Thiazolium-mediated multicomponent reactions: a facile synthesis of 3-aminofuran derivatives.
Ma, Cheng; Yang, Yewei; Organic letters 7 (2005) 1343–1345; doi:10.1021/ol0501368

data_1506517
_publ_section_title
;
 Thiazolium-mediated multicomponent reactions: a facile synthesis of
 3-aminofuran derivatives.
;
_journal_issue                   7
_journal_name_full               'Organic letters'
_journal_page_first              1343
_journal_page_last               1345
_journal_paper_doi               10.1021/ol0501368
_journal_volume                  7
_journal_year                    2005
_chemical_formula_moiety         'C16 H16 N2 O7 '
_chemical_formula_sum            'C16 H16 N2 O7'
_chemical_formula_weight         348.31
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_symmetry_cell_setting           triclinic
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_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                115.671(1)
_cell_angle_beta                 93.9504(5)
_cell_angle_gamma                99.789(1)
_cell_formula_units_Z            4
_cell_length_a                   8.3731(2)
_cell_length_b                   14.2379(1)
_cell_length_c                   15.5760(2)
_cell_measurement_reflns_used    5433
_cell_measurement_temperature    293(1)
_cell_measurement_theta_max      27.4
_cell_measurement_theta_min      1.6
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_computing_cell_refinement       PROCESS-AUTO
_computing_data_collection       PROCESS-AUTO
_computing_data_reduction        CrystalStructure
_computing_publication_material  'CrystalStructure 3.6.0'
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_diffrn_detector_area_resol_mean 10.00
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_diffrn_measurement_device_type  'Rigaku RAXIS-RAPID'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.024
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            15735
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         27.48
_exptl_absorpt_coefficient_mu    0.113
_exptl_absorpt_correction_T_max  0.978
_exptl_absorpt_correction_T_min  0.885
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
    Higashi, T. (1995). Program for Absorption Correction.
    Rigaku Corporation, Tokyo, Japan.
;
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.421
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       chunk
_exptl_crystal_F_000             728.00
_exptl_crystal_size_max          0.35
_exptl_crystal_size_mid          0.27
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.29
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_refine_ls_extinction_method     none
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_refine_ls_number_reflns         3973
_refine_ls_R_factor_gt           0.0560
_refine_ls_shift/su_max          0.0060
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[0.0046Fo^2^ + 1.0000\s(Fo^2^)]/(4Fo^2^)'
_refine_ls_weighting_scheme      calc
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_reflns_number_total             7408
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
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_cod_original_cell_volume        1627.88(5)
_cod_original_formula_sum        'C16 H16 N2 O7 '
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