Synthetic studies toward the haouamines.
Grundl, Marc A.; Trauner, Dirk; Organic letters 8 (2006) 23–25; doi:10.1021/ol052262h

data_1505809
_publ_section_title
;
 Synthetic studies toward the haouamines.
;
_journal_issue                   1
_journal_name_full               'Organic letters'
_journal_page_first              23
_journal_page_last               25
_journal_paper_doi               10.1021/ol052262h
_journal_volume                  8
_journal_year                    2006
_chemical_formula_moiety         'C19 H20 I N O5 '
_chemical_formula_sum            'C19 H20 I N O5'
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_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_audit_creation_date             'Mon Jun 13 14:16:36 2005'
_audit_creation_method           'by teXsan'
_cell_angle_alpha                90
_cell_angle_beta                 92.995(3)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   7.981(1)
_cell_length_b                   22.703(4)
_cell_length_c                   11.227(2)
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_cell_measurement_temperature    163.2
_cell_measurement_theta_max      22.5
_cell_measurement_theta_min      2.5
_cell_volume                     2031.5(6)
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_computing_data_collection       'Bruker-AXS SMART v5.631'
_computing_data_reduction        'Bruker-AXS SAINT v6.40'
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_diffrn_measured_fraction_theta_max 0.9868
_diffrn_measurement_device_type  'Bruker APEX'
_diffrn_measurement_method       \w-scans
_diffrn_radiation_type           'Mo K\a'
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_exptl_absorpt_process_details   'Blessing, 1995'
_exptl_crystal_colour            colorless
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_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       blocklike
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_exptl_crystal_size_mid          0.070
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[\s^2^(Fo) + 0.00022|Fo|^2^]'
_refine_ls_weighting_scheme      calc
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