Reactivity of bis[{2,6-(dimethylamino)methyl}phenyl]telluride with Pd(ii) and Hg(ii): isolation of the first Pd(ii) complex of an organotellurenium cation as a ligand
Gupta, Anand K.; Deka, Rajesh; Singh, Harkesh B.; Butcher, Ray J.; New Journal of Chemistry 43 (2019) 13225–; doi:10.1039/C9NJ02469G

data_7058632
_publ_section_title
;
 Reactivity of bis[{2,6-(dimethylamino)methyl}phenyl]telluride with Pd(ii)
 and Hg(ii): isolation of the first Pd(ii) complex of an organotellurenium
 cation as a ligand
;
_journal_issue                   33
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              13225
_journal_paper_doi               10.1039/C9NJ02469G
_journal_volume                  43
_journal_year                    2019
_chemical_formula_moiety         'C24 H38 N4 Te'
_chemical_formula_sum            'C24 H38 N4 Te'
_chemical_formula_weight         510.18
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_space_group_name_Hall           '-P 2yn'
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_symmetry_space_group_name_Hall  '-P 2yn'
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;
2019-01-26 deposited with the CCDC.    2019-07-22 downloaded from the CCDC.
;
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CrysAlisPro, Agilent Technologies,
Version 1.171.35.21 (release 20-01-2012 CrysAlis171 .NET)
(compiled Jan 23 2012,18:06:46)
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CrysAlisPro, Agilent Technologies,
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(compiled Jan 23 2012,18:06:46)
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CrysAlisPro, Agilent Technologies,
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_diffrn_reflns_point_group_measured_fraction_full 0.997
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CrysAlisPro, Agilent Technologies,
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Analytical numeric absorption correction using a multifaceted crystal
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(Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897)
;
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.338
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
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_exptl_crystal_size_max          0.34
_exptl_crystal_size_mid          0.15
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_refine_diff_density_max         0.662
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_refine_ls_number_reflns         5094
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0352P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0706
_refine_ls_wR_factor_ref         0.0748
_reflns_Friedel_coverage         0.000
_reflns_number_gt                4508
_reflns_number_total             5094
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c9nj02469g2.cif
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'Adding full bibliography for 7058632--7058635.cif.'
_cod_database_code               7058632
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