Rich Coordination Chemistry of π-Acceptor Dibenzoarsole Ligands.
Gupta, Arvind Kumar; Akkarasamiyo, Sunisa; Orthaber, Andreas; Inorganic chemistry 56 (2017) 4505–4512; doi:10.1021/acs.inorgchem.7b00100

data_4345791
_publ_section_title
;
 Rich Coordination Chemistry of \p-Acceptor Dibenzoarsole Ligands.
;
_journal_issue                   8
_journal_name_full               'Inorganic chemistry'
_journal_page_first              4505
_journal_page_last               4512
_journal_paper_doi               10.1021/acs.inorgchem.7b00100
_journal_volume                  56
_journal_year                    2017
_chemical_formula_sum            'C32 H34 As2 Cl2 Pd'
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_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
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_cell_length_b                   14.8474(4)
_cell_length_c                   10.5173(3)
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_cell_measurement_theta_min      2.46
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_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
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_diffrn_reflns_av_unetI/netI     0.0249
_diffrn_reflns_Laue_measured_fraction_full 0.996
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_exptl_absorpt_coefficient_mu    3.149
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_exptl_absorpt_correction_T_min  0.5429
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            yellow-orange
_exptl_crystal_density_diffrn    1.730
_exptl_crystal_description       prism
_exptl_crystal_F_000             744
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_refine_ls_extinction_method     none
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_refine_ls_number_parameters     170
_refine_ls_number_reflns         3546
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.053
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_refine_ls_R_factor_gt           0.0186
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0160P)^2^+0.9245P] where P=(Fo^2^+2Fc^2^)/3'
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