LMucko/crystallography-open-database huggingface dataset:
Crystal structure of Tutton's salts, Rb~2~[M^II^(H~2~O)~6~](SeO~4~)~2~, M^II^ = Mg, Co, Mn, Zn
Euler, H.; Barbier, B.; Meents, A.; Kirfel, A.; Zeitschrift für Kristallographie - New Crystal Structures 218 (2003) 265–268; doi:

data_8100422
_publ_section_title
;
Crystal structure of Tutton's salts, Rb~2~[M^II^(H~2~O)~6~](SeO~4~)~2~, 
M^II^ = Mg, Co, Mn, Zn
;
_journal_issue                   3
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              265
_journal_page_last               268
_journal_volume                  218
_journal_year                    2003
_chemical_formula_moiety         '(Rb 1+)2, Co 2+, (Se O4 2-)2, 6(H2O)'
_chemical_formula_sum            'Co H12 O14 Rb2 Se2'
_chemical_formula_weight         623.89
_chemical_name_common            'rubidium hexa-aquacobalte(II) selenate'
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yab'
_symmetry_space_group_name_H-M   'P 1 21/a 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 105.238(9)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   9.3628(11)
_cell_length_b                   12.6176(12)
_cell_length_c                   6.3562(7)
_cell_measurement_temperature    293(2)
_cell_volume                     724.50(14)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    2.860
_cod_original_sg_symbol_H-M      'P 21/a'
_cod_original_formula_sum        'H12 Co O14 Rb2 Se2'
_cod_database_code               8100422
Crystal structure of Tutton's salts, Rb~2~[M^II^(H~2~O)~6~](SeO~4~)~2~, M^II^ = Mg, Co, Mn, Zn
Euler, H.; Barbier, B.; Meents, A.; Kirfel, A.; Zeitschrift für Kristallographie - New Crystal Structures 218 (2003) 265–268; doi:

data_8100423
_publ_section_title
;
Crystal structure of Tutton's salts, Rb~2~[M^II^(H~2~O)~6~](SeO~4~)~2~, 
M^II^ = Mg, Co, Mn, Zn
;
_journal_issue                   3
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              265
_journal_page_last               268
_journal_volume                  218
_journal_year                    2003
_chemical_formula_moiety         '(Rb 1+)2, Mn 2+, (Se O4 2-)2, 6(H2O)'
_chemical_formula_sum            'H12 Mn O14 Rb2 Se2'
_chemical_formula_weight         619.90
_chemical_name_common            'rubidium hexa-aquamanganese(II) selenate'
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yab'
_symmetry_space_group_name_H-M   'P 1 21/a 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 105.189(7)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   9.4496(8)
_cell_length_b                   12.7603(13)
_cell_length_c                   6.3794(7)
_cell_measurement_temperature    293(2)
_cell_volume                     742.35(13)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    2.773
_cod_original_sg_symbol_H-M      'P 21/a'
_cod_database_code               8100423
Crystal structure of 1,3,5-trimethyl-6-phenyl-2,4-dioxohexa-hydro- 1,3,5-triazine, C~12~H~15~N~3~O~2~
Klepp, O. Kurt; Schmidt, Harald; Zeitschrift für Kristallographie - New Crystal Structures 218 (2003) 539–540; doi:

data_8100424
_publ_section_title
;
Crystal structure of 1,3,5-trimethyl-6-phenyl-2,4-dioxohexa-hydro-
1,3,5-triazine, C~12~H~15~N~3~O~2~
;
_journal_issue                   4
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              539
_journal_page_last               540
_journal_volume                  218
_journal_year                    2003
_chemical_formula_structural     'C12 H15 N3 O2'
_chemical_formula_sum            'C12 H15 N3 O2'
_chemical_formula_weight         233.27
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 98.84(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   8.902(6)
_cell_length_b                   12.674(2)
_cell_length_c                   10.647(4)
_cell_measurement_temperature    294
_cell_volume                     1187(1)
_diffrn_ambient_temperature      294
_exptl_crystal_density_diffrn    1.31
_refine_ls_R_factor_obs          0.048
_refine_ls_wR_factor_obs         0.048
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               8100424
Crystal structure of 4,4')-bipyridinum dibromide, (C~10~H~10~N~2~)Br~2~
Zhang, Bi-Song; Zheng, Yue-Qing; Zeitschrift für Kristallographie - New Crystal Structures 218 (2003) 421–422; doi:

