Catalytic Direct α-Amination of Arylacetic Acid Synthons with Anilines
Kumar, Jogendra; Suresh, Eringathodi; Bhadra, Sukalyan; The Journal of Organic Chemistry  (2020) –; doi:10.1021/acs.joc.0c02122

data_4038851
_publ_section_title
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 Catalytic Direct \a-Amination of Arylacetic Acid Synthons with Anilines
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_journal_name_full               'The Journal of Organic Chemistry'
_journal_paper_doi               10.1021/acs.joc.0c02122
_journal_year                    2020
_chemical_formula_sum            'C24 H18 N2 S'
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_cell_length_c                   20.6002(19)
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_diffrn_source                   'MICRO FOCUS TUBE'
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_exptl_absorpt_correction_type   multi-scan
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_exptl_crystal_colour            colourless
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0644P)^2^+0.3540P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.1500
_reflns_number_gt                5836
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            jo0c02122_si_004.cif
_cod_data_source_block           I1648
_cod_depositor_comments
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The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'MULTI SCAN' was
changed to 'multi-scan' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas 
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_cod_database_code               4038851
_shelx_res_checksum              2257
_shelx_hkl_checksum              52366