2D 4.82 Network with threefold parallel interpenetration from nanometer-sized tripodal ligand and lead(ii) nitrateElectronic supplementary information available: Fig. 1S. See http://www.rsc.org/suppdata/cc/b2/b207568g/
Wan, Shuang-Yi; Fan, Jian; Okamura, Taka-aki; Zhu, Hui-Fang; Ouyang, Xing-Mei; Sun, Wei-Yin; Ueyama, Norikazu; Chemical Communications  (2002) 2520–; doi:10.1039/b207568g

data_7111254
_publ_section_title
;
 2D 4.82 Network with threefold parallel interpenetration from
 nanometer-sized tripodal ligand and lead(ii) nitrateElectronic
 supplementary information available: Fig. 1S. See
 http://www.rsc.org/suppdata/cc/b2/b207568g/
;
_journal_issue                   21
_journal_name_full               'Chemical Communications'
_journal_page_first              2520
_journal_paper_doi               10.1039/b207568g
_journal_year                    2002
_chemical_formula_moiety         'C34.67 H31.50 N11 O6.58 Pb '
_chemical_formula_sum            'C34.67 H31.5 N11 O6.58 Pb'
_chemical_formula_weight         914.73
_chemical_name_systematic
; 
[Pb(timpt)(NO3)](NO3)-0.417(Et2O)-0.167(H2O) 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             'Sat Sep  7 18:45:43 2002'
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 116.0144(11)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   33.6859(7)
_cell_length_b                   7.7447(2)
_cell_length_c                   30.8578(10)
_cell_measurement_reflns_used    21554
_cell_measurement_temperature    200
_cell_measurement_theta_max      27.4
_cell_measurement_theta_min      1.3
_cell_volume                     7234.8(3)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SIR92 (Altomare, 1994)'
_diffrn_ambient_temperature      200
_diffrn_detector_area_resol_mean 10.00
_diffrn_measured_fraction_theta_full 0.979
_diffrn_measured_fraction_theta_max 0.979
_diffrn_measurement_device_type  'Rigaku RAXIS-RAPID Imaging Plate'
_diffrn_measurement_method       \w
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.1331
_diffrn_reflns_av_sigmaI/netI    0.1731
_diffrn_reflns_limit_h_max       43
_diffrn_reflns_limit_h_min       -43
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       40
_diffrn_reflns_limit_l_min       -40
_diffrn_reflns_number            28746
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         2.39
_exptl_absorpt_coefficient_mu    4.727
_exptl_absorpt_correction_T_max  0.910
_exptl_absorpt_correction_T_min  0.637
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(Higashi, 1995)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.680
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             3609
_exptl_crystal_size_max          0.300
_exptl_crystal_size_mid          0.020
_exptl_crystal_size_min          0.02
_refine_diff_density_max         1.018
_refine_diff_density_min         -1.067
_refine_diff_density_rms         0.146
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.887
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     488
_refine_ls_number_reflns         8120
_refine_ls_number_restraints     3
_refine_ls_restrained_S_all      0.889
_refine_ls_R_factor_all          0.1504
_refine_ls_R_factor_gt           0.0558
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0351P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0871
_refine_ls_wR_factor_ref         0.1027
_reflns_number_gt                3918
_reflns_number_total             8120
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b207568gsup1.cif
_cod_data_source_block           shelxl
_cod_original_formula_sum        'C34.67 H31.50 N11 O6.58 Pb'
_cod_database_code               7111254