Expanded segments of three-dimensional carbonaceous nets with chirality: synthesis and structures.
Fukunaga, Toshiya M.; Takaba, Kiyofumi; Yoshida, Satoshi; Maki-Yonekura, Saori; Yonekura, Koji; Isobe, Hiroyuki; Chemical science 16 (2025) 19594–19600; doi:10.1039/d5sc06999h

data_1576014
_publ_section_title
;
 Expanded segments of three-dimensional carbonaceous nets with chirality:
 synthesis and structures.
;
_journal_issue                   42
_journal_name_full               'Chemical science'
_journal_page_first              19594
_journal_page_last               19600
_journal_paper_doi               10.1039/d5sc06999h
_journal_volume                  16
_journal_year                    2025
_chemical_formula_moiety         '2(C204 H228 B6 O6)'
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_audit_update_record
;
2025-09-09 deposited with the CCDC.	2025-10-08 downloaded from the CCDC.
;
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_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_diffrn_ambient_temperature      93(2)
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_diffrn_measured_fraction_theta_max 0.973
_diffrn_measurement_device_type  'JEOL CRYO ARM 300'
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'transmission electron microscope, cold field emission gun'
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_refine_ls_extinction_coef       84412(504)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.2400P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 1576013--1576014.cif.'
_cod_original_cell_volume        20592(37)
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