<i>catena</i>-Poly[[(2,2'-bipyridine-<i>N</i>,<i>N</i>')cobalt(II)]-μ-4,4'-oxydibenzoato-<i>O</i>,<i>O</i>':<i>O</i>'',<i>O</i>''']
Skakle, Janet M. S.; Foreman, Mark R. St J.; Plater, M. John; Acta Crystallographica Section E 57 (2001) m169–m171; doi:10.1107/S1600536801004949

data_2200113
_publ_section_title
<i>catena</i>-Poly[[(2,2'-bipyridine-<i>N</i>,<i>N</i>')cobalt(II)]-\m-4,4'-oxydibenzoato-<i>O</i>,<i>O</i>':<i>O</i>'',<i>O</i>''']
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m169
_journal_page_last               m171
_journal_paper_doi               10.1107/S1600536801004949
_journal_volume                  57
_journal_year                    2001
_chemical_formula_iupac          '[Co (C14 H8 O5) (C10 H8 N2)]'
_chemical_formula_moiety         'C24 H16 Co N2 O5'
_chemical_formula_sum            'C24 H16 Co N2 O5'
_chemical_formula_weight         471.32
_chemical_name_systematic
;
catena-Poly[[(2,2'-bipyridine-N,N')cobalt(II)]-
\m-4,4'-oxydibenzoato-O,O':O'',O''']
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 96.3600(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   7.8975(4)
_cell_length_b                   17.6323(8)
_cell_length_c                   15.1057(7)
_cell_measurement_reflns_used    18261
_cell_measurement_temperature    302(2)
_cell_measurement_theta_max      29.99
_cell_measurement_theta_min      2.31
_cell_volume                     2090.54(17)
_computing_cell_refinement       'SAINT (Bruker, 1999)'
_computing_data_collection       'SMART (Bruker, 1999)'
_computing_data_reduction        SAINT
_computing_molecular_graphics
'ORTEP-3 for Windows (Farrugia, 1997) and PLATON (Spek, 2000)'
_computing_publication_material  SHELXL97
_computing_structure_refinement  'SHELXL97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      302(2)
_diffrn_measured_fraction_theta_full .995
_diffrn_measured_fraction_theta_max .995
_diffrn_measurement_device_type  'Bruker SMART 1000 area CCD'
_diffrn_measurement_method       \f--\w
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     .71073
_diffrn_reflns_av_R_equivalents  .0501
_diffrn_reflns_av_sigmaI/netI    .0523
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            18261
_diffrn_reflns_theta_full        29.99
_diffrn_reflns_theta_max         29.99
_diffrn_reflns_theta_min         2.31
_exptl_absorpt_coefficient_mu    .861
_exptl_absorpt_correction_T_max  .928
_exptl_absorpt_correction_T_min  .816
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SADABS; Bruker, 1999)'
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.497
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             964
_exptl_crystal_size_max          .4
_exptl_crystal_size_mid          .1
_exptl_crystal_size_min          .1
_refine_diff_density_max         .296
_refine_diff_density_min         -.341
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   .936
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     289
_refine_ls_number_reflns         6071
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      .936
_refine_ls_R_factor_all          .0810
_refine_ls_R_factor_gt           .0416
_refine_ls_shift/su_max          .001
_refine_ls_shift/su_mean         .000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^)+(0.075P)^2^] where P = (Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         .1350
_reflns_number_gt                3584
_reflns_number_total             6071
_reflns_threshold_expression     I>2\s(I)
_cod_data_source_file            bt6026.cif
_cod_data_source_block           I
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               2200113
_cod_database_fobs_code          2200113