LMucko/crystallography-open-database huggingface dataset:
Sur un fluorure mixte d'etain II et IV : (NH4)3Sn3F11
Soufiane, A.; Vilminot, S.; Revue de Chimie Minerale 22 (1985) 799–808; doi:

data_1518101
_publ_section_title
;
 Sur un fluorure mixte d'etain II et IV : (NH4)3Sn3F11
;
_journal_name_full               'Revue de Chimie Minerale'
_journal_page_first              799
_journal_page_last               808
_journal_volume                  22
_journal_year                    1985
_chemical_formula_sum            'F11 H12 N3 Sn3'
_chemical_formula_weight         619.23
_space_group_IT_number           35
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      35
_symmetry_space_group_name_Hall  'C 2 -2'
_symmetry_space_group_name_H-M   'C m m 2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   12.773(3)
_cell_length_b                   25.564(6)
_cell_length_c                   8.052(1)
_cell_volume                     2629.2(9)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    5.768
_exptl_crystal_density_diffrn    3.128
_exptl_crystal_density_meas      3.11
_refine_ls_number_reflns         1619
_refine_ls_R_factor_gt           0.042
_cod_data_source_file            RCM-1985-22-799-808.cif
_cod_data_source_block           '[NH4]3Sn3F11'
_cod_original_formula_sum        'H12 F11 N3 Sn3'
_cod_database_code               1518101
Die struktur von Na2Ta4O11
Mattes, R.; Schaper, J.; Revue de Chimie Minerale 22 (1985) 817–820; doi:

data_1518102
_publ_section_title
;
 Die struktur von Na2Ta4O11
;
_journal_name_full               'Revue de Chimie Minerale'
_journal_page_first              817
_journal_page_last               820
_journal_volume                  22
_journal_year                    1985
_chemical_formula_sum            'Na2 O11 Ta4'
_chemical_formula_weight         945.78
_space_group_IT_number           167
_symmetry_cell_setting           trigonal
_symmetry_Int_Tables_number      167
_symmetry_space_group_name_Hall  '-R 3 2"c'
_symmetry_space_group_name_H-M   'R -3 c :H'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            6
_cell_length_a                   6.198(3)
_cell_length_b                   6.198(3)
_cell_length_c                   36.56(2)
_cell_volume                     1216.3(11)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    53.962
_exptl_crystal_density_diffrn    7.747
_exptl_crystal_F_000             2412
_refine_ls_number_reflns         164
_refine_ls_R_factor_gt           0.048
_refine_ls_wR_factor_gt          0.044
_cod_data_source_file            RCM-1985-22-817-820.cif
_cod_data_source_block           Na2Ta4O11
_cod_original_cell_volume        1216.3(16)
_cod_original_sg_symbol_H-M      'R -3 c'
_cod_database_code               1518102
On Na6Ge2Se7, the first selenidosorogermanate(IV)
Eisenmann, Brigitte; Hansa, Jendy; Schafer, Herbert; Revue de Chimie Minerale 23 (1986) 8–13; doi:

data_1518103
_publ_section_title
;
 On Na6Ge2Se7, the first selenidosorogermanate(IV)
;
_journal_name_full               'Revue de Chimie Minerale'
_journal_page_first              8
_journal_page_last               13
_journal_volume                  23
_journal_year                    1986
_chemical_formula_sum            'Ge2 Na6 Se7'
_chemical_formula_weight         835.88
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 104.7(1)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.451(4)
_cell_length_b                   10.914(4)
_cell_length_c                   15.874(6)
_cell_volume                     1583.8(13)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    20.009
_exptl_crystal_density_diffrn    3.50
_exptl_crystal_density_meas      3.58
_exptl_crystal_F_000             1472
_refine_ls_number_parameters     71
_refine_ls_number_reflns         1308
_refine_ls_wR_factor_gt          0.068
_cod_data_source_file            RCM-1986-23-8-13.cif
_cod_data_source_block           Na6Ge2Se7
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               1518103
The crystal structure of dirhodium tetrabutyrate
Cotton, Albert; Shiu, Kom-Bei; Revue de Chimie Minerale 23 (1986) 14–19; doi:

