Concerning the 1,5-stereocontrol in tin(iv) chloride promoted reactions of 4- and 5-alkoxyalk-2-enylstannanes: trapping intermediate allyltin trichlorides using phenyllithium.
Hobson, Lindsay A.; Thomas, Eric J.; Organic & biomolecular chemistry 10 (2012) 7510–7526; doi:10.1039/c2ob25765c

data_7152550
_publ_section_title
;
 Concerning the 1,5-stereocontrol in tin(iv) chloride promoted reactions
 of 4- and 5-alkoxyalk-2-enylstannanes: trapping intermediate allyltin
 trichlorides using phenyllithium.
;
_journal_issue                   37
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              7510
_journal_page_last               7526
_journal_paper_doi               10.1039/c2ob25765c
_journal_volume                  10
_journal_year                    2012
_chemical_formula_moiety         'C31 H31 Br O2 Sn '
_chemical_formula_sum            'C31 H31 Br O2 Sn'
_chemical_formula_weight         634.18
_chemical_name_common            'C31 H31 Br1 O2 Sn1'
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
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_audit_creation_date             1997-06-19
_audit_creation_method           'by teXsan v1.7'
_audit_update_record
;
?
;
_cell_angle_alpha                92.81(2)
_cell_angle_beta                 113.88(1)
_cell_angle_gamma                90.83(1)
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_cell_length_a                   10.390(2)
_cell_length_b                   17.643(3)
_cell_length_c                   8.429(2)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293.2
_cell_measurement_theta_max      14.3
_cell_measurement_theta_min      11.4
_cell_volume                     1410.2(5)
_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
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;
'DIRDIF92 PATTY (Beurskens, 1992)
;
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_diffrn_measurement_device       'Rigaku AFC5R'
_diffrn_measurement_method       \w-2\q
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo) + 0.00005|Fo|^2^]'
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_reflns_number_total             4987
_reflns_observed_criterion       >3.00\s(I)
_cod_data_source_file            c2ob25765c.txt
_cod_data_source_block           S530
_cod_original_cell_volume        1410.2(4)
_cod_original_sg_symbol_H-M      'P -1 '
_cod_original_formula_sum        'C31 H31 Br O2 Sn '
_cod_database_code               7152550