Synthesis and reactivity of N,N'-1,4-diazabutadiene derived borocations.
Lawson, James R.; Wilkins, Lewis C.; André, Manon; Richards, Emma C.; Ali, Mohammed N.; Platts, James A.; Melen, Rebecca L.; Dalton transactions (Cambridge, England : 2003) 45 (2016) 16177–16181; doi:10.1039/c6dt03360a

data_7040765
_publ_section_title
;
 Synthesis and reactivity of N,N'-1,4-diazabutadiene derived borocations.
;
_journal_issue                   41
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              16177
_journal_page_last               16181
_journal_paper_doi               10.1039/c6dt03360a
_journal_volume                  45
_journal_year                    2016
_chemical_formula_moiety         'C28 H33 Al B Cl5 N2'
_chemical_formula_sum            'C28 H33 Al B Cl5 N2'
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_chemical_name_systematic
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 ?
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2016-08-14 deposited with the CCDC.
2016-09-28 downloaded from the CCDC.
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.35g (release 09-12-2014 CrysAlis171 .NET)
(compiled Dec  9 2014,15:38:47)
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.35g (release 09-12-2014 CrysAlis171 .NET)
(compiled Dec  9 2014,15:38:47)
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.35g (release 09-12-2014 CrysAlis171 .NET)
(compiled Dec  9 2014,15:38:47)
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'Agilent Supernova Dual Atlas with CCD detector'
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CrysAlisPro, Agilent Technologies,
Version 1.171.37.35g (release 09-12-2014 CrysAlis171 .NET)
(compiled Dec  9 2014,15:38:47)
Numerical absorption correction based on gaussian integration over
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Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm. 
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_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.316
_exptl_crystal_description       block
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_refine_ls_restrained_S_all      1.006
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_refine_ls_R_factor_gt           0.0451
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0436P)^2^+1.2962P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_gt                5744
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c6dt03360a2.cif
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_cod_depositor_comments
'Adding full bibliography for 7040765--7040767.cif.'
_cod_database_code               7040765
_shelx_estimated_absorpt_t_min   0.838
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_shelxl_version_number           2013-3
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