<i>catena</i>-Diaquatris(α-methylacrylato)lanthanum(III)
Lu, W.-M.; Wu, J.-B.; Dong, N.; Chun, W.-G.; Gu, J.-M.; Liang, K.-L.; Acta Crystallographica Section C 51 (1995) 1568–1570; doi:10.1107/S0108270194013223

data_2003808
_publ_section_title
;
 <i>catena</i>-Diaquatris(\a-methylacrylato)lanthanum(III)
;
_journal_issue                   8
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1568
_journal_page_last               1570
_journal_paper_doi               10.1107/S0108270194013223
_journal_volume                  51
_journal_year                    1995
_chemical_formula_moiety         'C24 H38 La2 O16'
_chemical_formula_sum            'C24 H38 La2 O16'
_chemical_formula_weight         860.37
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.
_cell_angle_beta                 95.27(1)
_cell_angle_gamma                90.
_cell_formula_units_Z            4
_cell_length_a                   10.060(2)
_cell_length_b                   13.953(5)
_cell_length_c                   23.804(4)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293
_cell_measurement_theta_max      12
_cell_measurement_theta_min      10
_cell_volume                     3327.2(15)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.021
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_number            3201
_diffrn_reflns_theta_max         25
_diffrn_standards_decay_%        <12
_diffrn_standards_interval_time  60
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    2.611
_exptl_absorpt_correction_T_max  0.999
_exptl_absorpt_correction_T_min  0.324
_exptl_absorpt_correction_type   'empirical via \y scans'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.718
_exptl_crystal_description       plate
_exptl_crystal_size_max          0.5
_exptl_crystal_size_mid          0.3
_exptl_crystal_size_min          0.1
_refine_diff_density_max         0.85
_refine_diff_density_min         -0.31
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   5.991
_refine_ls_hydrogen_treatment    'H atom parameters not refined'
_refine_ls_number_parameters     266
_refine_ls_number_reflns         2738
_refine_ls_R_factor_obs          0.0471
_refine_ls_shift/esd_max         0.01
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      unit
_refine_ls_wR_factor_obs         0.0560
_reflns_number_observed          2738
_reflns_number_total             3078
_reflns_observed_criterion       I>3\s(I)
_cod_data_source_file            mu1143.cif
_cod_data_source_block           mu1143a
_cod_depositor_comments
;
 Adding the _atom_site_type_symbol data item.

 Antanas Vaitkus,
 2017-01-30
;
_cod_original_cell_volume        3327.0(10)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               2003808