Synthetic and reactivity studies of hetero-tri-anionic sodium zincates.
Francos, Javier; Kennedy, Alan R.; O'Hara, Charles T; Dalton transactions (Cambridge, England : 2003) 45 (2016) 6222–6233; doi:10.1039/c5dt04329h

data_7037492
_publ_section_title
;
 Synthetic and reactivity studies of hetero-tri-anionic sodium zincates.
;
_journal_issue                   14
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              6222
_journal_page_last               6233
_journal_paper_doi               10.1039/c5dt04329h
_journal_volume                  45
_journal_year                    2016
_chemical_formula_sum            'C23 H54 N3 Na Si Zn'
_chemical_formula_weight         489.14
_chemical_properties_physical
'Air-sensitive, Moisture-sensitive, Oxygen-sensitive'
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;
2015-11-02 deposited with the CCDC.
2015-11-30 downloaded from the CCDC.
;
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_diffrn_measured_fraction_theta_max 0.985
_diffrn_measurement_device_type  'Oxford Diffraction Xcalibur E'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_monochromator  graphite
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_diffrn_radiation_type           MoK\a
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;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.34.40 (release 27-08-2010 CrysAlis171 .NET)
(compiled Aug 27 2010,11:50:40)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'calc w=1/[\s^2^(Fo^2^)+(0.0535P)^2^+1.0459P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_data_source_file            c5dt04329h2.cif
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_cod_depositor_comments
'Adding full bibliography for 7037489--7037496.cif.'
_cod_original_cell_volume        1460.69(14)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7037492