N-H cleavage as a route to new pincer complexes of high-valent rhenium.
Kosanovich, Alex J.; Shih, Wei-Chun; Ramírez-Contreras, Rodrigo; Ozerov, Oleg V.; Dalton transactions (Cambridge, England : 2003) 45 (2016) 18532–18540; doi:10.1039/c6dt03640f

data_7040930
_publ_section_title
;
 N-H cleavage as a route to new pincer complexes of high-valent rhenium.
;
_journal_issue                   46
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              18532
_journal_page_last               18540
_journal_paper_doi               10.1039/c6dt03640f
_journal_volume                  45
_journal_year                    2016
_chemical_formula_sum            'C31 H39 F3 N2 O4 P Re S'
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;
2016-09-16 deposited with the CCDC.
2016-10-17 downloaded from the CCDC.
;
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_exptl_absorpt_correction_type   multi-scan
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'Re-crystallisation from solvent: Et2O/ Pentane'
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0337P)^2^+2.1533P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0637
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_reflns_number_gt                6428
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           4-OTf
_cod_depositor_comments
'Adding full bibliography for 7040927--7040930.cif.'
_cod_database_code               7040930
_shelx_shelxl_version_number     2014/7
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