Activation of nitrogen brønsted acids: synthesis and reactivity of a new class of nitrogen Acid complexes.
Bohle, D. Scott; Chua, Zhijie; Inorganic chemistry 53 (2014) 11160–11172; doi:10.1021/ic5017033

data_4341219
_publ_section_title
;
 Activation of nitrogen br\/onsted acids: synthesis and reactivity of a
 new class of nitrogen Acid complexes.
;
_journal_issue                   20
_journal_name_full               'Inorganic chemistry'
_journal_page_first              11160
_journal_page_last               11172
_journal_paper_doi               10.1021/ic5017033
_journal_volume                  53
_journal_year                    2014
_chemical_formula_moiety         'C2 H4 N2 O3'
_chemical_formula_sum            'C2 H4 N2 O3'
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_symmetry_space_group_name_H-M   'P n m a'
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_audit_update_record
;
2011-07-02 # Formatted by publCIF
;
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_cell_measurement_temperature    100(2)
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_cell_volume                     414.5(3)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
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_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
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_diffrn_measured_fraction_theta_max 0.965
_diffrn_measurement_device_type  'CCD area detector'
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_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
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_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
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_exptl_crystal_density_meas      0
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       rectangular
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_refine_ls_shift/su_mean         0.004
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0406P)^2^+0.1362P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_depositor_comments
'Adding full bibliography for 4341213--4341219.cif.'
_cod_original_sg_symbol_H-M      Pnma
_cod_database_code               4341219