LMucko/crystallography-open-database huggingface dataset:
Structures of three 2,2-dimethyl-3a,4,5,7a-tetrahydro-1,3-benzodioxolan-4-ols
Mackay, M. F.; Banwell, M. G.; Reum, M. E.; Richards, S. L.; Acta Crystallographica Section C 48 (1992) 70–73; doi:10.1107/S0108270191004456

data_2001103
_publ_section_title
;
 Structures of three
 2,2-dimethyl-3a,4,5,7a-tetrahydro-1,3-benzodioxolan-4-ols
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              70
_journal_page_last               73
_journal_paper_doi               10.1107/S0108270191004456
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C16 H18 O5'
_chemical_formula_weight         290.3
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   10.7730(10)
_cell_length_b                   25.9530(10)
_cell_length_c                   10.8180(10)
_cell_volume                     3024.6(4)
_diffrn_radiation_type           Cu
_diffrn_radiation_wavelength     1.5418
_exptl_absorpt_coefficient_mu    0.70
_exptl_crystal_density_diffrn    1.275
_exptl_crystal_density_meas      1.276(5)
_exptl_crystal_F_000             1232
_cod_data_source_file            an0328.cif
_cod_data_source_block           an0328c
_cod_original_cell_volume        3024.6(3)
_cod_database_code               2001103
Structure of the high-temperature-melting polymorph of 2,2'-dipyridylamine
Pyrka, G. J.; Pinkerton, A. A.; Acta Crystallographica Section C 48 (1992) 91–94; doi:10.1107/S0108270191007163

data_2001104
_publ_section_title
;
 Structure of the high-temperature-melting polymorph of
 2,2'-dipyridylamine
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              91
_journal_page_last               94
_journal_paper_doi               10.1107/S0108270191007163
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C10 H9 N3'
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_cell_angle_alpha                92.93(2)
_cell_angle_beta                 93.01(2)
_cell_angle_gamma                107.5(2)
_cell_formula_units_Z            4
_cell_length_a                   8.229(2)
_cell_length_b                   10.654(3)
_cell_length_c                   10.668(2)
_cell_volume                     888.6(11)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    0.08
_exptl_crystal_density_diffrn    1.28
_exptl_crystal_F_000             360
_cod_data_source_file            cr0297.cif
_cod_data_source_block           cr0297a
_cod_depositor_comments
;
 Updating space group information and adding the symmetry operation list.

 Antanas Vaitkus,
 2018-06-14
;
_cod_original_cell_volume        888.6
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               2001104
Structure of photostable 1-(hydroxyalkyl)-2(1<i>H</i>)-pyrazinones
Mori, Y.; Hayakawa, A.; Maeda, K.; Acta Crystallographica Section C 48 (1992) 123–126; doi:10.1107/S0108270191007904

data_2001105
_publ_section_title
;
 Structure of photostable 1-(hydroxyalkyl)-2(1<i>H</i>)-pyrazinones
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              123
_journal_page_last               126
_journal_paper_doi               10.1107/S0108270191007904
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C18 H16 N2 O2'
_chemical_formula_weight         292.32
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ac 2ab'
_symmetry_space_group_name_H-M   'P b c a'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   13.320(4)
_cell_length_b                   31.654(15)
_cell_length_c                   6.991(3)
_cell_volume                     2948(2)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    0.081
_exptl_crystal_density_diffrn    1.317
_exptl_crystal_F_000             1232
_cod_data_source_file            as0499.cif
_cod_data_source_block           as0499a
_cod_database_code               2001105
Structure of photostable 1-(hydroxyalkyl)-2(1<i>H</i>)-pyrazinones
Mori, Y.; Hayakawa, A.; Maeda, K.; Acta Crystallographica Section C 48 (1992) 123–126; doi:10.1107/S0108270191007904

data_2001106
_publ_section_title
;
 Structure of photostable 1-(hydroxyalkyl)-2(1<i>H</i>)-pyrazinones
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              123
_journal_page_last               126
_journal_paper_doi               10.1107/S0108270191007904
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C19 H18 N2 O2'
_chemical_formula_weight         306.35
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                114.19(2)
_cell_angle_beta                 96.89(2)
_cell_angle_gamma                106.40(2)
_cell_formula_units_Z            2
_cell_length_a                   9.939(2)
_cell_length_b                   10.043(2)
_cell_length_c                   9.603(3)
_cell_volume                     807.8(4)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    0.077
_exptl_crystal_density_diffrn    1.259
_exptl_crystal_F_000             324
_cod_data_source_file            as0499.cif
_cod_data_source_block           as0499b
_cod_original_cell_volume        807.9(4)
_cod_database_code               2001106
Structure of 3,5-di-<i>tert</i>-butyl-10-iodoprotoadamantane
Kojić-Prodić, B.; Luić, M.; Nigović, B.; Duddeck, H.; Rosenbaum, D.; Acta Crystallographica Section C 48 (1992) 131–133; doi:10.1107/S0108270191007758

