Thiocyanate complexes of the lanthanides, Am and Cm.
Wilson, Richard E.; Carter, Tyler J.; Autillo, Matthieu; Stegman, Samantha; Chemical communications (Cambridge, England) 56 (2020) 2622–2625; doi:10.1039/c9cc07612c

data_7125915
_publ_section_title
;
 Thiocyanate complexes of the lanthanides, Am and Cm.
;
_journal_issue                   17
_journal_name_full
'Chemical communications (Cambridge, England)'
_journal_page_first              2622
_journal_page_last               2625
_journal_paper_doi               10.1039/c9cc07612c
_journal_volume                  56
_journal_year                    2020
_chemical_formula_sum            'C39 H0 Ce N11 O0 S7'
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_space_group_name_Hall           '-P 4 2 3'
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_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2019-09-26 deposited with the CCDC.	2020-01-13 downloaded from the CCDC.
;
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_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
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_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type  'BRUKER APEX II'
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_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.107
_exptl_crystal_description       block
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_exptl_crystal_size_mid          0.152
_exptl_crystal_size_min          0.094
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_refine_ls_extinction_method     none
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1315P)^2^+1.5000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1590
_refine_ls_wR_factor_ref         0.1590
_reflns_Friedel_coverage         0.000
_reflns_number_gt                512
_reflns_number_total             512
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c9cc07612c2.cif
_cod_data_source_block           pm3m
_cod_depositor_comments
'Adding full bibliography for 7125915--7125930.cif.'
_cod_original_cell_volume        1480.8(3)
_cod_database_code               7125915
_shelx_shelxl_version_number     2014/7
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