A New Self-Penetrating Uniform Net, (8,4) (or 86), Containing Planar Four-Coordinate Nodes
Ming-Liang Tong; Xiao-Ming Chen; Stuart R. Batten; Journal of the American Chemical Society 125 (2003) 16170–16171; doi:10.1021/ja0383266

data_4114553
_publ_contact_author
;
      Tong, Ming-Liang
      School of Chemistry and Chemical Engineering
      Sun Yat-Sen University
      Guangzhou, 510275
      P. R. China
;
_publ_contact_author_email       cestml@zsu.edu.cn
_publ_contact_author_fax         86-20-84112245
_publ_contact_author_phone       86-20-84113986
_publ_section_title
;
 A New Self-Penetrating Uniform Net, (8,4) (or 86), Containing Planar
 Four-Coordinate Nodes
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              16170
_journal_page_last               16171
_journal_paper_doi               10.1021/ja0383266
_journal_volume                  125
_journal_year                    2003
_chemical_formula_sum            'C16 H16 N2 Ni O6'
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; 
 ? 
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_cell_angle_beta                 95.080(10)
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_cell_length_a                   7.6036(5)
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_cell_measurement_temperature    293(2)
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_computing_cell_refinement
;       
SAINT-PLUS for Windows NT, Ver. 6.0, Bruker AXS Inc., 
Madison, Wisconsin, USA, 1997.
;
_computing_data_collection
;
SMART for Windows NT, Bruker AXS Inc., Madison, Wisconsin, USA, 1998.
;
_computing_data_reduction
;
SAINT-PLUS for Windows NT, Ver. 6.0, Bruker AXS Inc., 
Madison, Wisconsin, USA, 1997.
;
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.913
_diffrn_measured_fraction_theta_max 0.913
_diffrn_measurement_device_type  'Bruker Smart Apex CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0354
_diffrn_reflns_av_sigmaI/netI    0.0688
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -12
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_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            5475
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         3.09
_exptl_absorpt_coefficient_mu    1.280
_exptl_crystal_density_diffrn    1.663
_exptl_crystal_F_000             404
_refine_diff_density_max         1.191
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_refine_ls_extinction_method     none
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0752P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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