Tricarbonylrhenium(i) complexes with 2-acetylpyridine-derived hydrazones are cytotoxic to NCI-H460 human large cell lung cancer
Garcia, Camila Vargas; Parrilha, Gabrieli Lessa; Rodrigues, Bernardo Lages; Teixeira, Sarah Fernandes; de Azevedo, Ricardo Alexandre; Ferreira, Adilson Kleber; Beraldo, Heloisa; New J. Chem. 40 (2016) 7379–; doi:10.1039/C6NJ00050A

data_7055631
_publ_section_title
;
 Tricarbonylrhenium(i) complexes with 2-acetylpyridine-derived hydrazones
 are cytotoxic to NCI-H460 human large cell lung cancer
;
_journal_issue                   9
_journal_name_full               'New J. Chem.'
_journal_page_first              7379
_journal_paper_doi               10.1039/C6NJ00050A
_journal_volume                  40
_journal_year                    2016
_chemical_formula_sum            'C17 H13 Cl N3 O4 Re'
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2016-05-09 deposited with the CCDC.
2016-06-15 downloaded from the CCDC.
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
Version 1.171.35.21 (release 20-01-2012 CrysAlis171 .NET)
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CrysAlisPro, Agilent Technologies,
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ORTEP-3 for windows, version 2.02 (Farrugia, 1997)
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_diffrn_radiation_type           MoK\a
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_diffrn_reflns_av_unetI/netI     0.0238
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_diffrn_reflns_theta_max         33.014
_diffrn_reflns_theta_min         1.968
_diffrn_source                   'Enhance (Mo) X-ray Source'
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CrysAlisPro, Agilent Technologies,
Version 1.171.35.21 (release 20-01-2012 CrysAlis171 .NET)
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Empirical absorption correction using spherical harmonics,
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;
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    2.010
_exptl_crystal_description       prism
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_exptl_crystal_size_min          0.02
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_refine_ls_extinction_method     none
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_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
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_refine_ls_number_reflns         6375
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.211
_refine_ls_R_factor_all          0.0343
_refine_ls_R_factor_gt           0.0226
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0307P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0615
_refine_ls_wR_factor_ref         0.0662
_reflns_number_gt                5218
_reflns_number_total             6375
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c6nj00050a2.cif
_cod_data_source_block           RePh
_cod_depositor_comments
'Adding full bibliography for 7055630--7055632.cif.'
_cod_database_code               7055631
_shelx_shelxl_version_number     2014/7
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