<i>catena</i>-Poly[bis(μ~3~-3-aminobenzoato-κ^4^<i>N</i>:<i>O</i>:<i>O</i>,<i>O</i>')bis(μ~2~-3-aminobenzoato-κ^3^<i>O</i>,<i>O</i>':<i>O</i>)dilead(II)]
Shen, Fwu Ming; Lush, Shie Fu; Acta Crystallographica Section E 66 (2010) m1427–; doi:10.1107/S1600536810041322

data_2227940
_publ_section_title
;
 <i>catena</i>-Poly[bis(\m~3~-3-aminobenzoato-\k^4^<i>N</i>:<i>O</i>:<i>O</i>,<i>O</i>')bis(\m~2~-3-aminobenzoato-\k^3^<i>O</i>,<i>O</i>':<i>O</i>)dilead(II)]
;
_journal_coeditor_code           RK2229
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1427
_journal_paper_doi               10.1107/S1600536810041322
_journal_volume                  66
_journal_year                    2010
_chemical_formula_iupac          '[Pb2 (C7 H6 N O2)4]'
_chemical_formula_moiety         "'C28 H24 N4 O8 Pb2"
_chemical_formula_sum            'C28 H24 N4 O8 Pb2'
_chemical_formula_weight         958.92
_chemical_name_systematic
;
<i>catena</i>-Poly[bis(\m~3~-3-aminobenzoato-
\k^4^<i>N</i>:<i>O</i>:<i>O</i>,<i>O</i>')bis(\m~2~-3-aminobenzoato-
\k^3^<i>O</i>,<i>O</i>':<i>O</i>)dilead(II)]
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_cell_angle_alpha                76.030(2)
_cell_angle_beta                 88.103(2)
_cell_angle_gamma                70.154(2)
_cell_formula_units_Z            1
_cell_length_a                   6.8610(3)
_cell_length_b                   7.8943(3)
_cell_length_c                   13.9022(8)
_cell_measurement_reflns_used    12232
_cell_measurement_temperature    295
_cell_measurement_theta_max      25.35
_cell_measurement_theta_min      2.04
_cell_volume                     686.33(6)
_computing_cell_refinement       '<i>SCALEPACK</i> (Otwinowski & Minor 1997)'
_computing_data_collection       '<i>COLLECT</i>   (Nonius, 2000)'
_computing_data_reduction
'<i>DENZO</i> and <i>SCALEPACK</i> (Otwinowski & Minor 1997)'
_computing_molecular_graphics    '<i>PLATON</i>   (Spek, 2009)'
_computing_publication_material  '<i>PLATON</i> (Spek, 2009)'
_computing_structure_refinement  '<i>SHELXL97</i> (Sheldrick, 2008)'
_computing_structure_solution    '<i>SHELXS97</i> (Sheldrick, 2008)'
_diffrn_ambient_temperature      295
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measurement_device_type  'Nonius KappaCCD'
_diffrn_measurement_method       'CCD rotation images, thick slices'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine--focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1030
_diffrn_reflns_av_sigmaI/netI    0.0787
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       -7
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            5451
_diffrn_reflns_reduction_process
;
;
_diffrn_reflns_theta_full        25.28
_diffrn_reflns_theta_max         25.28
_diffrn_reflns_theta_min         2.83
_exptl_absorpt_coefficient_mu    12.308
_exptl_absorpt_correction_T_max  0.791
_exptl_absorpt_correction_T_min  0.215
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(SCALEPACK; Otwinowski & Minor, 1997)'
_exptl_crystal_colour            pink
_exptl_crystal_density_diffrn    2.320
_exptl_crystal_density_method    'Not Measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             448
_exptl_crystal_size_max          0.180
_exptl_crystal_size_mid          0.160
_exptl_crystal_size_min          0.020
_refine_diff_density_max         3.232
_refine_diff_density_min         -5.118
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.046
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     190
_refine_ls_number_reflns         2470
_refine_ls_number_restraints     12
_refine_ls_restrained_S_all      1.043
_refine_ls_R_factor_all          0.0702
_refine_ls_R_factor_gt           0.0645
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.1239P)^2^+1.1995P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1637
_refine_ls_wR_factor_ref         0.1694
_reflns_number_gt                2218
_reflns_number_total             2470
_reflns_threshold_expression     I>2\s(I)
_cod_data_source_file            rk2229.cif
_cod_data_source_block           I
_cod_database_code               2227940
_cod_database_fobs_code          2227940