<i>catena</i>-Poly[cobalt(II)-di-μ-chlorido-κ^4^<i>Cl</i>:<i>Cl</i>-μ-1,5-dimethyl-1<i>H</i>-tetrazole-κ^2^<i>N</i>^3^:<i>N</i>^4^]: an X-ray powder investigation
Ivashkevich, Ludmila S.; Lyakhov, Alexander S.; Mosalkova, Anastasiya P.; Gaponik, Pavel N.; Ivashkevich, Oleg A.; Acta Crystallographica Section E 65 (2009) m236–; doi:10.1107/S1600536809003018

data_2220746
_publ_section_title
;<i>catena</i>-Poly[cobalt(II)-di-\m-chlorido-\k^4^<i>Cl</i>:<i>Cl</i>-\m-1,5-dimethyl-1<i>H</i>-tetrazole-\k^2^<i>N</i>^3^:<i>N</i>^4^]:
 an X-ray powder investigation
;
_journal_coeditor_code           CV2491
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m236
_journal_paper_doi               10.1107/S1600536809003018
_journal_volume                  65
_journal_year                    2009
_chemical_formula_iupac          '[Co Cl2 (C3 H6 N4)]'
_chemical_formula_moiety         'C3 H6 Cl2 Co N4'
_chemical_formula_sum            'C3 H6 Cl2 Co N4'
_chemical_formula_weight         227.95
_chemical_name_systematic
;
<i>catena</i>-Poly[cobalt(II)-di-\m-chlorido-\k^4^Cl:Cl-\m-\
1,5-dimethyl-1<i>H</i>-tetrazole-\k^2^N^3^:N^4^]
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                108.639(2)
_cell_angle_beta                 107.259(3)
_cell_angle_gamma                105.769(3)
_cell_formula_units_Z            2
_cell_length_a                   6.7159(4)
_cell_length_b                   7.5986(4)
_cell_length_c                   8.9231(5)
_cell_measurement_temperature    295
_cell_volume                     376.72(4)
_computing_cell_refinement       'FULLPROF (Rodr\'iguez-Carvajal, 2001)'
_computing_data_collection       'Local program'
_computing_data_reduction        'Local program'
_computing_molecular_graphics    'PLATON (Spek, 2003)'
_computing_publication_material
;
FULLPROF (Rodr\'iguez-Carvajal, 2001),
SHELXL97 (Sheldrick, 2008) and PLATON (Spek, 2003)
;
_computing_structure_refinement  'FULLPROF (Rodr\'iguez-Carvajal, 2001)'
_diffrn_ambient_temperature      295
_diffrn_measurement_device_type  'HZG-4A (Carl Zeiss, Jena)'
_diffrn_measurement_method       '\q/2\q scan'
_diffrn_radiation_monochromator  'Fe filtered'
_diffrn_radiation_type           'Co K\a'
_diffrn_radiation_wavelength     1.79021
_exptl_crystal_density_diffrn    2.010
_exptl_crystal_density_method    'Not Measured'
_exptl_crystal_F_000             226
_refine_ls_goodness_of_fit_all   0.97
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           fullcycle
_refine_ls_number_constraints    0
_refine_ls_number_parameters     45
_refine_ls_number_reflns         896
_refine_ls_number_restraints     7
_refine_ls_shift/su_max          0.002
_refine_ls_structure_factor_coef Inet
_refine_ls_weighting_scheme      sigma
_cod_data_source_file            cv2491.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_database_code               2220746