Cobalt-mediated regio- and stereoselective assembly of dienamides by hydroaminative alkyne coupling of alpha,omega-diynes.
Gandon, Vincent; Aubert, Corinne; Malacria, Max; Vollhardt, K Peter C; Chemical communications (Cambridge, England)  (2008) 1599–1601; doi:10.1039/b716841a

data_7102999
_publ_section_title
;
 Cobalt-mediated regio- and stereoselective assembly of dienamides by
 hydroaminative alkyne coupling of alpha,omega-diynes.
;
_journal_issue                   13
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              1599
_journal_page_last               1601
_journal_paper_doi               10.1039/b716841a
_journal_year                    2008
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_audit_creation_date             'Wed Sep 19 11:14:10 2007'
_audit_creation_method           'by teXsan'
_cell_angle_alpha                81.578(3)
_cell_angle_beta                 84.642(3)
_cell_angle_gamma                62.402(3)
_cell_formula_units_Z            4
_cell_length_a                   9.437(2)
_cell_length_b                   9.472(2)
_cell_length_c                   25.437(6)
_cell_measurement_reflns_used    2540
_cell_measurement_temperature    154.2
_cell_measurement_theta_max      23.5
_cell_measurement_theta_min      3.5
_cell_volume                     1992.6(7)
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_computing_data_collection       'Bruker-AXS SMART v5.054'
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_diffrn_measurement_device_type  'Bruker SMART 1000'
_diffrn_measurement_method       \w-scans
_diffrn_radiation_type           'Mo K\a'
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_diffrn_reflns_limit_l_max       29
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo) + 0.00022|Fo|^2^]'
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