Lewis acid-base 1,2-addition reactions: synthesis of pyrylium borates from en-ynoate precursors.
Wilkins, Lewis C.; Hamilton, Hugh B.; Kariuki, Benson M.; Hashmi, A Stephen K; Hansmann, Max M.; Melen, Rebecca L.; Dalton transactions (Cambridge, England : 2003) 45 (2016) 5929–5932; doi:10.1039/c5dt03340c

data_7036670
_publ_section_title
;
 Lewis acid-base 1,2-addition reactions: synthesis of pyrylium borates
 from en-ynoate precursors.
;
_journal_issue                   14
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              5929
_journal_page_last               5932
_journal_paper_doi               10.1039/c5dt03340c
_journal_volume                  45
_journal_year                    2016
_chemical_formula_moiety         'C30 H10 B F15 O2'
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;
 ?
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2015-08-04 deposited with the CCDC.
2015-09-24 downloaded from the CCDC.
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.33 (release 27-03-2014 CrysAlis171 .NET)
(compiled Mar 27 2014,17:12:48)
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CrysAlisPro, Agilent Technologies,
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Numerical absorption correction based on gaussian integration over
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;
_exptl_crystal_colour            colourless
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0409P)^2^+2.8511P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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'Adding full bibliography for 7036670--7036671.cif.'
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