Concomitant Formation of N-Heterocyclic Carbene-Copper Complexes within a Supramolecular Network in the Self-Assembly of Imidazolium Dicarboxylate with Metal Ions
Jiseul Chun; Il Gu Jung; Hae Jin Kim; Mira Park; Myoung Soo Lah; Seung Uk Son; Inorganic Chemistry 48 (2009) 6353–6355; doi:10.1021/ic900846s

data_4302775
_publ_contact_author_address     'Sungkyunkwan University, Suwon, Korea'
_publ_contact_author_name        'Son, Seung Uk'
_publ_section_title
;
Concomitant Formation of N-Heterocyclic Carbene-Copper Complexes within a
Supramolecular Network in the Self-Assembly of Imidazolium Dicarboxylate
with Metal Ions
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              6353
_journal_page_last               6355
_journal_paper_doi               10.1021/ic900846s
_journal_volume                  48
_journal_year                    2009
_chemical_formula_sum            'C58 H70 Cd2 Cl2 N4 O8'
_chemical_formula_weight         1246.88
_chemical_name_systematic
; 
 ? 
;
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_atom_sites_solution_secondary   difmap
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_cell_angle_beta                 91.846(5)
_cell_angle_gamma                92.986(6)
_cell_formula_units_Z            2
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_cell_length_b                   15.0041(16)
_cell_length_c                   17.6073(16)
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_computing_cell_refinement       Nonius-SUPERGUI
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_computing_structure_refinement  SHELXTL
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_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.957
_diffrn_measured_fraction_theta_max 0.957
_diffrn_measurement_device_type  'Nonius Kappa CCD detector'
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_exptl_absorpt_coefficient_mu    0.656
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_exptl_crystal_colour            colorless
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.1884P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_depositor_comments
;
The following automatic conversions were performed:
'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4302775