Three new super water-stable lanthanide‒organic frameworks for luminescence sensing and magnetic properties
Tong, Wen-Quan; Liu, Ting-Ting; Li, Gao-Peng; Liang, Ji-Ye; Hou, Lei; Wang, Yao-Yu; New Journal of Chemistry 42 (2018) 9221–; doi:10.1039/C8NJ00348C

data_7057326
_publ_section_title
;
 Three new super water-stable lanthanide--organic frameworks for
 luminescence sensing and magnetic properties
;
_journal_issue                   11
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              9221
_journal_paper_doi               10.1039/C8NJ00348C
_journal_volume                  42
_journal_year                    2018
_chemical_formula_sum            'C14 H13 Eu N2 O11'
_chemical_formula_weight         537.22
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2018-03-05 deposited with the CCDC.
2018-03-27 downloaded from the CCDC.
;
_cell_angle_alpha                106.526(3)
_cell_angle_beta                 101.205(3)
_cell_angle_gamma                101.095(3)
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_cell_length_b                   10.071(2)
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_cell_measurement_temperature    296(2)
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_cell_measurement_theta_min      3.08
_cell_volume                     826.8(3)
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.971
_diffrn_measured_fraction_theta_max 0.970
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0176
_diffrn_reflns_av_unetI/netI     0.0370
_diffrn_reflns_Laue_measured_fraction_full 0.971
_diffrn_reflns_Laue_measured_fraction_max 0.970
_diffrn_reflns_limit_h_max       9
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_diffrn_reflns_limit_l_min       -12
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_diffrn_reflns_theta_max         25.998
_diffrn_reflns_theta_min         1.862
_diffrn_source                   'fine-focus sealed tube'
_exptl_absorpt_coefficient_mu    3.862
_exptl_absorpt_correction_T_max  0.6987
_exptl_absorpt_correction_T_min  0.6139
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.158
_exptl_crystal_description       block
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_refine_ls_extinction_method     none
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_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1991P)^2^+0.8823P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1375
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_reflns_Friedel_coverage         0.000
_reflns_number_gt                2895
_reflns_number_total             3162
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c8nj00348c2.cif
_cod_data_source_block           1-Eu
_cod_depositor_comments
'Adding full bibliography for 7057326--7057328.cif.'
_cod_database_code               7057326
_shelx_shelxl_version_number     2014/7
_shelx_estimated_absorpt_t_min   0.614
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_shelx_res_checksum              85555