4-Methoxy-1-[(1<i>R</i>,4<i>S</i>,5<i>R</i>)-8-phenylmenthoxycarbonyl]pyridinium hexachloroantimonate, C~23~H~30~NO~3~^+^.SbCl~6~^{-^}
Singh, P.; Comins, D.L.; Joseph, S.P.; Acta Crystallographica Section C 50 (1994) 25–27; doi:10.1107/S0108270193006031

data_2009373
_publ_section_title
;4-Methoxy-1-[(1<i>R</i>,4<i>S</i>,5<i>R</i>)-8-phenylmenthoxycarbonyl]pyridinium
 hexachloroantimonate, C~23~H~30~NO~3~^+^.SbCl~6~^{-^}
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              25
_journal_page_last               27
_journal_paper_doi               10.1107/S0108270193006031
_journal_volume                  50
_journal_year                    1994
_chemical_formula_moiety         'C23 H30 N1 O3,Cl6 Sb1'
_chemical_formula_sum            'C23 H30 Cl6 N O3 Sb'
_chemical_formula_weight         702.97
_space_group_crystal_system      monoclinic
_space_group_IT_number           4
_space_group_name_Hall           'P 2yb'
_space_group_name_H-M_alt        'P 1 21 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.
_cell_angle_beta                 96.52(2)
_cell_angle_gamma                90.
_cell_formula_units_Z            2
_cell_length_a                   7.905(2)
_cell_length_b                   24.110(11)
_cell_length_c                   7.929(2)
_cell_measurement_reflns_used    22
_cell_measurement_temperature    298
_cell_measurement_theta_max      20
_cell_measurement_theta_min      13
_cell_volume                     1501.4(9)
_diffrn_measurement_device       'Siemens R3m/\m'
_diffrn_measurement_method       \w
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.010
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       31
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       10
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            3924
_diffrn_reflns_theta_max         27.5
_diffrn_standards_decay_%        1.7
_diffrn_standards_interval_count 48
_diffrn_standards_number         2
_exptl_absorpt_coefficient_mu    1.5
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    1.55
_exptl_crystal_description       Plates
_exptl_crystal_size_max          0.27
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.65
_refine_diff_density_min         -0.72
_refine_ls_extinction_coef       6.0E-7(3)
_refine_ls_extinction_method     Zachariasen
_refine_ls_goodness_of_fit_obs   1.21
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     277
_refine_ls_number_reflns         2466
_refine_ls_R_factor_obs          0.047
_refine_ls_shift/esd_max         0.74
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w=1/[\s^2^(F~o~)+0.0009F~o~^2^]
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.056
_reflns_number_observed          2466
_reflns_number_total             3511
_reflns_observed_criterion       F~o~>=5\s(F~o~)
_cod_data_source_file            cr1060.cif
_cod_data_source_block           cr1060_structure_1_of_1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'w=1/[\s^2^(F~o~)+0.0009F~o~^2^]'
was changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to
'w=1/[\s^2^(F~o~)+0.0009F~o~^2^]'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        1501.4(8)
_cod_original_sg_symbol_H-M      'P 21'
_cod_original_formula_sum        'C23 H30 Cl6 N1 O3 Sb1'
_cod_database_code               2009373