data_1518110
_publ_section_title
;
 The crystal structure of dirhodium tetrabutyrate
;
_journal_name_full               'Revue de Chimie Minerale'
_journal_page_first              14
_journal_page_last               19
_journal_volume                  23
_journal_year                    1986
_chemical_formula_sum            'C16 H28 O8 Rh2'
_chemical_formula_weight         554.21
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                91.72(4)
_cell_angle_beta                 94.08(7)
_cell_angle_gamma                105.97(4)
_cell_formula_units_Z            1
_cell_length_a                   5.231(4)
_cell_length_b                   8.841(3)
_cell_length_c                   11.76(2)
_cell_volume                     520.9(10)
_diffrn_ambient_temperature      296(2)
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    1.5944
_exptl_crystal_density_diffrn    1.766
_refine_ls_number_parameters     118
_refine_ls_number_reflns         1073
_refine_ls_R_factor_gt           0.062
_refine_ls_wR_factor_gt          0.078
_cod_data_source_file            RCM-1986-23-14-19.cif
_cod_data_source_block           Rh-tetrabutyrate
_cod_original_formula_sum        'C16 H28 Rh2 O8'
_cod_database_code               1518110
Structure cristalline de l'oxyfluoromolybdate de sodium NaMoO3F
Moutou, Jpseph-Marie; Chaminade, Jean-Pierre; Pouchard, Michel; Hagenmuller, Paul; Revue de Chimie Minerale 23 (1986) 27–34; doi:

data_1518111
_publ_section_title
;
 Structure cristalline de l'oxyfluoromolybdate de sodium NaMoO3F
;
_journal_name_full               'Revue de Chimie Minerale'
_journal_page_first              27
_journal_page_last               34
_journal_volume                  23
_journal_year                    1986
_chemical_formula_sum            'F Mo Na O3'
_chemical_formula_weight         185.93
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      11
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 110.08(5)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   7.138(3)
_cell_length_b                   3.715(2)
_cell_length_c                   6.511(3)
_cell_volume                     162.16(14)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.70929
_exptl_absorpt_coefficient_mu    4.027
_exptl_crystal_density_diffrn    3.808
_exptl_crystal_F_000             172
_refine_ls_number_reflns         410
_refine_ls_R_factor_gt           0.054
_cod_data_source_file            RCM-1986-23-27-34.cif
_cod_data_source_block           NaMoO3F
_cod_original_sg_symbol_H-M      'P 21/m'
_cod_database_code               1518111
Structure cristalline de l'oxyfluorure TlU3OF11
Hsini, Sifeddine; Caignol, Elisabeth; Metin, Jacques; Avignant, Daniel; Cousseins, Jean-Claude; Revue de Chimie Minerale 23 (1986) 35–47; doi:

data_1518112
_publ_section_title
;
 Structure cristalline de l'oxyfluorure TlU3OF11
;
_journal_name_full               'Revue de Chimie Minerale'
_journal_page_first              35
_journal_page_last               47
_journal_volume                  23
_journal_year                    1986
_chemical_formula_sum            'F11 O Tl U3'
_chemical_formula_weight         1143.47
_space_group_IT_number           8
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      8
_symmetry_space_group_name_Hall  'C -2y'
_symmetry_space_group_name_H-M   'C 1 m 1'
_cell_angle_alpha                90
_cell_angle_beta                 90.00(3)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   14.051(3)
_cell_length_b                   8.106(3)
_cell_length_c                   8.389(2)
_cell_volume                     955.5(5)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    67.65
_exptl_crystal_density_diffrn    7.95
_exptl_crystal_density_meas      7.88
_exptl_crystal_F_000             1858
_refine_ls_number_reflns         1526
_refine_ls_R_factor_gt           0.060
_cod_data_source_file            RCM-1986-23-35-47.cif
_cod_data_source_block           TlU3OF11
_cod_original_sg_symbol_H-M      'C m'
_cod_database_code               1518112
Determination structurale du chromate de thallium trivalent Tl2(CrO4)3
Riou, A.; Gerault, Y.; Cudennec, Y.; Revue de Chimie Minerale 23 (1986) 70–79; doi:

