Aspects of the coordination chemistry of rac-trans-1,2-diphosphinocyclohexane and the preparation of reinforced 9aneP3 and 9anePN2 macrocycles.
Edwards, Peter G.; Kariuki, Benson M.; Newman, Paul D.; Tallis, Huw A.; Williams, Craig; Dalton transactions (Cambridge, England : 2003) 43 (2014) 15532–15545; doi:10.1039/c4dt02239d

data_7032170
_publ_section_title
;
 Aspects of the coordination chemistry of
 rac-trans-1,2-diphosphinocyclohexane and the preparation of reinforced
 9aneP3 and 9anePN2 macrocycles.
;
_journal_issue                   41
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              15532
_journal_page_last               15545
_journal_paper_doi               10.1039/c4dt02239d
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C32 H34 F I Mn O4 P3'
_chemical_formula_weight         776.34
_chemical_name_systematic
;
 ?
;
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_space_group_name_Hall           '-C 2y'
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_symmetry_space_group_name_Hall  '-C 2y'
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_diffrn_measurement_method       'CCD scans'
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_diffrn_source                   'fine-focus sealed tube'
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_exptl_absorpt_process_details   Sadabs/Denzo
_exptl_crystal_colour            yellow
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0903P)^2^+213.1648P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7032169--7032173.cif.'
_cod_original_cell_volume        7122.9(16)
_cod_database_code               7032170
_shelx_estimated_absorpt_t_min   0.602
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_shelx_res_checksum              36428