Phase identification and structure solution by three-dimensional electron diffraction tomography: gd-phosphate nanorods.
Mayence, Arnaud; Navarro, Julien R. G.; Ma, Yanhang; Terasaki, Osamu; Bergström, Lennart; Oleynikov, Peter; Inorganic chemistry 53 (2014) 5067–5072; doi:10.1021/ic500056r

data_4338215
_publ_section_title
;
 Phase identification and structure solution by three-dimensional electron
 diffraction tomography: gd-phosphate nanorods.
;
_journal_issue                   10
_journal_name_full               'Inorganic chemistry'
_journal_page_first              5067
_journal_page_last               5072
_journal_paper_doi               10.1021/ic500056r
_journal_volume                  53
_journal_year                    2014
_chemical_formula_sum            'Gd0.25 O4.25 P1.25'
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_chemical_name_systematic        ' ?'
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_cell_length_b                   6.9
_cell_length_c                   6.3096
_cell_measurement_temperature    293
_cell_volume                     260.154
_diffrn_ambient_temperature      293
_diffrn_measured_fraction_theta_full 0.86
_diffrn_measured_fraction_theta_max 0.86
_diffrn_radiation_probe          electron
_diffrn_radiation_type           electron
_diffrn_radiation_wavelength     0.02508
_diffrn_reflns_av_R_equivalents  0.2422
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_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -7
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_diffrn_reflns_limit_k_min       -9
_diffrn_reflns_limit_l_max       8
_diffrn_reflns_limit_l_min       -8
_diffrn_reflns_number            1402
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_diffrn_reflns_theta_min         0.17
_exptl_absorpt_coefficient_mu    0
_exptl_crystal_density_diffrn    11.1812
_exptl_crystal_F_000             333
_refine_ls_abs_structure_details
'  66 of Friedel pairs used in the refinement'
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_gt    20.70
_refine_ls_goodness_of_fit_ref   20.70
_refine_ls_number_constraints    0
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_refine_ls_number_reflns         213
_refine_ls_number_restraints     0
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_refine_ls_R_factor_gt           0.1540
_refine_ls_shift/su_max          0.0267
_refine_ls_shift/su_mean         0.0085
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     w=1/(\s^2^(F)+0.0001F^2^)
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.2523
_refine_ls_wR_factor_ref         0.2523
_reflns_number_gt                213
_reflns_number_total             213
_reflns_threshold_expression     I>3\s(I)
_cod_data_source_file            ic500056r_si_006.cif
_cod_data_source_block           I
_cod_depositor_comments          'Adding full bibliography for 4338215.cif.'
_cod_original_cell_volume        260.1541
_cod_original_sg_symbol_Hall     'P 62;2'
_cod_database_code               4338215