Diversified magnetic behaviors of new nickel(ii) and copper(ii) azido coordination polymers templated by diethyl or triethyl amines
Zeng, Ying; Liu, Sui-Jun; Liu, Cai-Ming; Xie, Yong-Rong; Du, Zi-Yi; New J. Chem. 41 (2017) 1212–; doi:10.1039/C6NJ03268K

data_7055921
_publ_section_title
;
 Diversified magnetic behaviors of new nickel(ii) and copper(ii) azido
 coordination polymers templated by diethyl or triethyl amines
;
_journal_issue                   3
_journal_name_full               'New J. Chem.'
_journal_page_first              1212
_journal_paper_doi               10.1039/C6NJ03268K
_journal_volume                  41
_journal_year                    2017
_chemical_formula_sum            'C6 H16 N8 Ni'
_chemical_formula_weight         258.98
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2016-12-18 deposited with the CCDC.
2016-12-22 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 97.1130(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
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_cell_length_b                   7.9731(6)
_cell_length_c                   13.5232(10)
_cell_measurement_reflns_used    2735
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.44
_cell_measurement_theta_min      2.97
_cell_volume                     1113.14(15)
_computing_cell_refinement       'Bruker SMART'
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_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0171
_diffrn_reflns_av_unetI/netI     0.0218
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.993
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -13
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_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
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_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.993
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_diffrn_reflns_theta_max         27.492
_diffrn_reflns_theta_min         2.972
_exptl_absorpt_coefficient_mu    1.727
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_correction_T_min  0.6591
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_exptl_crystal_colour            green
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_refine_ls_number_reflns         2540
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_refine_ls_R_factor_all          0.0282
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0275P)^2^+0.1543P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.0549
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_reflns_number_total             2540
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           1
_cod_depositor_comments
'Adding full bibliography for 7055920--7055922.cif.'
_cod_database_code               7055921
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