LMucko/crystallography-open-database huggingface dataset:
Structures of a partially deuterated sodium trihydrogen dimalonate and sodium hydrogen malonate (a reinvestigation) at 120 K
Kalsbeek, N.; Acta Crystallographica Section C 48 (1992) 878–883; doi:10.1107/S0108270191012489

data_2000902
_publ_section_title
;
 Structures of a partially deuterated sodium trihydrogen dimalonate and
 sodium hydrogen malonate (a reinvestigation) at 120 K
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              878
_journal_page_last               883
_journal_paper_doi               10.1107/S0108270191012489
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'Na1,C3 H3 O4,C3 H4 O4'
_chemical_formula_sum            'C6 H7 Na O8'
_chemical_formula_weight         230.11
_space_group_IT_number           62
_space_group_name_Hall           '-P 2ac 2n'
_space_group_name_H-M_alt        'P n m a'
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2n'
_symmetry_space_group_name_H-M   'P n m a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.484(2)
_cell_length_b                   6.859(2)
_cell_length_c                   14.950(5)
_cell_volume                     870.0(4)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    0.1951
_exptl_crystal_density_diffrn    1.757
_exptl_crystal_F_000             472
_cod_data_source_file            ab0248.cif
_cod_data_source_block           ab0248a
_cod_original_cell_volume        870.0(7)
_cod_original_formula_sum        'C6 H7 Na1 O8'
_cod_database_code               2000902
Structures of a partially deuterated sodium trihydrogen dimalonate and sodium hydrogen malonate (a reinvestigation) at 120 K
Kalsbeek, N.; Acta Crystallographica Section C 48 (1992) 878–883; doi:10.1107/S0108270191012489

data_2000903
_publ_section_title
;
 Structures of a partially deuterated sodium trihydrogen dimalonate and
 sodium hydrogen malonate (a reinvestigation) at 120 K
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              878
_journal_page_last               883
_journal_paper_doi               10.1107/S0108270191012489
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'Na1,C3 H3 O4'
_chemical_formula_sum            'C3 H3 Na O4'
_chemical_formula_weight         126.04
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 100.49(3)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   6.671(2)
_cell_length_b                   7.390(3)
_cell_length_c                   9.359(4)
_cell_volume                     453.7(3)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    0.2363
_exptl_crystal_density_diffrn    1.845
_exptl_crystal_F_000             256
_cod_data_source_file            ab0248.cif
_cod_data_source_block           ab0248b
_cod_original_cell_volume        453.7(5)
_cod_original_formula_sum        'C3 H3 Na1 O4'
_cod_database_code               2000903
Structure of (<i>Z</i>,<i>Z</i>)-3,11-diiodo-<i>N</i>,<i>N</i>-ditosyl-1,9-diazacyclohexadeca-3,11-diene
Anderson, M.; Gallagher, T.; Mahon, M. F.; Molloy, K. C.; Shaw, R.; Acta Crystallographica Section C 48 (1992) 883–885; doi:10.1107/S0108270191011782

data_2000904
_publ_section_title
;Structure of
 (<i>Z</i>,<i>Z</i>)-3,11-diiodo-<i>N</i>,<i>N</i>-ditosyl-1,9-diazacyclohexadeca-3,11-diene
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              883
_journal_page_last               885
_journal_paper_doi               10.1107/S0108270191011782
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C28 H36 I2 N2 O4 S2'
_chemical_formula_weight         782.5
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   11.153(4)
_cell_length_b                   14.833(3)
_cell_length_c                   19.332(5)
_cell_volume                     3198.1(16)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    2.103
_exptl_crystal_density_diffrn    1.62
_exptl_crystal_F_000             1552
_cod_data_source_file            al0477.cif
_cod_data_source_block           al0477_structure_1_of_1
_cod_original_cell_volume        3198.0
_cod_database_code               2000904
Spiro[(2,3-époxycyclohexane)-1:4'-(2',3'-dihydro-8'-méthoxybenzo-4<i>H</i>-pyranne)]
Rodier, N.; Zhang, Y. M.; Mayrargue, J.; Acta Crystallographica Section C 48 (1992) 885–887; doi:10.1107/S0108270191011605

