Supramolecular aggregation of yttrium thiocyanate with 4,4′-bipyridine
Petrosyants, Svetlana; Dobrokhotova, Zhanna; Ilyukhin, Andrey; Novotortsev, Vladimir; New Journal of Chemistry 38 (2014) 3803–; doi:10.1039/C4NJ00598H

data_7054354
_publ_section_title
;
 Supramolecular aggregation of yttrium thiocyanate with
 4,4&#x2032;-bipyridine
;
_journal_issue                   8
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              3803
_journal_paper_doi               10.1039/C4NJ00598H
_journal_volume                  38
_journal_year                    2014
_chemical_absolute_configuration ad
_chemical_formula_moiety         'C15 H20 N5 O4 S3 Y, C10 H8 N2'
_chemical_formula_sum            'C25 H28 N7 O4 S3 Y'
_chemical_formula_weight         675.63
_chemical_name_systematic
;
 ?
;
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_atom_sites_solution_hydrogens   mixed
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_cell_measurement_theta_min      2.6
_cell_volume                     3020.5(2)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
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_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
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_diffrn_measured_fraction_theta_max 0.975
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_monochromator  graphite
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_diffrn_reflns_limit_k_max       6
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            12585
_diffrn_reflns_point_group_measured_fraction_full 0.991
_diffrn_reflns_point_group_measured_fraction_max 0.973
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_diffrn_reflns_theta_max         27.492
_diffrn_reflns_theta_min         2.449
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_exptl_absorpt_correction_T_min  0.6291
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_refine_ls_abs_structure_details
;
 Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack   0.312(9)
_refine_ls_extinction_method     none
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_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0300P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                4438
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_cod_database_code               7054354