Nickel-catalyzed cycloadditions of unsaturated hydrocarbons, aldehydes, and ketones.
Tekavec, Thomas N.; Louie, Janis; The Journal of organic chemistry 73 (2008) 2641–2648; doi:10.1021/jo702508w

data_4029578
_publ_section_title
;
 Nickel-catalyzed cycloadditions of unsaturated hydrocarbons, aldehydes,
 and ketones.
;
_journal_issue                   7
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              2641
_journal_page_last               2648
_journal_paper_doi               10.1021/jo702508w
_journal_volume                  73
_journal_year                    2008
_chemical_formula_moiety         'C29 H38 O9'
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_atom_sites_solution_secondary   difmap
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_cell_angle_gamma                101.877(3)
_cell_formula_units_Z            2
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_cell_length_c                   13.8261(5)
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_computing_cell_refinement       DENZO-SMN
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_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'Nonius KappaCCD Diffractomer'
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0628P)^2^+1.4530P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1533
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_cod_data_source_file            jo702508w-file001.cif
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_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/usr/data/users/saulius/automatic-downloads/retrospective/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 
;
_cod_original_cell_volume        1365.30(9)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4029578