Proton-conducting layered structures based on transition metal oxo-clusters supported by Sb(iii) tartrate scaffolds.
Ma, Wen; Hu, Bing; Jing, Kaiqiang; Li, Zhong; Jin, Jiance; Zheng, Shoutian; Huang, Xiaoying; Dalton transactions (Cambridge, England : 2003) 49 (2020) 3849–3855; doi:10.1039/c9dt04333k

data_7702275
_publ_section_title
;
 Proton-conducting layered structures based on transition metal
 oxo-clusters supported by Sb(iii) tartrate scaffolds.
;
_journal_issue                   12
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              3849
_journal_page_last               3855
_journal_paper_doi               10.1039/c9dt04333k
_journal_volume                  49
_journal_year                    2020
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_chemical_formula_sum            'C24 H49 Cd2 Co4 O60 Sb7'
_chemical_formula_weight         2610.40
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_audit_update_record
;
2019-09-29 deposited with the CCDC.	2019-11-26 downloaded from the CCDC.
;
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_diffrn_radiation_type           MoK\a
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_exptl_absorpt_correction_type   multi-scan
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_exptl_crystal_description       rod-like
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_refine_ls_abs_structure_details
;
 Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack   0.01(4)
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0600P)^2^+4.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1250
_refine_ls_wR_factor_ref         0.1288
_reflns_Friedel_coverage         0.833
_reflns_Friedel_fraction_full    0.996
_reflns_Friedel_fraction_max     0.995
_reflns_number_gt                12815
_reflns_number_total             13823
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c9dt04333k2.cif
_cod_data_source_block           x_CCDC1
_cod_depositor_comments
'Adding full bibliography for 7702274--7702275.cif.'
_cod_original_cell_volume        6173(4)
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