Synthesis of novel six-, seven- and eight-membered aluminum-containing rings by alumole ring expansion.
Drescher, Regina; Ritschel, Benedikt; Dewhurst, Rian D.; Deißenberger, Andrea; Hofmann, Alexander; Braunschweig, Holger; Chemical communications (Cambridge, England) 57 (2021) 7505–7508; doi:10.1039/d1cc02993b

data_7128579
_publ_section_title
;
 Synthesis of novel six-, seven- and eight-membered aluminum-containing
 rings by alumole ring expansion.
;
_journal_issue                   61
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              7505
_journal_page_last               7508
_journal_paper_doi               10.1039/d1cc02993b
_journal_volume                  57
_journal_year                    2021
_chemical_formula_moiety         'C34 H60 Al N O3'
_chemical_formula_sum            'C34 H60 Al N O3'
_chemical_formula_weight         557.81
_chemical_name_common            'Morpholine Addukt'
_chemical_name_systematic        'Morpholine Addukt'
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_audit_update_record
;
2021-05-17 deposited with the CCDC.	2021-06-29 downloaded from the CCDC.
;
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_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0504P)^2^+3.3604P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                4994
_reflns_number_total             6040
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d1cc02993b2.cif
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_cod_depositor_comments
'Adding full bibliography for 7128576--7128580.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7128579
_shelx_shelxl_version_number     2018/3
_shelx_estimated_absorpt_t_min   0.956
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_shelx_res_checksum              30545
_shelx_hkl_checksum              94569