Unusual flash cooling-induced phase in a crystal of triphenylsilanol.
Krawczyk, Monika K.; Acta crystallographica Section B, Structural science, crystal engineering and materials 79 (2023) 245–251; doi:10.1107/S2052520623004006

data_2312123
_publ_section_title
;
 Unusual flash cooling-induced phase in a crystal of triphenylsilanol.
;
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'Acta crystallographica Section B, Structural science, crystal engineering and materials'
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_journal_paper_doi               10.1107/S2052520623004006
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_journal_year                    2023
_chemical_formula_sum            'C18 H16 O Si'
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;
CrysAlisPro 1.171.41.89a (Rigaku Oxford Diffraction, 2020)
Analytical numeric absorption correction using a multifaceted crystal
model based on expressions derived by R.C. Clark & J.S. Reid.
(Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colorless
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_refine_ls_abs_structure_details
;
 Refined as an inversion twin.
;
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0813P)^2^+2.6062P] where P=(Fo^2^+2Fc^2^)/3'
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'Adding full bibliography for 2312118--2312124.cif.'
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_publcif_datablock.id            {782c73c7-d8d0-438c-9232-53bf38c99f2d}
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