Oxidations of chromene-annulated chlorins.
Hewage, Nisansala; Zeller, Matthias; Brückner, Christian; Organic & biomolecular chemistry 15 (2017) 396–407; doi:10.1039/c6ob02395a

data_7155393
_publ_section_title
;
 Oxidations of chromene-annulated chlorins.
;
_journal_issue                   2
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              396
_journal_page_last               407
_journal_paper_doi               10.1039/c6ob02395a
_journal_volume                  15
_journal_year                    2017
_chemical_formula_moiety
'C45 H11 F19 N4 O2 S, 0.651(C H2 Cl2), 0.135(C H4 S) '
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_space_group_name_Hall           '-P 1'
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_audit_update_record
;
2016-09-17 deposited with the CCDC.
2016-11-29 downloaded from the CCDC.
;
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;  
SHELXL-2014/7 (Sheldrick, 2014), 
SHELXLE Rev714 (H\"ubschle et al., 2011)
;
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
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_diffrn_measured_fraction_theta_max 0.977
_diffrn_measurement_device_type  'Bruker AXS X8 Prospector CCD diffractometer'
_diffrn_measurement_method       'omega and phi scans'
_diffrn_radiation_monochromator  'laterally graded multilayer (Goebel) mirror'
_diffrn_radiation_type           CuK\a
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_exptl_absorpt_correction_T_min  0.6574
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_exptl_absorpt_process_details   'Apex2 v2014.11 (Bruker, 2014)'
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0413P)^2^+5.8592P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.1018
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_reflns_number_gt                12701
_reflns_number_total             14572
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c6ob02395a2.cif
_cod_data_source_block           Prosp15mz169_0m
_cod_depositor_comments
'Adding full bibliography for 7155391--7155393.cif.'
_cod_original_formula_sum        'C45.79 H12.84 Cl1.30 F19 N4 O2 S1.14'
_cod_database_code               7155393
_shelx_shelxl_version_number     2014/7
_shelx_res_checksum              16146