Meso-Fused Carbatriphyrins(2.1.1) and Its Organo Phosphorus(V) Complex.
Kumar, Ankit; Thorat, Kishor G.; Sinha, Avisikta; Butcher, Ray J.; Ravikanth, Mangalampalli; The Journal of organic chemistry 84 (2019) 9067–9074; doi:10.1021/acs.joc.9b01015

data_4034204
_publ_section_title
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 Meso-Fused Carbatriphyrins(2.1.1) and Its Organo Phosphorus(V) Complex.
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_journal_issue                   14
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              9067
_journal_page_last               9074
_journal_paper_doi               10.1021/acs.joc.9b01015
_journal_volume                  84
_journal_year                    2019
_chemical_formula_sum            'C40 H0 F5 N2 O P S'
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_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_diffrn_ambient_temperature      150(2)
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_diffrn_measurement_device_type  dtrek-CrysAlisPro-abstract
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_diffrn_reflns_theta_full        67.679
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_exptl_absorpt_coefficient_mu    1.969
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_exptl_absorpt_correction_T_min  0.09051
_exptl_absorpt_correction_type   multi-scan
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_exptl_crystal_description       niddle
_exptl_crystal_F_000             2704
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_exptl_crystal_size_min          0.065
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1442P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_original_sg_symbol_Hall     -i_2yc
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