Volatility and High Thermal Stability in Mid- to Late-First-Row Transition-Metal Diazadienyl Complexes
Knisley, Thomas J.; Saly, Mark J.; Heeg, Mary Jane; Roberts, John L.; Winter, Charles H.; Organometallics 30 (2011) 5010–; doi:10.1021/om200626w

data_4065213
_publ_section_title
;
 Volatility and High Thermal Stability in Mid- to Late-First-Row
 Transition-Metal Diazadienyl Complexes
;
_journal_issue                   18
_journal_name_full               Organometallics
_journal_page_first              5010
_journal_paper_doi               10.1021/om200626w
_journal_volume                  30
_journal_year                    2011
_chemical_formula_sum            'C20 H40 Cr N4'
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_chemical_name_systematic
; 
 ? 
;
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_cell_length_b                   14.0988(13)
_cell_length_c                   14.4001(14)
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_computing_molecular_graphics    SHELXTL-Plus
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_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.968
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_diffrn_measurement_method       'Bruker APEX2'
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_exptl_absorpt_coefficient_mu    0.518
_exptl_absorpt_correction_T_max  0.8728
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_exptl_absorpt_process_details   'SADABS, Sheldrick, 1997'
_exptl_crystal_colour            dark
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_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.1162P)^2^+0.3581P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_data_source_file            om200626w_si_002.cif
_cod_data_source_block           otos
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 

 Adding full bibliography for 4065213--4065216.cif.
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_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4065213