (1093,X'S) H   (1092,X'S) H   (1091,X'S) 
RIDE C   ( 110,X'S) H   (1101,X'S) 
RIDE C   ( 111,X'S) H   (1111,X'S) H   (1112,X'S) H   (1113,X'S) 
RIDE C   ( 112,X'S) H   (1123,X'S) H   (1122,X'S) H   (1121,X'S) 
RIDE C   ( 202,X'S) H   (2021,X'S) 
RIDE C   ( 204,X'S) H   (2041,X'S) 
RIDE C   ( 206,X'S) H   (2061,X'S) 
RIDE C   ( 210,X'S) H   (2101,X'S) 
RIDE C   ( 212,X'S) H   (2121,X'S) 
RIDE C   ( 214,X'S) H   (2141,X'S) 
RIDE C   ( 218,X'S) H   (2181,X'S) 
RIDE C   ( 220,X'S) H   (2201,X'S) 
RIDE C   ( 222,X'S) H   (2221,X'S) 
RIDE C   ( 226,X'S) H   (2261,X'S) 
RIDE C   ( 228,X'S) H   (2281,X'S) 
RIDE C   ( 230,X'S) H   (2301,X'S) 
RIDE C   ( 302,X'S) H   (3021,X'S) 
RIDE C   ( 304,X'S) H   (3041,X'S) 
RIDE C   ( 306,X'S) H   (3061,X'S) 
RIDE C   ( 309,X'S) H   (3091,X'S) 
RIDE C   ( 311,X'S) H   (3111,X'S) 
RIDE C   ( 313,X'S) H   (3131,X'S) 
RIDE C   (  80,X'S) H   ( 801,X'S) H   ( 802,X'S) 
RIDE C   (  81,X'S) H   ( 811,X'S) H   ( 812,X'S) 
RIDE C   (  90,X'S) H   ( 901,X'S) H   ( 902,X'S) 
RIDE C   (  91,X'S) H   ( 912,X'S) H   ( 913,X'S) 
RIDE C   (  70,X'S) H   ( 701,X'S) H   ( 702,X'S) 
RIDE C   (  71,X'S) H   ( 711,X'S) H   ( 712,X'S) 
RIDE C   ( 411,X'S) H   (4111,X'S) 
RIDE C   ( 410,X'S) H   (4101,X'S) 
RIDE C   ( 430,X'S) H   (4301,X'S) H   (4302,X'S) H   (4303,X'S) 
RIDE C   ( 431,X'S) H   (4311,X'S) H   (4312,X'S) H   (4313,X'S) 
RIDE C   ( 420,X'S) H   (4203,X'S) H   (4202,X'S) H   (4201,X'S) 
RIDE C   ( 421,X'S) H   (4211,X'S) H   (4212,X'S) H   (4213,X'S) 
RIDE C   (1050,X'S) H   (1051,X'S) H   (1052,X'S) 
RIDE C   (1051,X'S) H   (1053,X'S) H   (1054,X'S) 
END                                                                             
;
_iucr_refine_instructions_details_restraints
;
NO 
REM   HREST   START (DO NOT REMOVE THIS LINE) 
SAME C(219) C(223) F(130) F(141) F(151) AND 
CONT C(219) C(223) F(141) F(151) F(130) AND 
CONT C(219) C(223) F(151) F(130) F(141) AND 
CONT C(219) C(223) F(131) F(140) F(150) AND 
CONT C(219) C(223) F(140) F(150) F(131) AND 
CONT C(219) C(223) F(150) F(131) F(140) 
DELU 0.015 C(219) C(223) F(130) F(141) F(151) AND 
CONT C(219) C(223) F(141) F(151) F(130) AND 
CONT C(219) C(223) F(151) F(130) F(141) AND 
CONT C(219) C(223) F(131) F(140) F(150) AND 
CONT C(219) C(223) F(140) F(150) F(131) AND 
CONT C(219) C(223) F(150) F(131) F(140) 
SIMU 0.015 C(219) C(223) F(130) F(141) F(151) AND 
CONT C(219) C(223) F(141) F(151) F(130) AND 
CONT C(219) C(223) F(151) F(130) F(141) AND 
CONT C(219) C(223) F(131) F(140) F(150) AND 
CONT C(219) C(223) F(140) F(150) F(131) AND 
CONT C(219) C(223) F(150) F(131) F(140) 
SAME C(205) C(208) F(40) F(50) F(61) AND 
CONT C(205) C(208) F(50) F(61) F(40) AND 
CONT C(205) C(208) F(61) F(40) F(50) AND 
