POSSaxanes: active-template synthesis of organic-inorganic rotaxanes incorporating cubic silsesquioxane stoppers.
Grzelczak, Rafał A; Władyczyn, Anna; Białońska, Agata; John, Łukasz; Szyszko, Bartosz; Chemical communications (Cambridge, England) 59 (2023) 7579–7582; doi:10.1039/d3cc01706k

data_7131738
_publ_section_title
;
 POSSaxanes: active-template synthesis of organic-inorganic rotaxanes
 incorporating cubic silsesquioxane stoppers.
;
_journal_issue                   49
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              7579
_journal_page_last               7582
_journal_paper_doi               10.1039/d3cc01706k
_journal_volume                  59
_journal_year                    2023
_chemical_formula_moiety
;
C59 H91 N3 O13 Si8, C32 H34 N2 O2, C4 H8 O2
;
_chemical_formula_sum            'C95 H133 N5 O17 Si8'
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;
2023-05-04 deposited with the CCDC.	2023-05-09 downloaded from the CCDC.
;
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;
CrysAlisPro 1.171.42.42a (Rigaku Oxford Diffraction, 2022)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colorless
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0743P)^2^+11.1132P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_depositor_comments
'Adding full bibliography for 7131737--7131738.cif.'
_cod_database_code               7131738
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_oxdiff_exptl_absorpt_empirical_full_min 0.847
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;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_shelx_res_checksum              62984
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