The Zinc–Acetic Anhydride Reduction of Pyridines
Beddoes, R. L.; Arshad, N.; Joule, J. A.; Acta Crystallographica Section C 52 (1996) 654–656; doi:10.1107/S0108270195013539

data_2004640
_publ_contact_author
;
Prof John A. Joule
Department of Chemistry
University of Manchester
Oxford Road
Manchester M13 9PL
England
;
_publ_section_title
;
 The Zinc--Acetic Anhydride Reduction of Pyridines
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              654
_journal_page_last               656
_journal_paper_doi               10.1107/S0108270195013539
_journal_volume                  52
_journal_year                    1996
_chemical_formula_iupac          'C15 H15 N1 O2'
_chemical_formula_moiety         'C15 H15 N1 O2'
_chemical_formula_sum            'C15 H15 N O2'
_chemical_formula_weight         241.29
_chemical_melting_point          370
_chemical_name_systematic
;
1,4-diacetyl-1,4-dihydro-4-phenylpyridine
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
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_cell_angle_gamma                90
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_cell_measurement_theta_min      29.11
_cell_volume                     1299.4(5)
_computing_cell_refinement       'MSC/AFC Diffractometer Control (1985)'
_computing_data_collection       'MSC/AFC Diffractometer Control (1985)'
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_computing_publication_material  'TEXSAN: FINISH (MSC, 1985)'
_computing_structure_refinement  'TEXSAN: LS (MSC, 1985)'
_computing_structure_solution    'SHELXS86 (Sheldrick, 1986)'
_diffrn_ambient_temperature      294
_diffrn_measurement_device       'Rigaku AFC-5R'
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Rigaku rotating anode'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.5418
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_diffrn_reflns_limit_h_min       -6
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_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.623
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.233
_exptl_crystal_density_meas      ?
_exptl_crystal_description       prismatic
_exptl_crystal_F_000             512
_exptl_crystal_size_max          0.45
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_refine_ls_extinction_method     'Zachariasen type II, Gaussian isotropic'
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_reflns_observed_criterion       I>3\s(I)
_cod_data_source_file            li1140.cif
_cod_data_source_block           S436-1
_cod_original_cell_volume        1299.5(5)
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C15 H15 N1 O2'
_cod_database_code               2004640