Interplay between H-bonding and interpenetration in aqueous copper(II)−aminoalcohol−pyromellitic acid system: Self-assembly synthesis, structural features and catalysis
Fernandes, Tiago; Kirillova, Marina; André, Vânia; Kirillov, Alexander M.; Dalton Transactions  (2018) –; doi:10.1039/C8DT02983K

data_7047920
_publ_section_title
;
 Interplay between H-bonding and interpenetration in aqueous
 copper(II)&#x2212;aminoalcohol&#x2212;pyromellitic acid system:
 Self-assembly synthesis, structural features and catalysis
;
_journal_name_full               'Dalton Transactions'
_journal_paper_doi               10.1039/C8DT02983K
_journal_year                    2018
_chemical_formula_sum            'C30 H54 Cu2 N4 O16'
_chemical_formula_weight         853.8658
_space_group_crystal_system      triclinic
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_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   mixed
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_audit_update_record
;
2018-10-14 deposited with the CCDC.
2018-10-29 downloaded from the CCDC.
;
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_cell_volume                     1009.8(4)
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_diffrn_ambient_temperature      298(2)
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_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
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_diffrn_reflns_limit_l_min       -14
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0445P)^2^+1.0599P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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