Aminoguanidinium nitrate
Akella, Annapoorna; Keszler, Douglas A.; Acta Crystallographica Section C 50 (1994) 1974–1976; doi:10.1107/S0108270194007730

data_2010255
_publ_section_title
;
 Aminoguanidinium nitrate
;
_journal_issue                   12
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1974
_journal_page_last               1976
_journal_paper_doi               10.1107/S0108270194007730
_journal_volume                  50
_journal_year                    1994
_chemical_formula_moiety         'C H7 N4 1+, N O3 1-'
_chemical_formula_sum            'C H7 N5 O3'
_chemical_formula_weight         137.10
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_type_scat_source           'IntTabIV Table 2.4.6B'
_cell_angle_alpha                110.47(2)
_cell_angle_beta                 102.64(2)
_cell_angle_gamma                104.87(2)
_cell_formula_units_Z            2
_cell_length_a                   7.3410(10)
_cell_length_b                   7.722(2)
_cell_length_c                   6.0240(10)
_cell_measurement_reflns_used    20
_cell_measurement_temperature    296
_cell_measurement_theta_max      14
_cell_measurement_theta_min      10
_cell_volume                     290.70(13)
_computing_data_collection
; MSC/AFC Diffractometer Control Software
(Molecular Structure Corporation, 1988)
;
_computing_data_reduction
' TEXSAN (Molecular Structure Corporation, 1989)'
_computing_molecular_graphics    'ORTEPII (Johnson, 1976)'
_computing_structure_refinement
' TEXSAN (Molecular Structure Corporation, 1989)'
_computing_structure_solution    'SHELXS86 (Sheldrick, 1985)'
_diffrn_measurement_device       'Rigaku AFC6R'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.076
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       8
_diffrn_reflns_limit_l_min       -8
_diffrn_reflns_number            3384
_diffrn_reflns_theta_max         30
_diffrn_standards_decay_%        1.9
_diffrn_standards_interval_count 200
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.136
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.566
_exptl_crystal_description       block
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.15
_refine_diff_density_max         0.27
_refine_diff_density_min         -0.40
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   1.44
_refine_ls_hydrogen_treatment    refall
_refine_ls_number_parameters     110
_refine_ls_number_reflns         1126
_refine_ls_R_factor_obs          0.044
_refine_ls_shift/esd_max         0.01
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_obs         0.054
_reflns_number_observed          1126
_reflns_number_total             1692
_reflns_observed_criterion       I>3\s(I)
_cod_data_source_file            bk1062.cif
_cod_data_source_block           structure
_cod_original_cell_volume        290.70(10)
_cod_database_code               2010255