data_2000905
_publ_section_title
Spiro[(2,3-\'epoxycyclohexane)-1:4'-(2',3'-dihydro-8'-m\'ethoxybenzo-4<i>H</i>-pyranne)]
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              885
_journal_page_last               887
_journal_paper_doi               10.1107/S0108270191011605
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'C15 H18 O3'
_chemical_formula_sum            'C15 H18 O3'
_chemical_formula_weight         246.3
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_H-M   'P b c n'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   26.085(7)
_cell_length_b                   7.211(2)
_cell_length_c                   13.653(6)
_cell_volume                     2568.1(15)
_diffrn_radiation_type           Cu
_diffrn_radiation_wavelength     1.5418
_exptl_absorpt_coefficient_mu    0.67
_exptl_crystal_density_diffrn    1.274
_exptl_crystal_F_000             1056
_cod_data_source_file            pa0239.cif
_cod_data_source_block           pa0239a
_cod_original_cell_volume        2568(3)
_cod_database_code               2000905
Structures of 2,2'-polymethylene-1,1'-biisoquinolinium dibromides
Mori, Y.; Matsuyama, Y.; Yamada, S.; Maeda, K.; Acta Crystallographica Section C 48 (1992) 894–897; doi:10.1107/S0108270191011885

data_2000906
_publ_section_title
;
 Structures of 2,2'-polymethylene-1,1'-biisoquinolinium dibromides
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              894
_journal_page_last               897
_journal_paper_doi               10.1107/S0108270191011885
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'C20 H16 Br2 N2'
_chemical_formula_sum            'C20 H16 Br2 N2'
_chemical_formula_weight         444.15
_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_Hall  'I 4bw -1bw'
_symmetry_space_group_name_H-M   'I 41/a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   14.696(3)
_cell_length_b                   14.696(3)
_cell_length_c                   15.853(3)
_cell_volume                     3423.8(12)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71068
_exptl_absorpt_coefficient_mu    4.69
_exptl_crystal_density_diffrn    1.72
_exptl_crystal_F_000             1760
_cod_data_source_file            as0544.cif
_cod_data_source_block           as0544_structure_1_of_2
_cod_original_cell_volume        3423.6(12)
_cod_database_code               2000906
Structures of 2,2'-polymethylene-1,1'-biisoquinolinium dibromides
Mori, Y.; Matsuyama, Y.; Yamada, S.; Maeda, K.; Acta Crystallographica Section C 48 (1992) 894–897; doi:10.1107/S0108270191011885

data_2000907
_publ_section_title
;
 Structures of 2,2'-polymethylene-1,1'-biisoquinolinium dibromides
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              894
_journal_page_last               897
_journal_paper_doi               10.1107/S0108270191011885
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'C21 H18 Br2 N2,H2 O1'
_chemical_formula_sum            'C21 H20 Br2 N2 O'
_chemical_formula_weight         476.17
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_cell_angle_alpha                95.320(10)
_cell_angle_beta                 92.64(2)
_cell_angle_gamma                114.70(2)
_cell_formula_units_Z            2
_cell_length_a                   9.934(2)
_cell_length_b                   13.285(3)
_cell_length_c                   7.9690(10)
_cell_volume                     947.2(3)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71068
_exptl_absorpt_coefficient_mu    4.25
_exptl_crystal_density_diffrn    1.67
_exptl_crystal_F_000             476
_cod_data_source_file            as0544.cif
_cod_data_source_block           as0544_structure_2_of_2
_cod_depositor_comments
;
 Updating space group information and adding the symmetry operation list.

 Antanas Vaitkus,
 2018-06-14

 Marking attached hydrogen atoms.

 Antanas Vaitkus,
 2017-03-24
;
_cod_original_cell_volume        947.1(3)
_cod_original_formula_sum        'C21 H20 Br2 N2 O1'
_cod_database_code               2000907
The first structure of a benzo[<i>b</i>][1,4]diazocine
Wallis, J. D.; Acta Crystallographica Section C 48 (1992) 897–899; doi:10.1107/S0108270191012337

data_2000908
_publ_section_title
;
 The first structure of a benzo[<i>b</i>][1,4]diazocine
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              897
_journal_page_last               899
_journal_paper_doi               10.1107/S0108270191012337
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C19 H18 N2 O'
_chemical_formula_weight         290.4
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 91.67(4)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.714(3)
_cell_length_b                   10.087(5)
_cell_length_c                   15.758(8)
_cell_volume                     1543.4(12)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    0.073
_exptl_crystal_density_diffrn    1.25
_exptl_crystal_F_000             616
_cod_data_source_file            al0503.cif
_cod_data_source_block           al0503a
_cod_original_cell_volume        1543.4
_cod_original_formula_sum        'C19 H18 N2 O1'
_cod_database_code               2000908
Refined molecular structure of tetrabenzo[<i>de</i>,<i>hi</i>,<i>op</i>,<i>st</i>]pentacene
Izuoka, A.; Wakui, K.; Fukuda, T.; Sato, N.; Sugawara, T.; Acta Crystallographica Section C 48 (1992) 900–902; doi:10.1107/S0108270191011800

