New three-dimensional inorganic frameworks based on the uranophane-type sheet in monoamine templated uranyl-vanadates
Jouffret, Laurent; Shao, Zhenmian; Rivenet, Murielle; Abraham, Francis; Journal of Solid State Chemistry 183 (2010) 2290–2297; doi:10.1016/j.jssc.2010.07.035

data_1563491
_publ_section_title
;
 New three-dimensional inorganic frameworks based on the uranophane-type
 sheet in monoamine templated uranyl-vanadates
;
_journal_issue                   10
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              2290
_journal_page_last               2297
_journal_paper_doi               10.1016/j.jssc.2010.07.035
_journal_volume                  183
_journal_year                    2010
_chemical_absolute_configuration .
_chemical_formula_sum            'C6 H20 N O23 U4 V3'
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_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
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_cell_angle_beta                 96.437(3)
_cell_angle_gamma                105.955(3)
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_cell_length_a                   9.8273(6)
_cell_length_b                   11.0294(7)
_cell_length_c                   12.7506(8)
_cell_measurement_temperature    100
_cell_volume                     1297.31(14)
_computing_publication_material
'Jana2000 (Petricek, Dusek & Palatinus, 2000)'
_computing_structure_refinement
'Jana2000 (Petricek, Dusek & Palatinus, 2000)'
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_diffrn_measured_fraction_theta_full 0.99
_diffrn_measured_fraction_theta_max 0.87
_diffrn_measurement_device_type  SMART-1K-CCD
_diffrn_measurement_method       'omega scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           'Mo K\a'
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_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       20
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_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_gt    1.36
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_refine_ls_R_factor_gt           0.0342
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_refine_ls_structure_factor_coef F
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_reflns_threshold_expression     I>3\s(I)
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_cod_data_source_block           (I)
_cod_original_formula_sum        'C6 H20 N1 O23 U4 V3'
_cod_database_code               1563491