Self-assembly processes of 2D Au(I)-S(CH<sub>2</sub>)<sub>2</sub>COOH lamellae.
Zhang, Shengrui; Yu, Zhongqi; Demessence, Aude; Guillou, Nathalie; Xu, Shujue; Liu, Han; Fu, Yuru; Zhang, Jingpei; Li, Minjie; Nanoscale 17 (2025) 5270–5279; doi:10.1039/d4nr05118a

data_1573753
_publ_section_title
;
 Self-assembly processes of 2D Au(I)-S(CH<sub>2</sub>)<sub>2</sub>COOH
 lamellae.
;
_journal_issue                   9
_journal_name_full               Nanoscale
_journal_page_first              5270
_journal_page_last               5279
_journal_paper_doi               10.1039/d4nr05118a
_journal_volume                  17
_journal_year                    2025
_chemical_formula_moiety         'C3 H5 Ag O2 S'
_chemical_formula_sum            'C3 H5 Ag O2 S'
_chemical_formula_weight         213.00
_chemical_name_mineral           '[Ag(SC2H4COOH]n'
_chemical_name_systematic        Ag-MPA
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_audit_update_record
;
2024-09-23 deposited with the CCDC.	2025-01-21 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 99.6952(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   13.61196(17)
_cell_length_b                   6.63372(6)
_cell_length_c                   5.94002(5)
_cell_measurement_temperature    293
_cell_volume                     528.711(9)
_computing_molecular_graphics    DIAMOND
_computing_structure_refinement  TOPAS
_computing_structure_solution    TOPAS
_diffrn_ambient_temperature      293
_diffrn_measurement_device_type  'Mythen Detector'
_diffrn_radiation_monochromator  'Si(111) double monochromator'
_diffrn_radiation_type           'X-ray synchrotron'
_diffrn_radiation_wavelength     0.6887
_diffrn_source                   Synchrotron
_exptl_crystal_colour            colourless
_exptl_crystal_description       polycrystalline
_pd_meas_2theta_range_inc        0.003544
_pd_meas_2theta_range_max        66.06574
_pd_meas_2theta_range_min        0.99993
_pd_proc_2theta_range_inc        0.005
_pd_proc_2theta_range_max        48.0
_pd_proc_2theta_range_min        2.0
_pd_proc_ls_background_function  'Chebychev polynomial and two additional peaks'
_pd_proc_ls_profile_function
'Thomson-Cox-Hastings pseudo-Voigt convoluted with Finger et al function'
_pd_proc_ls_prof_R_factor        0.034
_pd_proc_ls_prof_wR_factor       0.047
_pd_spec_mounting                'glass capillary'
_pd_spec_mount_mode              transmission
_pd_spec_shape                   cylinder
_refine_ls_goodness_of_fit_all   2.90
_refine_ls_number_reflns         940
_refine_ls_R_I_factor            0.016
_cod_data_source_file            d4nr05118a2.cif
_cod_data_source_block           '[Ag(SC2H4COOH]n'
_cod_depositor_comments          'Adding full bibliography for 1573753.cif.'
_cod_original_cell_volume        528.710(10)
_cod_original_sg_symbol_H-M      P21/c
_cod_database_code               1573753
_refine_ls_number_structural_parameters 24
_refine_ls_number_profile_parameters 27