Coordination Polymers Containing Manganese(II)-Azido Layers Connected by Dipyridyl-tetrazine and 4,4'-Azobis(pyridine) Linkers
Paramita Kar; Michael G. B. Drew; Carlos J. Gómez-García; Ashutosh Ghosh; Inorganic Chemistry 52 (2013) 1640–1649; doi:10.1021/ic302548z

data_4333766
_publ_section_title
;
 Coordination Polymers Containing Manganese(II)-Azido Layers Connected by
 Dipyridyl-tetrazine and 4,4'-Azobis(pyridine) Linkers
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1640
_journal_page_last               1649
_journal_paper_doi               10.1021/ic302548z
_journal_volume                  52
_journal_year                    2013
_chemical_formula_sum            'C10 H8 Mn N10'
_chemical_formula_weight         323.20
_chemical_name_systematic
; 
 ? 
;
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_diffrn_ambient_temperature      150(2)
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_diffrn_measured_fraction_theta_max 0.935
_diffrn_measurement_device       'Oxford Diffaction X-Calibur System'
_diffrn_measurement_method       '321 frames, counting time 10 s.'
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_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
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_refine_ls_R_factor_gt           0.1102
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
_refine_ls_weighting_details 
  w=1/[\s^2^(Fo^2^)+(0.1386P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3 
;
_refine_ls_weighting_scheme      calc
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