data_1518113
_publ_section_title
;
 Determination structurale du chromate de thallium trivalent Tl2(CrO4)3
;
_journal_name_full               'Revue de Chimie Minerale'
_journal_page_first              70
_journal_page_last               79
_journal_volume                  23
_journal_year                    1986
_chemical_formula_sum            'Cr3 O12 Tl2'
_chemical_formula_weight         756.76
_space_group_IT_number           60
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      60
_symmetry_space_group_name_Hall  '-P 2n 2ab'
_symmetry_space_group_name_H-M   'P b c n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   12.869(2)
_cell_length_b                   8.716(5)
_cell_length_c                   8.6989(13)
_cell_volume                     975.7(6)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    36.212
_exptl_crystal_density_diffrn    5.152
_exptl_crystal_density_meas      5.07
_exptl_crystal_F_000             1320
_refine_ls_number_parameters     79
_refine_ls_number_reflns         626
_refine_ls_R_factor_gt           0.049
_refine_ls_wR_factor_gt          0.058
_cod_data_source_file            RCM-1986-23-70-79.cif
_cod_data_source_block           Tl2[CrO4]3
_cod_database_code               1518113
Phases de type quartz alpha ; structure de FePO4 et spectrometrie Mossbauer du fer-57
Goiffon, Aline; Jumas, Jean-Claude; Philippot, Etienne; Revue de Chimie Minerale 23 (1986) 99–110; doi:

data_1518114
_publ_section_title
;
 Phases de type quartz alpha ; structure de FePO4 et spectrometrie
 Mossbauer du fer-57
;
_journal_name_full               'Revue de Chimie Minerale'
_journal_page_first              99
_journal_page_last               110
_journal_volume                  23
_journal_year                    1986
_chemical_formula_sum            'Fe O4 P'
_chemical_formula_weight         150.82
_space_group_IT_number           152
_symmetry_cell_setting           trigonal
_symmetry_Int_Tables_number      152
_symmetry_space_group_name_Hall  'P 31 2"'
_symmetry_space_group_name_H-M   'P 31 2 1'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            3
_cell_length_a                   5.021(2)
_cell_length_b                   5.021(2)
_cell_length_c                   11.229(4)
_cell_volume                     245.16(16)
_diffrn_ambient_temperature      173
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    4.931
_exptl_crystal_density_diffrn    3.064
_exptl_crystal_F_000             219
_refine_ls_number_reflns         373
_refine_ls_R_factor_gt           0.032
_cod_data_source_file            RCM-1986-23-99-110-1.cif
_cod_data_source_block           FePO4-173K
_cod_original_cell_volume        245.2(2)
_cod_database_code               1518114
Phases de type quartz alpha ; structure de FePO4 et spectrometrie Mossbauer du fer-57
Goiffon, Aline; Jumas, Jean-Claude; Philippot, Etienne; Revue de Chimie Minerale 23 (1986) 99–110; doi:

data_1518115
_publ_section_title
;
 Phases de type quartz alpha ; structure de FePO4 et spectrometrie
 Mossbauer du fer-57
;
_journal_name_full               'Revue de Chimie Minerale'
_journal_page_first              99
_journal_page_last               110
_journal_volume                  23
_journal_year                    1986
_chemical_formula_sum            'Fe O4 P'
_chemical_formula_weight         150.82
_space_group_IT_number           152
_symmetry_cell_setting           trigonal
_symmetry_Int_Tables_number      152
_symmetry_space_group_name_Hall  'P 31 2"'
_symmetry_space_group_name_H-M   'P 31 2 1'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            3
_cell_length_a                   5.027(2)
_cell_length_b                   5.027(2)
_cell_length_c                   11.234(4)
_cell_volume                     245.86(16)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    4.917
_exptl_crystal_density_diffrn    3.055
_exptl_crystal_F_000             219
_refine_ls_number_reflns         335
_refine_ls_R_factor_gt           0.028
_cod_data_source_file            RCM-1986-23-99-110-2.cif
_cod_data_source_block           FePO4-293K
_cod_original_cell_volume        245.9(2)
_cod_database_code               1518115
Structure et proprietes d'optique non lineaire de KTiOAsO4
El Brahimi, M.; Durand, J.; Revue de Chimie Minerale 23 (1986) 146–153; doi:

