A facile and benign synthesis of binuclear ruthenium(I) “sawhorse” complexes
Kepert, Christopher M.; Deacon, Glen B.; Spiccia, Leone; Fallon, Gary D.; Skelton, Brian W.; White, Allan H.; Journal of the Chemical Society, Dalton Transactions  (2000) 2867–; doi:10.1039/b002304n

data_7009616
_publ_section_title
;
 A facile and benign synthesis of binuclear ruthenium(I)
 &#x201C;sawhorse&#x201D; complexes
;
_journal_issue                   16
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              2867
_journal_paper_doi               10.1039/b002304n
_journal_year                    2000
_chemical_formula_analytical     'C20 H20 N2 O8 Ru2'
_chemical_formula_sum            'C20 H20 N2 O8 Ru2'
_chemical_formula_weight         618.53
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_audit_creation_date             97-07-22
_audit_creation_method           from_xtal_archive_file_using_CIFIO
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_cell_angle_beta                 108.78(2)
_cell_angle_gamma                90.00000
_cell_formula_units_Z            4
_cell_length_a                   10.890(3)
_cell_length_b                   15.706(2)
_cell_length_c                   14.390(4)
_cell_measurement_reflns_used    10
_cell_measurement_temperature    293
_cell_measurement_theta_max      21.8
_cell_measurement_theta_min      20
_cell_volume                     2330.2(10)
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_diffrn_measurement_device       CAD4
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_diffrn_radiation_monochromator  graphite
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_diffrn_reflns_theta_min         1.98
_diffrn_standards_decay_%        0
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_exptl_absorpt_coefficient_mu    1.34
_exptl_absorpt_correction_T_max  0.83
_exptl_absorpt_correction_T_min  0.61
_exptl_absorpt_correction_type   gaussian
_exptl_absorpt_process_details   'XTAl absorb'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.763
_exptl_crystal_description       prism
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_refine_ls_extinction_expression Eq22_p292_"Cryst._Comp."_Munksgaard_1970
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_refine_ls_structure_factor_coef F
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_cod_data_source_file            b002304n.txt
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_cod_original_sg_symbol_Hall     -p_2yn
_cod_original_sg_symbol_H-M      p_1_21/n_1
_cod_database_code               7009616
_refine_ls_r_factor_ref          .067