Ethanol- and heat-mediated phase change from a kinetic (Z′ = 4) polymorph to a thermodynamic (Z′ = 1) polymorph for an N2,6-diaryl-1,3,5-triazine-2,4-diamine
Tan, Sang Loon; Tan, Yee Seng; Bin Shahari, Muhammad Syafiq; Junaid, Ahmad; Dolzhenko, Anton V.; Tiekink, Edward R. T.; CrystEngComm 25 (2023) 798–812; doi:10.1039/D2CE01548J

data_7246021
_publ_section_title
;
 Ethanol- and heat-mediated phase change from a kinetic (Z&#x2032; = 4)
 polymorph to a thermodynamic (Z&#x2032; = 1) polymorph for an
 N2,6-diaryl-1,3,5-triazine-2,4-diamine
;
_journal_issue                   5
_journal_name_full               CrystEngComm
_journal_page_first              798
_journal_page_last               812
_journal_paper_doi               10.1039/D2CE01548J
_journal_volume                  25
_journal_year                    2023
_chemical_formula_moiety         'C19 H21 N5 O4'
_chemical_formula_sum            'C19 H21 N5 O4'
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_space_group_name_Hall           '-P 2yn'
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_atom_sites_solution_secondary   difmap
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_audit_update_record
;
2022-10-28 deposited with the CCDC.	2022-12-19 downloaded from the CCDC.
;
_cell_angle_alpha                90
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_computing_cell_refinement       'CrysAlisPro (Rigaku OD, 2017)'
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'ORTEP-3 for Windows (Farrugia, 2012), DIAMOND (Brandenburg, 2006)'
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_diffrn_ambient_temperature      100(2)
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0558P)^2^+0.5212P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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'Adding full bibliography for 7246020--7246021.cif.'
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