data_2001107
_publ_section_title
;
 Structure of 3,5-di-<i>tert</i>-butyl-10-iodoprotoadamantane
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              131
_journal_page_last               133
_journal_paper_doi               10.1107/S0108270191007758
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C18 H31 I'
_chemical_formula_weight         374.35
_space_group_crystal_system      monoclinic
_space_group_IT_number           4
_space_group_name_Hall           'P 2yb'
_space_group_name_H-M_alt        'P 1 21 1'
_cell_angle_alpha                90
_cell_angle_beta                 107.87(3)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   9.0950(10)
_cell_length_b                   7.0870(10)
_cell_length_c                   14.149(2)
_cell_volume                     868.0(2)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    1.81
_exptl_crystal_density_diffrn    1.432
_exptl_crystal_F_000             384
_cod_data_source_file            ha0064.cif
_cod_data_source_block           ha0064a
_cod_original_cell_volume        867.9(2)
_cod_original_formula_sum        'C18 H31 I1'
_cod_database_code               2001107
(<i>E</i>)-4-Chloro-2,6-dimethylbenzaldehyde oxime at 110 K
Jerslev, B.; Larsen, S.; Acta Crystallographica Section C 48 (1992) 136–138; doi:10.1107/S0108270191007850

data_2001108
_publ_section_title
;
 (<i>E</i>)-4-Chloro-2,6-dimethylbenzaldehyde oxime at 110 K
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              136
_journal_page_last               138
_journal_paper_doi               10.1107/S0108270191007850
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C9 H10 Cl N O'
_chemical_formula_weight         183.6
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 95.763(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   6.8553(10)
_cell_length_b                   15.399(2)
_cell_length_c                   8.5628(9)
_cell_volume                     899.4(2)
_diffrn_radiation_type           Cu
_diffrn_radiation_wavelength     1.54178
_exptl_absorpt_coefficient_mu    3.403
_exptl_crystal_density_diffrn    1.356
_exptl_crystal_F_000             384
_cod_data_source_file            ab0222.cif
_cod_data_source_block           ab0222a
_cod_original_cell_volume        899.3(3)
_cod_original_formula_sum        'C9 H10 Cl1 N1 O1'
_cod_database_code               2001108
Crystal studies of musk compounds. IV. Structure of 4-acetyl-6-<i>tert</i>-butyl-1,1-dimethylindan (musk celestolide)
De Ridder, D. J. A.; Schenk, H.; Acta Crystallographica Section C 48 (1992) 140–142; doi:10.1107/S0108270191008211

data_2001109
_publ_section_title
;
 Crystal studies of musk compounds. IV. Structure of
 4-acetyl-6-<i>tert</i>-butyl-1,1-dimethylindan (musk celestolide)
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              140
_journal_page_last               142
_journal_paper_doi               10.1107/S0108270191008211
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C17 H24 O'
_chemical_formula_weight         244.38
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_cell_angle_alpha                105.735(6)
_cell_angle_beta                 99.58(2)
_cell_angle_gamma                90.090(10)
_cell_formula_units_Z            4
_cell_length_a                   10.160(2)
_cell_length_b                   12.230(2)
_cell_length_c                   12.7960(10)
_cell_volume                     1507.2(5)
_diffrn_radiation_type           Cu
_diffrn_radiation_wavelength     1.54184
_exptl_absorpt_coefficient_mu    0.461
_exptl_crystal_density_diffrn    1.08
_exptl_crystal_F_000             536
_cod_data_source_file            mu0236.cif
_cod_data_source_block           mu0236a
_cod_depositor_comments
;
 Updating space group information and adding the symmetry operation list.

 Antanas Vaitkus,
 2018-06-14
;
_cod_original_sg_symbol_H-M      P-1
_cod_original_formula_sum        'C17 H24 O1'
_cod_database_code               2001109
Structures of 6-amino-1,3-dimethyl-5-nitrosouracil monohydrate and 6-amino-5-formyl-1,3-dimethyluracil monohydrate
Low, J. N.; Howie, R. A.; Hueso-Ureña, F.; Moreno-Carretero, M. N.; Acta Crystallographica Section C 48 (1992) 145–147; doi:10.1107/S010827019100820X

data_2001110
_publ_section_title
;
 Structures of 6-amino-1,3-dimethyl-5-nitrosouracil monohydrate and
 6-amino-5-formyl-1,3-dimethyluracil monohydrate
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              145
_journal_page_last               147
_journal_paper_doi               10.1107/S010827019100820X
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C6 H10 N4 O4'
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_H-M   'P n a 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   13.978(10)
_cell_length_b                   9.638(8)
_cell_length_c                   6.338(11)
_cell_volume                     853.9(18)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    0.088
_exptl_crystal_density_diffrn    1.57
_exptl_crystal_F_000             424
_cod_data_source_file            mu0225.cif
_cod_data_source_block           mu0225a
_cod_depositor_comments
;
 Adding the _atom_site_type_symbol data item.