CONT C(205) C(208) F(41) F(51) F(60) AND 
CONT C(205) C(208) F(51) F(60) F(41) AND 
CONT C(205) C(208) F(60) F(41) F(51) 
DELU 0.015 C(205) C(208) F(40) F(50) F(61) AND 
CONT C(205) C(208) F(50) F(61) F(40) AND 
CONT C(205) C(208) F(61) F(40) F(50) AND 
CONT C(205) C(208) F(41) F(51) F(60) AND 
CONT C(205) C(208) F(51) F(60) F(41) AND 
CONT C(205) C(208) F(60) F(41) F(51) 
SIMU 0.015 C(205) C(208) F(40) F(50) F(61) AND 
CONT C(205) C(208) F(50) F(61) F(40) AND 
CONT C(205) C(208) F(61) F(40) F(50) AND 
CONT C(205) C(208) F(41) F(51) F(60) AND 
CONT C(205) C(208) F(51) F(60) F(41) AND 
CONT C(205) C(208) F(60) F(41) F(51) 
SAME C(227) C(231) F(190) F(201) F(211) AND 
CONT C(227) C(231) F(201) F(211) F(190) AND 
CONT C(227) C(231) F(211) F(190) F(201) AND 
CONT C(227) C(231) F(191) F(200) F(210) AND 
CONT C(227) C(231) F(200) F(210) F(191) AND 
CONT C(227) C(231) F(210) F(191) F(200) 
DELU 0.015 C(227) C(231) F(190) F(201) F(211) AND 
CONT C(227) C(231) F(201) F(211) F(190) AND 
CONT C(227) C(231) F(211) F(190) F(201) AND 
CONT C(227) C(231) F(191) F(200) F(210) AND 
CONT C(227) C(231) F(200) F(210) F(191) AND 
CONT C(227) C(231) F(210) F(191) F(200) 
SIMU 0.015 C(227) C(231) F(190) F(201) F(211) AND 
CONT C(227) C(231) F(201) F(211) F(190) AND 
CONT C(227) C(231) F(211) F(190) F(201) AND 
CONT C(227) C(231) F(191) F(200) F(210) AND 
CONT C(227) C(231) F(200) F(210) F(191) AND 
CONT C(227) C(231) F(210) F(191) F(200) 
SAME C(213) C(216) F(101) F(111) F(120) AND 
CONT C(213) C(216) F(111) F(120) F(101) AND 
CONT C(213) C(216) F(120) F(101) F(111) AND 
CONT C(213) C(216) F(100) F(110) F(121) AND 
CONT C(213) C(216) F(110) F(121) F(100) AND 
CONT C(213) C(216) F(121) F(100) F(110) 
DELU 0.015 C(213) C(216) F(101) F(111) F(120) AND 
CONT C(213) C(216) F(111) F(120) F(101) AND 
CONT C(213) C(216) F(120) F(101) F(111) AND 
CONT C(213) C(216) F(100) F(110) F(121) AND 
CONT C(213) C(216) F(110) F(121) F(100) AND 
CONT C(213) C(216) F(121) F(100) F(110) 
SIMU 0.015 C(213) C(216) F(101) F(111) F(120) AND 
CONT C(213) C(216) F(111) F(120) F(101) AND 
CONT C(213) C(216) F(120) F(101) F(111) AND 
CONT C(213) C(216) F(100) F(110) F(121) AND 
CONT C(213) C(216) F(110) F(121) F(100) AND 
CONT C(213) C(216) F(121) F(100) F(110) 
SAME C(305) C(308) F(280) F(291) F(301) AND 
CONT C(305) C(308) F(291) F(301) F(280) AND 
CONT C(305) C(308) F(301) F(280) F(291) AND 
CONT C(305) C(308) F(281) F(290) F(300) AND 
CONT C(305) C(308) F(290) F(300) F(281) AND 
CONT C(305) C(308) F(300) F(281) F(290) 
DELU 0.02 C(305) C(308) F(280) F(291) F(301) AND 
CONT C(305) C(308) F(291) F(301) F(280) AND 
CONT C(305) C(308) F(301) F(280) F(291) AND 
CONT C(305) C(308) F(281) F(290) F(300) AND 
