Stabilization and Extraction of Fluoride Anion Using a Tetralactam Receptor.
Liu, Wenqi; Oliver, Allen G.; Smith, Bradley D.; The Journal of organic chemistry 84 (2019) 4050–4057; doi:10.1021/acs.joc.9b00042

data_4034287
_publ_section_title
;
 Stabilization and Extraction of Fluoride Anion Using a Tetralactam
 Receptor.
;
_journal_issue                   7
_journal_name_full               'The Journal of organic chemistry'
_journal_page_first              4050
_journal_page_last               4057
_journal_paper_doi               10.1021/acs.joc.9b00042
_journal_volume                  84
_journal_year                    2019
_chemical_formula_moiety         'C36 H36 N4 O4, C2 H6 O S'
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_diffrn_measurement_device_type  'Bruker Kappa X8-APEX-II'
_diffrn_measurement_method       'combination of \w and \f-scans '
_diffrn_radiation_monochromator  graphite
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_refine_ls_number_reflns         7765
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_refine_ls_R_factor_all          0.0730
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0471P)^2^+0.7200P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_total             7765
_reflns_threshold_expression     'I > 2\s(I)'
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_shelx_shelxl_version_number     2014/7
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_shelx_estimated_absorpt_t_max   0.991
_shelx_res_checksum              11023
_shelx_hkl_checksum              66225