Lead(IV) acetate: intriguing reactivity profile
Khan, Faiz Ahmed; Sudheer, Ch.; Soma, Laxminarayana; Chemical Communications (Cambridge, United Kingdom)  (2007) 4239–4241; doi:10.1039/b708268a

data_7113227
_publ_section_title
;
 Lead(IV) acetate: intriguing reactivity profile
;
_journal_coden_ASTM              CHCOFS
_journal_issue                   41
_journal_name_full
;
 Chemical Communications (Cambridge, United Kingdom)
;
_journal_page_first              4239
_journal_page_last               4241
_journal_paper_doi               10.1039/b708268a
_journal_year                    2007
_chemical_formula_moiety         'C15 H22 Cl2 O6'
_chemical_formula_sum            'C15 H22 Cl2 O6'
_chemical_formula_weight         369.23
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_cell_measurement_reflns_used    7082
_cell_measurement_temperature    100(2)
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_computing_cell_refinement       'SAINT 6.45 (Bruker, 2003)'
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_computing_data_reduction        'SAINT 6.45 (Bruker, 2003)'
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_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'CCD area Detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
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_diffrn_radiation_type           MoK\a
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_diffrn_reflns_limit_l_min       -8
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_diffrn_reflns_theta_max         28.35
_diffrn_reflns_theta_min         2.05
_diffrn_standards_decay_%        0.5
_diffrn_standards_interval_time  60
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.422
_exptl_absorpt_correction_T_max  0.9739
_exptl_absorpt_correction_T_min  0.9602
_exptl_absorpt_correction_type   empirical
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_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.491
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
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_refine_ls_R_factor_all          0.0664
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0893P)^2^+45.6370P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1242
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_reflns_number_gt                3504
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_reflns_threshold_expression     >2sigma(I)
_cod_duplicate_entry             7102222
_cod_data_source_file            b708268a.txt
_cod_data_source_block           compound_13c
_cod_depositor_comments
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The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Trigonal' changed to 'trigonal'
according to
/usr/data/users/saulius/automatic-downloads/retrospective/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 
;
_cod_original_cell_volume        7404.0(9)
_cod_original_sg_symbol_H-M      R-3
_cod_database_code               7113227