Varied forms of lamellar [Sn3Se7]n(2n-) anion: the competitive and synergistic structure-directing effects of metal-amine complex and imidazolium cations.
Du, Cheng-Feng; Li, Jian-Rong; Feng, Mei-Ling; Zou, Guo-Dong; Shen, Nan-Nan; Huang, Xiao-Ying; Dalton transactions (Cambridge, England : 2003) 44 (2015) 7364–7372; doi:10.1039/c5dt00620a

data_7034321
_publ_section_title
;
 Varied forms of lamellar [Sn3Se7]n(2n-) anion: the competitive and
 synergistic structure-directing effects of metal-amine complex and
 imidazolium cations.
;
_journal_issue                   16
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7364
_journal_page_last               7372
_journal_paper_doi               10.1039/c5dt00620a
_journal_volume                  44
_journal_year                    2015
_chemical_formula_moiety         'C70 H154 Mn2 N24 Se35 Sn15'
_chemical_formula_sum            'C70 H154 Mn2 N24 Se35 Sn15'
_chemical_formula_weight         5985.99
_chemical_name_systematic
;
 ?
;
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_space_group_name_Hall           '-P 2yb'
_space_group_name_H-M_alt        'P 1 21/m 1'
_symmetry_space_group_name_Hall  '-P 2yb'
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_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2015-01-09 deposited with the CCDC.
2015-03-09 downloaded from the CCDC.
;
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;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET)
(compiled Aug 13 2014,18:06:01)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
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_refine_diff_density_min         -1.747
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
 w=1/[\s^2^(Fo^2^)+(0.0200P)^2^+450.0000P]
 where P=(Fo^2^+2Fc^2^)/3
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1650
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_reflns_number_gt                12266
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7034318--7034321.cif.'
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