Optimized synthesis of a tert-butyl-phenyl-substituted tetrapyridophenazine ligand and its Ru(ii) complexes and determination of dimerization behaviour of the complexes through supramolecular "Fingerhakel".
Ritter, K.; Pehlken, C.; Sorsche, D.; Rau, S.; Dalton transactions (Cambridge, England : 2003) 44 (2015) 8889–8905; doi:10.1039/c5dt00214a

data_1518965
_publ_section_title
;
 Optimized synthesis of a tert-butyl-phenyl-substituted
 tetrapyridophenazine ligand and its Ru(ii) complexes and determination of
 dimerization behaviour of the complexes through supramolecular
 &quot;Fingerhakel&quot;.
;
_journal_issue                   19
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              8889
_journal_page_last               8905
_journal_paper_doi               10.1039/c5dt00214a
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety         'C32 H32 N2'
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2015-02-27 deposited with the CCDC.
2015-03-26 downloaded from the CCDC.
;
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        Empirical absorption correction using spherical harmonics,
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
 w=1/[\s^2^(Fo^2^)+(0.1244P)^2^+0.3933P]
 where P=(Fo^2^+2Fc^2^)/3
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.187
_refine_ls_wR_factor_ref         0.2194
_reflns_number_gt                3180
_reflns_number_total             4800
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c5dt00214a2.cif
_cod_data_source_block           phen(tbp)2
_cod_depositor_comments
'Adding full bibliography for 1518963--1518971.cif.'
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               1518965