data_8100425
_publ_section_title
;
Crystal structure of 4,4')-bipyridinum dibromide, (C~10~H~10~N~2~)Br~2~
;
_journal_issue                   4
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              421
_journal_page_last               422
_journal_volume                  218
_journal_year                    2003
_chemical_formula_structural     'C5 H5 Br N'
_chemical_formula_sum            'C5 H5 Br N'
_chemical_formula_weight         159.01
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                70.468(9)
_cell_angle_beta                 87.029(9)
_cell_angle_gamma                77.153(11)
_cell_formula_units_Z            2
_cell_length_a                   4.8975(6)
_cell_length_b                   7.6539(11)
_cell_length_c                   7.9711(9)
_cell_measurement_temperature    293(2)
_cell_volume                     274.47(6)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.924
_cod_original_formula_sum        'C5 H5 Br1 N1'
_cod_database_code               8100425
Crystal structure of 5,11,17,23-tetra-tert-butyl-25,26- bis (diphenylphosphinoylmethoxy)-27,28-bis(benzoyl-methoxy)calix[4]-arene—ethyl acetate—hexane (1:1:0.5), C~86~H~90~O~8~P~2~ · C~4~H~8~O~2~ · 0.5C~6~H~14~, a new cavity-shaped ligand with eight oxygen donors
Steyer, Stéphane; Matt, Dominique; Welter, Richard; Louati, Alain; Zeitschrift für Kristallographie - New Crystal Structures 218 (2003) 423–426; doi:

data_8100426
_publ_section_title
;
Crystal structure of 5,11,17,23-tetra-tert-butyl-25,26- bis
(diphenylphosphinoylmethoxy)-27,28-bis(benzoyl-methoxy)calix[4]-arene---ethyl 
acetate---hexane (1:1:0.5), C~86~H~90~O~8~P~2~ &#x00B7; C~4~H~8~O~2~ &#x00B7; 
0.5C~6~H~14~, a new cavity-shaped ligand with eight oxygen donors
;
_journal_issue                   4
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              423
_journal_page_last               426
_journal_volume                  218
_journal_year                    2003
_chemical_formula_moiety         'C86 H90 O8 P2, C4 H8 O2, 1/2(C6 H14)'
_chemical_formula_structural     '(C86 H90 O8 P2)(C4 H8 O2) 0.5(C6 H14)'
_chemical_formula_sum            'C93 H105 O10 P2'
_chemical_formula_weight         1444.71
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                103.1431(9)
_cell_angle_beta                 91.4030(7)
_cell_angle_gamma                95.4738(7)
_cell_formula_units_Z            2
_cell_length_a                   10.4556(2)
_cell_length_b                   15.1838(2)
_cell_length_c                   26.8979(5)
_cell_measurement_temperature    173(2)
_cell_volume                     4134.68(12)
_diffrn_ambient_temperature      173(2)
_exptl_crystal_density_diffrn    1.160
_cod_database_code               8100426
Crystal structure of 5,11,17,23-tetra-t-butyl-25,27-dihydroxy- 26, 28-di-tosyloxy-calix[4]arene, C~58~H~68~O~8~S~2~
Paulus, E. F.; Joswig, W.; Boehmer, V.; Saadioui, M.; Krilow, M.; Peikert-Regelien, M.; Urschel, B.; Zeitschrift für Kristallographie - New Crystal Structures 218 (2003) 429–431; doi:

