Phosphorus–nitrogen compounds: part 71. Novel unsymmetrically-substituted dispiro-cyclotriphosphazenes: synthesis, characterization, antituberculosis activity, and phototunable charge storage studies
Cemaloğlu, Reşit; Berberoğlu, İpek; Yakut, Mehtap; Binici, Arzu; Asmafiliz, Nuran; Kılıç, Zeynel; Güzel, Remziye; Erdal, Gülbahar; Şimşek, Hülya; Hökelek, Tuncer; New Journal of Chemistry 47 (2023) 19788–19800; doi:10.1039/D3NJ04099B

data_7062777
_publ_section_title
;
 Phosphorus--nitrogen compounds: part 71. Novel
 unsymmetrically-substituted dispiro-cyclotriphosphazenes: synthesis,
 characterization, antituberculosis activity, and phototunable charge
 storage studies
;
_journal_issue                   42
_journal_name_full               'New Journal of Chemistry'
_journal_page_first              19788
_journal_page_last               19800
_journal_paper_doi               10.1039/D3NJ04099B
_journal_volume                  47
_journal_year                    2023
_chemical_formula_moiety         'C26 H36 Cl2 Fe N7 P3'
_chemical_formula_sum            'C26 H36 Cl2 Fe N7 P3'
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_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
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_atom_sites_solution_hydrogens   geom
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_audit_update_record
;
2023-06-01 deposited with the CCDC.	2023-10-03 downloaded from the CCDC.
;
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'WinGX publication routines (Farrugia, 2012) and PLATON (Spek, 2009)'
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_diffrn_ambient_temperature      173(2)
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'Bruker APEX II QUAZAR three-circle diffractometer'
_diffrn_measurement_method       '\f and \w scans'
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_refine_ls_shift/su_mean         0.000
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'w=1/[\s^2^(Fo^2^)+(0.0356P)^2^+0.5605P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7062776--7062778.cif.'
_cod_original_cell_volume        1487.50(9)
_cod_database_code               7062777
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_iucr_geom_hbonds_special_details
;
Cg6 is the centroid of the (C6...C11) ring.
;
_shelx_res_checksum              33760