Borylation and rearrangement reactions of azasilaanthracenes to afford B,N-doped nanographenes.
Zender, Elena; Valverde, Danillo; Neubaur, Robert; Karger, Sebastian; Virovets, Alexander; Bolte, Michael; Lerner, Hans-Wolfram; Olivier, Yoann; Wagner, Matthias; Dalton transactions (Cambridge, England : 2003) 53 (2024) 9294–9300; doi:10.1039/d4dt01166j

data_7715979
_publ_section_title
;
 Borylation and rearrangement reactions of azasilaanthracenes to afford
 B,N-doped nanographenes.
;
_journal_issue                   22
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              9294
_journal_page_last               9300
_journal_paper_doi               10.1039/d4dt01166j
_journal_volume                  53
_journal_year                    2024
_chemical_formula_moiety         'C51 H36 B3 N3, 2(C H Cl3)'
_chemical_formula_sum            'C53 H38 B3 Cl6 N3'
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;
2024-05-06 deposited with the CCDC.	2024-05-08 downloaded from the CCDC.
;
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;
CrysAlisPro 1.171.42.43a (Rigaku Oxford Diffraction, 2022)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            brownish-yellow
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1642P)^2^+1.8586P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7715973--7715981.cif.'
_cod_original_cell_volume        2274.3(3)
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