Slow magnetic relaxation in octahedral low-spin Ni(iii) complexes.
Bhowmick, Indrani; Roehl, Andrew J.; Neilson, James R.; Rappé, Anthony K; Shores, Matthew P.; Chemical science 9 (2018) 6564–6571; doi:10.1039/c7sc04482h

data_1549679
_publ_section_title
;
 Slow magnetic relaxation in octahedral low-spin Ni(iii) complexes.
;
_journal_issue                   31
_journal_name_full               'Chemical science'
_journal_page_first              6564
_journal_page_last               6571
_journal_paper_doi               10.1039/c7sc04482h
_journal_volume                  9
_journal_year                    2018
_chemical_formula_sum            'C12 H24 Cl N6 Ni O4 S2'
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_space_group_name_Hall           '-P 1'
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_audit_update_record
;
2017-10-11 deposited with the CCDC.
2018-06-29 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'Bruker Apex 2 CCD'
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_exptl_crystal_density_diffrn    1.560
_exptl_crystal_description       block
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_exptl_crystal_preparation       'Magnetic properties'
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0557P)^2^+6.8344P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                2332
_reflns_number_total             3212
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c7sc04482h8.cif
_cod_data_source_block           shelx_CCDC3
_cod_depositor_comments
'Adding full bibliography for 1549676--1549679.cif.'
_cod_original_cell_volume        1013(14)
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_shelxl_version_number           2013-4
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