(E)-N-(4-{[1-(Prop-2-en-1-yl)-1H-1,2,3-triazol-4-yl]meth-oxy}benzyl-idene)morpholin-4-amine.
Akkurt, Mehmet; Jarrahpour, Aliasghar; Chermahini, Mehdi Mohammadi; Shiri, Pezhman; Ozdemir, Namık; Acta crystallographica. Section E, Structure reports online 70 (2014) o289–90; doi:10.1107/S1600536814002827

data_2311217
_publ_section_title
;
 (E)-N-(4-{[1-(Prop-2-en-1-yl)-1H-1,2,3-triazol-4-yl]meth-oxy}benzyl-idene)morpholin-4-amine.
;
_journal_coeditor_code           HG5381
_journal_issue                   'Pt 3'
_journal_name_full
'Acta crystallographica. Section E, Structure reports online'
_journal_page_first              o289
_journal_page_last               90
_journal_paper_doi               10.1107/S1600536814002827
_journal_volume                  70
_journal_year                    2014
_chemical_formula_iupac          'C17 H21 N5 O2'
_chemical_formula_moiety         'C17 H21 N5 O2'
_chemical_formula_sum            'C17 H21 N5 O2'
_chemical_formula_weight         327.39
_chemical_name_systematic
(<i>E</i>)-<i>N</i>-(4-{[1-(Prop-2-en-1-yl)-1<i>H</i>-1,2,3-triazol-4-yl]methoxy}benzylidene)morpholin-4-amine
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
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_cell_angle_beta                 100.724(6)
_cell_angle_gamma                99.838(6)
_cell_formula_units_Z            4
_cell_length_a                   10.5992(8)
_cell_length_b                   11.6351(10)
_cell_length_c                   14.8758(13)
_cell_measurement_reflns_used    12937
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.92
_cell_measurement_theta_min      1.41
_cell_volume                     1759.1(3)
_computing_cell_refinement       'X-AREA (Stoe & Cie, 2002)'
_computing_data_collection       'X-AREA (Stoe & Cie, 2002)'
_computing_data_reduction        'X-RED32 (Stoe & Cie, 2002)'
_computing_molecular_graphics    'ORTEP-3 for Windows (Farrugia, 2012)'
_computing_publication_material  'WinGX (Farrugia, 2012)'
_computing_structure_refinement  'SHELXL2013 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS2013 (Sheldrick, 2008)'
_diffrn_ambient_temperature      296(2)
_diffrn_detector_area_resol_mean 6.67
_diffrn_measured_fraction_theta_full 0.977
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device       '2-circle goniometer'
_diffrn_measurement_device_type  'Stoe IPDS 2'
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_monochromator  'plane graphite'
_diffrn_radiation_type           'Mo K\a'
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_diffrn_reflns_av_R_equivalents  0.0966
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_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
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_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            18485
_diffrn_reflns_reduction_process
;
;
_diffrn_reflns_theta_full        25.24
_diffrn_reflns_theta_max         25.00
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_exptl_absorpt_correction_T_min  0.9680
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_exptl_crystal_colour            colourless
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_exptl_crystal_density_method    'Not Measured'
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_refine_ls_matrix_type           full
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_refine_ls_number_reflns         6210
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_refine_ls_R_factor_all          0.1748
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.1115P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_refine_ls_wR_factor_ref         0.2235
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_reflns_threshold_expression     I>2\s(I)
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