data_1518116
_publ_section_title
;
 Structure et proprietes d'optique non lineaire de KTiOAsO4
;
_journal_name_full               'Revue de Chimie Minerale'
_journal_page_first              146
_journal_page_last               153
_journal_volume                  23
_journal_year                    1986
_chemical_formula_sum            'As K O5 Ti'
_chemical_formula_weight         241.89
_space_group_IT_number           33
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      33
_symmetry_space_group_name_Hall  'P -2ac -2n'
_symmetry_space_group_name_H-M   'P n 21 a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   13.103(2)
_cell_length_b                   10.746(1)
_cell_length_c                   6.558(1)
_cell_volume                     923.4(2)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    9.783
_exptl_crystal_density_diffrn    3.480
_exptl_crystal_density_meas      3.484
_exptl_crystal_F_000             912
_refine_ls_number_reflns         760
_refine_ls_R_factor_gt           0.03
_cod_data_source_file            RCM-1986-23-146-153.cif
_cod_data_source_block           KTiOAsO4
_cod_database_code               1518116
Structures et magnetisme des nouveaux siliciures ternaires RMnSi2 (R = La-Sm) et RFeSi2 (R = La-Nd)
Venturini, G.; Malaman, B.; Meot-Meyer, M.; Fruchart, D.; Le Caer, G.; Malterre, D.; Roques, B.; Revue de Chimie Minerale 23 (1986) 162–182; doi:

data_1518117
_publ_section_title
;
 Structures et magnetisme des nouveaux siliciures ternaires RMnSi2 (R =
 La-Sm) et RFeSi2 (R = La-Nd)
;
_journal_name_full               'Revue de Chimie Minerale'
_journal_page_first              162
_journal_page_last               182
_journal_volume                  23
_journal_year                    1986
_chemical_formula_sum            'La Mn Si2'
_chemical_formula_weight         250.03
_space_group_IT_number           63
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      63
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   4.191(3)
_cell_length_b                   17.68(1)
_cell_length_c                   4.073(3)
_cell_volume                     301.8(4)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.542
_exptl_crystal_density_diffrn    5.503
_refine_ls_R_I_factor            0.04
_cod_data_source_file            RCM-1986-23-162-182.cif
_cod_data_source_block           LaMnSi2
_cod_database_code               1518117
Perovskite to Postperovskite Transition in NaFeF3
Bernal, Fabian L.; Yusenko, Kirill V.; Sottmann, Jonas; Drathen, Christina; Guignard, Jérémy; Løvvik, Ole Martin; Crichton, Wilson A.; Margadonna, Serena; Inorganic Chemistry  (2014) 141029080759008–; doi:10.1021/ic502224y

data_4341415
_publ_section_title
;
 Perovskite to Postperovskite Transition in NaFeF3
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              141029080759008
_journal_paper_doi               10.1021/ic502224y
_journal_year                    2014
_chemical_formula_analytical     NaFeF3
_chemical_formula_moiety         NaFeF3
_chemical_formula_structural     NaFeF3
_chemical_formula_sum            'F3 Fe Na'
_chemical_formula_weight         135.84
_space_group_IT_number           63
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_audit_update_record
;
2014-09-10 # Formatted by publCIF

