Entrapment of Lithium Salts by the Lithium Amidinate Li[(nBu)C(NtBu)2]
Tristram Chivers; Andrew Downard; Masood Parvez; Inorganic Chemistry 38 (1999) 4347–4353; doi:10.1021/ic990757v

data_4322486
_publ_section_title
;
 Entrapment of Lithium Salts by the Lithium Amidinate Li[(nBu)C(NtBu)2]
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              4347
_journal_page_last               4353
_journal_paper_doi               10.1021/ic990757v
_journal_volume                  38
_journal_year                    1999
_chemical_formula_moiety         'C30 H62 Br Li3 N4 O '
_chemical_formula_sum            'C30 H62 Br Li3 N4 O'
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_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2yn'
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_audit_creation_method           'by teXsan v1.7'
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_cell_angle_gamma                90
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_cell_length_c                   17.024(6)
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_cell_measurement_temperature    170
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_computing_data_reduction        'teXsan (MSC, 1995)'
_computing_publication_material  'teXsan (MSC, 1995)'
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_diffrn_measurement_device       'Rigaku AFC6S'
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_diffrn_orient_matrix_UB_33      -0.03418
_diffrn_radiation_detector       'scintillation counter'
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_diffrn_radiation_type           'Mo K\a'
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_diffrn_reflns_av_R_equivalents  0.04020
_diffrn_reflns_av_sigmaI/netI    0.180
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_diffrn_reflns_theta_min         2.54
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_diffrn_standards_interval_count 200
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_exptl_crystal_colour            colorless
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo) + 0.00010|Fo|^2^]'
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_reflns_observed_criterion       >3.00\s(I)
_cod_data_source_file            ic990757v_2.cif
_cod_data_source_block           Andrew-12
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'w = 1/[\s^2^(Fo) +
0.00010|Fo|^2^]' was changed to 'calc'. New tag
'_refine_ls_weighting_details' was created. The value of the new tag
was set to 'w = 1/[\s^2^(Fo) + 0.00010|Fo|^2^]'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        3835.7(18)
_cod_original_sg_symbol_H-M      'P 21/n '
_cod_original_formula_sum        'C30 H62 Br Li3 N4 O '
_cod_database_code               4322486