A Tripodal Benzylene-Linked Trisamidophosphine Ligand Scaffold: Synthesis and Coordination Chemistry with Group(IV) Metals.
Batke, Sonja; Sietzen, Malte; Wadepohl, Hubert; Ballmann, Joachim; Inorganic chemistry 53 (2014) 4144–4153; doi:10.1021/ic500163c

data_4338072
_publ_section_title
;
 A Tripodal Benzylene-Linked Trisamidophosphine Ligand Scaffold: Synthesis
 and Coordination Chemistry with Group(IV) Metals.
;
_journal_issue                   8
_journal_name_full               'Inorganic chemistry'
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_journal_page_last               4153
_journal_paper_doi               10.1021/ic500163c
_journal_volume                  53
_journal_year                    2014
_chemical_formula_sum            'C30 H48 N3 P Si3'
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CrysAlisPro, Agilent Technologies,
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omega____ theta____ kappa____ phi______ frames
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  2 omega  -88.00    2.00   0.5000   25.0000
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  3 omega  -35.00   58.00   0.5000   25.0000
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  5 omega    6.00   79.00   0.5000   25.0000
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  6 omega  -40.00   57.00   0.5000   25.0000
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  7 omega    1.00   69.00   0.5000   25.0000
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  8 omega    0.00   95.00   0.5000   25.0000
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  9 omega  -39.00   53.00   0.5000   25.0000
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 10 omega  -38.00   55.00   0.5000   25.0000
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 11 omega  -41.00   50.00   0.5000   25.0000
omega____ theta____ kappa____ phi______ frames
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 12 omega  -97.00   -6.00   0.5000   25.0000
omega____ theta____ kappa____ phi______ frames
    -      -28.0026  -57.0000   60.0000 182

 13 omega  -99.00    4.00   0.5000   25.0000
omega____ theta____ kappa____ phi______ frames
    -      -28.0026  -77.0000  -60.0000 206

 14 omega  -41.00   50.00   0.5000   25.0000
omega____ theta____ kappa____ phi______ frames
    -       28.0026  -57.0000  -90.0000 182

 15 omega    1.00   26.00   0.5000   25.0000
omega____ theta____ kappa____ phi______ frames
    -       28.0026   38.0000   60.0000 50

 16 omega  -43.00   60.00   0.5000   25.0000
omega____ theta____ kappa____ phi______ frames
    -       28.0026  -77.0000   60.0000 206

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CrysAlisPro, Agilent Technologies,
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Analytical numeric absorption correction using a multifaceted crystal
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 w=1/[\s^2^(Fo^2^)+(0.0402P)^2^+1.6709P]
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