Copper-Catalyzed Synthesis of Quinoline Derivatives via Tandem Knoevenagel Condensation, Amination and Cyclization
Dhiman, Shiv; Saini, Hitesh K.; Nandwana, Nitesh k; Kumar, Dalip; Kumar, Anil; RSC Adv.  (2016) –; doi:10.1039/C6RA03798D

data_7224377
_publ_section_title
;
 Copper-Catalyzed Synthesis of Quinoline Derivatives via Tandem
 Knoevenagel Condensation, Amination and Cyclization
;
_journal_name_full               'RSC Adv.'
_journal_paper_doi               10.1039/C6RA03798D
_journal_year                    2016
_chemical_formula_sum            'C H Br N O'
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_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2015-10-25 deposited with the CCDC.
2016-02-18 downloaded from the CCDC.
;
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_cell_measurement_temperature    296(2)
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_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      296(2)
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_diffrn_radiation_type           MoK\a
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_diffrn_reflns_av_unetI/netI     0.3056
_diffrn_reflns_laue_measured_fraction_full 0.998
_diffrn_reflns_laue_measured_fraction_max 0.979
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_diffrn_reflns_limit_l_max       17
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_exptl_absorpt_coefficient_mu    12.492
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_refine_diff_density_rms         0.339
_refine_ls_extinction_method     none
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_refine_ls_matrix_type           full
_refine_ls_number_parameters     343
_refine_ls_number_reflns         6642
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_refine_ls_restrained_S_all      1.360
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+0.6035P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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