CONT C(305) C(308) F(290) F(300) F(281) AND 
CONT C(305) C(308) F(300) F(281) F(290) 
SIMU 0.02 C(305) C(308) F(280) F(291) F(301) AND 
CONT C(305) C(308) F(291) F(301) F(280) AND 
CONT C(305) C(308) F(301) F(280) F(291) AND 
CONT C(305) C(308) F(281) F(290) F(300) AND 
CONT C(305) C(308) F(290) F(300) F(281) AND 
CONT C(305) C(308) F(300) F(281) F(290) 
SAME C(310) C(316) F(341) F(350) F(361) AND 
CONT C(310) C(316) F(350) F(361) F(341) AND 
CONT C(310) C(316) F(361) F(341) F(350) AND 
CONT C(310) C(316) F(340) F(351) F(360) AND 
CONT C(310) C(316) F(351) F(360) F(340) AND 
CONT C(310) C(316) F(360) F(340) F(351) 
DELU 0.015 C(310) C(316) F(341) F(350) F(361) AND 
CONT C(310) C(316) F(350) F(361) F(341) AND 
CONT C(310) C(316) F(361) F(341) F(350) AND 
CONT C(310) C(316) F(340) F(351) F(360) AND 
CONT C(310) C(316) F(351) F(360) F(340) AND 
CONT C(310) C(316) F(360) F(340) F(351) 
SIMU 0.015 C(310) C(316) F(341) F(350) F(361) AND 
CONT C(310) C(316) F(350) F(361) F(341) AND 
CONT C(310) C(316) F(361) F(341) F(350) AND 
CONT C(310) C(316) F(340) F(351) F(360) AND 
CONT C(310) C(316) F(351) F(360) F(340) AND 
CONT C(310) C(316) F(360) F(340) F(351) 
SAME C(312) C(315) F(311) F(321) F(330) AND 
CONT C(312) C(315) F(321) F(330) F(311) AND 
CONT C(312) C(315) F(330) F(311) F(321) AND 
CONT C(312) C(315) F(310) F(320) F(331) AND 
CONT C(312) C(315) F(320) F(331) F(310) AND 
CONT C(312) C(315) F(331) F(310) F(320) 
DELU 0.015 C(312) C(315) F(311) F(321) F(330) AND 
CONT C(312) C(315) F(321) F(330) F(311) AND 
CONT C(312) C(315) F(330) F(311) F(321) AND 
CONT C(312) C(315) F(310) F(320) F(331) AND 
CONT C(312) C(315) F(320) F(331) F(310) AND 
CONT C(312) C(315) F(331) F(310) F(320) 
SIMU 0.015 C(312) C(315) F(311) F(321) F(330) AND 
CONT C(312) C(315) F(321) F(330) F(311) AND 
CONT C(312) C(315) F(330) F(311) F(321) AND 
CONT C(312) C(315) F(310) F(320) F(331) AND 
CONT C(312) C(315) F(320) F(331) F(310) AND 
CONT C(312) C(315) F(331) F(310) F(320) 
SAME C(221) C(224) F(160) F(171) F(181) AND 
CONT C(221) C(224) F(171) F(181) F(160) AND 
CONT C(221) C(224) F(181) F(160) F(171) AND 
CONT C(221) C(224) F(161) F(170) F(180) AND 
CONT C(221) C(224) F(170) F(180) F(161) AND 
CONT C(221) C(224) F(180) F(161) F(170) 
DELU 0.015 C(221) C(224) F(160) F(171) F(181) AND 
CONT C(221) C(224) F(171) F(181) F(160) AND 
CONT C(221) C(224) F(181) F(160) F(171) AND 
CONT C(221) C(224) F(161) F(170) F(180) AND 
CONT C(221) C(224) F(170) F(180) F(161) AND 
CONT C(221) C(224) F(180) F(161) F(170) 
SIMU 0.015 C(221) C(224) F(160) F(171) F(181) AND 
CONT C(221) C(224) F(171) F(181) F(160) AND 
CONT C(221) C(224) F(181) F(160) F(171) AND 
CONT C(221) C(224) F(161) F(170) F(180) AND 
