New Entries in Lewis Acid-Lewis Base Bifunctional Asymmetric Catalyst: Catalytic Enantioselective Reissert Reaction of Pyridine Derivatives
Eiko Ichikawa; Masato Suzuki; Kazuo Yabu; Matthias Albert; Motomu Kanai; Masakatsu Shibasaki; Journal of the American Chemical Society 126 (2004) 11808–11809; doi:10.1021/ja045966f

data_4112958
_publ_section_title
;
 New Entries in Lewis Acid-Lewis Base Bifunctional Asymmetric Catalyst:
 Catalytic Enantioselective Reissert Reaction of Pyridine Derivatives
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              11808
_journal_page_last               11809
_journal_paper_doi               10.1021/ja045966f
_journal_volume                  126
_journal_year                    2004
_chemical_formula_moiety         'C34 H22 O4 S2 '
_chemical_formula_sum            'C34 H22 O4 S2'
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_symmetry_cell_setting           monoclinic
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_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
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_cell_angle_gamma                90
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_cell_length_c                   11.588(3)
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_cell_measurement_temperature    296.1
_cell_measurement_theta_max      27.4
_cell_measurement_theta_min      3.1
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_computing_data_collection       PROCESS-AUTO
_computing_data_reduction        CrystalStructure
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_computing_structure_refinement  CRYSTALS
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_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
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_diffrn_reflns_theta_max         27.49
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_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colorless
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_exptl_crystal_description       block
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_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.30
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     'w = 1/[0.8540\s(Fo^2^)]/(4Fo^2^)'
_refine_ls_weighting_scheme      calc
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_cod_original_formula_sum        'C34 H22 O4 S2 '
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