Sequential one-pot combination of multireactions through multicatalysis: a general approach to rapid assembly of functionalized push-pull olefins, phenols, and 2-methyl-2H-chromenes.
Ramachary, Dhevalapally B.; Ramakumar, Kinthada; Bharanishashank, Adluri; Narayana, Vidadala V.; Journal of combinatorial chemistry 12 (2010) 855–876; doi:10.1021/cc100104k

data_1502631
_publ_section_title
;
 Sequential one-pot combination of multireactions through multicatalysis:
 a general approach to rapid assembly of functionalized push-pull olefins,
 phenols, and 2-methyl-2H-chromenes.
;
_journal_issue                   6
_journal_name_full               'Journal of combinatorial chemistry'
_journal_page_first              855
_journal_page_last               876
_journal_paper_doi               10.1021/cc100104k
_journal_volume                  12
_journal_year                    2010
_chemical_formula_sum            'C19 H19 N O5'
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_chemical_name_systematic
; 
 ? 
;
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_atom_sites_solution_hydrogens   geom
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_atom_sites_solution_secondary   difmap
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_cell_formula_units_Z            2
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_cell_measurement_temperature    298(2)
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_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
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_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.986
_diffrn_measured_fraction_theta_max 0.986
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_diffrn_radiation_monochromator  graphite
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_exptl_absorpt_correction_T_min  0.9733
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    1.337
_exptl_crystal_density_method    'not measured'
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0706P)^2^+0.6742P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1894
_refine_ls_wR_factor_ref         0.2121
_reflns_number_gt                2113
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_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cc100104k_si_006.cif
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_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        848.2(5)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               1502631