The recent weathering of uraninite from the Cervena vein, Jachymov (Czech Republic): a fingerprint of the primary mineralization geochemistry onto the alteration association
Jakub Plasil; Jiri Sejkora; Radek Skoda; Pavel Skacha; Journal of GeoSciences 59 (2014) 223–253; doi:10.3190/jgeosci.171

data_1566324
_publ_section_title
;
 The recent weathering of uraninite from the Cervena vein, Jachymov (Czech
 Republic): a fingerprint of the primary mineralization geochemistry onto
 the alteration association
;
_journal_name_full               'Journal of GeoSciences'
_journal_page_first              223
_journal_page_last               253
_journal_paper_doi               10.3190/jgeosci.171
_journal_volume                  59
_journal_year                    2014
_chemical_absolute_configuration .
_chemical_formula_sum            'O37.895 S U6'
_chemical_formula_weight         2066.5
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                96.749(12)
_cell_angle_beta                 98.754(12)
_cell_angle_gamma                99.726(9)
_cell_formula_units_Z            2
_cell_length_a                   8.8556(9)
_cell_length_b                   13.9819(15)
_cell_length_c                   14.307(3)
_cell_measurement_reflns_used    1785
_cell_measurement_temperature    301.0(10)
_cell_measurement_theta_max      26.38
_cell_measurement_theta_min      3.43
_cell_volume                     1706.9(4)
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.24 (release 03-12-2012 CrysAlis171 .NET)
(compiled Dec  3 2012,18:21:49)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.24 (release 03-12-2012 CrysAlis171 .NET)
(compiled Dec  3 2012,18:21:49)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.24 (release 03-12-2012 CrysAlis171 .NET)
(compiled Dec  3 2012,18:21:49)
;
_diffrn_ambient_temperature      301
_diffrn_detector_area_resol_mean 10.3784
_diffrn_measured_fraction_theta_full 0.98
_diffrn_measured_fraction_theta_max 0.84
_diffrn_measurement_device       'four-cycle diffractometer'
_diffrn_measurement_device_type  'Xcalibur, Atlas, Gemini ultra'
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_source         'Enhance (Mo) X-ray Source'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.1552
_diffrn_reflns_av_unetI/netI     0.3315
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            17859
_diffrn_reflns_theta_full        27.11
_diffrn_reflns_theta_max         29.46
_diffrn_reflns_theta_min         2.84
_exptl_absorpt_coefficient_mu    28.54
_exptl_absorpt_correction_T_max  0.466
_exptl_absorpt_correction_T_min  0.083
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.24 (release 03-12-2012 CrysAlis171 .NET)
(compiled Dec  3 2012,18:21:49)
Analytical numeric absorption correction using a multifaceted crystal
			model based on expressions derived by R.C. Clark & J.S. Reid.
(Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
;
_exptl_crystal_colour
;
;
_exptl_crystal_density_diffrn    4.0194
_exptl_crystal_description
;
;
_exptl_crystal_F_000             1742
_exptl_crystal_size_max          0.146
_exptl_crystal_size_mid          0.046
_exptl_crystal_size_min          0.029
_refine_diff_density_max         20.04
_refine_diff_density_min         -8.42
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_gt    1.59
_refine_ls_goodness_of_fit_ref   1.14
_refine_ls_number_constraints    0
_refine_ls_number_parameters     219
_refine_ls_number_reflns         11370
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.2719
_refine_ls_R_factor_gt           0.0995
_refine_ls_shift/su_max          0.0298
_refine_ls_shift/su_mean         0.0032
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     w=1/(\s^2^(I)+0.0004I^2^)
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.2094
_refine_ls_wR_factor_ref         0.3162
_reflns_number_gt                2487
_reflns_number_total             11370
_reflns_threshold_expression     I>3\s(I)
_cod_data_source_file            jgeosci.171_plasil_uranopilite.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_diffrn_radiation_probe' value 'X-ray' was changed to
'x-ray' in accordance with the built-in table derived from the CIF
Core dictionary named 'cif_core.dic' version 2.4.5 last updated on
2014-11-21.

Automatic conversion script
Id: cif_fix_values 8738 2021-04-28 16:35:53Z antanas 
;
_cod_original_formula_sum        'O37.895 S1 U6'
_cod_database_code               1566324