Synthesis and Photophysical Properties of Difluoroboron Complexes of Curcuminoid Derivatives Bearing Different Terminal Aromatic Units and a meso-Aryl Ring
Abdellah Felouat; Anthony D'Aléo; Fredéric Fages; Journal of Organic Chemistry 78 (2013) 4446–4455; doi:10.1021/jo400389h

data_4028211
_publ_section_title
;
 Synthesis and Photophysical Properties of Difluoroboron Complexes of
 Curcuminoid Derivatives Bearing Different Terminal Aromatic Units and a
 meso-Aryl Ring
;
_journal_name_full               'Journal of Organic Chemistry'
_journal_page_first              4446
_journal_page_last               4455
_journal_paper_doi               10.1021/jo400389h
_journal_volume                  78
_journal_year                    2013
_chemical_compound_source        'synthesis as described'
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_chemical_name_systematic
;
 ?
;
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_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                94.74(1)
_cell_angle_beta                 102.62(2)
_cell_angle_gamma                90.301(7)
_cell_formula_units_Z            2
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_cell_length_c                   14.093(4)
_cell_measurement_reflns_used    20515
_cell_measurement_temperature    293(2)
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_cell_measurement_theta_min      1.49
_cell_measurement_wavelength     0.71073
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_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX publication routines (Farrugia, 1999)'
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_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.928
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_diffrn_measurement_device_type  KappaCCD
_diffrn_measurement_method       'Omega + Phi scan'
_diffrn_radiation_monochromator  graphite
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_diffrn_radiation_type           MoK\a
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_exptl_absorpt_coefficient_mu    0.098
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_exptl_crystal_colour            red
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_exptl_crystal_description       prism
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.1933P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_database_code               4028211