<i>catena</i>-Poly[zinc(II)-bis{μ-(<i>N</i>-carbamoylglycinato)}-<i>O</i>:<i>O</i>'';<i>O</i>'':<i>O</i>], [Zn(C~3~H~5~N~2~O~3~)~2~]
Menabue, L.; Saladini, M.; Acta Crystallographica Section C 50 (1994) 887–889; doi:10.1107/S0108270193011564

data_2009791
_publ_section_title
;<i>catena</i>-Poly[zinc(II)-bis{\m-(<i>N</i>-carbamoylglycinato)}-<i>O</i>:<i>O</i>'';<i>O</i>'':<i>O</i>],
 [Zn(C~3~H~5~N~2~O~3~)~2~]
;
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              887
_journal_page_last               889
_journal_paper_doi               10.1107/S0108270193011564
_journal_volume                  50
_journal_year                    1994
_chemical_formula_sum            'C6 H10 N4 O6 Zn'
_chemical_formula_weight         299.55
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90
_cell_angle_beta                 102.40(9)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   7.871(7)
_cell_length_b                   10.233(4)
_cell_length_c                   13.318(2)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    298
_cell_measurement_theta_max      15
_cell_measurement_theta_min      6
_cell_volume                     1047.7(11)
_diffrn_measurement_device       'Enraf-Nonius CAD4'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.033
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            2042
_diffrn_reflns_theta_max         25
_diffrn_standards_decay_%        <0.1
_diffrn_standards_interval_time  4
_diffrn_standards_number         2
_exptl_absorpt_coefficient_mu    2.42
_exptl_absorpt_correction_T_max  1.02
_exptl_absorpt_correction_T_min  0.98
_exptl_absorpt_correction_type   'empirical (Ugozzoli, 1983)'
_exptl_crystal_colour            White
_exptl_crystal_density_diffrn    1.90
_exptl_crystal_density_meas      1.88
_exptl_crystal_density_method    'flotation in ?'
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.12
_refine_diff_density_max         0.5
_refine_diff_density_min         -0.6
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     154
_refine_ls_number_reflns         1366
_refine_ls_R_factor_obs          0.048
_refine_ls_shift/esd_max         0.35
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      unit
_refine_ls_wR_factor_obs         0.048
_reflns_number_observed          '1366 unique'
_reflns_number_total             1961
_reflns_observed_criterion       I>2\s(I)
_cod_data_source_file            mu1067.cif
_cod_data_source_block           mu1067a
_cod_original_cell_volume        1048.0(10)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2009791