data_2000909
_publ_section_title
;
 Refined molecular structure of
 tetrabenzo[<i>de</i>,<i>hi</i>,<i>op</i>,<i>st</i>]pentacene
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              900
_journal_page_last               902
_journal_paper_doi               10.1107/S0108270191011800
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C34 H18'
_chemical_formula_weight         426.48
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90
_cell_angle_beta                 91.41(4)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   11.814(5)
_cell_length_b                   7.8030(10)
_cell_length_c                   10.871(4)
_cell_volume                     1001.8(6)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    0.075
_exptl_crystal_density_diffrn    1.411
_exptl_crystal_F_000             444
_cod_data_source_file            as0534.cif
_cod_data_source_block           as0534a
_cod_original_cell_volume        1001.9(6)
_cod_original_sg_symbol_H-M      'P 21'
_cod_database_code               2000909
Studies on nonlinear optical materials: structure of diphenylmethyl (<i>Z</i>)-1-(1-methylthio-2-nitrovinyl)tetrahydropyrrole-2-carboxylate
Begum, N. S.; Venkatesan, K.; Acta Crystallographica Section C 48 (1992) 902–905; doi:10.1107/S0108270191011836

data_2000910
_publ_section_title
;
 Studies on nonlinear optical materials: structure of diphenylmethyl
 (<i>Z</i>)-1-(1-methylthio-2-nitrovinyl)tetrahydropyrrole-2-carboxylate
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              902
_journal_page_last               905
_journal_paper_doi               10.1107/S0108270191011836
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C21 H22 N2 O4 S'
_chemical_formula_weight         245.0
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.7990(10)
_cell_length_b                   11.8530(10)
_cell_length_c                   17.316(2)
_cell_volume                     2011.2(4)
_diffrn_radiation_type           Cu
_diffrn_radiation_wavelength     1.5418
_exptl_absorpt_coefficient_mu    1.57
_exptl_crystal_density_diffrn    1.314
_exptl_crystal_density_meas      1.320
_exptl_crystal_F_000             840
_cod_data_source_file            li0088.cif
_cod_data_source_block           li0088a
_cod_original_cell_volume        2011.4
_cod_original_formula_sum        'C21 H22 N2 O4 S1'
_cod_database_code               2000910
Structure of 1-acetylthymine
Tari, L. W.; Secco, A. S.; Acta Crystallographica Section C 48 (1992) 905–907; doi:10.1107/S0108270191012556

data_2000911
_publ_section_title
;
 Structure of 1-acetylthymine
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              905
_journal_page_last               907
_journal_paper_doi               10.1107/S0108270191012556
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'C7 H8 N2 O3'
_chemical_formula_sum            'C7 H8 N2 O3'
_chemical_formula_weight         168.5
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 94.57(4)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   5.074(3)
_cell_length_b                   8.611(3)
_cell_length_c                   17.476(4)
_cell_volume                     761.1(6)
_diffrn_radiation_type           Cu
_diffrn_radiation_wavelength     1.54178
_exptl_absorpt_coefficient_mu    0.95
_exptl_crystal_density_diffrn    1.467
_exptl_crystal_F_000             352
_cod_data_source_file            br0006.cif
_cod_data_source_block           br0006a
_cod_original_cell_volume        761.2(5)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2000911
Structure of [(1,2-η^2^)-1,3,5,7-cycloheptatetraene]bis(triphenylphosphine)platinum(0)
Abboud, K. A.; Lu, Z.; Jones, W. M.; Acta Crystallographica Section C 48 (1992) 909–912; doi:10.1107/S0108270191011289

data_2000912
_publ_section_title
;
 Structure of
 [(1,2-\h^2^)-1,3,5,7-cycloheptatetraene]bis(triphenylphosphine)platinum(0)
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              909
_journal_page_last               912
_journal_paper_doi               10.1107/S0108270191011289
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'C43 H36 P2 Pt1'
_chemical_formula_sum            'C43 H36 P2 Pt'
_chemical_formula_weight         809.82
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 111.68(4)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   13.664(7)
_cell_length_b                   16.783(8)
_cell_length_c                   16.702(8)
_cell_volume                     3559(3)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    4.10
_exptl_crystal_density_diffrn    1.51
_exptl_crystal_F_000             1608
_cod_data_source_file            st0542.cif
_cod_data_source_block           st0542a
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C43 H36 P2 Pt1'
_cod_database_code               2000912
Structure of di-μ-chloro-bis[1,3-bis(di-<i>tert</i>-butylphosphino)propaneplatinum(II)] tetrafluoroborate 0.8-dichloromethane solvate
Litster, S. A.; Mole, L.; Redhouse, A. D.; Spencer, J. L.; Acta Crystallographica Section C 48 (1992) 913–915; doi:10.1107/S0108270191012611

