Ring-forming transformation associated with hydrazone changes of hexadecanuclear dysprosium phosphonates.
Tian, Haiquan; Huang, Fu-Ping; Li, Yongfei; Chen, Peiqiong; Chai, Keyu; Lu, Jing; Liu, Hou-Ting; Zeng, Suyuan; Li, Dacheng; Dou, Jianmin; Dalton transactions (Cambridge, England : 2003) 50 (2021) 1119–1125; doi:10.1039/d0dt03536j

data_7706032
_publ_section_title
;
 Ring-forming transformation associated with hydrazone changes of
 hexadecanuclear dysprosium phosphonates.
;
_journal_issue                   3
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1119
_journal_page_last               1125
_journal_paper_doi               10.1039/d0dt03536j
_journal_volume                  50
_journal_year                    2021
_chemical_formula_moiety         'C80 H69 Dy4 N6 O24 P6, 2.5(C H4 O), 3(H2 O)'
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_audit_update_record
;
2020-12-11 deposited with the CCDC.	2020-12-11 downloaded from the CCDC.
;
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_diffrn_measured_fraction_theta_max 0.996
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_diffrn_source                   'micro-focus sealed X-ray tube'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1220P)^2^+499.6931P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                12693
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d0dt03536j2.cif
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_cod_depositor_comments
'Adding full bibliography for 7706031--7706032.cif.'
_cod_original_cell_volume        20343.3(6)
_cod_original_sg_symbol_H-M      'P 42/n'
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