Radical Trifluoromethylative Dearomatization of Indoles and Furans with CO2
Ye, Jian-Heng; Zhu, Lei; Yan, Si-Shun; Miao, Meng; Zhang, Xin-Chi; Zhou, Wen-Jun; Li, Jing; Lan, Yu; Yu, Da-Gang; ACS Catalysis 7 (2017) 8324–; doi:10.1021/acscatal.7b02533

data_4514289
_publ_section_title
;
 Radical Trifluoromethylative Dearomatization of Indoles and Furans with
 CO2
;
_journal_issue                   12
_journal_name_full               'ACS Catalysis'
_journal_page_first              8324
_journal_paper_doi               10.1021/acscatal.7b02533
_journal_volume                  7
_journal_year                    2017
_chemical_formula_sum            'C23 H19 F3 N4 O2'
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_diffrn_ambient_temperature      150(2)
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_diffrn_radiation_type           CuK\a
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_diffrn_reflns_theta_min         4.964
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_refine_ls_extinction_method     none
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_refine_ls_matrix_type           full
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_refine_ls_number_reflns         4017
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_refine_ls_restrained_S_all      1.060
_refine_ls_R_factor_all          0.0582
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0941P)^2^+0.6856P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_depositor_comments          'Adding full bibliography for 4514289.cif.'
_cod_original_cell_volume        2068.64(8)
_cod_database_code               4514289
_shelx_shelxl_version_number     2014/7
_shelx_res_checksum              9046
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