A New Decaoxidooctaborate(2-) Anion, [B8O10(OH)6](2-): Synthesis and Characterization of [Co(en)3][B5O6(OH)4][B8O10(OH)6)]·5H2O (en = 1,2-Diaminoethane).
Altahan, Mohammed A.; Beckett, Michael A.; Coles, Simon J.; Horton, Peter N.; Inorganic chemistry 54 (2015) 412–414; doi:10.1021/ic5027834

data_4342008
_publ_section_title
;
 A New Decaoxidooctaborate(2-) Anion, [B8O10(OH)6](2-): Synthesis and
 Characterization of [Co(en)3][B5O6(OH)4][B8O10(OH)6)]&#x00B7;5H2O (en =
 1,2-Diaminoethane).
;
_journal_issue                   2
_journal_name_full               'Inorganic chemistry'
_journal_page_first              412
_journal_page_last               414
_journal_paper_doi               10.1021/ic5027834
_journal_volume                  54
_journal_year                    2015
_chemical_formula_moiety
'3(C2 H8 N2), Co, B8 H6 O16, B5 H4 O10, 5(H2 O)'
_chemical_formula_sum            'C6 H44 B13 Co N6 O31'
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Rigaku CrystalClear-SM Expert 3.1 b27
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Rigaku CrystalClear-SM Expert 3.1 b27
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Rigaku CrystalClear-SM Expert 3.1 b27
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_diffrn_ambient_temperature      100(2)
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Rigaku CrystalClear-SM Expert 3.1 b27
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_exptl_crystal_colour            Orange
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_exptl_crystal_size_max          0.050
_exptl_crystal_size_mid          0.050
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0629P)^2^+1.5958P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1182
_refine_ls_wR_factor_ref         0.1280
_reflns_Friedel_coverage         0.000
_reflns_number_gt                6226
_reflns_number_total             7900
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            ic5027834_si_001.cif
_cod_data_source_block           shelx
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/home/saulius/struct/COD-crude-data--automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2935 2014-11-11 08:27:57Z andrius 

 Adding full bibliography for 4342008.cif.
;
_cod_database_code               4342008
_shelx_estimated_absorpt_t_min   0.970
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_shelxl_version_number           2013-4
_shelx_res_checksum              35325
_shelx_hkl_checksum              83308