 Antanas Vaitkus,
 2017-01-30
;
_cod_original_cell_volume        853.9
_cod_database_code               2001110
Structures of 6-amino-1,3-dimethyl-5-nitrosouracil monohydrate and 6-amino-5-formyl-1,3-dimethyluracil monohydrate
Low, J. N.; Howie, R. A.; Hueso-Ureña, F.; Moreno-Carretero, M. N.; Acta Crystallographica Section C 48 (1992) 145–147; doi:10.1107/S010827019100820X

data_2001111
_publ_section_title
;
 Structures of 6-amino-1,3-dimethyl-5-nitrosouracil monohydrate and
 6-amino-5-formyl-1,3-dimethyluracil monohydrate
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              145
_journal_page_last               147
_journal_paper_doi               10.1107/S010827019100820X
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C7 H11 N3 O4'
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 116.69(5)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   15.557(11)
_cell_length_b                   7.562(11)
_cell_length_c                   16.972(13)
_cell_volume                     1784(3)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    0.081
_exptl_crystal_density_diffrn    1.50
_exptl_crystal_F_000             848
_cod_data_source_file            mu0225.cif
_cod_data_source_block           mu0225b
_cod_depositor_comments
;
 Updating space group information and adding the symmetry operation list.

 Antanas Vaitkus,
 2018-06-14

  Adding the _atom_site_type_symbol data item, to prevent confusion
  between hydrogen and holmium atoms.

  Saulius Gra\<zulis
  2013-10-17
;
_cod_original_cell_volume        1783.88
_cod_original_sg_symbol_H-M      C2/c
_cod_original_formula_sum        C7H11N3O4
_cod_database_code               2001111
Structure of aquabis(2,2'-bipyrimidine-<i>N</i>,<i>N</i>')copper(II) perchlorate dihydrate
Morgan, L. W.; Pennington, W. T.; Petersen, J. D.; Ruminski, R. R.; Bennett, D. W.; Rommel, J. S.; Acta Crystallographica Section C 48 (1992) 163–165; doi:10.1107/S0108270191004602

data_2001112
_publ_section_title
;
 Structure of aquabis(2,2'-bipyrimidine-<i>N</i>,<i>N</i>')copper(II)
 perchlorate dihydrate
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              163
_journal_page_last               165
_journal_paper_doi               10.1107/S0108270191004602
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         '[Cu(C8 H6 N4)2 (H2 O)](Cl O4)2,2(H2 O)'
_chemical_formula_sum            'C16 H18 Cl2 Cu N8 O11'
_chemical_formula_weight         632.86
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 96.27(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   18.232(3)
_cell_length_b                   7.6130(10)
_cell_length_c                   16.842(4)
_cell_volume                     2323.7(7)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    1.254
_exptl_crystal_density_diffrn    1.82
_exptl_crystal_F_000             1284
_cod_data_source_file            st0503.cif
_cod_data_source_block           st0503a
_cod_original_cell_volume        2323.6(8)
_cod_original_formula_sum        'C16 H18 N8 O11 Cl2 Cu'
_cod_database_code               2001112
Tris(4-fluoro-2,2'-bipyridyl)iron(II) hexafluorophosphate
Cho, C. K.; Secco, A. S.; Acta Crystallographica Section C 48 (1992) 165–167; doi:10.1107/S0108270191008788

data_2001113
_publ_section_title
;
 Tris(4-fluoro-2,2'-bipyridyl)iron(II) hexafluorophosphate
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              165
_journal_page_last               167
_journal_paper_doi               10.1107/S0108270191008788
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'C30 H21 F3 Fe1 N6,2(F6 P1)'
_chemical_formula_sum            'C30 H21 F15 Fe N6 P2'
_chemical_formula_weight         868.31
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 94.560(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   10.4220(10)
_cell_length_b                   17.294(2)
_cell_length_c                   18.581(3)
_cell_volume                     3338.4(7)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    0.659
_exptl_crystal_density_diffrn    1.728
_exptl_crystal_F_000             1736
_cod_data_source_file            br0002.cif
_cod_data_source_block           br0002a
_cod_original_cell_volume        3338.3(7)
_cod_original_formula_sum        'C30 H21 F15 Fe1 N6 P2'
_cod_database_code               2001113
Structure of <i>trans</i>-diaquabis[(2-oxopyrrolidin-1-yl)acetamide]copper(II) perchlorate
Delacruz, X.; Martínez-Balbás, A.; Tormo, J.; Verdaguer, N.; Acta Crystallographica Section C 48 (1992) 167–169; doi:10.1107/S0108270191008971

