Expeditious Metal-Free Access to Functionalized Polycyclic Acetals under Mild Aqueous Conditions.
Kasare, Sanghratna; Bankar, Siddheshwar K.; Ramasastry, S. S. V.; Organic letters 16 (2014) 4284–4287; doi:10.1021/ol501986f

data_1517248
_publ_section_title
;
 Expeditious Metal-Free Access to Functionalized Polycyclic Acetals under
 Mild Aqueous Conditions.
;
_journal_issue                   16
_journal_name_full               'Organic letters'
_journal_page_first              4284
_journal_page_last               4287
_journal_paper_doi               10.1021/ol501986f
_journal_volume                  16
_journal_year                    2014
_chemical_formula_sum            'C10 H12 O4'
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_cell_length_b                   19.225(13)
_cell_length_c                   10.568(9)
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_computing_structure_refinement  'SHELXL-2013 (Sheldrick, 2013)'
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_diffrn_measured_fraction_theta_max 0.998
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_av_R_equivalents  0.0406
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_exptl_absorpt_coefficient_mu    0.103
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0836P)^2^+1.2535P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            ol501986f_si_002.cif
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_cod_depositor_comments
'Adding full bibliography for 1517248--1517249.cif.'
_cod_original_cell_volume        3906(6)
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_cod_database_code               1517248
_shelx_estimated_absorpt_t_min   0.98
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