Interpenetrated nano-MOFs for ultrahigh-performance supercapacitors and excellent dye adsorption performance
Wang, Kuaibing; Wang, Xin; Zhang, Dan; Wang, Huijian; Wang, Zikai; Zhao, Minyan; Xi, Rui; Wu, Hua; Zheng, Mingbo; CrystEngComm 20 (2018) 6940–; doi:10.1039/C8CE01067F

data_7231601
_publ_section_title
;
 Interpenetrated nano-MOFs for ultrahigh-performance supercapacitors and
 excellent dye adsorption performance
;
_journal_issue                   43
_journal_name_full               CrystEngComm
_journal_page_first              6940
_journal_paper_doi               10.1039/C8CE01067F
_journal_volume                  20
_journal_year                    2018
_chemical_formula_sum            'C30 H30 Co8 N10 O10'
_chemical_formula_weight         1162.08
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2017-08-26 deposited with the CCDC.
2018-10-01 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 96.816(7)
_cell_angle_gamma                90.00
_cell_formula_units_Z            5
_cell_length_a                   9.711(4)
_cell_length_b                   16.824(7)
_cell_length_c                   26.957(11)
_cell_measurement_temperature    293(2)
_cell_volume                     4373(3)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.982
_diffrn_measured_fraction_theta_max 0.967
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.2139
_diffrn_reflns_av_sigmaI/netI    0.1564
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       34
_diffrn_reflns_limit_l_min       -35
_diffrn_reflns_number            30011
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         27.59
_diffrn_reflns_theta_min         1.43
_exptl_absorpt_coefficient_mu    3.769
_exptl_crystal_density_diffrn    2.206
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             2880
_refine_diff_density_max         1.470
_refine_diff_density_min         -1.017
_refine_diff_density_rms         0.208
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.065
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     443
_refine_ls_number_reflns         9813
_refine_ls_number_restraints     5
_refine_ls_restrained_S_all      1.074
_refine_ls_R_factor_all          0.1735
_refine_ls_R_factor_gt           0.1248
_refine_ls_shift/su_max          0.957
_refine_ls_shift/su_mean         0.060
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.2000P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3220
_refine_ls_wR_factor_ref         0.3633
_reflns_number_gt                5049
_reflns_number_total             9813
_reflns_threshold_expression     >2\s(I)
_cod_data_source_file            c8ce01067f2.cif
_cod_data_source_block           p21c
_cod_depositor_comments          'Adding full bibliography for 7231601.cif.'
_cod_database_code               7231601