Nitric Oxide Sensing through 1,2,3,4-Oxatriazole Formation from Acylhydrazide: A Kinetic Study.
Islam, Abu Saleh Musha; Bhowmick, Rahul; Chandra Garain, Bidhan; Katarkar, Atul; Ali, Mahammad; The Journal of organic chemistry 83 (2018) 13287–13295; doi:10.1021/acs.joc.8b02110

data_4035758
_publ_section_title
;
 Nitric Oxide Sensing through 1,2,3,4-Oxatriazole Formation from
 Acylhydrazide: A Kinetic Study.
;
_journal_issue                   21
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              13287
_journal_page_last               13295
_journal_paper_doi               10.1021/acs.joc.8b02110
_journal_volume                  83
_journal_year                    2018
_chemical_formula_moiety         'C11 H10 N O3, N O3, O'
_chemical_formula_sum            'C11 H10 N2 O7'
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_space_group_crystal_system      triclinic
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_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2014/7 (Sheldrick 2014'
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_refine_ls_number_parameters     364
_refine_ls_number_reflns         5456
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.021
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_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+0.1128P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_total             5946
_reflns_threshold_expression     'I > 2\s(I)'
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