Mechanism of Reversible Alkyne Coupling at Zirconocene: Ancillary Ligand Effects
Adam D. Miller; Jennifer L. McBee; T. Don Tilley; Journal of the American Chemical Society 130 (2008) 4992–4999; doi:10.1021/ja800025u

data_4107671
_publ_section_title
;
 Mechanism of Reversible Alkyne Coupling at Zirconocene: Ancillary Ligand
 Effects
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              4992
_journal_page_last               4999
_journal_paper_doi               10.1021/ja800025u
_journal_volume                  130
_journal_year                    2008
_chemical_formula_moiety         'C37 H48 Si2 Zr'
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_chemical_name_systematic
; 
 ? 
;
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_cell_volume                     1708.4(3)
_computing_cell_refinement       'Bruker SMART'
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_diffrn_measurement_device_type  'Bruker P4'
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_diffrn_reflns_theta_min         3.53
_diffrn_standards_decay_%        0
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_refine_ls_R_factor_all          0.0443
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_refine_ls_shift/su_max          0.031
_refine_ls_shift/su_mean         0.005
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0560P)^2^+1.0017P] where P=(Fo^2^+2Fc^2^)/3'
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