Integration of rigid and flexible organic parts for the construction of a homochiral metal-organic framework with high porosity.
Xu, Zhong-Xuan; Tan, Yan-Xi; Fu, Hong-Ru; Kang, Yao; Zhang, Jian; Chemical communications (Cambridge, England) 51 (2015) 2565–2568; doi:10.1039/c4cc09821h

data_7116177
_publ_section_title
;
 Integration of rigid and flexible organic parts for the construction of a
 homochiral metal-organic framework with high porosity.
;
_journal_issue                   13
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              2565
_journal_page_last               2568
_journal_paper_doi               10.1039/c4cc09821h
_journal_volume                  51
_journal_year                    2015
_chemical_absolute_configuration R
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; 
 ? 
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;
2014-10-27 deposited with the CCDC.
2014-12-23 downloaded from the CCDC.
;
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_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
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_diffrn_measurement_device_type  'multiwire proportional'
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;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb  1 2013,16:14:44)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
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_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   -0.001(14)
_refine_ls_extinction_method     none
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_refine_ls_R_factor_all          0.0816
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                3142
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_reflns_threshold_expression     >2sigma(I)
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_cod_depositor_comments          'Adding full bibliography for 7116177.cif.'
_cod_original_sg_symbol_H-M      P4(3)32
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