Bis(1-<i>tert</i>-butyl-1<i>H</i>-imidazole-κ<i>N</i>^3^)dichloridocobalt(II)
Herdtweck, Eberhardt; Zeller, Alexander; Strassner, Thomas; Acta Crystallographica Section C 68 (2012) m166–m168; doi:10.1107/S0108270112020884

data_2018491
_publ_section_title
;
 Bis(1-<i>tert</i>-butyl-1<i>H</i>-imidazole-\k<i>N</i>^3^)dichloridocobalt(II)
;
_journal_coeditor_code           EG3092
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m166
_journal_page_last               m168
_journal_paper_doi               10.1107/S0108270112020884
_journal_volume                  68
_journal_year                    2012
_chemical_formula_iupac          '[Co Cl2 (C7 H12 N2)2]'
_chemical_formula_moiety         'C14 H24 Cl2 Co N4'
_chemical_formula_sum            'C14 H24 Cl2 Co N4'
_chemical_formula_weight         378.20
_chemical_name_systematic
;
Bis(1-<i>tert</i>-butyl-1<i>H</i>-imidazole-\k<i>N</i>^3^)dichloridocobalt(II)
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
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_atom_sites_solution_secondary   difmap
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_computing_molecular_graphics
;
DIAMOND (Brandenburg, 2010) and PLATON (Spek, 2009)
;
_computing_publication_material  'PLATON (Spek, 2009)'
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_computing_structure_solution    'SIR92 (Altomare <i>et al.</i>, 1994'
_diffrn_ambient_temperature      173.0(10)
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_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device       '\k-geometry diffractometer'
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_diffrn_reflns_limit_k_min       -17
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_diffrn_standards_decay_%        0
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_exptl_absorpt_correction_T_min  0.857
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_exptl_absorpt_process_details
;
[applied during the scaling procedure (DENZO; Otwinowski & Minor, 1997)]
;
_exptl_crystal_colour            blue
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_refine_ls_number_reflns         6741
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.034
_refine_ls_R_factor_all          0.0450
_refine_ls_R_factor_gt           0.0315
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0321P)^2^+2.5029P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      sigma
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_reflns_threshold_expression     I>2\s(I)
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_cod_data_source_block           I
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               2018491
_cod_database_fobs_code          2018491