Crystal structure of cis-dichlorobis(5-methyl-isoxazole)platinum(II), PtCl~2~(C~4~H~5~NO)~2~
E. Horn; A. Horiuchi; M. Yamanaka; M. Murakami; C. A. Horiuchi; Zeitschrift für Kristallographie - New Crystal Structures 220 (2005) 239–240; doi:

data_8101758
_publ_section_title
;
Crystal structure of cis-dichlorobis(5-methyl-isoxazole)platinum(II), 
PtCl~2~(C~4~H~5~NO)~2~
;
_journal_issue                   2
_journal_name_full
'Zeitschrift f\"ur Kristallographie - New Crystal Structures'
_journal_page_first              239
_journal_page_last               240
_journal_volume                  220
_journal_year                    2005
_chemical_formula_moiety         PtCl~2~(C~4~H~5~NO)~2~
_chemical_formula_sum            'C8 H10 Cl2 N2 O2 Pt'
_chemical_formula_weight         432.18
_chemical_name_systematic
' cis-dichlorobis(5-methylisoxazole)platinum(II)'
_space_group_IT_number           56
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      56
_symmetry_space_group_name_Hall  '-P 2ab 2ac'
_symmetry_space_group_name_H-M   'P c c n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   8.1012(9)
_cell_length_b                   21.113(2)
_cell_length_c                   14.014(2)
_cell_measurement_temperature    273.2
_cell_volume                     2397.0(5)
_computing_cell_refinement       'Bruker Software, SAINT-plus'
_computing_data_collection       'Bruker AXS Smart Apex CCD Diffractometer'
_computing_data_reduction        'Bruker Software, SAINT-plus'
_computing_molecular_graphics    ORTEP
_computing_publication_material  'teXsan Ver. 1.11'
_computing_structure_refinement  SHELXL-97
_computing_structure_solution    SIR92
_diffrn_measured_fraction_theta_full 1.3346
_diffrn_measured_fraction_theta_max 1.3346
_diffrn_measurement_device_type  'Bruker SMART APEX CCD'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.057
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       26
_diffrn_reflns_limit_k_min       -26
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -10
_diffrn_reflns_number            14768
_diffrn_reflns_theta_full        28.29
_diffrn_reflns_theta_max         28.29
_exptl_absorpt_coefficient_mu    12.088
_exptl_absorpt_correction_type   'SADABS [2]'
_exptl_crystal_colour            yellow'
_exptl_crystal_density_diffrn    2.395
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prismatic'
_exptl_crystal_size_max          0.150
_exptl_crystal_size_mid          0.150
_exptl_crystal_size_min          0.200
_refine_diff_density_max         1.72
_refine_diff_density_min         -1.82
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.079
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     136
_refine_ls_number_reflns         1929
_refine_ls_R_factor_gt           0.0353
_refine_ls_shift/su_max          0.0038
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      unit
_refine_ls_wR_factor_ref         0.0402
_reflns_number_gt                1929
_reflns_number_total             3978
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            1267-1504.cff
_cod_data_source_block           A_TEXRAY.INF_file_is_not_p
_cod_original_sg_symbol_H-M      Pccn
_cod_database_code               8101758