CONT C(221) C(224) F(170) F(180) F(161) AND 
CONT C(221) C(224) F(180) F(161) F(170) 
SAME C(203) C(207) F(1100) F(2000) F(3100) AND 
CONT C(203) C(207) F(2000) F(3100) F(1100) AND 
CONT C(203) C(207) F(3100) F(1100) F(2000) AND 
CONT C(203) C(207) F(1000) F(2100) F(3000) AND 
CONT C(203) C(207) F(2100) F(3000) F(1000) AND 
CONT C(203) C(207) F(3000) F(1000) F(2100) 
DELU 0.015 C(203) C(207) F(1100) F(2000) F(3100) AND 
CONT C(203) C(207) F(2000) F(3100) F(1100) AND 
CONT C(203) C(207) F(3100) F(1100) F(2000) AND 
CONT C(203) C(207) F(1000) F(2100) F(3000) AND 
CONT C(203) C(207) F(2100) F(3000) F(1000) AND 
CONT C(203) C(207) F(3000) F(1000) F(2100) 
SIMU 0.015 C(203) C(207) F(1100) F(2000) F(3100) AND 
CONT C(203) C(207) F(2000) F(3100) F(1100) AND 
CONT C(203) C(207) F(3100) F(1100) F(2000) AND 
CONT C(203) C(207) F(1000) F(2100) F(3000) AND 
CONT C(203) C(207) F(2100) F(3000) F(1000) AND 
CONT C(203) C(207) F(3000) F(1000) F(2100) 
SAME P(1) C(80) C(91) C(70) P(2) AND 
CONT P(2) C(70) C(91) C(80) P(1) AND 
CONT P(1) C(81) C(90) C(71) P(2) AND 
CONT P(2) C(71) C(90) C(81) P(1) 
SIMU 0.01 C(80) C(91) C(70) AND 
CONT C(70) C(91) C(80) AND 
CONT C(81) C(90) C(71) AND 
CONT C(71) C(90) C(81) 
DELU 0.015 C(80) C(91) C(70) AND 
CONT C(70) C(91) C(80) AND 
CONT C(81) C(90) C(71) AND 
CONT C(71) C(90) C(81) 
SAME  C(410) C(420) C(430)  AND 
CONT  C(410) C(430) C(420)  AND 
CONT  C(411) C(421) C(431)  AND 
CONT  C(411) C(431) C(421) 
DELU 0.015  C(410) C(420) C(430)  AND 
CONT  C(410) C(430) C(420)  AND 
CONT  C(411) C(421) C(431)  AND 
CONT  C(411) C(431) C(421) 
SIMU 0.015  C(410) C(420) C(430)  AND 
CONT  C(410) C(430) C(420)  AND 
CONT  C(411) C(421) C(431)  AND 
CONT  C(411) C(431) C(421) 
REM   HREST   END (DO NOT REMOVE THIS LINE) 
SAME P(3) C(1050) C(106) C(1050,-2,1,1,0,1) P(3,-2,1,1,0,1) AND 
CONT P(3,-2,1,1,0,1) C(1050,-2,1,1,0,1) C(106) C(1050) P(3) AND 
CONT P(3) C(1051) C(106,-2,1,1,0,1) C(1051,-2,1,1,0,1) P(3,-2,1,1,0,1) AND 
CONT P(3,-2,1,1,0,1) C(1051,-2,1,1,0,1) C(106,-2,1,1,0,1) C(1051) P(3) 
SIMU 0.015 P(3) C(1050) C(106) C(1050,-2,1,1,0,1) P(3,-2,1,1,0,1) AND 
CONT P(3,-2,1,1,0,1) C(1050,-2,1,1,0,1) C(106) C(1050) P(3) AND 
CONT P(3) C(1051) C(106,-2,1,1,0,1) C(1051,-2,1,1,0,1) P(3,-2,1,1,0,1) AND 
CONT P(3,-2,1,1,0,1) C(1051,-2,1,1,0,1) C(106,-2,1,1,0,1) C(1051) P(3) 
DELU 0.015 P(3) C(1050) C(106) C(1050,-2,1,1,0,1) P(3,-2,1,1,0,1) AND 
CONT P(3,-2,1,1,0,1) C(1050,-2,1,1,0,1) C(106) C(1050) P(3) AND 
CONT P(3) C(1051) C(106,-2,1,1,0,1) C(1051,-2,1,1,0,1) P(3,-2,1,1,0,1) AND 
CONT P(3,-2,1,1,0,1) C(1051,-2,1,1,0,1) C(106,-2,1,1,0,1) C(1051) P(3) 
END                                                                             
;