(<i>S</i>)-2,2'-Bis(methoxymethoxy)[1,1'-binaphthyl]-3,3'-dicarbaldehyde
Tachi, Yoshimitsu; Nakayama, Shinya; Tani, Fumito; Ueno, Go; Naruta, Yoshinori; Acta Crystallographica Section C 55 (1999) 1351–1353; doi:10.1107/S0108270199004680

data_2008766
_publ_section_title
;
 (<i>S</i>)-2,2'-Bis(methoxymethoxy)[1,1'-binaphthyl]-3,3'-dicarbaldehyde
;
_journal_issue                   8
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1351
_journal_page_last               1353
_journal_paper_doi               10.1107/S0108270199004680
_journal_volume                  55
_journal_year                    1999
_chemical_formula_analytical     'C26 H22 O6'
_chemical_formula_moiety         'C26 H22 O6'
_chemical_formula_structural     ' (C10 H5(O CH2 O CH3)2(C H O)2)2 '
_chemical_formula_sum            'C26 H22 O6'
_chemical_formula_weight         430.456
_chemical_melting_point          .39E-305
_chemical_name_common            binaphthalene
_space_group_IT_number           92
_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_Hall  'P 4abw 2nw'
_symmetry_space_group_name_H-M   'P 41 21 2'
_audit_creation_method           'from TEXRAY.INF file'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   10.764(3)
_cell_length_b                   10.764(3)
_cell_length_c                   37.939(7)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    298.2
_cell_measurement_theta_max      29.7
_cell_measurement_theta_min      25.6
_cell_volume                     4395.8(19)
_computing_cell_refinement       ' MSC/AFC Diffractometer Control Software'
_computing_data_collection
; MSC/AFC Diffractometer Control Software (Molecular Structure Corporation,
1996)
;
_computing_data_reduction
' TEXSAN PROCESS (Molecular Structure Corporation, 1995)'
_computing_molecular_graphics    ' TEXSAN and ORTEPII (Johnson, 1976)'
_computing_publication_material  ' TEXSAN SAPI91 '
_computing_structure_refinement  ' TEXSAN LS and SAPI91'
_computing_structure_solution    ' TEXSAN SAPI91 (Fan Hai-fu, 1991)'
_diffrn_ambient_temperature      298.2
_diffrn_measurement_device_type  'Rigaku AFC7R'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Rigaku rotating anode'
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.5418
_diffrn_reflns_av_R_equivalents  0.000
_diffrn_reflns_av_sigmaI/netI    0.062
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       47
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            2566
_diffrn_reflns_reduction_process 'Lp corrections applied'
_diffrn_reflns_theta_max         76.33
_diffrn_reflns_theta_min         2.33
_diffrn_standards_decay_%        8.59
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.762
_exptl_absorpt_correction_T_max  0.840
_exptl_absorpt_correction_T_min  0.731
_exptl_absorpt_correction_type   '\Y-scans '
_exptl_absorpt_process_details   '(North et al., 1968)'
_exptl_crystal_colour            'pale yellow'
_exptl_crystal_density_diffrn    1.301
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prismatic
_exptl_crystal_F_000             1808.00
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.34
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.16
_refine_diff_density_min         -0.16
_refine_ls_extinction_coef       0.060(4)
_refine_ls_extinction_method     'Zachariasen(1967) type 2 Gaussian isotropic'
_refine_ls_goodness_of_fit_ref   1.424
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_constraints    1
_refine_ls_number_parameters     300
_refine_ls_number_reflns         2526
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0676
_refine_ls_R_factor_gt           0.0413
_refine_ls_shift/su_max          0.0010
_refine_ls_shift/su_mean         0.0000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo^2^) + 0.00203(Fo^2^)^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1287
_reflns_number_gt                1932
_reflns_number_total             2566
_reflns_threshold_expression     I>2\s(I)
_cod_data_source_file            cf1308.cif
_cod_data_source_block           binapMOMCHO
_cod_original_cell_volume        4395(2)
_cod_original_sg_symbol_Hall     'P 43n 2nw'
_cod_database_code               2008766