Synthesis and Characterization of Copper Complexes with Cu<sup>I</sup>Cu<sup>I</sup>, Cu<sup>1.5</sup>Cu<sup>1.5</sup>m and Cu<sup>II</sup>Cu<sup>II</sup> Core Structures Supported by a Flexible Dipyridylamide Ligand.
McMoran, Ethan P.; Powell, Douglas R.; Perez, Felio; Rowe, Gerard T.; Yang, Lei; Inorganic chemistry 55 (2016) 11462–11472; doi:10.1021/acs.inorgchem.6b02006

data_4349162
_publ_section_title
;
 Synthesis and Characterization of Copper Complexes with
 Cu<sup>I</sup>Cu<sup>I</sup>, Cu<sup>1.5</sup>Cu<sup>1.5</sup>m and
 Cu<sup>II</sup>Cu<sup>II</sup> Core Structures Supported by a Flexible
 Dipyridylamide Ligand.
;
_journal_issue                   21
_journal_name_full               'Inorganic chemistry'
_journal_page_first              11462
_journal_page_last               11472
_journal_paper_doi               10.1021/acs.inorgchem.6b02006
_journal_volume                  55
_journal_year                    2016
_chemical_formula_moiety         'C22 H16 Cl2 Cu3 N6 O2'
_chemical_formula_sum            'C22 H16 Cl2 Cu3 N6 O2'
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_diffrn_measurement_method       '\f and \w scans'
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0400P)^2^+1.9000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0621
_refine_ls_wR_factor_ref         0.0705
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            ic6b02006_si_002.cif
_cod_data_source_block           15088a
_cod_depositor_comments
;
The following automatic conversions were performed:

data name '_iucr_refine_instruction_details' was replaced with
'_iucr_refine_instructions_details' as specified in the replacement
file 'data/replacement-values/replacement_tags.lst'.

Automatic conversion script
Id: cif_correct_tags 9268 2022-04-12 08:56:07Z antanas 
;
_cod_database_code               4349162
_shelx_estimated_absorpt_t_min   0.786
_shelx_estimated_absorpt_t_max   0.833
_shelx_res_checksum              10498
_shelx_hkl_checksum              84228