Synthesis and Structural Characterization of Hydrolysis Products within the Uranyl Iminodiacetate and Malate Systems
Daniel K. Unruh; Kyle Gojdas; Erin Flores; Anna Libo; Tori Z. Forbes; Inorganic Chemistry 52 (2013) 10191–10198; doi:10.1021/ic401705j

data_4335925
_publ_contact_author_address
;Department of Chemistry
W374 Chemistry Building
The University of Iowa
Iowa City, IA 52242-1294
USA
;
_publ_contact_author_fax         1-319-335-1270
_publ_contact_author_name        'Forbes, Tori M.'
_publ_contact_author_phone       1-319-384-1908
_publ_section_title
;
 Synthesis and Structural Characterization of Hydrolysis Products within
 the Uranyl Iminodiacetate and Malate Systems
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              10191
_journal_page_last               10198
_journal_paper_doi               10.1021/ic401705j
_journal_volume                  52
_journal_year                    2013
_chemical_formula_moiety         'C12 H9 K O24 U3, 2(C4 H12 N2), 4(O)'
_chemical_formula_sum            'C20 H31 K N4 O28 U3'
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_chemical_name_systematic
;
 ?
;
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_space_group_name_Hall           '-C 2yc'
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_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
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_cell_length_c                   16.5578(9)
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_cell_measurement_theta_min      2.39
_cell_volume                     7771.1(8)
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_computing_molecular_graphics    'CrystalMaker v2.5.0'
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_computing_structure_solution    'SHELXL-2013 (Sheldrick, 2013)'
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_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  KappaCCD
_diffrn_measurement_method       'CCD phi and omega scans'
_diffrn_radiation_monochromator  graphite
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_diffrn_reflns_limit_h_min       -29
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_exptl_absorpt_correction_type   multi-scan
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_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
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;
 w=1/[\s^2^(Fo^2^)+(0.0543P)^2^+137.6764P]
 where P=(Fo^2^+2Fc^2^)/3
;
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