Magnetic on-off switching in redox non-innocent ligand bridged binuclear cobalt complexes.
Wang, Yichen; Li, Jing; Zhang, Li; Chen, Chao; Feng, Rui; Zhao, Yue; Zhang, Yi-Quan; Tan, Gengwen; Song, You; Wang, Xinping; Dalton transactions (Cambridge, England : 2003) 47 (2018) 17211–17215; doi:10.1039/c8dt04157a

data_7048116
_publ_section_title
;
 Magnetic on-off switching in redox non-innocent ligand bridged binuclear
 cobalt complexes.
;
_journal_issue                   48
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              17211
_journal_page_last               17215
_journal_paper_doi               10.1039/c8dt04157a
_journal_volume                  47
_journal_year                    2018
_chemical_formula_sum            'C66 H88 Co2 N8'
_chemical_formula_weight         1111.30
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2018-08-17 deposited with the CCDC.
2018-11-13 downloaded from the CCDC.
;
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_computing_structure_solution    'SHELXT (Sheldrick, 2014)'
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_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker D8 Quest'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_radiation_type           MoK\a
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_diffrn_source                   'microfocus sealed tube (Incoatec ImS)'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0279P)^2^+3.1558P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.1019
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_reflns_number_total             5405
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c8dt04157a2.cif
_cod_data_source_block           P2_a
_cod_depositor_comments
'Adding full bibliography for 7048116--7048117.cif.'
_cod_original_cell_volume        3081.9(8)
_cod_database_code               7048116
_shelx_shelxl_version_number     2014/7
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_shelx_res_checksum              79789