data_8100427
_publ_section_title
;
Crystal structure of 5,11,17,23-tetra-t-butyl-25,27-dihydroxy- 26,
28-di-tosyloxy-calix[4]arene, C~58~H~68~O~8~S~2~
;
_journal_issue                   4
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              429
_journal_page_last               431
_journal_volume                  218
_journal_year                    2003
_chemical_formula_sum            'C58 H68 O8 S2'
_chemical_formula_weight         957.24
_space_group_IT_number           9
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'C -2yc'
_symmetry_space_group_name_H-M   'C 1 c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 112.41(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   23.888(5)
_cell_length_b                   11.225(2)
_cell_length_c                   21.431(4)
_cell_measurement_temperature    293(2)
_cell_volume                     5312.6(18)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.197
_cod_original_sg_symbol_H-M      'C c'
_cod_database_code               8100427
Crystal structure of bis(2,6-diaminopyridinium) diaqua-bis-(2,6- pyridinedicarboxylato)-bis(2,6-pyridinedicarboxylato)-dibismuthate(III) tetrahydrate, (C~28~H~16~O~18~N~4~Bi~2~)(C~5~H~8~N~3~)~2~ · 4H~2~O
Ranjbar, M.; Aghabozorg, Hossein; Moghimi, Abolghasem; Zeitschrift für Kristallographie - New Crystal Structures 218 (2003) 432–434; doi:

data_8100428
_publ_section_title
;
Crystal structure of bis(2,6-diaminopyridinium) diaqua-bis-(2,6-
pyridinedicarboxylato)-bis(2,6-pyridinedicarboxylato)-dibismuthate(III) 
tetrahydrate, (C~28~H~16~O~18~N~4~Bi~2~)(C~5~H~8~N~3~)~2~ &#x00B7; 4H~2~O
;
_journal_issue                   4
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              432
_journal_page_last               434
_journal_volume                  218
_journal_year                    2003
_chemical_formula_moiety
'C28 H16 O18 N4 Bi2 2-, (C5 N3 H8+)2, (H2 O)4'
_chemical_formula_structural     '(C28 H16 O18 N4 Bi2)(C5 N3 H8+)2 4H2 O'
_chemical_formula_sum            'C38 H40 Bi2 N10 O22'
_chemical_formula_weight         1406.76
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                85.587(3)
_cell_angle_beta                 88.128(3)
_cell_angle_gamma                84.257(3)
_cell_formula_units_Z            1
_cell_length_a                   9.6994(12)
_cell_length_b                   10.4996(14)
_cell_length_c                   10.8903(14)
_cell_measurement_temperature    295(2)
_cell_volume                     1099.9(2)
_diffrn_ambient_temperature      295(2)
_exptl_crystal_density_diffrn    2.124
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               8100428
Crystal structure of 2,2'-bis(4,5-dimethylimidazole)-(dithiocyanato) mercury(II), Hg(C~10~H~14~N~4~)(CNS)~2~
Mahjoub, A.R.; Ramazani, A.; Morsali, A.; Zeitschrift für Kristallographie - New Crystal Structures 218 (2003) 435–436; doi:

data_8100429
_publ_section_title
;
Crystal structure of 2,2'-bis(4,5-dimethylimidazole)-(dithiocyanato)
mercury(II), Hg(C~10~H~14~N~4~)(CNS)~2~
;
_journal_issue                   4
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              435
_journal_page_last               436
_journal_volume                  218
_journal_year                    2003
_chemical_formula_structural     'C12 H14 Hg1 N6 S2'
_chemical_formula_sum            'C12 H14 Hg N6 S2'
_chemical_formula_weight         507.00
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                65.57(3)
_cell_angle_beta                 72.19(3)
_cell_angle_gamma                88.13(3)
_cell_formula_units_Z            2
_cell_length_a                   7.7321(15)
_cell_length_b                   10.252(2)
_cell_length_c                   11.802(2)
_cell_measurement_temperature    293(2)
_cell_volume                     806.3(3)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    2.088
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               8100429
Crystal structure of {2-[4-(4-chlorophenyl)-4-hydroxy-1-piperidinyl- methyl]cyclopentyl}-(4-fluorophenyl)-methanone, C~24~H~27~ClFNO~2~
Casellato, U.; Graziani, R.; Teijeira, M.; Uriarte, E.; Zeitschrift für Kristallographie - New Crystal Structures 218 (2003) 437–438; doi:

data_8100430
_publ_section_title
;
Crystal structure of {2-[4-(4-chlorophenyl)-4-hydroxy-1-piperidinyl-
methyl]cyclopentyl}-(4-fluorophenyl)-methanone, C~24~H~27~ClFNO~2~
;
_journal_issue                   4
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              437
_journal_page_last               438
_journal_volume                  218
_journal_year                    2003
_chemical_formula_structural     'C24 H27 Cl1 F1 N1 O2'
_chemical_formula_sum            'C24 H27 Cl F N O2'
_chemical_formula_weight         416.92
_chemical_melting_point          105.0(10)
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                87.18(3)
_cell_angle_beta                 67.27(3)
_cell_angle_gamma                88.01(3)
_cell_formula_units_Z            2
_cell_length_a                   9.494(2)
_cell_length_b                   10.769(2)
_cell_length_c                   11.377(3)
_cell_measurement_temperature    293
_cell_volume                     1071.4(5)
_diffrn_ambient_temperature      293
_exptl_crystal_density_diffrn    1.292
_refine_ls_R_factor_obs          0.0761
_refine_ls_wR_factor_obs         0.3021
_cod_depositor_comments
;
The following automatic conversions were performed:

'_chemical_melting_point' value '104-106' was changed to '105.0(10)'
- the average value was taken and precision was estimated.

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_formula_sum        'C24 H27 Cl1 F1 N1 O2'
_cod_database_code               8100430
Refinement of the crystal structure of the δ-modification of tris(8-hydroxyquinoline)aluminum(III), δ-Al(C~9~H~6~NO)~3~, the blue luminescent Alq3
Rajeswaran, Manju; Blanton, Thomas N.; Klubek, Kevin P.; Zeitschrift für Kristallographie - New Crystal Structures 218 (2003) 439–440; doi:

data_8100431
_publ_section_title
;
Refinement of the crystal structure of the \d-modification of 
tris(8-hydroxyquinoline)aluminum(III), \d-Al(C~9~H~6~NO)~3~, 
the blue luminescent Alq3
;
_journal_issue                   4
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              439
_journal_page_last               440
_journal_volume                  218
_journal_year                    2003
_chemical_formula_moiety         'C27 H18 Al N3 O3'
_chemical_formula_structural     'Al(C9 H6 NO)3'
_chemical_formula_sum            'C27 H18 Al N3 O3'
_chemical_formula_weight         459.42
_chemical_name_common            AlQ3
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                66.06(3)
_cell_angle_beta                 88.56(3)
_cell_angle_gamma                84.03(3)
_cell_formula_units_Z            2
_cell_length_a                   6.1810(12)
_cell_length_b                   13.268(3)
_cell_length_c                   14.430(3)
_cell_measurement_temperature    293(2)
_cell_volume                     1075.5(4)
_diffrn_ambient_temperature      293(2)
_diffrn_source_type              KappaCCD
_exptl_crystal_density_diffrn    1.419
_cod_database_code               8100431
Crystal structure of di(1,10-phenanthroline-N,N')di[μ-(2-furancarboxylato- O,O')-μ-(2-furancarboxylato-O,O':O')]di(nitrato)diterbium(III), Tb~2~(NO~3~)~2~(C~5~H~3~O~3~)~4~(C~12~H~8~N~2~)~2~
Li, Xia; Zou, Ying-Quan; Zeitschrift für Kristallographie - New Crystal Structures 218 (2003) 453–454; doi:

