Total synthesis and structural revision of (±)-nidemone.
Hsu, Day-Shin; Liou, Chang-Yan; Organic & biomolecular chemistry 16 (2018) 4990–4995; doi:10.1039/c8ob01207e

data_7156289
_publ_section_title
;
 Total synthesis and structural revision of (+-)-nidemone.
;
_journal_issue                   27
_journal_name_full               'Organic &amp; biomolecular chemistry'
_journal_page_first              4990
_journal_page_last               4995
_journal_paper_doi               10.1039/c8ob01207e
_journal_volume                  16
_journal_year                    2018
_chemical_formula_moiety         'C15 H14 O4'
_chemical_formula_sum            'C14 H14 O4'
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_space_group_name_H-M_alt        'P b c a'
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_audit_update_record
;
2018-06-13 deposited with the CCDC.
2018-06-19 downloaded from the CCDC.
;
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_cell_volume                     2423.6(8)
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
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_diffrn_measurement_device_type  'Bruker Smart Apex'
_diffrn_measurement_method       'phi-omega scan'
_diffrn_radiation_type           MoK\a
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0790P)^2^+0.6314P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1168
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c8ob01207e2.cif
_cod_data_source_block           LCY14
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Empirical' changed to
'empirical' according to
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 4973 2017-02-22 13:04:09Z antanas 

 Adding full bibliography for 7156289.cif.
;
_cod_original_cell_volume        2423.6(9)
_cod_database_code               7156289
_shelx_shelxl_version_number     2014/7
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