Asymmetric Synthesis of Azepine-Fused Cyclobutanes from Yne-Methylenecyclopropanes Involving Cyclopropanation/C-C Cleavage/Wagner-Meerwein Rearrangement and Reaction Mechanism.
Li, Chen-Long; Yu, Zhi-Xiang; The Journal of organic chemistry 84 (2019) 9913–9928; doi:10.1021/acs.joc.9b01071

data_4034023
_publ_section_title
;
 Asymmetric Synthesis of Azepine-Fused Cyclobutanes from
 Yne-Methylenecyclopropanes Involving Cyclopropanation/C-C
 Cleavage/Wagner-Meerwein Rearrangement and Reaction Mechanism.
;
_journal_issue                   16
_journal_name_full               'The Journal of organic chemistry'
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_journal_paper_doi               10.1021/acs.joc.9b01071
_journal_volume                  84
_journal_year                    2019
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;
CrysAlisPro 1.171.39.29a (Rigaku Oxford Diffraction, 2015)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
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'w=1/[\s^2^(Fo^2^)+(0.0400P)^2^+3.5000P] where P=(Fo^2^+2Fc^2^)/3'
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