Synthesis and structural characterization of 20-membered macrocyclic rings bearing trans-chelating bis(N-heterocyclic carbene) ligands and the catalytic activity of their palladium(ii) complexes.
Thapa, Rajesh; Kilyanek, Stefan M.; Dalton transactions (Cambridge, England : 2003) 48 (2019) 12577–12590; doi:10.1039/c9dt02147g

data_7700625
_publ_section_title
;
 Synthesis and structural characterization of 20-membered macrocyclic
 rings bearing trans-chelating bis(N-heterocyclic carbene) ligands and the
 catalytic activity of their palladium(ii) complexes.
;
_journal_issue                   33
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              12577
_journal_page_last               12590
_journal_paper_doi               10.1039/c9dt02147g
_journal_volume                  48
_journal_year                    2019
_chemical_formula_moiety         'C80 H92 Ag3 Br2 N12, Ag Br2, 2(C H2 Cl2)'
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_space_group_name_Hall           '-C 2yc'
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_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
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;
2019-06-13 deposited with the CCDC.    2019-07-23 downloaded from the CCDC.
;
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_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
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'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+238.0000P] where P=(Fo^2^+2Fc^2^)/3'
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'Adding full bibliography for 7700623--7700627.cif.'
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