data_2000913
_publ_section_title
;
 Structure of
 di-\m-chloro-bis[1,3-bis(di-<i>tert</i>-butylphosphino)propaneplatinum(II)]
 tetrafluoroborate 0.8-dichloromethane solvate
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              913
_journal_page_last               915
_journal_paper_doi               10.1107/S0108270191012611
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'C38 H84 Cl2 P4 Pt2,2(B1 F4),0.8(C1 H2 Cl2)'
_chemical_formula_sum            'C39 H86 B2 Cl4 F8 P4 Pt2'
_chemical_formula_weight         1367.7
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                65.35(2)
_cell_angle_beta                 77.58(2)
_cell_angle_gamma                66.31(2)
_cell_formula_units_Z            1
_cell_length_a                   11.191(3)
_cell_length_b                   11.512(3)
_cell_length_c                   13.134(3)
_cell_volume                     1406.0(7)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.7107
_exptl_absorpt_coefficient_mu    5.36
_exptl_crystal_density_diffrn    1.615
_exptl_crystal_F_000             677.6
_cod_data_source_file            li0109.cif
_cod_data_source_block           li0109a
_cod_depositor_comments
;
 Marking attached hydrogen atoms.

 Antanas Vaitkus,
 2018-06-16

 Marking atoms 'Cl(3)', 'Cl(4)' and 'Cl(3A)', 'Cl(4A)' as belonging to disorder
 sites '1' and '2' with the occupancies of 0.6 and 0.2 respectively after
 consulting the original publication.

 Marking the 'C11A' atom as having the occupancy of 0.8 after consulting
 the original publication.

 Antanas Vaitkus,
 2018-06-15
;
_cod_original_cell_volume        1406.1(6)
_cod_database_code               2000913
Structure of tris(dicyclohexylphenylphosphine)gold(I) perchlorate
Muir, J. A.; Cuadrado, S. I.; Muir, M. M.; Acta Crystallographica Section C 48 (1992) 915–917; doi:10.1107/S0108270191011551

data_2000914
_publ_section_title
;
 Structure of tris(dicyclohexylphenylphosphine)gold(I) perchlorate
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              915
_journal_page_last               917
_journal_paper_doi               10.1107/S0108270191011551
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'C54 H81 Au1 P3,Cl1 O4'
_chemical_formula_sum            'C54 H81 Au Cl O4 P3'
_chemical_formula_weight         1119.59
_space_group_crystal_system      trigonal
_space_group_IT_number           161
_space_group_name_Hall           'R 3 -2"c'
_space_group_name_H-M_alt        'R 3 c :H'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                120
_cell_formula_units_Z            6
_cell_length_a                   13.192(5)
_cell_length_b                   13.192(5)
_cell_length_c                   52.83(2)
_cell_volume                     7962(5)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    2.95
_exptl_crystal_density_diffrn    1.401
_exptl_crystal_F_000             3468
_cod_data_source_file            st0543.cif
_cod_data_source_block           st0543a
_cod_depositor_comments
;
 Adding more significant digits to the coordinates of the 'Cl' and 
 'O1' atoms after consulting the original publication.

 Antanas Vaitkus,
 2017-12-03
;
_cod_original_cell_volume        7962(9)
_cod_original_sg_symbol_Hall     'R 3* -2"'
_cod_original_sg_symbol_H-M      'R 3 c'
_cod_original_formula_sum        'C54 H81 Au1 Cl1 O4 P3'
_cod_database_code               2000914
Structure of 2-chloroimidazolium aquatrichlorocuprate(II)
Valle, G.; Ettorre, R.; Acta Crystallographica Section C 48 (1992) 919–921; doi:10.1107/S0108270191011757

data_2000915
_publ_section_title
;
 Structure of 2-chloroimidazolium aquatrichlorocuprate(II)
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              919
_journal_page_last               921
_journal_paper_doi               10.1107/S0108270191011757
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'C3 H4 Cl1 N2,H2 Cl3 Cu1 O1'
_chemical_formula_sum            'C3 H6 Cl4 Cu N2 O'
_chemical_formula_weight         291.5
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 97.8(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.0230(10)
_cell_length_b                   13.881(2)
_cell_length_c                   7.3410(10)
_cell_volume                     910.9(5)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.7107
_exptl_absorpt_coefficient_mu    3.372
_exptl_crystal_density_diffrn    2.13
_exptl_crystal_F_000             572
_cod_data_source_file            ge0278.cif
_cod_data_source_block           ge0278a
_cod_original_formula_sum        'C3 H6 Cl4 Cu1 N2 O1'
_cod_database_code               2000915