Three-component synthesis of alpha,beta-cyclopropyl-gamma-amino acids.
Wipf, Peter; Stephenson, Corey R. J.; Organic letters 7 (2005) 1137–1140; doi:10.1021/ol0501525

data_1506527
_publ_section_title
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 Three-component synthesis of alpha,beta-cyclopropyl-gamma-amino acids.
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_journal_issue                   6
_journal_name_full               'Organic letters'
_journal_page_first              1137
_journal_page_last               1140
_journal_paper_doi               10.1021/ol0501525
_journal_volume                  7
_journal_year                    2005
_chemical_formula_sum            'C30 H32 N2 O5'
_chemical_formula_weight         500.58
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_atom_sites_solution_primary     direct
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_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
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_cell_length_a                   10.4318(5)
_cell_length_b                   14.7988(6)
_cell_length_c                   35.7592(15)
_cell_measurement_reflns_used    5249
_cell_measurement_temperature    295(2)
_cell_measurement_theta_max      31.82
_cell_measurement_theta_min      2.19
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_computing_cell_refinement       'Bruker SMART'
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_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      295(2)
_diffrn_measured_fraction_theta_full 1.000
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_diffrn_measurement_device_type  'CCD area detector'
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_diffrn_radiation_type           MoK\a
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_diffrn_reflns_av_sigmaI/netI    0.0836
_diffrn_reflns_limit_h_max       12
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_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       42
_diffrn_reflns_limit_l_min       -42
_diffrn_reflns_number            44716
_diffrn_reflns_theta_full        25.00
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_diffrn_reflns_theta_min         1.49
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_exptl_crystal_density_diffrn    1.205
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0780P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1393
_refine_ls_wR_factor_ref         0.1639
_reflns_number_gt                5519
_reflns_number_total             9744
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ol0501525si20050122_030335.cif
_cod_data_source_block           cory121s
_cod_depositor_comments
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The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Orthorhombic' changed to
'orthorhombic' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
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_cod_original_sg_symbol_H-M      P2(1)2(1)2(1)
_cod_database_code               1506527