2-D Interwoven and 3-D 5-fold Interpenetrating Silver(I) Complexes of 1-(Isocyanidomethyl)-1H-benzotriazole and 1,3-Bis(dicyanomethylidene)indan
Ichiro Ino; Jian Chu Zhong; Megumu Munakata; Takayoshi Kuroda-Sowa; Masahiko Maekawa; Yusaku Suenaga; Yoshinobu Kitamori; Inorganic Chemistry 39 (2000) 4273–4279; doi:10.1021/ic000459u

data_4321371
_publ_section_title
;
 2-D Interwoven and 3-D 5-fold Interpenetrating Silver(I) Complexes of
 1-(Isocyanidomethyl)-1H-benzotriazole and
 1,3-Bis(dicyanomethylidene)indan
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              4273
_journal_page_last               4279
_journal_paper_doi               10.1021/ic000459u
_journal_volume                  39
_journal_year                    2000
_chemical_formula_moiety         'C30 H10 Ag2 N8 '
_chemical_formula_sum            'C30 H10 Ag2 N8'
_chemical_formula_weight         698.20
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                86.55(2)
_cell_angle_beta                 80.87(2)
_cell_angle_gamma                74.47(1)
_cell_formula_units_Z            2
_cell_length_a                   14.920(2)
_cell_length_b                   11.896(2)
_cell_length_c                   7.400(4)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    296.2
_cell_measurement_theta_max      14.7
_cell_measurement_theta_min      12.1
_cell_volume                     1249.2(7)
_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
_computing_data_reduction        'teXsan Ver. 1.10'
_computing_publication_material  'teXsan Ver. 1.10'
_computing_structure_refinement  'teXsan Ver. 1.10'
_computing_structure_solution    SIR88
_diffrn_measured_fraction_theta_full 1.0005
_diffrn_measured_fraction_theta_max 1.0005
_diffrn_measurement_device_type  'Rigaku AFC7R'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.050
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       9
_diffrn_reflns_limit_l_min       -9
_diffrn_reflns_number            6018
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_standards_decay_%        0.52
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    1.601
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    1.856
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prismatic
_exptl_crystal_size_max          0.300
_exptl_crystal_size_mid          0.150
_exptl_crystal_size_min          0.150
_refine_diff_density_max         2.66
_refine_diff_density_min         -2.48
_refine_ls_extinction_coef       0.001(1)
_refine_ls_extinction_method     'Zachariasen(1967) type 2 Gaussian isotropic'
_refine_ls_goodness_of_fit_ref   1.365
_refine_ls_hydrogen_treatment    noref
_refine_ls_number_parameters     368
_refine_ls_number_reflns         3936
_refine_ls_R_factor_gt           0.0510
_refine_ls_shift/su_max          0.0000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^) + (0.06000(Max(Fo^2^,0) + 2Fc^2^)/3)^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1537
_reflns_number_gt                4011
_reflns_number_total             5741
_reflns_threshold_expression     F^2^>2.0\s(F^2^)
_cod_data_source_file            ic000459u_3.cif
_cod_data_source_block           '[Ag2(L3)2]n(3)'
_cod_original_cell_volume        1249.2(6)
_cod_original_sg_symbol_H-M      'P -1 '
_cod_original_formula_sum        'C30 H10 Ag2 N8 '
_cod_database_code               4321371