Facile Buchwald-Hartwig coupling of sterically encumbered substrates effected by PNP ligands.
Kathewad, Neha; M C, Anagha; Parvin, Nasrina; Parambath, Sneha; Parameswaran, Pattiyil; Khan, Shabana; Dalton transactions (Cambridge, England : 2003) 48 (2019) 2730–2734; doi:10.1039/c9dt00159j

data_7048752
_publ_section_title
;
 Facile Buchwald-Hartwig coupling of sterically encumbered substrates
 effected by PNP ligands.
;
_journal_issue                   8
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2730
_journal_page_last               2734
_journal_paper_doi               10.1039/c9dt00159j
_journal_volume                  48
_journal_year                    2019
_chemical_formula_sum            'C24 H35 N'
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_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2018-10-09 deposited with the CCDC.
2019-01-24 downloaded from the CCDC.
;
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_exptl_absorpt_coefficient_mu    0.059
_exptl_crystal_colour            colorless
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_exptl_crystal_size_max          0.1
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_exptl_crystal_size_min          0.1
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     'w=1/[\s^2^(Fo^2^)] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0959
_refine_ls_wR_factor_ref         0.1004
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_reflns_number_gt                2362
_reflns_number_total             3899
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c9dt00159j2.cif
_cod_data_source_block           NVK039
_cod_depositor_comments
'Adding full bibliography for 7048750--7048752.cif.'
_cod_original_cell_volume        2149.9(12)
_cod_database_code               7048752
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