2-Methoxypyridine derivatives: synthesis, liquid crystalline and photo-physical properties
N., Ahipa T.; Adhikari, Airody Vasudeva; New J. Chem. 38 (2014) 5018–; doi:10.1039/C4NJ00911H

data_7054314
_publ_section_title
;
 2-Methoxypyridine derivatives: synthesis, liquid crystalline and
 photo-physical properties
;
_journal_issue                   10
_journal_name_full               'New J. Chem.'
_journal_page_first              5018
_journal_paper_doi               10.1039/C4NJ00911H
_journal_volume                  38
_journal_year                    2014
_chemical_compound_source        'see text'
_chemical_formula_moiety         'C48 H51 N4 O4 S2'
_chemical_formula_structural     'C48 H51 N4 O4 S2'
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_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   14.8343(5)
_cell_length_b                   44.690(2)
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_computing_cell_refinement
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CrysAlisPro, Agilent Technologies,
Version 1.171.36.20 (release 27-06-2012 CrysAlis171 .NET)
(compiled Jul 11 2012,15:38:31)
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CrysAlisPro, Agilent Technologies,
Version 1.171.36.20 (release 27-06-2012 CrysAlis171 .NET)
(compiled Jul 11 2012,15:38:31)
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_computing_data_reduction
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CrysAlisPro, Agilent Technologies,
Version 1.171.36.20 (release 27-06-2012 CrysAlis171 .NET)
(compiled Jul 11 2012,15:38:31)
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;
;
_diffrn_reflns_theta_full        25.00
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_exptl_absorpt_coefficient_mu    0.152
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;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.20 (release 27-06-2012 CrysAlis171 .NET)
(compiled Jul 11 2012,15:38:31)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.105
_exptl_crystal_density_method    'Not Measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             1724
_exptl_crystal_size_max          0.35
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_refine_ls_R_factor_gt           0.0844
_refine_ls_shift/su_max          0.297
_refine_ls_shift/su_mean         0.015
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.1797P)^2^+0.1631P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2355
_refine_ls_wR_factor_ref         0.2599
_reflns_number_gt                3338
_reflns_number_total             4301
_reflns_threshold_expression     I>2\s(I)
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_cod_depositor_comments
'Adding full bibliography for 7054313--7054314.cif.'
_cod_original_sg_symbol_Hall     'A 2 -2ac'
_cod_database_code               7054314