Merging metal-ligand cooperation and redox promoted strategy for tailored synthesis of alkylated 9<i>H</i>-fluorenes.
Samanta, Arup; Phukan, Hirak Jyoti; Tripathi, Ujjwal Kumar; Srimani, Dipankar; Chemical communications (Cambridge, England) 61 (2025) 12582–12585; doi:10.1039/d5cc02867a

data_7134824
_publ_section_title
;
 Merging metal-ligand cooperation and redox promoted strategy for tailored
 synthesis of alkylated 9<i>H</i>-fluorenes.
;
_journal_issue                   67
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              12582
_journal_page_last               12585
_journal_paper_doi               10.1039/d5cc02867a
_journal_volume                  61
_journal_year                    2025
_chemical_formula_sum            'C19 H18 Cl2'
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_audit_update_record
;
2025-05-20 deposited with the CCDC.	2025-07-09 downloaded from the CCDC.
;
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_diffrn_reflns_theta_min         2.440
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0435P)^2^+0.2982P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0955
_refine_ls_wR_factor_ref         0.1001
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2449
_reflns_number_total             2676
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d5cc02867a2.cif
_cod_data_source_block           AS_0m_a
_cod_depositor_comments
'Adding full bibliography for 7134820--7134825.cif.'
_cod_database_code               7134824
_shelx_shelxl_version_number     2018/3
_shelx_res_checksum              63103
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