First experimental charge density study using a Bruker CMOS-type PHOTON 100 detector: the case of ammonium tetraoxalate dihydrate.
Jarzembska, Katarzyna N.; Kamiński, Radosław; Dobrzycki, Lukasz; Cyrański, Michał K; Acta crystallographica Section B, Structural science, crystal engineering and materials 70 (2014) 847–855; doi:10.1107/S2052520614017570

data_2311664
_publ_section_title
;
 First experimental charge density study using a Bruker CMOS-type PHOTON
 100 detector: the case of ammonium tetraoxalate dihydrate.
;
_journal_coeditor_code           PI5019
_journal_issue                   'Pt 5'
_journal_name_full
'Acta crystallographica Section B, Structural science, crystal engineering and materials'
_journal_page_first              847
_journal_page_last               855
_journal_paper_doi               10.1107/S2052520614017570
_journal_volume                  70
_journal_year                    2014
_chemical_formula_moiety         'C2 H2 O4, C2 H O4, 2(H2 O), H4 N'
_chemical_formula_sum            'C4 H11 N O10'
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_symmetry_space_group_name_Hall  '-P 1'
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_cell_volume                     457.45(5)
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_diffrn_measured_fraction_theta_full 0.98
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_diffrn_measurement_device_type  'Bruker AXS CMOS-type PHOTON 100 detector'
_diffrn_measurement_method       \w-scans
_diffrn_radiation_monochromator  'Bruker AXS TRIUMPH monochromator'
_diffrn_radiation_source         'Mo sealed tube'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0274
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
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_diffrn_reflns_reduction_process
;
Blessing, R. H. (1987). Cryst. Rev. 1, 3,
Blessing, R. H. (1997). J. Appl. Cryst. 30, 421.
;
_diffrn_reflns_theta_full        51.2
_diffrn_reflns_theta_max         62.67
_diffrn_reflns_theta_min         2.87
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_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
Blessing, R. H. (1995). Acta Cryst. A51, 33.
;
_exptl_crystal_colour            colourless
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_refine_diff_density_max         0.21
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