Syntheses, structures and multinuclear NMR (45Sc, 89Y, 31P) studies of Ph3PO, Ph2MePO and Me3PO complexes of scandium and yttrium nitrates
Deakin, Lucy; Levason, William; Popham, Michael C.; Reid, Gillian; Webster, Michael; Journal of the Chemical Society, Dalton Transactions  (2000) 2439–; doi:10.1039/b001669l

data_7009530
_publ_section_title
;
 Syntheses, structures and multinuclear NMR (45Sc, 89Y, 31P) studies of
 Ph3PO, Ph2MePO and Me3PO complexes of scandium and yttrium nitrates
;
_journal_issue                   14
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              2439
_journal_paper_doi               10.1039/b001669l
_journal_year                    2000
_chemical_formula_sum            'C9 H27 N3 O12 P3 Y'
_chemical_formula_weight         551.15
_chemical_name_systematic
;
tris(nitrato-O,O')tris(trimethylphosphineoxide)yttrium(III)
;
_space_group_IT_number           2
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;
?
;
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_cell_angle_beta                 93.0(1)
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_cell_length_a                   14.578(10)
_cell_length_b                   15.39(2)
_cell_length_c                   10.57(2)
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;
SHELXS86 (Sheldrick, 1985)
;
_diffrn_ambient_temperature      150
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;
(North,Phillips & Matthews, 1968)
;
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_refine_ls_shift/su_mean         0.0070
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo) + 0.00000|Fo|^2^]'
_refine_ls_weighting_scheme      sigma
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_reflns_threshold_expression     I>2.00\s(I)
_cod_data_source_file            b001669l.txt
_cod_data_source_block           Ilev99_11
_cod_original_sg_symbol_H-M      'P -1       '
_cod_original_formula_sum        'C9 H27 N3 O12 P3 Y '
_cod_database_code               7009530