PNN' & P<sub>2</sub>NN' ligands via reductive amination with phosphine aldehydes: synthesis and base-metal coordination chemistry.
Gradiski, Matthew V.; Tsui, Brian T. H.; Lough, Alan J.; Morris, Robert H.; Dalton transactions (Cambridge, England : 2003) 48 (2019) 2150–2159; doi:10.1039/c8dt04058c

data_7048647
_publ_section_title
;
 PNN' &amp; P<sub>2</sub>NN' ligands via reductive amination with
 phosphine aldehydes: synthesis and base-metal coordination chemistry.
;
_journal_issue                   6
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2150
_journal_page_last               2159
_journal_paper_doi               10.1039/c8dt04058c
_journal_volume                  48
_journal_year                    2019
_chemical_formula_moiety         'C34 H34 Cl2 Fe N2 P2'
_chemical_formula_sum            'C34 H34 Cl2 Fe N2 P2'
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_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2018-10-09 deposited with the CCDC.
2019-01-16 downloaded from the CCDC.
;
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'sealed tube with Bruker Triumph monochromator'
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0259P)^2^+0.4404P] where P=(Fo^2^+2Fc^2^)/3'
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'Adding full bibliography for 7048646--7048653.cif.'
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