Bispidine Analogues of Cisplatin, Carboplatin, and Oxaliplatin. Synthesis, Structures, and Cytotoxicity.
Cui, Huiling; Goddard, Richard; Pörschke, Klaus-Richard; Hamacher, Alexandra; Kassack, Matthias U.; Inorganic chemistry 53 (2014) 3371–; doi:10.1021/ic402737f

data_4337864
_publ_section_title
;
 Bispidine Analogues of Cisplatin, Carboplatin, and Oxaliplatin.
 Synthesis, Structures, and Cytotoxicity.
;
_journal_issue                   7
_journal_name_full               'Inorganic chemistry'
_journal_page_first              3371
_journal_paper_doi               10.1021/ic402737f
_journal_volume                  53
_journal_year                    2014
_chemical_compound_source        water
_chemical_formula_moiety         'C13 H20 N2 O4 Pt, 5(H2 O)'
_chemical_formula_sum            'C13 H30 N2 O9 Pt'
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_chemical_name_systematic
;
N,N'-3,7-diazabicyclo[3.3.1]nonane-1,1-cyclobutane-dicarboxylato-platinum(ii)
penta-hydrate
;
_space_group_IT_number           2
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_diffrn_ambient_temperature      100
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_diffrn_reflns_theta_max         36.98
_diffrn_reflns_theta_min         1.29
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_exptl_crystal_description       prism
_exptl_crystal_F_000             1088
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_exptl_crystal_size_min          0.20
_refine_diff_density_max         4.743
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_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.055
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     539
_refine_ls_number_reflns         18025
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.055
_refine_ls_R_factor_all          0.0310
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'calc w=1/[\s^2^(Fo^2^)+(0.0330P)^2^+1.7569P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic402737f_si_002.cif
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_cod_depositor_comments
'Adding full bibliography for 4337861--4337865.cif.'
_cod_original_sg_symbol_Hall     '-p 1'
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_cod_database_code               4337864