[<i>N</i>,<i>N</i>'-Bis(2-aminoethyl-κ<i>N</i>)-<i>N</i>,<i>N</i>'-bis(2-ammonioethyl)ethylenediamine-κ^2^<i>N</i>,<i>N</i>']platinum(II) Bis(tetrachloroplatinate) Trihydrate
Sakai, K.; Tanaka, Y.; Tsubomura, T.; Acta Crystallographica Section C 52 (1996) 541–543; doi:10.1107/S0108270195011413

data_2004664
_publ_section_title
;[<i>N</i>,<i>N</i>'-Bis(2-aminoethyl-\k<i>N</i>)-<i>N</i>,<i>N</i>'-bis(2-ammonioethyl)ethylenediamine-\k^2^<i>N</i>,<i>N</i>']platinum(II)
 Bis(tetrachloroplatinate) Trihydrate
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              541
_journal_page_last               543
_journal_paper_doi               10.1107/S0108270195011413
_journal_volume                  52
_journal_year                    1996
_chemical_formula_iupac          '[Pt (C10 H30 N6)][Pt Cl4]2, 3H2 O1'
_chemical_formula_moiety         'C10 H30 N6 Pt 4+, (Cl4 Pt 2-)2, 3(H2 O)'
_chemical_formula_structural     '(Pt (C10 H30 N6)) (Pt Cl4)2 3(H2 O)'
_chemical_formula_sum            'C10 H36 Cl8 N6 O3 Pt3'
_chemical_formula_weight         1157.33
_chemical_name_systematic
;
N,N'-bis(2-aminoethyl)-N,N'-bis(2-ammonioethyl)ethylenediamineplatinum(II)
bis(tetrachloroplatinate) trihydrate
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 97.030(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   12.141(2)
_cell_length_b                   12.0100(10)
_cell_length_c                   19.248(2)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    296.0
_cell_measurement_theta_max      23.18
_cell_measurement_theta_min      20.13
_cell_volume                     2785.5(6)
_computing_cell_refinement       'MSC/AFC Diffractometer Control Software'
_computing_data_collection
;
MSC/AFC Diffractometer Control Software
(Molecular Structure Corporation, 1988)
;
_computing_data_reduction
'TEXSAN PRECESS (Molecular Structure Corporation, 1993)'
_computing_publication_material  'TEXSAN FINISH'
_computing_structure_refinement  'TEXSAN LS'
_computing_structure_solution    'SAPI90 (Fan, 1990)'
_diffrn_ambient_temperature      296.0
_diffrn_measurement_device       'Rigaku AFC5S'
_diffrn_measurement_method       \q/2\q
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'X-ray tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.1338
_diffrn_reflns_av_sigmaI/netI    0.2381
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            5437
_diffrn_reflns_theta_max         25
_diffrn_reflns_theta_min         1.69
_diffrn_standards_decay_%        0.29
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    15.821
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.348
_exptl_absorpt_correction_type   'empirical via \y scan'
_exptl_absorpt_process_details   psi-scan
_exptl_crystal_colour            reddish-brown
_exptl_crystal_density_diffrn    2.760
_exptl_crystal_description       plate
_exptl_crystal_F_000             2128
_exptl_crystal_size_max          0.43
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.05
_refine_diff_density_max         2.23
_refine_diff_density_min         -2.79
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_obs   1.51
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_constraints    0
_refine_ls_number_parameters     192
_refine_ls_number_reflns         1826
_refine_ls_number_restraints     0
_refine_ls_R_factor_obs          0.0669
_refine_ls_shift/esd_max         0.5670
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme
'sigma, w = 1/\s^2^(F); \s(F) from counting statistics'
_refine_ls_wR_factor_obs         0.0443
_reflns_number_observed          1826
_reflns_number_total             5179
_reflns_observed_criterion       I>3.0\s(I)
_cod_data_source_file            ta1044.cif
_cod_data_source_block           ta1044
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C10 Cl8 H36 N6 O3 Pt3'
_cod_database_code               2004664