Two-electron oxidation of a homoleptic U(iii) guanidinate complex by diphenyldiazomethane.
Settineri, Nicholas S.; Shiau, Angela A.; Arnold, John; Chemical communications (Cambridge, England) 54 (2018) 10913–10916; doi:10.1039/c8cc06514d

data_7122337
_publ_section_title
;
 Two-electron oxidation of a homoleptic U(iii) guanidinate complex by
 diphenyldiazomethane.
;
_journal_issue                   77
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              10913
_journal_page_last               10916
_journal_paper_doi               10.1039/c8cc06514d
_journal_volume                  54
_journal_year                    2018
_chemical_formula_moiety         'C39 H84 Cl N9 U, C6 H14, C3 H7'
_chemical_formula_sum            'C48 H105 Cl N9 U'
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_symmetry_space_group_name_Hall  '-P 2ybc'
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;
2018-08-07 deposited with the CCDC.
2018-09-06 downloaded from the CCDC.
;
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Olex2 1.2-ac3
(compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381)
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0365P)^2^+4.7613P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c8cc06514d2.cif
_cod_data_source_block           UCl(TIG)3
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'Adding full bibliography for 7122334--7122339.cif.'
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