A Novel Dimeric Zinc Complex: Bis{μ-[(dimercaptomethylene)propanedinitrilato -S,S']}tetrakis(4-methylpyridine)dizinc(II)-Chloroform
Ren-Gen Xiong; Jing-Lin Zuo; Xiao-Zeng You; Inorganic Chemistry 36 (1997) 2472–2474; doi:10.1021/ic951029k

data_4323429
_publ_section_title
;
 A Novel Dimeric Zinc Complex:
 Bis{\m-[(dimercaptomethylene)propanedinitrilato
 -S,S']}tetrakis(4-methylpyridine)dizinc(II)-Chloroform
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              2472
_journal_page_last               2474
_journal_paper_doi               10.1021/ic951029k
_journal_volume                  36
_journal_year                    1997
_chemical_formula_moiety         'C33 H29 Cl3 N8 S8 Zn2 '
_chemical_formula_sum            'C33 H29 Cl3 N8 S4 Zn2'
_chemical_formula_weight         903.00
_space_group_IT_number           13
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      13
_symmetry_space_group_name_Hall  '-P 2yc'
_symmetry_space_group_name_H-M   'P 1 2/c 1'
_audit_creation_date             'Thu Feb 17  1997'
_audit_creation_method           'from TEXRAY.INF file'
_cell_angle_alpha                90
_cell_angle_beta                 93.93(1)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   13.372(2)
_cell_length_b                   9.198(3)
_cell_length_c                   16.872(2)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    296
_cell_measurement_theta_max      14.93
_cell_measurement_theta_min      13.58
_cell_volume                     2070.3(8)
_computing_cell_refinement       CAD4/PC
_computing_data_collection       CAD4/PC
_computing_data_reduction        teXsan
_computing_publication_material  teXsan
_computing_structure_refinement  teXsan
_computing_structure_solution    SIR-92
_diffrn_ambient_temperature      296
_diffrn_measurement_device       CAD4
_diffrn_measurement_method       'omega/2-theta scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_type           MoKalpha
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.027
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       0
_diffrn_reflns_limit_k_min       -10
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_diffrn_reflns_theta_max         24.97
_diffrn_reflns_theta_min         2.0
_diffrn_standards_decay_%        0.00
_diffrn_standards_interval_count 300
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    1.61
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.45
_exptl_crystal_description       needle
_exptl_crystal_F_000             916.00
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.18
_refine_diff_density_max         0.70
_refine_diff_density_min         -0.80
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   1.56
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
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_refine_ls_number_restraints     0
_refine_ls_R_factor_obs          0.045
_refine_ls_shift/esd_max         0.36
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      sigma
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_cod_data_source_file            ic951029k.cif
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_cod_original_cell_volume        2070.4(7)
_cod_original_formula_sum        'C33 H29 Cl3 N8 S4 Zn2 '
_cod_database_code               4323429