Tetramethylammonium Dichlorotriphenylstannate
Ng, S. W.; Acta Crystallographica Section C 51 (1995) 1124–1125; doi:10.1107/S0108270194014678

data_2003610
_publ_section_title
;
 Tetramethylammonium Dichlorotriphenylstannate
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_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1124
_journal_page_last               1125
_journal_paper_doi               10.1107/S0108270194014678
_journal_volume                  51
_journal_year                    1995
_chemical_formula_moiety         'C22 H27 Cl2 N1 Sn1'
_chemical_formula_sum            'C22 H27 Cl2 N Sn'
_chemical_formula_weight         495.06
_space_group_IT_number           5
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'C 2y'
_symmetry_space_group_name_H-M   'C 1 2 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.
_cell_angle_beta                 134.984(3)
_cell_angle_gamma                90.
_cell_formula_units_Z            2
_cell_length_a                   14.648(2)
_cell_length_b                   9.8802(5)
_cell_length_c                   10.900(1)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    300
_cell_measurement_theta_max      12
_cell_measurement_theta_min      10
_cell_volume                     1115.8(2)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.025
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       9
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_number            1093
_diffrn_reflns_theta_max         25
_diffrn_standards_decay_%        0
_diffrn_standards_interval_time  60
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    1.396
_exptl_absorpt_correction_T_max  1.0892
_exptl_absorpt_correction_T_min  0.9007
_exptl_absorpt_correction_type
;
empirical (Walker & Stuart, 1983)
;
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.474
_exptl_crystal_description       irregular
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.14
_exptl_crystal_size_min          0.14
_exptl_crystal_size_rad          0.16
_refine_diff_density_max         0.19(2)
_refine_diff_density_min         0.07(2)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   0.389
_refine_ls_number_parameters     119
_refine_ls_number_reflns         1004
_refine_ls_R_factor_obs          0.020
_refine_ls_shift/esd_max         0.01
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(F) + 0.0004F^2^ + 1]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.025
_reflns_number_observed          1004
_reflns_number_total             1007
_reflns_observed_criterion       I>3\s(I)
_cod_data_source_file            ta1012.cif
_cod_data_source_block           ta1012a
_cod_depositor_comments
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The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'w = 1/[\s^2^(F) + 0.0004F^2^ +
1]' was changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to 'w = 1/[\s^2^(F) +
0.0004F^2^ + 1]'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        1115.7(2)
_cod_original_sg_symbol_H-M      'C 2'
_cod_original_formula_sum        'C22 H27 Cl2 N1 Sn1'
_cod_database_code               2003610