Technetium tetrachloride as a precursor for small technetium(IV) complexes.
Hagenbach, Adelheid; Yegen, Eda; Abram, Ulrich; Inorganic chemistry 45 (2006) 7331–7338; doi:10.1021/ic060896u

data_4350445
_publ_section_title
;
 Technetium tetrachloride as a precursor for small technetium(IV)
 complexes.
;
_journal_issue                   18
_journal_name_full               'Inorganic chemistry'
_journal_page_first              7331
_journal_page_last               7338
_journal_paper_doi               10.1021/ic060896u
_journal_volume                  45
_journal_year                    2006
_chemical_formula_moiety         '[TcCl3(DMSO)3]2[TcCl6]'
_chemical_formula_sum            'C12 H36 Cl12 O6 S6 Tc3'
_chemical_formula_weight         1188.17
_chemical_name_common            '[TcCl3(DMSO)3]2[TcCl6]'
_chemical_name_systematic
;
trichlorotris(dimethylsulfoxide)technetium(IV)) hexachlorotechnetate(IV) 
;
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
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_diffrn_measured_fraction_theta_full 0.928
_diffrn_measured_fraction_theta_max 0.928
_diffrn_measurement_device_type  'STOE IPDS 2T'
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_exptl_crystal_colour            yellow
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0867P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
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