Lanthanoid "bottlebrush" clusters: remarkably elongated metal-oxo core structures with controllable lengths.
D'Alessio, Daniel; Sobolev, Alexandre N.; Skelton, Brian W.; Fuller, Rebecca O.; Woodward, Robert C.; Lengkeek, Nigel A.; Fraser, Benjamin H.; Massi, Massimiliano; Ogden, Mark I.; Journal of the American Chemical Society 136 (2014) 15122–15125; doi:10.1021/ja506677h

data_4122809
_publ_section_title
;
 Lanthanoid &quot;bottlebrush&quot; clusters: remarkably elongated
 metal-oxo core structures with controllable lengths.
;
_journal_issue                   43
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              15122
_journal_page_last               15125
_journal_paper_doi               10.1021/ja506677h
_journal_volume                  136
_journal_year                    2014
_chemical_formula_moiety
;
C588 H799 Dy19 N96 O116, 12(C4 H8 O2), 12(C2 H6 O), 10.5(H2 O)
;
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 ? 
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CrysAlisPro, Agilent Technologies,
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CrysAlisPro, Agilent Technologies,
Version 1.171.35.21 (release 20-01-2012 CrysAlis171 .NET)
(compiled Jan 23 2012,18:06:46)
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CrysAlisPro, Agilent Technologies,
Version 1.171.35.21 (release 20-01-2012 CrysAlis171 .NET)
(compiled Jan 23 2012,18:06:46)
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CrysAlisPro, Agilent Technologies,
Version 1.171.35.21 (release 20-01-2012 CrysAlis171 .NET)
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Empirical absorption correction using spherical harmonics,
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_exptl_crystal_colour            yellow
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;
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.1500P)^2^+500.0000P] where P=(Fo^2^+2Fc^2^)/3'
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'Adding full bibliography for 4122807--4122810.cif.'
_cod_original_sg_symbol_H-M      'R -3 c'
_cod_original_formula_sum        'C660 H988 Dy19 N96 O162.50'
_cod_database_code               4122809