Recyclable chemosensor for oxalate based on bimetallic complexes of a dinucleating bis(iminopyridine) ligand.
Beattie, J. W.; White, D. S.; Bheemaraju, A.; Martin, P. D.; Groysman, S.; Dalton transactions (Cambridge, England : 2003) 43 (2014) 7979–7986; doi:10.1039/c4dt00577e

data_7029562
_publ_section_title
;
 Recyclable chemosensor for oxalate based on bimetallic complexes of a
 dinucleating bis(iminopyridine) ligand.
;
_journal_issue                   21
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              7979
_journal_page_last               7986
_journal_paper_doi               10.1039/c4dt00577e
_journal_volume                  43
_journal_year                    2014
_chemical_formula_sum            'C37 H57 Br3 Ca N2 Ni O3'
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_chemical_name_systematic
;
 ?
;
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_cell_length_c                   23.5169(12)
_cell_measurement_temperature    100(2)
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_computing_structure_refinement  'SHELXL-2013 (Sheldrick, 2013)'
_diffrn_ambient_temperature      100(2)
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_diffrn_measured_fraction_theta_max 0.953
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_av_unetI/netI     0.0540
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_diffrn_reflns_Laue_measured_fraction_max 0.953
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_diffrn_reflns_limit_l_min       -26
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_diffrn_reflns_point_group_measured_fraction_full 0.876
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_refine_diff_density_min         -0.740
_refine_diff_density_rms         0.108
_refine_ls_extinction_method     none
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_refine_ls_R_factor_all          0.0775
_refine_ls_R_factor_gt           0.0494
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
 w=1/[\s^2^(Fo^2^)+(0.0485P)^2^+8.9668P]
 where P=(Fo^2^+2Fc^2^)/3
;
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                4613
_reflns_number_total             6230
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c4dt00577e2.cif
_cod_data_source_block           sg135_0m
_cod_depositor_comments
'Adding full bibliography for 7029558--7029562.cif.'
_cod_database_code               7029562
_shelx_estimated_absorpt_t_min   0.524
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_shelxl_version_number           2013-2
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