[Pd(CH~3~COO)~2~]~<i>n~</i> from X-ray powder diffraction data
Kirik, Sergei D.; Mulagaleev Ruslan F.; Blokhin Alexander I.; Acta Crystallographica Section C 60 (2004) m449–m450; doi:10.1107/S0108270104016129

data_2014232
_publ_section_title
;
 [Pd(CH~3~COO)~2~]~<i>n~</i> from X-ray powder diffraction data
;
_journal_issue                   9
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m449
_journal_page_last               m450
_journal_paper_doi               10.1107/S0108270104016129
_journal_volume                  60
_journal_year                    2004
_chemical_formula_analytical     '[Pd (C2 H3 O2)2]'
_chemical_formula_iupac          '[Pd (C2 H3 O2)2]'
_chemical_formula_moiety         'C4 H6 O4 Pd'
_chemical_formula_structural     (Pd(CH3COO)2)
_chemical_formula_sum            'C4 H6 O4 Pd'
_chemical_formula_weight         224.51
_chemical_name_common            diacetato-palladat(II)
_chemical_name_systematic
;
catena-poly[palladium(II)-di-\m-acetato-\k^4^O:O']
;
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 93.460(10)
_cell_angle_gamma                90.0
_cell_formula_units_Z            2
_cell_length_a                   7.44670(10)
_cell_length_b                   5.83830(10)
_cell_length_c                   7.99000(10)
_cell_measurement_temperature    293
_cell_volume                     346.741(9)
_computing_cell_refinement       'POWDER (Kirik et al., 1979)'
_computing_data_collection       'DRON-4 data collection software'
_computing_data_reduction        ' '
_computing_molecular_graphics    'XP (Siemems, 1989)'
_computing_structure_refinement  'Modified DBWM'
_computing_structure_solution    'Modified DBWM (Wiles & Young, 1981)'
_diffrn_ambient_temperature      293
_diffrn_measurement_device       'DRON-4 powder diffractometer'
_diffrn_measurement_method       '\q/2\q scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'conventional sealed tube'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.5418
_diffrn_reflns_av_R_equivalents  0
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       5
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       7
_diffrn_reflns_limit_l_min       -6
_diffrn_reflns_number            321
_diffrn_reflns_theta_max         45.
_diffrn_reflns_theta_min         2.5
_exptl_absorpt_coefficient_mu    21.214
_exptl_absorpt_correction_type   none
_exptl_absorpt_process_details   none
_exptl_crystal_density_diffrn    2.15
_exptl_crystal_F_000             216.0
_refine_ls_goodness_of_fit_all   1.38
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_constraints    0
_refine_ls_number_parameters     41
_refine_ls_number_restraints     0
_refine_ls_shift/su_max          0.1
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_scheme      sigma
_reflns_number_total             321
_cod_data_source_file            sk1735.cif
_cod_data_source_block           I
_cod_original_cell_volume        346.740(10)
_cod_original_sg_symbol_H-M      'P 21/m'
_cod_database_code               2014232