First Cationic Uranyl-Organic Framework with Anion-Exchange Capabilities.
Bai, Zhuanling; Wang, Yanlong; Li, Yuxiang; Liu, Wei; Chen, Lanhua; Sheng, Daopeng; Diwu, Juan; Chai, Zhifang; Albrecht-Schmitt, Thomas E; Wang, Shuao; Inorganic chemistry 55 (2016) 6358–6360; doi:10.1021/acs.inorgchem.6b00930

data_4348062
_publ_section_title
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 First Cationic Uranyl-Organic Framework with Anion-Exchange Capabilities.
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_journal_issue                   13
_journal_name_full               'Inorganic chemistry'
_journal_page_first              6358
_journal_page_last               6360
_journal_paper_doi               10.1021/acs.inorgchem.6b00930
_journal_volume                  55
_journal_year                    2016
_chemical_formula_moiety         C31H29N3O14U2
_chemical_formula_sum            'C31 H29 N3 O14 U2'
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_space_group_crystal_system      triclinic
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_cell_volume                     1726.4(3)
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_diffrn_ambient_temperature      273(2)
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_diffrn_measurement_device_type  'BRUKER apex II'
_diffrn_measurement_method       '0.5 wide w/ exposures'
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_diffrn_reflns_limit_l_min       -17
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_diffrn_reflns_theta_max         27.536
_diffrn_reflns_theta_min         2.290
_diffrn_source                   'fine-focus sealed tube'
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_exptl_absorpt_correction_T_max  0.863
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_exptl_absorpt_process_details   'SADABS, Bruker'
_exptl_crystal_colour            YELLOW
_exptl_crystal_density_diffrn    2.200
_exptl_crystal_description       BULK
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_refine_ls_R_factor_all          0.0412
_refine_ls_R_factor_gt           0.0339
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0900P)^2^+14.7318P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1026
_refine_ls_wR_factor_ref         0.1120
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_reflns_number_gt                6911
_reflns_number_total             7925
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            ic6b00930_si_002.cif
_cod_data_source_block           SCU-6
_cod_depositor_comments
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The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'Multi-scan' was
changed to 'multi-scan' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/ACS/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
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_cod_database_code               4348062
_shelx_shelxl_version_number     2014/7
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_shelx_fab_checksum              94149