Modifying the donor properties of tris(pyridyl)aluminates in lanthanide(ii) sandwich compounds.
García-Rodríguez, Raúl; Kopf, Sara; Wright, Dominic S.; Dalton transactions (Cambridge, England : 2003) 47 (2018) 2232–2239; doi:10.1039/c7dt04657j

data_7045311
_publ_section_title
;
 Modifying the donor properties of tris(pyridyl)aluminates in
 lanthanide(ii) sandwich compounds.
;
_journal_issue                   7
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2232
_journal_page_last               2239
_journal_paper_doi               10.1039/c7dt04657j
_journal_volume                  47
_journal_year                    2018
_chemical_formula_moiety         'C28 H39 Al I N3 O2 Yb, C4 H8 O'
_chemical_formula_sum            'C32 H47 Al I N3 O3 Yb'
_chemical_formula_weight         848.64
_chemical_properties_physical    Air-sensitive,Moisture-sensitive
_space_group_crystal_system      monoclinic
_space_group_IT_number           11
_space_group_name_Hall           '-P 2yb'
_space_group_name_H-M_alt        'P 1 21/m 1'
_symmetry_space_group_name_Hall  '-P 2yb'
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_atom_sites_solution_hydrogens   mixed
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_audit_update_record
;
2017-11-24 deposited with the CCDC.
2018-01-16 downloaded from the CCDC.
;
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_diffrn_radiation_type           CuK\a
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'Re-crystallisation from solvent: THF/hexane'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0802P)^2^+5.9532P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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'Adding full bibliography for 7045310--7045315.cif.'
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