data_8100432
_publ_section_title
;
Crystal structure of di(1,10-phenanthroline-N,N')di[\m-(2-furancarboxylato-
O,O')-\m-(2-furancarboxylato-O,O':O')]di(nitrato)diterbium(III), 
Tb~2~(NO~3~)~2~(C~5~H~3~O~3~)~4~(C~12~H~8~N~2~)~2~
;
_journal_issue                   4
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              453
_journal_page_last               454
_journal_volume                  218
_journal_year                    2003
_chemical_formula_structural     'Tb2 (NO3)2(C5 H3 O3)4(C12 H8N2)2'
_chemical_formula_sum            'C22 H14 N3 O9 Tb'
_chemical_formula_weight         623.28
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                81.201(6)
_cell_angle_beta                 88.491(6)
_cell_angle_gamma                67.595(5)
_cell_formula_units_Z            2
_cell_length_a                   10.383(3)
_cell_length_b                   10.512(3)
_cell_length_c                   11.001(3)
_cell_measurement_temperature    293(2)
_cell_volume                     1096.4(6)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.888
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               8100432
Crystal structure of N-(4-(3,6-dioxo-4-phenylsulfanylcyclo-1,4-dienylamino))- 5-dimethylaminonaphtalene-sulfonamide, C~30~H~25~N~3~O~4~S~2~
Rubin-Preminger, J. M.; Illos, R. A.; Bittner, S.; Zeitschrift für Kristallographie - New Crystal Structures 218 (2003) 441–442; doi:

data_8100433
_publ_section_title
;
Crystal structure of N-(4-(3,6-dioxo-4-phenylsulfanylcyclo-1,4-dienylamino))-
5-dimethylaminonaphtalene-sulfonamide, C~30~H~25~N~3~O~4~S~2~
;
_journal_issue                   4
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              441
_journal_page_last               442
_journal_volume                  218
_journal_year                    2003
_chemical_formula_moiety         'C30 H25 N3 O4 S2'
_chemical_formula_structural     'C30 H25 N3 O4 S2'
_chemical_formula_sum            'C30 H25 N3 O4 S2'
_chemical_formula_weight         555.68
_chemical_melting_point          485.15
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 119.627(13)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   7.031(2)
_cell_length_b                   33.122(10)
_cell_length_c                   13.149(4)
_cell_measurement_temperature    293(2)
_cell_volume                     2661.8(14)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    1.387
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_chemical_melting_point' value '212\%' was changed to '485.15' - it
was converted from degrees Celsius(C) to Kelvins(K).

Automatic conversion script
Id: cif_fix_values 1646 2011-03-28 12:23:43Z adriana 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               8100433
Crystal structure of di[potassium(diaza-18-crown-6)]-dicaesium nonastannide (4‒) diethylenediamine, [K(C~12~H~26~N~2~O~4~)]~2~Cs2[Sn~9~] · 2C~2~N~2~H~8~, a polyanion [KCs~2SN9~] ‒ with low-dimensional arrangement of [Sn~9~] clusters
Hauptmann, Ralf; Fässler, Thomas F.; Zeitschrift für Kristallographie - New Crystal Structures 218 (2003) 455–457; doi:

data_8100434
_publ_section_title
;
Crystal structure of di[potassium(diaza-18-crown-6)]-dicaesium nonastannide
(4--) diethylenediamine, [K(C~12~H~26~N~2~O~4~)]~2~Cs2[Sn~9~] &#x00B7; 
2C~2~N~2~H~8~, a polyanion [KCs~2SN9~] -- with low-dimensional arrangement 
of [Sn~9~] clusters
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_journal_issue                   4
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              455
_journal_page_last               457
_journal_volume                  218
_journal_year                    2003
_chemical_formula_structural     'C28 H68 Cs2 K2 N8 O8 Sn9'
_chemical_formula_sum            'C28 H68 Cs2 K2 N8 O8 Sn9'
_chemical_formula_weight         2057.13
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 91.03(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   13.897(3)
_cell_length_b                   16.091(3)
_cell_length_c                   26.432(5)
_cell_measurement_temperature    153(2)
_cell_volume                     5909(2)
_diffrn_ambient_temperature      293(2)
_exptl_crystal_density_diffrn    2.312
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               8100434