Dual aminoquinolate diarylboron and nickel catalysed metallaphotoredox platform for carbon-oxygen bond construction.
Zu, Weisai; Day, Craig; Wei, Lanfeng; Jia, Xin; Xu, Liang; Chemical communications (Cambridge, England) 56 (2020) 8273–8276; doi:10.1039/d0cc03230a

data_7126756
_publ_section_title
;
 Dual aminoquinolate diarylboron and nickel catalysed metallaphotoredox
 platform for carbon-oxygen bond construction.
;
_journal_issue                   59
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              8273
_journal_page_last               8276
_journal_paper_doi               10.1039/d0cc03230a
_journal_volume                  56
_journal_year                    2020
_chemical_formula_sum            'C30 H25 B N2 O'
_chemical_formula_weight         440.33
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_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2020-01-20 deposited with the CCDC.	2020-06-15 downloaded from the CCDC.
;
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_diffrn_ambient_temperature      173(2)
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_diffrn_measurement_device_type  'Bruker D8 Venture'
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_exptl_absorpt_coefficient_mu    0.076
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_exptl_absorpt_correction_T_min  0.6636
_exptl_absorpt_correction_type   multi-scan
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_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0297P)^2^+0.8391P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0934
_refine_ls_wR_factor_ref         0.1016
_reflns_Friedel_coverage         0.000
_reflns_number_gt                3976
_reflns_number_total             4885
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d0cc03230a2.cif
_cod_data_source_block           11_a
_cod_depositor_comments          'Adding full bibliography for 7126756.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7126756
_shelx_shelxl_version_number     2018/3
_shelx_estimated_absorpt_t_min   0.980
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_shelx_res_checksum              71603