Tris(1,10-phenanthroline)cobalt(II) bis(trichloroacetate)
Li, Li-Min; Li, Yu-Feng; Liu, Li; Zhang, Zeng-Hui; Acta Crystallographica Section E 67 (2011) m973–; doi:10.1107/S160053681102410X

data_2230777
_publ_section_title
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 Tris(1,10-phenanthroline)cobalt(II) bis(trichloroacetate)
;
_journal_coeditor_code           LH5253
_journal_issue                   7
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m973
_journal_paper_doi               10.1107/S160053681102410X
_journal_volume                  67
_journal_year                    2011
_chemical_formula_iupac          '[Co (C12 H8 N2)3] (C2 Cl3 O2)2'
_chemical_formula_moiety         'C36 H24 Co N6 2+, 2(C2 Cl3 O2 -)'
_chemical_formula_sum            'C40 H24 Cl6 Co N6 O4'
_chemical_formula_weight         924.28
_chemical_name_systematic
;
Tris(1,10-phenanthroline)cobalt(II) bis(trichloroacetate)
;
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_cell_length_b                   10.753(2)
_cell_length_c                   19.020(4)
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_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      27.48
_cell_measurement_theta_min      3.25
_cell_volume                     3688.2(14)
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_computing_structure_solution    'SHELXS97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      293(2)
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_diffrn_measurement_method       '\f and \w'
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_exptl_crystal_colour            yellow
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_exptl_crystal_density_method    'not measured'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'calc w=1/[\s^2^(Fo^2^)+(0.1000P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_cod_original_sg_symbol_H-M      'C 2/c'
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