Silver(i) complexes with 2-acetylpyridinebenzoylhydrazones exhibit antimicrobial effects against yeast and filamentous fungi
Santos, Ane F.; Ferreira, Isabella P.; Takahashi, Jacqueline A.; Rodrigues, Gabriel L. S.; Pinheiro, Carlos B.; Teixeira, Letícia R.; Rocha, Willian R.; Beraldo, Heloisa; New Journal of Chemistry 42 (2018) 2125–; doi:10.1039/C7NJ04280A

data_7056885
_publ_section_title
;
 Silver(i) complexes with 2-acetylpyridinebenzoylhydrazones exhibit
 antimicrobial effects against yeast and filamentous fungi
;
_journal_issue                   3
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              2125
_journal_paper_doi               10.1039/C7NJ04280A
_journal_volume                  42
_journal_year                    2018
_chemical_formula_moiety         'C28 H24 Ag Cl2 N6 O2 +, N O3 -'
_chemical_formula_sum            'C28 H24 Ag Cl2 N7 O5'
_chemical_formula_weight         717.31
_space_group_crystal_system      triclinic
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_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
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_audit_update_record
;
2017-10-28 deposited with the CCDC.
2018-01-11 downloaded from the CCDC.
;
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_diffrn_measurement_device_type  'Xcalibur, Atlas, Gemini ultra'
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_diffrn_reflns_av_R_equivalents  0.0521
_diffrn_reflns_av_unetI/netI     0.0560
_diffrn_reflns_Laue_measured_fraction_full 0.999
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_diffrn_reflns_point_group_measured_fraction_full 0.999
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_diffrn_source                   'Enhance (Mo) X-ray Source'
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;
CrysAlisPro, Agilent Technologies,
Version 1.171.37.34 (release 22-05-2014 CrysAlis171 .NET)
(compiled May 22 2014,16:03:01)
Analytical numeric absorption correction using a multifaceted crystal
            model based on expressions derived by R.C. Clark & J.S. Reid.
(Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            colourless
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_refine_ls_R_factor_all          0.0735
_refine_ls_R_factor_gt           0.0452
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0493P)^2^+0.8249P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1024
_refine_ls_wR_factor_ref         0.1204
_reflns_Friedel_coverage         0.000
_reflns_number_gt                4190
_reflns_number_total             5925
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c7nj04280a2.cif
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_cod_depositor_comments
'Adding full bibliography for 7056882--7056885.cif.'
_cod_original_cell_volume        1445.35(13)
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_shelx_shelxl_version_number     2017/1
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