Sr~11~InSb~9~ grown from molten In
Hullmann, Jonathan; Xia, Shengqing; Bobev, Svilen; Acta Crystallographica Section E 63 (2007) i178–i178; doi:10.1107/S1600536807040615

data_2215287
_publ_section_title
;
 Sr~11~InSb~9~ grown from molten In
;
_journal_coeditor_code           WM2135
_journal_issue                   9
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i178
_journal_page_last               i178
_journal_paper_doi               10.1107/S1600536807040615
_journal_volume                  63
_journal_year                    2007
_chemical_formula_iupac          'Sr11 In Sb9'
_chemical_formula_moiety         'In Sb4, 5(Sb), 11(Sr)'
_chemical_formula_structural     'In Sb9 Sr11'
_chemical_formula_sum            'In Sb9 Sr11'
_chemical_formula_weight         2174.39
_chemical_name_systematic
;
undecastrontium indium nonaantimonide
;
_space_group_IT_number           45
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'I 2 -2c'
_symmetry_space_group_name_H-M   'I b a 2'
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   12.3885(13)
_cell_length_b                   13.1003(14)
_cell_length_c                   17.4966(18)
_cell_measurement_reflns_used    3124
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      27.10
_cell_measurement_theta_min      2.26
_cell_volume                     2839.6(5)
_computing_cell_refinement       'SAINT (Bruker, 2002)'
_computing_data_collection       'SMART (Bruker, 2002)'
_computing_data_reduction        'SAINT (Bruker, 2002)'
_computing_molecular_graphics    'XP in SHELXTL (Bruker, 2002)'
_computing_publication_material  'SHELXTL (Bruker, 2002)'
_computing_structure_refinement  'SHELXTL (Bruker, 2002)'
_computing_structure_solution    'SHELXTL (Bruker, 2002)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker SMART APEX'
_diffrn_measurement_method       \w
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
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_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            15129
_diffrn_reflns_theta_full        27.10
_diffrn_reflns_theta_max         27.10
_diffrn_reflns_theta_min         2.26
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    29.640
_exptl_absorpt_correction_T_max  0.308
_exptl_absorpt_correction_T_min  0.172
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Sheldrick, 2003)'
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    5.086
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       irregular
_exptl_crystal_F_000             3704
_exptl_crystal_size_max          0.08
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.04
_refine_diff_density_max         0.896
_refine_diff_density_min         -1.005
_refine_ls_abs_structure_details 'Flack (1983), 1496 Friedel pairs'
_refine_ls_abs_structure_Flack   0.017(6)
_refine_ls_extinction_coef       0.000020(3)
_refine_ls_extinction_method     'SHELXTL (Bruker, 2002)'
_refine_ls_goodness_of_fit_ref   0.896
_refine_ls_matrix_type           full
_refine_ls_number_parameters     99
_refine_ls_number_reflns         3124
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      0.896
_refine_ls_R_factor_all          0.0249
_refine_ls_R_factor_gt           0.0223
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.001P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.0353
_refine_ls_wR_factor_ref         0.0341
_reflns_number_gt                2972
_reflns_number_total             3124
_reflns_threshold_expression     I>2\s(I)
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_cod_data_source_block           I
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_cod_database_fobs_code          2215287