Synthesis of a 2D phosphorus material in a MOF-based 2D nano-reactor.
Li, Ming; Ma, Chuang; Liu, Xiong; Su, Jun; Cui, Xiaofeng; He, Yunbin; Chemical science 9 (2018) 5912–5918; doi:10.1039/c8sc01439f

data_1549536
_publ_section_title
;
 Synthesis of a 2D phosphorus material in a MOF-based 2D nano-reactor.
;
_journal_issue                   27
_journal_name_full               'Chemical science'
_journal_page_first              5912
_journal_page_last               5918
_journal_paper_doi               10.1039/c8sc01439f
_journal_volume                  9
_journal_year                    2018
_chemical_formula_moiety         'C17 H19 Co N2 O7'
_chemical_formula_sum            'C17 H19 Co N2 O7'
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_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
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_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2018-06-07 deposited with the CCDC.
2018-06-12 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_cell_length_c                   16.111(2)
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_cell_measurement_theta_max      23.26
_cell_measurement_theta_min      1.54
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_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      100(2)
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71076
_diffrn_reflns_av_R_equivalents  0.0310
_diffrn_reflns_av_unetI/netI     0.0332
_diffrn_reflns_Laue_measured_fraction_full 0.998
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_diffrn_reflns_limit_h_max       18
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_diffrn_reflns_theta_full        25.243
_diffrn_reflns_theta_max         25.491
_diffrn_reflns_theta_min         2.915
_exptl_absorpt_coefficient_mu    0.895
_exptl_crystal_colour            purple
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_exptl_crystal_size_mid          0.100
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_refine_ls_shift/su_mean         0.004
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0911P)^2^+15.7606P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.1775
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_reflns_number_gt                2807
_reflns_number_total             3726
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c8sc01439f2.cif
_cod_data_source_block           huda1_0m
_cod_depositor_comments
'Adding full bibliography for 1549536--1549537.cif.'
_cod_original_cell_volume        4009.7(9)
_cod_database_code               1549536
_shelx_shelxl_version_number     2014/7
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_shelx_res_checksum              56228