data_2001114
_publ_section_title
;
 Structure of
 <i>trans</i>-diaquabis[(2-oxopyrrolidin-1-yl)acetamide]copper(II)
 perchlorate
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              167
_journal_page_last               169
_journal_paper_doi               10.1107/S0108270191008971
_journal_volume                  48
_journal_year                    1992
_chemical_formula_sum            'C12 H24 Cl2 Cu N4 O14'
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 103.94(5)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   7.231(10)
_cell_length_b                   10.633(3)
_cell_length_c                   15.767(3)
_cell_volume                     1176.6(17)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     .71069
_exptl_absorpt_coefficient_mu    12.08
_exptl_crystal_density_diffrn    1.645
_exptl_crystal_F_000             594.99
_cod_data_source_file            mu0207.cif
_cod_data_source_block           mu0207a
_cod_depositor_comments
;
 Updating space group information and adding the symmetry operation list.

 Antanas Vaitkus,
 2018-06-15
;
_cod_original_cell_volume        1176.57
_cod_original_formula_sum        'Cu1 Cl2 C12 N4 O14 H24'
_cod_database_code               2001114
Structure of carbonyl(4-methoxy-<i>N</i>-methylbenzothiohydroxamato-κ<i>O</i>,κ<i>S</i>)(tricyclohexylphosphine)rhodium(I) benzene solvate
Basson, S. S.; Leipoldt, J. G.; Purcell, W.; Lamprecht, G. J.; Preston, H.; Acta Crystallographica Section C 48 (1992) 169–171; doi:10.1107/S0108270191008405

data_2001115
_publ_section_title
;Structure of
 carbonyl(4-methoxy-<i>N</i>-methylbenzothiohydroxamato-\k<i>O</i>,\k<i>S</i>)(tricyclohexylphosphine)rhodium(I)
 benzene solvate
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              169
_journal_page_last               171
_journal_paper_doi               10.1107/S0108270191008405
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'C9 H10 N1 O2 S1,C18 H33 P1,C7 H6 O1 Rh1'
_chemical_formula_sum            'C34 H49 N O3 P Rh S'
_chemical_formula_weight         685.7
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                80.030(10)
_cell_angle_beta                 87.870(10)
_cell_angle_gamma                61.940(10)
_cell_formula_units_Z            2
_cell_length_a                   9.764(2)
_cell_length_b                   10.185(2)
_cell_length_c                   19.885(3)
_cell_volume                     1716.5(6)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    0.624
_exptl_crystal_density_diffrn    1.33
_exptl_crystal_density_meas      1.310(10)
_exptl_crystal_F_000             720
_cod_data_source_file            ab0215.cif
_cod_data_source_block           ab0215a
_cod_original_cell_volume        1716.5(5)
_cod_original_formula_sum        'C34 H49 N1 O3 P1 S1 Rh1'
_cod_database_code               2001115
Structure of carbonyl(<i>N</i>-hydroxy-<i>N</i>-nitrosobenzenaminato-<i>O</i>,<i>O</i>')(4-methyl-2,6,7-trioxa-1-phosphabicyclo[2.2.2]octane)rhodium(I)
Basson, S. S.; Leipoldt, J. G.; Purcell, W.; Venter, J. A.; Acta Crystallographica Section C 48 (1992) 171–173; doi:10.1107/S0108270191008223

data_2001116
_publ_section_title
;Structure of
 carbonyl(<i>N</i>-hydroxy-<i>N</i>-nitrosobenzenaminato-<i>O</i>,<i>O</i>')(4-methyl-2,6,7-trioxa-1-phosphabicyclo[2.2.2]octane)rhodium(I)
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              171
_journal_page_last               173
_journal_paper_doi               10.1107/S0108270191008223
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         'C6 H5 N2 O2,C5 H9 O3 P1,C1 O1 Rh1'
_chemical_formula_sum            'C12 H14 N2 O6 P Rh'
_chemical_formula_weight         416.1
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 92.857(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   11.9900(10)
_cell_length_b                   6.1950(10)
_cell_length_c                   20.906(3)
_cell_volume                     1550.9(4)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    1.212
_exptl_crystal_density_diffrn    1.78
_exptl_crystal_density_meas      1.780(10)
_exptl_crystal_F_000             832
_cod_data_source_file            ab0217.cif
_cod_data_source_block           ab0217a
_cod_original_cell_volume        1550.8(4)
_cod_original_formula_sum        'C12 H14 N2 O6 P1 Rh1'
_cod_database_code               2001116