Evidence of Nanotubular Self-Organization in Solution and Solid States of Heterochiral Cyclo 1:1 [α/α-N(α)-Bn-hydrazino]mers Series.
Moussodia, Ralph-Olivier; Acherar, Samir; Romero, Eugénie; Didierjean, Claude; Jamart-Grégoire, Brigitte; The Journal of organic chemistry 80 (2015) 3022–3029; doi:10.1021/jo502684g

data_4030799
_publ_section_title
;
 Evidence of Nanotubular Self-Organization in Solution and Solid States of
 Heterochiral Cyclo 1:1 [\a/\a-N(\a)-Bn-hydrazino]mers Series.
;
_journal_issue                   6
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              3022
_journal_page_last               3029
_journal_paper_doi               10.1021/jo502684g
_journal_volume                  80
_journal_year                    2015
_chemical_absolute_configuration syn
_chemical_compound_source        'synthesis as described'
_chemical_formula_moiety         'C32 H46 N6 O4'
_chemical_formula_sum            'C32 H46 N6 O4'
_chemical_formula_weight         578.75
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           5
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_symmetry_Int_Tables_number      5
_symmetry_space_group_name_Hall  'C 2y'
_symmetry_space_group_name_H-M   'C 1 2 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             2013-10-31T12:39:32-00:00
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                90
_cell_angle_beta                 120.110(10)
_cell_angle_gamma                90
_cell_formula_units_Z            8
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_cell_length_b                   9.7527(4)
_cell_length_c                   27.915(2)
_cell_measurement_reflns_used    0
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      0
_cell_measurement_theta_min      0
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_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_limit_h_max       28
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_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.175
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
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_refine_ls_structure_factor_coef Fsqd
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'calc w=1/[\s^2^(Fo^2^)+(0.2000P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     >2\s(I)
_cod_data_source_file            jo502684g_si_002.cif
_cod_data_source_block           rom89
_cod_depositor_comments          'Adding full bibliography for 4030799.cif.'
_cod_original_cell_volume        6545.5(7)
_cod_database_code               4030799