Reactivity of bis(organoamino)phosphanes with magnesium(ii) compounds.
Vrána, Jan; Jambor, Roman; R°užička, Aleš; Alonso, Mercedes; De Proft, Frank; Lyčka, Antonín; Dostál, Libor; Dalton transactions (Cambridge, England : 2003) 44 (2015) 4533–4545; doi:10.1039/c4dt03929g

data_7033670
_publ_section_title
;
 Reactivity of bis(organoamino)phosphanes with magnesium(ii) compounds.
;
_journal_issue                   10
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              4533
_journal_page_last               4545
_journal_paper_doi               10.1039/c4dt03929g
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety         'C52 H62 Mg2 N4 O4 P2, 2(C6 H6)'
_chemical_formula_sum            'C64 H74 Mg2 N4 O4 P2'
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;
2014-12-17 deposited with the CCDC.
2015-01-16 downloaded from the CCDC.
;
_cell_angle_alpha                97.586(5)
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_cell_angle_gamma                110.470(4)
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'COLLECT (Hooft, 1998) and DENZO (Otwinowski & Minor, 1997)'
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_diffrn_ambient_temperature      150(1)
_diffrn_detector_area_resol_mean 9.091
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Bruker Nonius KappaCCD area detector'
_diffrn_measurement_method       '\f and \w scans to fill the Ewald sphere'
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;
Gaussian integration (Coppens, 1970)
;
_exptl_crystal_colour            colourless
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_refine_ls_structure_factor_coef Fsqd
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'calc w=1/[\s^2^(Fo^2^)+(0.0402P)^2^+1.0720P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_depositor_comments
'Adding full bibliography for 7033670--7033677.cif.'
_cod_original_cell_volume        1402.33(14)
_cod_database_code               7033670