A Mixed-Ligand Zinc(II) Complex Containing a Bridging Dithiolate Ligand
Gronlund, P. J.; Wacholtz, W. F.; Mague, J. T.; Acta Crystallographica Section C 51 (1995) 1540–1543; doi:10.1107/S0108270195001995

data_2003758
_publ_section_title
;
 A Mixed-Ligand Zinc(II) Complex Containing a Bridging Dithiolate
 Ligand
;
_journal_issue                   8
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1540
_journal_page_last               1543
_journal_paper_doi               10.1107/S0108270195001995
_journal_volume                  51
_journal_year                    1995
_chemical_compound_source        'see text'
_chemical_formula_sum            'C28 H20 N8 S4 Zn2'
_chemical_formula_weight         727.5
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
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_atom_type_scat_source           IntTabIV
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_cell_formula_units_Z            2
_cell_length_a                   9.349(8)
_cell_length_b                   13.439(8)
_cell_length_c                   11.703(8)
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CAD-4 Software (Schagen, Staver, van Meurs & Williams, 1989)
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CAD-4 Software (Schagen, Staver, van Meurs & Williams, 1989)
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MolEN (Fair, 1990)
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ORTEP11 (Johnson, 1976)
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WP/WIN 5.1/5.2
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MolEN (Fair, 1990)
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SIR-88 (Burla, Camalli, Cascarano, Giacovazzo, Polidori, Spagna & Viterbo, 19
89)
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_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       '\w/2\q scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
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_diffrn_standards_decay_%        <1
_diffrn_standards_interval_time  120
_diffrn_standards_number         2
_exptl_absorpt_coefficient_mu    2.083
_exptl_absorpt_correction_T_max  0.9983
_exptl_absorpt_correction_T_min  0.5120
_exptl_absorpt_correction_type   '\y scans (North, Phillips & Mathews, 1968)'
_exptl_crystal_colour            'dark red'
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_exptl_crystal_description       plate
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_refine_ls_extinction_method     none
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_refine_ls_hydrogen_treatment    'H atoms: see text'
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;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value ' w=1/\s^2^(F)' was changed to
'calc'. New tag '_refine_ls_weighting_details' was created. The value
of the new tag was set to 'w=1/\s^2^(F)'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        1397(4)
_cod_original_sg_symbol_H-M      'P 21/n'
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