Molecular complex of 2-[4-(dimethylamino)phenylimino]-3-oxo-<i>N</i>-phenylbutanamide and <i>N</i>,<i>N</i>-dimethyl-4-nitrosoaniline
Lewinski, K.; Nitek, W.; Milart, P.; Acta Crystallographica Section C 49 (1993) 188–190; doi:10.1107/S0108270192010461

data_2002113
_publ_contact_author
;
                                         Dr Krzysztof Lewinski
                                         Department of Chemistry
                                         University of South Carolina
                                         Columbia, SC 29208
                                         USA
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_publ_section_title
;
 Molecular complex of
 2-[4-(dimethylamino)phenylimino]-3-oxo-<i>N</i>-phenylbutanamide and
 <i>N</i>,<i>N</i>-dimethyl-4-nitrosoaniline
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              188
_journal_page_last               190
_journal_paper_doi               10.1107/S0108270192010461
_journal_volume                  49
_journal_year                    1993
_chemical_formula_moiety         'C18 H19 N3 O2 , C8 H10 N2 O'
_chemical_formula_sum            'C26 H29 N5 O3'
_chemical_formula_weight         459.55
_chemical_name_systematic
;
      2-[4-(Dimethylamino)phenyl]imino]-3-oxo-N-phenylbutanamide
      N,N-dimethyl-4-nitroso-benzenamine
;
_space_group_IT_number           19
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2ac 2ab'
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_computing_molecular_graphics
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                                        CHAIN (Sack, 1989)
                                        MOLDRAW (Ugliengo, Boranzi & Viterbo,
                                          1988)
                                        ORTEP (Johnson, 1965)
;
_computing_publication_material  'PARST88 (Nardelli, 1983)'
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KM-4 four circle diffractometer (KUMA Diffraction)
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_exptl_absorpt_coefficient_mu    6.410
_exptl_absorpt_correction_type   none
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_exptl_crystal_description       Prism
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_refine_ls_weighting_details     'w = 1/[\s^2^(F)+0.003F^2^]'
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_reflns_observed_criterion       'F > 3\s(F)'
_cod_data_source_file            ab1020.cif
_cod_data_source_block           default
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;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value '1/[\s^2^(F)+0.003F^2^]' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to 'w =
1/[\s^2^(F)+0.003F^2^]'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        2444.0(10)
_cod_database_code               2002113