The Bi2O3‒Fe2O3‒Sb2O5 system phase diagram refinement, Bi3FeSb2O11 structure peculiarities and magnetic properties
Egorysheva, A.V.; Ellert, O.G.; Gajtko, O.M.; Efimov, N.N.; Svetogorov, R.D.; Zubavichus, Y.V.; Grigorieva, A.V.; Journal of Solid State Chemistry 225 (2015) 278–284; doi:10.1016/j.jssc.2014.12.032

data_1562034
_publ_section_title
;
 The Bi2O3--Fe2O3--Sb2O5 system phase diagram refinement, Bi3FeSb2O11
 structure peculiarities and magnetic properties
;
_journal_name_full               'Journal of Solid State Chemistry'
_journal_page_first              278
_journal_page_last               284
_journal_paper_doi               10.1016/j.jssc.2014.12.032
_journal_volume                  225
_journal_year                    2015
_chemical_absolute_configuration .
_chemical_formula_sum            'Bi3 Fe O11 Sb2'
_chemical_formula_weight         1102.3
_space_group_IT_number           201
_space_group_name_Hall           '-P 2ab 2bc 3'
_space_group_name_H-M_alt        'P n -3 :2'
_symmetry_cell_setting           cubic
_symmetry_Int_Tables_number      201
_symmetry_space_group_name_Hall  '-P 2ab 2bc 3'
_symmetry_space_group_name_H-M   'P n -3 :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.51521(2)
_cell_length_b                   9.51521(2)
_cell_length_c                   9.51521(2)
_cell_measurement_temperature    293
_cell_volume                     861.500(3)
_diffrn_ambient_temperature      293
_diffrn_radiation_probe          x-ray
_diffrn_radiation_wavelength     0.68886
_exptl_absorpt_coefficient_mu    63.477
_exptl_crystal_density_diffrn    8.4958
_exptl_crystal_F_000             1860
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.01
_pd_meas_2theta_range_max        52.157
_pd_meas_2theta_range_min        0.005
_pd_meas_number_of_points        5000
_pd_proc_2theta_range_inc        0.01
_pd_proc_2theta_range_max        49.997
_pd_proc_2theta_range_min        3.01
_pd_proc_ls_background_function  '12 Chebyshev polynoms'
_pd_proc_ls_pref_orient_corr     none
_pd_proc_ls_profile_function     Pseudo-Voigt
_pd_proc_ls_prof_R_factor        0.0143
_pd_proc_ls_prof_wR_expected     0.1793
_pd_proc_ls_prof_wR_factor       0.0234
_refine_ls_goodness_of_fit_all   0.13
_refine_ls_number_constraints    6
_refine_ls_number_parameters     39
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0310
_refine_ls_R_factor_gt           0.0269
_refine_ls_shift/su_max          0.0196
_refine_ls_shift/su_mean         0.0040
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_all         0.0349
_refine_ls_wR_factor_gt          0.0321
_cod_data_source_file            JSSC-2015-225-278.cif
_cod_data_source_block           I
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_diffrn_radiation_probe' value 'X-ray' was changed to
'x-ray' in accordance with the built-in table derived from the CIF
Core dictionary named 'cif_core.dic' version 2.4.5 last updated on
2014-11-21.

Automatic conversion script
Id: cif_fix_values 8369 2020-08-20 11:38:08Z andrius 
;
_cod_original_sg_symbol_Hall     '-P 2ab;2bc;3'
_cod_original_sg_symbol_H-M      'P n -3'
_cod_original_formula_sum        'Bi3 Fe1 O11 Sb2'
_cod_database_code               1562034