Tetranuclear silver(i) clusters showing high ionic conductivity in a bicontinuous cubic mesophase.
Su, Padi Y. S.; Tseng, Jing C. W.; Lee, Kwang-Ming; Wang, Ju-Chun; Lin, Ivan J. B.; Inorganic chemistry 53 (2014) 5902–5910; doi:10.1021/ic500627d

data_4338710
_publ_section_title
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 Tetranuclear silver(i) clusters showing high ionic conductivity in a
 bicontinuous cubic mesophase.
;
_journal_issue                   12
_journal_name_full               'Inorganic chemistry'
_journal_page_first              5902
_journal_page_last               5910
_journal_paper_doi               10.1021/ic500627d
_journal_volume                  53
_journal_year                    2014
_chemical_formula_sum            'C96 H186 Ag4 B4 F16 N18'
_chemical_formula_weight         2371.35
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_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 93.782(5)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   25.605(4)
_cell_length_b                   15.317(3)
_cell_length_c                   15.290(3)
_cell_measurement_temperature    273(2)
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_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      273(2)
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measurement_device_type  'CCC area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
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_diffrn_reflns_limit_h_min       -34
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            96348
_diffrn_reflns_theta_full        29.04
_diffrn_reflns_theta_max         29.04
_diffrn_reflns_theta_min         1.55
_exptl_absorpt_coefficient_mu    0.717
_exptl_absorpt_correction_T_max  0.7458
_exptl_absorpt_correction_T_min  0.5891
_exptl_absorpt_correction_type   multi-scan
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.316
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             2480
_exptl_crystal_size_max          0.40
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_refine_diff_density_max         0.518
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_refine_ls_extinction_method     none
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_refine_ls_R_factor_all          0.1063
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_refine_ls_shift/su_max          0.021
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0550P)^2^+0.8797P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1065
_refine_ls_wR_factor_ref         0.1308
_reflns_number_gt                7765
_reflns_number_total             15798
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ic500627d_si_001.cif
_cod_data_source_block           CCDC942251
_cod_depositor_comments
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The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to
/usr/data/users/saulius/crontab/automatic-downloads/rss-feeds/ACS/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 2281 2013-09-26 08:29:07Z andrius 

 Adding full bibliography for 4338710.cif.
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_cod_original_cell_volume        5983.5(17)
_cod_original_sg_symbol_H-M      'P2(1)/c  '
_cod_database_code               4338710