A two-dimensional silver(I) coordination polymer constructed from 4-aminophenylarsonate and triphenylphosphane: poly[[(μ~3~-4-aminophenylarsonato-κ^3^<i>N</i>:<i>O</i>:<i>O</i>)(triphenylphosphane-κ<i>P</i>)silver(I)] monohydrate]
Xiao, Zu-Ping; Wen, Meng; Wang, Chun-Ya; Huang, Xi-He; Acta Crystallographica Section C 71 (2015) –; doi:10.1107/S2053229615003885

data_2019894
_publ_section_title
;
 A two-dimensional silver(I) coordination polymer constructed from
 4-aminophenylarsonate and triphenylphosphane:
 poly[[(\m~3~-4-aminophenylarsonato-\k^3^<i>N</i>:<i>O</i>:<i>O</i>)(triphenylphosphane-\k<i>P</i>)silver(I)]
 monohydrate]
;
_journal_coeditor_code           KU3147
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first
;
;
_journal_paper_doi               10.1107/S2053229615003885
_journal_volume                  71
_journal_year                    2015
_chemical_formula_iupac          '[Ag (C6 H7 As N O3) (C18 H15 P)] , H2 O'
_chemical_formula_moiety         'C24 H22 Ag As N O3 P, H2 O'
_chemical_formula_sum            'C24 H24 Ag As N O4 P'
_chemical_formula_weight         604.20
_chemical_name_systematic
;Poly[[(\m~3~-4-aminophenylarsonato-\k^3^<i>N</i>:<i>O</i>:<i>O</i>)(triphenylphosphane-\k<i>P</i>)silver(I)]
monohydrate]
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL97
_cell_angle_alpha                90.00
_cell_angle_beta                 106.13(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.751(3)
_cell_length_b                   10.014(2)
_cell_length_c                   16.418(4)
_cell_measurement_reflns_used    7233
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.4855
_cell_measurement_theta_min      3.2870
_cell_volume                     2329.7(9)
_computing_cell_refinement
;
CrystalClear (Rigaku, 2007)
;
_computing_data_collection
;
CrystalClear (Rigaku, 2007)
;
_computing_data_reduction
;
CrystalClear (Rigaku, 2007)
;
_computing_molecular_graphics
;
SHELXTL (Sheldrick, 2008)
;
_computing_publication_material
;
SHELXTL (Sheldrick, 2008)
;
_computing_structure_refinement
;
SHELXL97 (Sheldrick, 2008)
;
_computing_structure_solution
;
SHELXS97 (Sheldrick, 2008)
;
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 28.5714
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Rigaku Mercury CCD area-detector'
_diffrn_measurement_method       \w
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0417
_diffrn_reflns_av_sigmaI/netI    0.0350
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            18980
_diffrn_reflns_theta_full        25.50
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         3.29
_exptl_absorpt_coefficient_mu    2.375
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.7461
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(RAPID-AUTO; Rigaku, 1998)
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.723
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1208
_exptl_crystal_size_max          0.31
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.454
_refine_diff_density_min         -0.461
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.198
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     289
_refine_ls_number_reflns         5331
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.198
_refine_ls_R_factor_all          0.0491
_refine_ls_R_factor_gt           0.0433
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w = 1/[\s^2^(Fo^2^)+(0.0166P)^2^+2.6980P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0773
_refine_ls_wR_factor_ref         0.0794
_reflns_number_gt                4947
_reflns_number_total             5331
_reflns_threshold_expression     I>2\s(I)
_cod_data_source_file            ku3147sup1.cf
_cod_data_source_block           I
_cod_original_cell_volume        2329.8(9)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2019894
_cod_database_fobs_code          2019894