Sels de <i>S</i>,<i>S</i>'-(alcane-α,ω-diyle)bis(thiouronium). II. Tétrachloroplatinate(II) de <i>S</i>,<i>S</i>'-(octane-1,8-diyle)bis(thiouronium)
Nguyen-Huy Dung; Viossat, B.; Lancelot, J.C.; Acta Crystallographica Section C 50 (1994) 1434–1437; doi:10.1107/S0108270194001198

data_2010067
_publ_section_title
;
 Sels de <i>S</i>,<i>S</i>'-(alcane-\a,\w-diyle)bis(thiouronium). II.
 T\'etrachloroplatinate(II) de
 <i>S</i>,<i>S</i>'-(octane-1,8-diyle)bis(thiouronium)
;
_journal_issue                   9
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1434
_journal_page_last               1437
_journal_paper_doi               10.1107/S0108270194001198
_journal_volume                  50
_journal_year                    1994
_chemical_formula_sum            'C10 H24 Cl4 N4 Pt S2'
_chemical_formula_weight         601.34
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2bc'
_symmetry_space_group_name_H-M   'P 1 1 21/b'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.
_cell_angle_beta                 90.
_cell_angle_gamma                100.12(3)
_cell_formula_units_Z            2
_cell_length_a                   7.144(4)
_cell_length_b                   9.417(3)
_cell_length_c                   14.862(5)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293.0(10)
_cell_measurement_theta_max      10.07
_cell_measurement_theta_min      2.9
_cell_volume                     984.3(7)
_diffrn_measurement_device       'Syntex-Nicolet P2~1~ quatre-cercles'
_diffrn_measurement_method       \q-2\q
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            4582
_diffrn_reflns_theta_max         35
_diffrn_standards_decay_%        <0.1
_diffrn_standards_interval_count 50
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    7.96
_exptl_absorpt_correction_T_max  0.5844
_exptl_absorpt_correction_T_min  0.0653
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'ABSCOR (Coppens, Leiserowitz & Rabinovich, 1965)'
_exptl_crystal_colour            orang\'e
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_exptl_crystal_density_meas      2.00(2)
_exptl_crystal_description       plaquette
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.24
_exptl_crystal_size_min          0.08
_refine_diff_density_max         1.91
_refine_diff_density_min         -1.79
_refine_ls_extinction_method     n\'eant
_refine_ls_goodness_of_fit_obs   3.5
_refine_ls_number_parameters     111
_refine_ls_number_reflns         2252
_refine_ls_R_factor_obs          0.034
_refine_ls_shift/esd_max         0.2
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/\s^2^(F)'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.038
_reflns_number_observed          2252
_reflns_number_total             4582
_reflns_observed_criterion       I>3\s(I)
_cod_data_source_file            pa1084.cif
_cod_data_source_block           pa1084_structure_1_of_1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value '1/\s^2^(F)' was changed to
'calc'. New tag '_refine_ls_weighting_details' was created. The value
of the new tag was set to 'w = 1/\s^2^(F)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        984.2(6)
_cod_database_code               2010067