Heptaphosphide cluster anions bearing group 14 element amide functionalities.
Quintero, Gabriela Espinoza; Paterson-Taylor, Isabelle; Rees, Nicholas H.; Goicoechea, Jose M.; Dalton transactions (Cambridge, England : 2003) 45 (2016) 1930–1936; doi:10.1039/c5dt02380g

data_7035823
_publ_section_title
;
 Heptaphosphide cluster anions bearing group 14 element amide
 functionalities.
;
_journal_issue                   5
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1930
_journal_page_last               1936
_journal_paper_doi               10.1039/c5dt02380g
_journal_volume                  45
_journal_year                    2016
_chemical_formula_moiety
'2(C12 H24 K O6), C6 H18 N P7 Si2 Sn, 2(C5 H5 N)'
_chemical_formula_sum            'C40 H76 K2 N3 O12 P7 Si2 Sn'
_chemical_formula_weight         1260.89
_chemical_name_systematic
;
 [K(18-crown-6)]2[P7Sn{N(SiMe3)2}]*2py
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014
_audit_update_record
;
2015-06-23 deposited with the CCDC.
2015-07-17 downloaded from the CCDC.
;
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_computing_cell_refinement
;
KappaCCD software "DENZO" (Otwinowski & Minor, 1996)
;
_computing_data_collection
;
KappaCCD software "Collect" (Nonius, 2000)
;
_computing_data_reduction
;
KappaCCD software "DENZO" (Otwinowski & Minor, 1996)
;
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_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.991
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'Nonius KappaCCD'
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0615P)^2^+4.8420P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7035822--7035823.cif.'
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