Optimal diamagnetic dilution concentration for suppressing the dipole-dipole interaction in single-ion magnets.
Hu, Zhao-Bo; Feng, Xin; Li, Jing; Zhang, Yi-Quan; Yin, Lei; Wang, Zhenxing; Ouyang, Zhongwen; Kurmoo, Mohamedally; Song, You; Dalton transactions (Cambridge, England : 2003) 49 (2020) 2159–2167; doi:10.1039/c9dt04403e

data_7703680
_publ_section_title
;
 Optimal diamagnetic dilution concentration for suppressing the
 dipole-dipole interaction in single-ion magnets.
;
_journal_issue                   7
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2159
_journal_page_last               2167
_journal_paper_doi               10.1039/c9dt04403e
_journal_volume                  49
_journal_year                    2020
_chemical_formula_sum            'C20 H18 Co N2 O3'
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_space_group_name_Hall           '-P 2n 2ab'
_space_group_name_H-M_alt        'P b c n'
_atom_sites_solution_hydrogens   mixed
_audit_block_doi                 10.5517/ccdc.csd.cc229cxp
_audit_creation_method           SHELXL-2017/1
_audit_update_record
;
2019-05-11 deposited with the CCDC.	2020-01-08 downloaded from the CCDC.
;
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_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      23.47
_cell_measurement_theta_min      3.24
_cell_volume                     1671.9(7)
_computing_structure_refinement  'SHELXL-2017/1 (Sheldrick, 2017)'
_computing_structure_solution    'SHELXT 2014/4 (Sheldrick, 2014)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_Laue_measured_fraction_full 1.000
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_exptl_crystal_size_mid          0.280
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0508P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0937
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_reflns_number_gt                1028
_reflns_number_total             1475
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c9dt04403e2.cif
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_shelx_estimated_absorpt_t_min   0.744
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_shelx_res_checksum              74814