Radical-cation salts of BEDT-TTF with lithium tris(oxalato)metallate(iii).
Martin, Lee; Engelkamp, Hendrik; Akutsu, Hiroki; Nakatsuji, Shin'ichi; Yamada, Jun'ichi; Horton, Peter; Hursthouse, Michael B.; Dalton transactions (Cambridge, England : 2003) 44 (2015) 6219–6223; doi:10.1039/c5dt00183h

data_7034174
_publ_section_title
;
 Radical-cation salts of BEDT-TTF with lithium
 tris(oxalato)metallate(iii).
;
_journal_issue                   13
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              6219
_journal_page_last               6223
_journal_paper_doi               10.1039/c5dt00183h
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety         'C6 H2 Fe Li O13, 4(C10 H8 S8)'
_chemical_formula_sum            'C46 H34 Fe Li O13 S32'
_chemical_formula_weight         1883.44
_chemical_name_systematic
;
 ?
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2013
_audit_update_record
;
2015-01-08 deposited with the CCDC.
2015-02-25 downloaded from the CCDC.
;
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_cell_measurement_theta_max      27.485
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_computing_cell_refinement
'DENZO (Otwinowski & Minor, 1997) & COLLECT (Hooft, R.W.W., 1998)'
_computing_data_collection       'COLLECT (Hooft, R.W.W., 1998)'
_computing_data_reduction
'DENZO (Otwinowski & Minor, 1997) & COLLECT (Hooft, R.W.W., 1998)'
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_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type
'Bruker-Nonius APEX II CCD camera on \k-goniostat'
_diffrn_measurement_method       '\f & \w scans'
_diffrn_radiation_monochromator  '10cm confocal mirrors'
_diffrn_radiation_source         'Bruker-Nonius FR591 rotating anode'
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_diffrn_reflns_limit_h_max       11
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_exptl_crystal_colour            'Dark Brown'
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_refine_ls_extinction_method     none
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0084P)^2^+105.4418P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_total             16265
_reflns_threshold_expression     'I > 2\s(I)'
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'Adding full bibliography for 7034174--7034176.cif.'
_cod_original_cell_volume        7170.4(8)
_cod_database_code               7034174
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_shelx_res_checksum              8135
_shelx_fab_checksum              89587