Multilayer structure of an unsymmetrical monolayer lipid membrane with a ‘head-to-tail’ interface
Masuda, Mitsutoshi; Shimizu, Toshimi; Chemical Communications  (2001) 2442–; doi:10.1039/b106581p

data_7114968
_publ_section_title
;
 Multilayer structure of an unsymmetrical monolayer lipid membrane with a
 &#x2018;head-to-tail&#x2019; interface
;
_journal_issue                   23
_journal_name_full               'Chemical Communications'
_journal_page_first              2442
_journal_paper_doi               10.1039/b106581p
_journal_year                    2001
_chemical_formula_moiety         'C22 H44 N O8 '
_chemical_formula_sum            'C22 H44 N O8'
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_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      4
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_audit_creation_date             'Thu Apr 26 16:26:02 2001'
_audit_creation_method           'by teXsan'
_cell_angle_alpha                90
_cell_angle_beta                 106.48(1)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   4.905(1)
_cell_length_b                   40.139(1)
_cell_length_c                   6.289(1)
_cell_measurement_reflns_used    20
_cell_measurement_temperature    273.2
_cell_measurement_theta_max      27.56
_cell_measurement_theta_min      19.39
_cell_volume                     1187.3(3)
_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
_computing_data_reduction        'teXsan Ver. 1.11'
_computing_publication_material  'teXsan Ver. 1.11'
_computing_structure_refinement  'teXsan Ver. 1.10'
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_diffrn_measured_fraction_theta_full 0.5526
_diffrn_measured_fraction_theta_max 0.5526
_diffrn_measurement_device_type  'Rigaku AFC7R'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.5418
_diffrn_reflns_av_R_equivalents  0.014
_diffrn_reflns_limit_h_max       5
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       45
_diffrn_reflns_limit_k_min       0
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_diffrn_reflns_theta_full        59.96
_diffrn_reflns_theta_max         59.96
_diffrn_standards_decay_%        0.15
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.779
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_exptl_absorpt_correction_type   psi-scan
_exptl_absorpt_process_details   '(North, Phillips & Mathews, 1968)'
_exptl_crystal_colour            colorless
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_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prismatic
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.100
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_refine_diff_density_min         -0.17
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_refine_ls_R_factor_gt           0.0304
_refine_ls_shift/su_max          0.0657
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo) + 0.00126|Fo|^2^]'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                1900
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