Contrasting coordination behavior of Group 12 perchlorate salts with an acyclic N3O2 donor ligand by X-ray crystallography and (1)H NMR.
Tice, Daniel B.; Pike, Robert D.; Bebout, Deborah C.; Dalton transactions (Cambridge, England : 2003) 45 (2016) 12871–12883; doi:10.1039/c6dt02322c

data_7039961
_publ_section_title
;
 Contrasting coordination behavior of Group 12 perchlorate salts with an
 acyclic N3O2 donor ligand by X-ray crystallography and (1)H NMR.
;
_journal_issue                   32
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              12871
_journal_page_last               12883
_journal_paper_doi               10.1039/c6dt02322c
_journal_volume                  45
_journal_year                    2016
_chemical_formula_sum            'C38 H38 Cl4 Hg2 N6 O20'
_chemical_formula_weight         1441.72
_chemical_melting_point          476
_chemical_name_systematic
'(perchlorato-O)(perchlorato-O,O')(2,6-bis(2-pyridylmethoxymethyl)pyridine-N,N',N'',O,O') mercury(ii)'
_space_group_crystal_system      triclinic
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_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_space_group_name_Hall  '-P 1'
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_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/5
_audit_update_record
;
2016-06-10 deposited with the CCDC.
2016-07-20 downloaded from the CCDC.
;
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_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0360P)^2^+7.0131P] where P=(Fo^2^+2Fc^2^)/3'
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'Adding full bibliography for 7039959--7039962.cif.'
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_solvent_exptl_crystal_recrystallization_method acetonitrile/m-xylene