Nitrogen Ligands on Phosphorus(III) Lewis Acceptors: A Versatile New Synthetic Approach to Unusual N-P Structural Arrangements
Neil Burford; Pierre Losier; Andrew D. Phillips; Paul J. Ragogna; T. Stanley Cameron; Inorganic Chemistry 42 (2003) 1087–1091; doi:10.1021/ic026090l

data_4313184
_publ_section_title
;
 Nitrogen Ligands on Phosphorus(III) Lewis Acceptors: A Versatile New
 Synthetic Approach to Unusual N-P Structural Arrangements
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              1087
_journal_page_last               1091
_journal_paper_doi               10.1021/ic026090l
_journal_volume                  42
_journal_year                    2003
_chemical_formula_moiety         'C20 H20 F3 N2 O3 P1 S1 '
_chemical_formula_sum            'C20 H20 F3 N2 O3 P S'
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_symmetry_space_group_name_H-M   'P 21 21 21'
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_cell_length_c                   8.410(3)
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_cell_measurement_theta_max      18.1
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_computing_cell_refinement       'MSC/AFC Diffractometer Control'
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'teXsan for Windows version 1.06 (MSC, 1997-1999)'
_computing_publication_material
'teXsan for Windows version 1.06 (MSC, 1997-1999)'
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'teXsan for Windows version 1.06 (MSC, 1997-1999)'
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;
SIR92 (Altomare, et. al. 1994)
;
_diffrn_ambient_temperature      238
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_diffrn_measurement_method       \w-2\q
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;
\y scans (North,Phillips & Matthews, 1968)
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_exptl_crystal_colour            'light yellow'
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_refine_ls_extinction_expression 'equ(3) Acta Cryst.(1968) A24, p213.'
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     unit
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_refine_ls_wR_factor_ref         0.0700
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_reflns_threshold_expression     I>3.00\s(I)
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_cod_data_source_block           '_paul17minus35'
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        2151.7(9)
_cod_original_sg_symbol_H-M      'P 21 21 21 '
_cod_original_formula_sum        'C20 H20 F3 N2 O3 P1 S1 '
_cod_database_code               4313184