Ru(II)-catalyzed site-selective <i>N</i>-directed C(sp<sup>2</sup>)-H alkylation of quinoxalinones with maleimide.
Monika, ?; Kumar, Prashant; Singh, Brajendra K.; Organic & biomolecular chemistry 23 (2025) 10743–10752; doi:10.1039/d5ob01524c

data_7160843
_publ_section_title
;
 Ru(II)-catalyzed site-selective <i>N</i>-directed C(sp<sup>2</sup>)-H
 alkylation of quinoxalinones with maleimide.
;
_journal_issue                   47
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              10743
_journal_page_last               10752
_journal_paper_doi               10.1039/d5ob01524c
_journal_volume                  23
_journal_year                    2025
_chemical_formula_sum            'C20 H17 N3 O3'
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_space_group_name_Hall           '-P 2ac 2ab'
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_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2025-04-08 deposited with the CCDC.	2025-11-07 downloaded from the CCDC.
;
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_cell_angle_gamma                90
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_cell_length_c                   27.6587(18)
_cell_measurement_temperature    256(2)
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_computing_structure_refinement  'SHELXL-2016/4 (Sheldrick, 2016)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_diffrn_ambient_temperature      256(2)
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.2000P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           3a_auto
_cod_depositor_comments
'Adding full bibliography for 7160843--7160844.cif.'
_cod_database_code               7160843
_shelx_shelxl_version_number     2016/4
_shelx_estimated_absorpt_t_min   0.991
_shelx_estimated_absorpt_t_max   0.991
_shelx_res_checksum              47760