Construction of Chiral-Fused Tricyclic γ-Lactams via a trans-Perhydroindolic Acid-Catalyzed Asymmetric Domino Reaction.
An, Qianjin; Shen, Jiefeng; Liu, Delong; Liu, Yangang; Zhang, Wanbin; Organic letters 19 (2017) 2925–2928; doi:10.1021/acs.orglett.7b01160

data_1546021
_publ_section_title
;
 Construction of Chiral-Fused Tricyclic \g-Lactams via a
 trans-Perhydroindolic Acid-Catalyzed Asymmetric Domino Reaction.
;
_journal_issue                   11
_journal_name_full               'Organic letters'
_journal_page_first              2925
_journal_page_last               2928
_journal_paper_doi               10.1021/acs.orglett.7b01160
_journal_volume                  19
_journal_year                    2017
_chemical_formula_moiety         'C15 H15 N O3'
_chemical_formula_sum            'C15 H15 N O3'
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_diffrn_measurement_device_type  'Bruker APEX-II CCD'
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_diffrn_reflns_theta_min         5.606
_exptl_absorpt_coefficient_mu    0.754
_exptl_crystal_colour            colorless
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_exptl_crystal_description       block
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_exptl_crystal_size_mid          0.240
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_refine_diff_density_min         -0.278
_refine_diff_density_rms         0.087
_refine_ls_extinction_method     none
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_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
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_refine_ls_number_reflns         2336
_refine_ls_number_restraints     0
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0813P)^2^+0.4723P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                2314
_reflns_number_total             2336
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           t_0m
_cod_depositor_comments
'Adding full bibliography for 1546020--1546021.cif.'
_cod_database_code               1546021
_shelx_shelxl_version_number     2014/7
_shelx_estimated_absorpt_t_min   0.805
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_shelx_hkl_checksum              4836