Visible-Light-Induced Photocatalytic Aerobic Oxidation/Povarov Cyclization Reaction: Synthesis of Substituted Quinoline-Fused Lactones.
Dong, Wuheng; Hu, Bei; Gao, Xiaoshuang; Li, Yuyuan; Xie, Xiaomin; Zhang, Zhaoguo; The Journal of organic chemistry 81 (2016) 8770–8776; doi:10.1021/acs.joc.6b01253

data_4037009
_publ_section_title
;
 Visible-Light-Induced Photocatalytic Aerobic Oxidation/Povarov
 Cyclization Reaction: Synthesis of Substituted Quinoline-Fused Lactones.
;
_journal_issue                   19
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              8770
_journal_page_last               8776
_journal_paper_doi               10.1021/acs.joc.6b01253
_journal_volume                  81
_journal_year                    2016
_chemical_formula_moiety         'C18 H13 N O2, C H4 O'
_chemical_formula_sum            'C19 H17 N O3'
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_cell_length_c                   20.980(4)
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_cell_measurement_theta_min      5.56
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_computing_molecular_graphics    'Bruker SHELXTL'
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_computing_structure_solution    'SHELXS-97 (Sheldrick 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.976
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_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_type           CuK\a
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_diffrn_reflns_theta_max         69.812
_diffrn_reflns_theta_min         4.299
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_exptl_absorpt_coefficient_mu    0.735
_exptl_absorpt_correction_type   none
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_exptl_crystal_size_min          0.03
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0618P)^2^+0.7719P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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