Synthesis through 3D printing: formation of 3D coordination polymers
Halevi, Oded; Chen, Jingwei; Thangavel, Gurunathan; Morris, Samuel Alexander; Ben Uliel, Tal; Tischler, Yaakov Raphael; Lee, Pooi See; Magdassi, Shlomo; RSC Advances 10 (2020) 14812–14817; doi:10.1039/D0RA01887B

data_7240328
_publ_section_title
;
 Synthesis through 3D printing: formation of 3D coordination polymers
;
_journal_issue                   25
_journal_name_full               'RSC Advances'
_journal_page_first              14812
_journal_page_last               14817
_journal_paper_doi               10.1039/D0RA01887B
_journal_volume                  10
_journal_year                    2020
_chemical_formula_sum            'C12 H24 N6 Ni O12'
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_atom_sites_solution_hydrogens   difmap
_audit_creation_method           SHELXL-2016/6
_audit_update_record
;
2020-01-23 deposited with the CCDC.	2020-04-03 downloaded from the CCDC.
;
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_cell_measurement_theta_min      2.41
_cell_volume                     535.14(7)
_computing_cell_refinement       'Bruker SAINT'
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_computing_molecular_graphics    'Bruker SHELXTL'
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_diffrn_ambient_temperature      296(2)
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_monochromator  graphite
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_diffrn_radiation_type           MoK\a
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_exptl_crystal_size_max          0.6
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_refine_ls_extinction_coef       0.079(6)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2016/6 (Sheldrick 2016)'
_refine_ls_goodness_of_fit_ref   1.076
_refine_ls_hydrogen_treatment    refall
_refine_ls_matrix_type           full
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_refine_ls_number_reflns         4466
_refine_ls_number_restraints     30
_refine_ls_restrained_S_all      1.073
_refine_ls_R_factor_all          0.0353
_refine_ls_R_factor_gt           0.0300
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0486P)^2^+0.1095P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0819
_refine_ls_wR_factor_ref         0.0881
_reflns_Friedel_coverage         0.000
_reflns_number_gt                4111
_reflns_number_total             4466
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d0ra01887b2.cif
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_cod_depositor_comments          'Adding full bibliography for 7240328.cif.'
_cod_database_code               7240328
_shelx_shelxl_version_number     2016/6
_shelx_res_checksum              17832