Two new Cu(ii) and La(iii) 2D coordination polymers, synthesis and in situ structural analysis by X-ray diffraction.
Lundvall, F.; Wragg, D. S.; Dietzel, P. D. C.; Fjellvåg, H; Dalton transactions (Cambridge, England : 2003) 45 (2016) 12827–12834; doi:10.1039/c6dt02195f

data_7040043
_publ_section_title
;
 Two new Cu(ii) and La(iii) 2D coordination polymers, synthesis and in
 situ structural analysis by X-ray diffraction.
;
_journal_issue                   32
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              12827
_journal_page_last               12834
_journal_paper_doi               10.1039/c6dt02195f
_journal_volume                  45
_journal_year                    2016
_chemical_formula_moiety         'C19 H19 Cu N O7'
_chemical_formula_sum            'C19 H19 Cu N O7'
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_chemical_name_systematic        CPO-71-Cu
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_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2014/6
_audit_update_record
;
2016-06-01 deposited with the CCDC.
2016-07-25 downloaded from the CCDC.
;
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_cell_volume                     4357.6(3)
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_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      105(2)
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_diffrn_measurement_device_type  'Bruker PHOTON CCD'
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_diffrn_radiation_type           MoK\a
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_exptl_crystal_description       needle
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_exptl_crystal_recrystallization_method 'solvothermal synthesis'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0295P)^2^+9.3159P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_gt                4065
_reflns_number_total             5023
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c6dt02195f2.cif
_cod_data_source_block           CPO-71-Cu
_cod_depositor_comments
'Adding full bibliography for 7040043--7040044.cif.'
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_shelx_res_checksum              89149