(<i>E</i>)-<i>N</i>'-[1-(2-Hydroxyphenyl)ethylidene]-3-methoxybenzohydrazide
Li, Cong-Ming; Ban, Hong-Yan; Acta Crystallographica Section E 65 (2009) o876–; doi:10.1107/S1600536809010228

data_2221308
_publ_section_title
;
 (<i>E</i>)-<i>N</i>'-[1-(2-Hydroxyphenyl)ethylidene]-3-methoxybenzohydrazide
;
_journal_coeditor_code           BX2198
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o876
_journal_paper_doi               10.1107/S1600536809010228
_journal_volume                  65
_journal_year                    2009
_chemical_formula_iupac          'C16 H16 N2 O3'
_chemical_formula_moiety         'C16 H16 N2 O3'
_chemical_formula_sum            'C16 H16 N2 O3'
_chemical_formula_weight         284.31
_chemical_name_systematic
;
(<i>E</i>)-<i>N</i>'-[1-(2-Hydroxyphenyl)ethylidene]-3-methoxybenzohydrazide
;
_space_group_IT_number           61
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_cell_length_c                   25.784(3)
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_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      24.6
_cell_measurement_theta_min      2.3
_cell_volume                     2919.6(9)
_computing_cell_refinement       'SAINT (Bruker, 1998)'
_computing_data_collection       'SMART (Bruker, 1998)'
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_computing_molecular_graphics    'SHELXTL (Sheldrick, 2008)'
_computing_publication_material  'SHELXTL (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker SMART CCD area-detector'
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_diffrn_reflns_theta_max         27.00
_diffrn_reflns_theta_min         1.58
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_exptl_absorpt_correction_T_min  0.9759
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_exptl_absorpt_process_details   '(SADABS; Sheldrick, 1996)'
_exptl_crystal_colour            colourless
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_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0537P)^2^+0.9645P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_database_code               2221308
_cod_database_fobs_code          2221308