fac-Re(CO)<sub>3</sub>-based neutral heteroleptic tetrahedrons.
Arumugam, Ramar; Shankar, Bhaskaran; Soumya, K. R.; Sathiyendiran, Malaichamy; Dalton transactions (Cambridge, England : 2003) 48 (2019) 7425–7431; doi:10.1039/c8dt05065a

data_7049669
_publ_section_title
;
 fac-Re(CO)<sub>3</sub>-based neutral heteroleptic tetrahedrons.
;
_journal_issue                   21
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7425
_journal_page_last               7431
_journal_paper_doi               10.1039/c8dt05065a
_journal_volume                  48
_journal_year                    2019
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_symmetry_space_group_name_Hall  '-P 2yn'
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;
2019-04-06 deposited with the CCDC.    2019-04-11 downloaded from the CCDC.
;
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_diffrn_ambient_temperature      296(2)
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_diffrn_reflns_av_unetI/netI     0.2532
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_exptl_absorpt_process_details
;
CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            Colourless
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_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
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_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     'w=1/[\s^2^(Fo^2^)] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                1349
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c8dt05065a2.cif
_cod_data_source_block           L4
_cod_depositor_comments
'Adding full bibliography for 7049668--7049673.cif.'
_cod_original_cell_volume        3486.3(19)
_cod_database_code               7049669
_shelx_shelxl_version_number     2018/3
_shelx_estimated_absorpt_t_min   0.920
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_shelx_res_checksum              53195