Time-Resolved Assembly of Chiral Uranyl Peroxo Cage Clusters Containing Belts of Polyhedra
Jie Qiu; Kevin Nguyen; Laurent Jouffret; Jennifer E. S. Szymanowski; Peter C. Burns; Inorganic Chemistry 52 (2013) 337–345; doi:10.1021/ic3020817

data_4331721
_publ_section_title
;
 Time-Resolved Assembly of Chiral Uranyl Peroxo Cage Clusters Containing
 Belts of Polyhedra
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              337
_journal_page_last               345
_journal_paper_doi               10.1021/ic3020817
_journal_volume                  52
_journal_year                    2013
_chemical_formula_moiety         K14.73[(UO2)22(O2)15(HPO3)20(H2O)10](H2O)38
_chemical_formula_sum            'K14.73 O182 P20 U22'
_chemical_formula_weight         9344.10
_chemical_name_common            U22(PO3)20
_chemical_name_systematic
; 
 ? 
;
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_computing_cell_refinement       'SMART SAINT'
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_computing_publication_material  'SHELCIF-97 (Sheldrick, 2008)'
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_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_detector_area_resol_mean 0
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker APEX'
_diffrn_measurement_method       '0.5 wide w/ exposures'
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_diffrn_reflns_theta_min         1.07
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_exptl_crystal_colour            'green yellow'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0808P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1960
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_cod_data_source_file            ic3020817_si_002_1.cif
_cod_data_source_block           final22
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'n/a' was changed to '?' - the
value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        22377(9)
_cod_database_code               4331721