Ultrabright and Fluorogenic Probes for Multicolor Imaging and Tracking of Lipid Droplets in Cells and Tissues.
Collot, Mayeul; Fam, Tkhe Kyong; Ashokkumar, Pichandi; Faklaris, Orestis; Galli, Thierry; Danglot, Lydia; Klymchenko, Andrey S.; Journal of the American Chemical Society 140 (2018) 5401–5411; doi:10.1021/jacs.7b12817

data_4131909
_publ_section_title
;
 Ultrabright and Fluorogenic Probes for Multicolor Imaging and Tracking of
 Lipid Droplets in Cells and Tissues.
;
_journal_issue                   16
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              5401
_journal_page_last               5411
_journal_paper_doi               10.1021/jacs.7b12817
_journal_volume                  140
_journal_year                    2018
_chemical_formula_moiety         'C39 H46 B F2 N3 O4'
_chemical_formula_sum            'C39 H46 B F2 N3 O4'
_chemical_formula_weight         669.60
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_space_group_name_H-M_alt        'P 1 21/c 1'
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_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2013
_cell_angle_alpha                90
_cell_angle_beta                 101.322(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   15.6805(11)
_cell_length_b                   10.4626(7)
_cell_length_c                   21.9659(15)
_cell_measurement_reflns_used    9962
_cell_measurement_temperature    173(2)
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_cell_measurement_theta_min      2.44
_cell_volume                     3533.6(4)
_computing_cell_refinement       'Bruker SAINT'
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_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.996
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_diffrn_measurement_method       '\f and \w scans'
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_diffrn_reflns_point_group_measured_fraction_max 0.996
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_diffrn_reflns_theta_max         28.073
_diffrn_reflns_theta_min         1.324
_diffrn_source                   'fine focus sealed tube'
_exptl_absorpt_coefficient_mu    0.088
_exptl_absorpt_correction_T_max  0.7456
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_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            green
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_refine_ls_extinction_method     none
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_refine_ls_number_reflns         8549
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.038
_refine_ls_R_factor_all          0.1126
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_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0965P)^2^+2.9170P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_total             8549
_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           ymmc161130
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4131909
_shelx_estimated_absorpt_t_min   0.972
_shelx_estimated_absorpt_t_max   0.987
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_shelx_res_checksum              36882
_shelx_hkl_checksum              26639