Towards a global greener process: from solvent-less synthesis of molybdenum(vi) ONO Schiff base complexes to catalyzed olefin epoxidation under organic-solvent-free conditions
Cindrić, Marina; Pavlović, Gordana; Katava, Robert; Agustin, Dominique; New J. Chem. 41 (2017) 594–; doi:10.1039/C6NJ03174A

data_1544795
_publ_section_title
;
 Towards a global greener process: from solvent-less synthesis of
 molybdenum(vi) ONO Schiff base complexes to catalyzed olefin epoxidation
 under organic-solvent-free conditions
;
_journal_issue                   2
_journal_name_full               'New J. Chem.'
_journal_page_first              594
_journal_paper_doi               10.1039/C6NJ03174A
_journal_volume                  41
_journal_year                    2017
_chemical_formula_moiety         'C15 H15 Mo N O5,(C H4 O)'
_chemical_formula_sum            'C16 H19 Mo N O6'
_chemical_formula_weight         417.27
_chemical_name_common
cis-dioxo(2-(N-(salicylidene)amino)-4-methylphenolato-N,O,O')-(methanol)-molybdenum(VI)
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_space_group_name_Hall           '-P 2yn'
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_symmetry_space_group_name_Hall  '-P 2yn'
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;
2016-12-01 deposited with the CCDC.
2016-12-07 downloaded from the CCDC.
;
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'CrysAlis RED, Oxford Diffraction Ltd.Version 1.171.34.44'
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'CrysAlis CCD, Oxford Diffraction Ltd.Version 1.171.34.44'
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'CrysAlis RED, Oxford Diffraction Ltd.Version 1.171.34.44'
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_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type  'Xcalibur, Sapphire3'
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;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.34.44.
Empirical absorption correction using 
spherical harmonics,
implemented in SCALE3 ABSPACK scaling 
algorithm.
;
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0303P)^2^+0.2932P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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'Adding full bibliography for 1544795--1544799.cif.'
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