2,6-Bis(azaindole)pyridine: reactivity with iron(III) and copper(II) salts
Collins, Sibrina N.; Taylor, Stephen; Krause, Jeanette A.; Connick, William B.; Acta Crystallographica Section C 63 (2007) m436–m439; doi:10.1107/S0108270107039686

data_2016187
_publ_section_title
;
 2,6-Bis(azaindole)pyridine: reactivity with iron(III) and copper(II)
 salts
;
_journal_coeditor_code           GD3124
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m436
_journal_page_last               m439
_journal_paper_doi               10.1107/S0108270107039686
_journal_volume                  63
_journal_year                    2007
_chemical_formula_iupac          'C19 H13 N5'
_chemical_formula_moiety         'C19 H13 N5'
_chemical_formula_sum            'C19 H13 N5'
_chemical_formula_weight         311.34
_chemical_name_common            2,6-bis(azaindole)pyridine
_chemical_name_systematic
;
2,6-bis(1H-pyrrolo[2,3-b]pyridin-1-yl)pyridine
;
_space_group_IT_number           2
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_symmetry_space_group_name_Hall  '-P 1'
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_cell_length_b                   10.1397(3)
_cell_length_c                   21.9214(6)
_cell_measurement_reflns_used    6337
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      67.40
_cell_measurement_theta_min      4.15
_cell_volume                     1432.56(7)
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_computing_molecular_graphics    SHELXTL
_computing_publication_material  SHELXTL
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_computing_structure_solution    'SHELXTL (Sheldrick, 2003)'
_diffrn_ambient_temperature      150(2)
_diffrn_detector_area_resol_mean 0.8
_diffrn_measured_fraction_theta_full 0.943
_diffrn_measured_fraction_theta_max 0.943
_diffrn_measurement_device_type  'Bruker SMART 6000 CCD'
_diffrn_measurement_method       '\w scans'
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_diffrn_radiation_source         'fine-focus sealed tube'
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_diffrn_reflns_limit_k_min       -11
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_diffrn_reflns_theta_full        67.41
_diffrn_reflns_theta_max         67.41
_diffrn_reflns_theta_min         2.08
_diffrn_standards_decay_%        0
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_exptl_absorpt_coefficient_mu    0.721
_exptl_absorpt_correction_T_max  0.9648
_exptl_absorpt_correction_T_min  0.7865
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Sheldrick, 2003)'
_exptl_crystal_colour            colorless
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_refine_ls_R_factor_all          0.0540
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_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0853P)^2^+0.0170P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1149
_refine_ls_wR_factor_ref         0.1221
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_reflns_threshold_expression     I>2\s(I)
_cod_data_source_file            gd3124.cif
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_cod_database_fobs_code          2016187