In situ reduction of Fe(iii) into Fe(ii): an example of post-crystallisation transformation.
Dechambenoit, Pierre; Ferlay, Sylvie; Kyritsakas, Nathalie; Hosseini, Mir Wais; Chemical communications (Cambridge, England)  (2009) 6798–6800; doi:10.1039/b914964c

data_7105026
_publ_section_title
;
 In situ reduction of Fe(iii) into Fe(ii): an example of
 post-crystallisation transformation.
;
_journal_issue                   44
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              6798
_journal_page_last               6800
_journal_paper_doi               10.1039/b914964c
_journal_year                    2009
_chemical_formula_moiety
'3(C26 H44 N4), 2(C6 Fe N6), 6( C0.11 O0.11 H0.33)'
_chemical_formula_sum            'C90.66 H134.64 Fe2 N24 O0.66'
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_chemical_name_systematic
;
?
;
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_diffrn_reflns_theta_min         2.27
_exptl_absorpt_coefficient_mu    0.355
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0515P)^2^+0.6668P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Trigonal' changed to 'trigonal' according
to '/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'none' was changed to '?' - the
value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_sg_symbol_H-M      P-3
_cod_database_code               7105026