Studies on Antibiotics Active against Resistant Bacteria. Total Synthesis of MRSA-Active Tetarimycin A and Its Analogues.
Huang, Jing-Kai; Yang Lauderdale, Tsai-Ling; Shia, Kak-Shan; Organic letters 17 (2015) 4248–4251; doi:10.1021/acs.orglett.5b02039

data_1529398
_publ_section_title
;
 Studies on Antibiotics Active against Resistant Bacteria. Total Synthesis
 of MRSA-Active Tetarimycin A and Its Analogues.
;
_journal_issue                   17
_journal_name_full               'Organic letters'
_journal_page_first              4248
_journal_page_last               4251
_journal_paper_doi               10.1021/acs.orglett.5b02039
_journal_volume                  17
_journal_year                    2015
_chemical_formula_sum            'C25 H23 N O6'
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_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
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_cell_measurement_reflns_used    3094
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_cell_volume                     4154.5(4)
_computing_cell_refinement       'SAINT V8.34A (Bruker AXS Inc., 2013)'
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_computing_data_reduction        'SAINT V8.34A (Bruker AXS Inc., 2013)'
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_computing_publication_material  SHELXTL
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_diffrn_ambient_temperature      296(2)
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
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_diffrn_reflns_point_group_measured_fraction_full 1.000
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_exptl_crystal_colour            Yellow
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_exptl_crystal_description       Lump
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0550P)^2^+1.3251P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                2938
_reflns_number_total             4254
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            ol5b02039_si_002.cif
_cod_data_source_block           mo_150318_0m
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3271 2015-04-21 07:52:19Z andrius 

 Adding full bibliography for 1529398.cif.
;
_cod_database_code               1529398
_shelxl_version_number           2014/6
_shelx_res_checksum              3566
_shelx_hkl_checksum              80727