[<i>N</i>,<i>N</i>'-Bis(3-aminopropyl)-<i>trans</i>-1,2-cyclohexanediamine-<i>N</i>,<i>N</i>',<i>N</i>'',<i>N</i>''']di(perchlorato-<i>O</i>)copper(II)
Tahirov, T.H.; Lu, T.-H.; Shu, K.; Chung, C.-S.; Acta Crystallographica Section C 50 (1994) 518–520; doi:10.1107/S0108270193010005

data_2009586
_publ_section_title
'[<i>N</i>,<i>N</i>'-Bis(3-aminopropyl)-<i>trans</i>-1,2-cyclohexanediamine-<i>N</i>,<i>N</i>',<i>N</i>'',<i>N</i>''']di(perchlorato-<i>O</i>)copper(II)'
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              518
_journal_page_last               520
_journal_paper_doi               10.1107/S0108270193010005
_journal_volume                  50
_journal_year                    1994
_chemical_formula_moiety         'Cu (C12 H28 N4 ) (Cl O4 )2'
_chemical_formula_sum            'C12 H28 Cl2 Cu N4 O8'
_chemical_formula_weight         490.828
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                89.66(2)
_cell_angle_beta                 77.03(2)
_cell_angle_gamma                73.280(10)
_cell_formula_units_Z            2
_cell_length_a                   8.743(2)
_cell_length_b                   9.6560(10)
_cell_length_c                   12.088(3)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    298(3)
_cell_measurement_theta_max      15.35
_cell_measurement_theta_min      5.32
_cell_volume                     950.5(4)
_diffrn_measurement_device       'Nonius CAD-4'
_diffrn_measurement_method       \q/2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.7093
_diffrn_reflns_av_R_equivalents  0.011
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            5763
_diffrn_reflns_theta_max         29.9
_diffrn_standards_decay_%        +-0.8
_diffrn_standards_interval_time  60
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    1.48
_exptl_absorpt_correction_T_max  0.9837
_exptl_absorpt_correction_T_min  0.9679
_exptl_absorpt_correction_type   empirical
_exptl_crystal_density_diffrn    1.715
_exptl_crystal_description       parallelepiped
_exptl_crystal_size_max          0.53
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.19
_refine_diff_density_max         0.48
_refine_diff_density_min         -0.36
_refine_ls_extinction_coef       '0.42(1) length in mm'
_refine_ls_extinction_method     'Zachariasen (1967)'
_refine_ls_goodness_of_fit_obs   0.53
_refine_ls_hydrogen_treatment    refU
_refine_ls_number_parameters     273
_refine_ls_number_reflns         4295
_refine_ls_R_factor_obs          0.032
_refine_ls_shift/esd_max         0.004
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      unit
_refine_ls_wR_factor_obs         0.032
_reflns_number_observed          4295
_reflns_number_total             5522
_reflns_observed_criterion       I>=2.5\s(I)
_cod_data_source_file            as1069.cif
_cod_data_source_block           as1069_structure_1_of_1
_cod_original_cell_volume        950.5(3)
_cod_original_formula_sum        'C12 H28 Cl2 Cu1 N4 O8'
_cod_database_code               2009586