Ruthenium(ii)-catalyzed remote C-H addition of 8 aminoquinoline amide to activated aldehyde.
Mondal, Susmita; Hajra, Alakananda; Organic & biomolecular chemistry 16 (2018) 2846–2850; doi:10.1039/c8ob00537k

data_7156173
_publ_section_title
;
 Ruthenium(ii)-catalyzed remote C-H addition of 8 aminoquinoline amide to
 activated aldehyde.
;
_journal_issue                   16
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              2846
_journal_page_last               2850
_journal_paper_doi               10.1039/c8ob00537k
_journal_volume                  16
_journal_year                    2018
_chemical_formula_moiety         'C21 H20 N2 O5'
_chemical_formula_sum            'C21 H20 N2 O5'
_chemical_formula_weight         380.39
_chemical_name_common            vbchem293S
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   mixed
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_audit_update_record
;
2018-03-22 deposited with the CCDC.
2018-03-26 downloaded from the CCDC.
;
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_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
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_diffrn_reflns_theta_max         28.234
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_exptl_absorpt_coefficient_mu    0.100
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_exptl_crystal_description       vbchem293S
_exptl_crystal_F_000             800
_refine_diff_density_max         0.514
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_refine_ls_extinction_method     none
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_refine_ls_hydrogen_treatment    mixed
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_refine_ls_number_reflns         4428
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+0.8738P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c8ob00537k2.cif
_cod_data_source_block           vbchem293S
_cod_depositor_comments          'Adding full bibliography for 7156173.cif.'
_cod_database_code               7156173
_shelx_shelxl_version_number     2014/7
_shelx_res_checksum              20088