Cubes, Squares, and Books: A Simple Transition Metal/Bridging Ligand Combination Can Lead to a Surprising Range of Structural Types with the Same Metal/Ligand Proportions
Adel M. Najar; Ian S. Tidmarsh; Harry Adams; Michael D. Ward; Inorganic Chemistry 48 (2009) 11871–11881; doi:10.1021/ic901892y

data_4303914
_publ_contact_author
; 
        Prof. Mike Ward
        Department of Chemistry
        University of Sheffield
        SHEFFIELD
        S3 7HF
;
_publ_contact_author_email       m.d.ward@sheffield.ac.uk
_publ_contact_author_fax         '0114 2229346'
_publ_section_title
;
Cubes, Squares, and Books: A Simple Transition Metal/Bridging Ligand
Combination Can Lead to a Surprising Range of Structural Types with the
Same Metal/Ligand Proportions
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              11871
_journal_page_last               11881
_journal_paper_doi               10.1021/ic901892y
_journal_volume                  48
_journal_year                    2009
_chemical_formula_sum            'C276 H228 Cl16 N84 O64 Zn8'
_chemical_formula_weight         6835.58
_chemical_name_systematic
; 
 ? 
;
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_audit_creation_method           SHELXL-97
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_cell_angle_beta                 89.833(6)
_cell_angle_gamma                61.512(5)
_cell_formula_units_Z            1
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_cell_length_b                   23.307(6)
_cell_length_c                   26.686(6)
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_computing_cell_refinement       'Bruker SMART'
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_diffrn_radiation_monochromator  graphite
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_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            Colourless
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.2000P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_data_source_file            ic901892y_si_001_3.cif
_cod_data_source_block           imw1283
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan' changed
to 'multi-scan' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P -1 '
_cod_database_code               4303914