Tetrathiafulvalene Derivatives Linking a Dichalcogenolane Ring through the σ-Bond: New Donor Components for Organic Metals
Yamada, Jun-ichi; Oka, Rika; Mangetsu, Takashi; Akutsu, Hiroki; Nakatsuji, Shin'ichi; Nishikawa, Hiroyuki; Ikemoto, Isao; Kikuchi, Koichi; Chemistry of Materials 13 (2001) 1770–1777; doi:10.1021/cm000842x

data_4000046
_publ_section_title
;
 Tetrathiafulvalene Derivatives Linking a Dichalcogenolane Ring through the
 \s-Bond: New Donor Components for Organic Metals
;
_journal_coden_ASTM              CMATEX
_journal_issue                   5
_journal_name_full               'Chemistry of Materials'
_journal_page_first              1770
_journal_page_last               1777
_journal_paper_doi               10.1021/cm000842x
_journal_volume                  13
_journal_year                    2001
_chemical_formula_sum            'C23 H12 N4 O2 S8'
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_symmetry_cell_setting           triclinic
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_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                90.35(2)
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_cell_angle_gamma                95.495(8)
_cell_formula_units_Z            2
_cell_length_a                   8.0813(4)
_cell_length_b                   24.418(3)
_cell_length_c                   6.707(2)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    296
_cell_measurement_theta_max      37.8
_cell_measurement_theta_min      22.5
_cell_volume                     1267.2(4)
_diffrn_ambient_temperature      296.2
_diffrn_measurement_device       CAD4
_diffrn_measurement_method       theta/2theta
_diffrn_orient_matrix_UB_11      -0.12226
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_diffrn_orient_matrix_UB_13      0.00555
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_diffrn_orient_matrix_UB_33      0.13093
_diffrn_radiation_detector       'scintillation counter'
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_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_type           'Mo K\a'
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_exptl_absorpt_correction_type   PSI
_exptl_crystal_colour            Black
_exptl_crystal_density_diffrn    1.658
_exptl_crystal_density_meas      ?
_exptl_crystal_description       Plate
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_cod_original_sg_symbol_H-M      'P -1       '
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