A confinement-regulated (H<sub>3</sub>C-NH<sub>3</sub>)<sup>+</sup> ion as a smallest dual-wheel rotator showing bisected rotation dynamics.
Li, Wang; Xie, Miao; Zhang, Shi-Yong; Zeng, Cheng-Hui; Du, Zi-Yi; He, Chun-Ting; Physical chemistry chemical physics : PCCP 26 (2024) 7269–7275; doi:10.1039/d3cp05406c

data_7247885
_publ_section_title
;
 A confinement-regulated (H<sub>3</sub>C-NH<sub>3</sub>)<sup>+</sup> ion
 as a smallest dual-wheel rotator showing bisected rotation dynamics.
;
_journal_issue                   9
_journal_name_full               'Physical chemistry chemical physics : PCCP'
_journal_page_first              7269
_journal_page_last               7275
_journal_paper_doi               10.1039/d3cp05406c
_journal_volume                  26
_journal_year                    2024
_chemical_formula_sum            'C13 H30 Cl3 Cu N O6'
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_space_group_crystal_system      triclinic
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_space_group_name_Hall           '-P 1'
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_audit_creation_method           SHELXL-2014
_audit_update_record
;
2023-10-21 deposited with the CCDC.	2023-12-19 downloaded from the CCDC.
;
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_cell_measurement_theta_min      2.4210
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_computing_cell_refinement       'Bruker FRAMBO'
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_diffrn_measurement_device_type  'multiwire proportional'
_diffrn_measurement_method       'phi and omega scans'
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_diffrn_reflns_Laue_measured_fraction_full 0.973
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0969P)^2^+9.3703P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                3433
_reflns_number_total             3933
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7247884--7247885.cif.'
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