Two tris(3,5-disubstituted phenyl)phosphines and their isostructural P^V^ oxides
Hill, Nathan D. D.; Boeré, René T.; Acta Crystallographica Section E 74 (2018) 889–894; doi:10.1107/S2056989018007831

data_2242519
_publ_section_title
;
 Two tris(3,5-disubstituted phenyl)phosphines and their isostructural P^V^
 oxides
;
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              889
_journal_page_last               894
_journal_paper_doi               10.1107/S2056989018007831
_journal_volume                  74
_journal_year                    2018
_chemical_formula_iupac          'C27 H33 O3 P'
_chemical_formula_moiety         'C27 H33 O3 P'
_chemical_formula_sum            'C27 H33 O3 P'
_chemical_formula_weight         436.50
_chemical_name_common
;
Tris(4-methoxy-3,5-dimethylphenyl)phosphine
;
_chemical_name_systematic
;
Tris(4-methoxy-3,5-dimethylphenyl)phosphane
;
_space_group_crystal_system      orthorhombic
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_space_group_name_Hall           '-P 2ac 2ab'
_space_group_name_H-M_alt        'P b c a'
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
_atom_sites_solution_hydrogens   geom
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OLEX2 1.2
(compiled 2018.04.26 svn.r3504 for OlexSys, GUI svn.r5492)
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_computing_cell_refinement
;
CrysAlis PRO (Rigaku OD, 2015)
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CrysAlis PRO (Rigaku OD, 2015)
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CrysAlis PRO (Rigaku OD, 2015)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>,  2009)
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<i>OLEX2</i> (Dolomanov <i>et al.</i>,  2009)
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SHELXL2016 (Sheldrick, 2015b)
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SHELXT (Sheldrick, 2015a)
;
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'Rigaku Oxford Diffraction SuperNova, Dual, Cu at zero, Pilatus 200K'
_diffrn_measurement_method       '\w scans'
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_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       12
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;
(CrysAlis PRO; Rigaku OD, 2015)
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0756P)^2^+11.1312P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_shelx_res_checksum              24094