Synthesis and Characterization of a Series of [M2(β-SiW8O31)2](n-) Clusters and Mechanistic Insight into the Reorganization of {β-SiW8O31} into {α-SiW9O34}.
Winter, Ross S.; Long, De-Liang; Cronin, Leroy; Inorganic chemistry 54 (2015) 4151–4155; doi:10.1021/acs.inorgchem.5b00405

data_4342750
_publ_section_title
;
 Synthesis and Characterization of a Series of [M2(\b-SiW8O31)2](n-)
 Clusters and Mechanistic Insight into the Reorganization of {\b-SiW8O31}
 into {\a-SiW9O34}.
;
_journal_issue                   8
_journal_name_full               'Inorganic chemistry'
_journal_page_first              4151
_journal_page_last               4155
_journal_paper_doi               10.1021/acs.inorgchem.5b00405
_journal_volume                  54
_journal_year                    2015
_chemical_formula_sum            'H99 Na15 O111 Si2 W16 Zn2'
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0466P)^2^+2.6108P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            Zn2W16.cif
_cod_data_source_block           rw9381
_cod_depositor_comments
;Adding full bibliography for 4342749--4342755.cif.

The following automatic conversions were performed:

'_atom_sites_solution_primary' value 'direct methods' was changed to
'direct'.

Automatic conversion script
Id: cif_fix_values 6452 2018-10-05 10:23:21Z andrius 
;
_cod_database_code               4342750
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_shelx_res_checksum              15907
_shelx_hkl_checksum              35650