;
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   3.13774(4)
_cell_length_b                   10.20870(10)
_cell_length_c                   7.45875(9)
_cell_measurement_temperature    300
_cell_volume                     238.921(5)
_computing_structure_refinement  GSAS
_diffrn_ambient_temperature      300
_diffrn_measurement_device_type  ID31
_diffrn_radiation_type           synchrotron
_diffrn_radiation_wavelength     0.3999
_pd_block_id                     2014-09-10T16:28|PPV_RT_phase1|BaAs_233-2||
_pd_phase_name                   'NaFeF3 FM001 RT ID09 ESRF'
_refine_ls_goodness_of_fit_all   1.33
_refine_ls_matrix_type           full
_refine_ls_number_parameters     23
_refine_ls_number_restraints     0
_refine_ls_shift/su_max          0.07
_refine_ls_shift/su_mean         0.01
_cod_data_source_file            ic502224y_si_002.cif
_cod_data_source_block           PPV_RT_phase_1
_cod_original_cell_volume        238.921(4)
_cod_original_formula_sum        F3FeNa
_cod_database_code               4341415
_publcif_datablock.id            {15d6793f-0b54-44dd-81a5-d864469fb48d}
Hydrothermal synthesis and single-crystal structural characterization of the layered vanadium(IV) phosphate VOC6H5PO3.cntdot.H2O
Huan, Guohe; Jacobson, Allan J.; Johnson, Jack W.; Corcoran, Edward W.; Chemistry of Materials 2 (1990) 91–; doi:10.1021/cm00008a002

data_4002072
_publ_section_title
;
 Hydrothermal synthesis and single-crystal structural characterization of
 the layered vanadium(IV) phosphate VOC6H5PO3.cntdot.H2O
;
_journal_issue                   2
_journal_name_full               'Chemistry of Materials'
_journal_page_first              91
_journal_paper_doi               10.1021/cm00008a002
_journal_volume                  2
_journal_year                    1990
_chemical_formula_moiety         'V O C6 H5 P O3, H2 O'
_chemical_formula_sum            'C6 H7 O5 P V'
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 97.1(2)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   28.50(3)
_cell_length_b                   7.18(2)
_cell_length_c                   9.42(2)
_cell_volume                     1913(7)
_computing_structure_solution
'TEXSAN (TEXRAY Structure Analysis Package, Molecular Structure Corp., 1985)'
_diffrn_ambient_temperature      296.15
_diffrn_measurement_device_type  'Rigaku AFC6R'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_theta_max         25
_diffrn_source_power             12
_diffrn_source_type              'rotating anode'
_exptl_absorpt_correction_T_max  1.42
_exptl_absorpt_correction_T_min  0.60
_exptl_absorpt_process_details   '(DIFABS; Walker & Stuart, 1983)'
_exptl_crystal_density_diffrn    1.661
_exptl_crystal_size_max          0.45
_exptl_crystal_size_mid          0.45
_exptl_crystal_size_min          0.05
_refine_ls_goodness_of_fit_all   3.03
_refine_ls_R_factor_all          0.091
_refine_ls_R_I_factor            0.078
_refine_ls_wR_factor_all         0.109
_reflns_number_gt                1092
_reflns_number_observed          1092
_reflns_number_total             1868
_reflns_observed_criterion       I>3u(I)
_cod_data_source_file            cm00008a002_si_001.cif
_cod_data_source_block           cm00008a002_si_001
_cod_depositor_comments
;
 Correcting several typos in the '_geom_angle_atom_site_label_2' data item
 values. Values '0(1)', '0(2)', '0(3)', '0(4)', 'c(1)' and 'v(1)' were changed
 to 'O(1)', 'O(2)', 'O(3)', 'O(4)', 'C(1)' and 'V(1)' accordingly.

 Antanas Vaitkus,
 2017-03-03

 Replacing the '_geom_bond_adc' data item with the '_geom_bond_site_symmetry_2'
 data item after consulting the supplementary material of the original
 publication. The values were also updated accordingly to meet the format
 recommended by the core CIF dictionary v. 2.4.5.

 Antanas Vaitkus,
 2017-03-03
;
_cod_original_cell_volume        1912(8)
_cod_database_code               4002072
_cod_database_fobs_code          4002072
_reflns_number_unique            1828