A study of di(amino)stibines with terminal Sb(iii) hydrogen-ligands by X-ray- and neutron-diffraction.
Schwamm, Ryan J.; Edwards, Alison J.; Fitchett, Christopher M.; Coles, Martyn P.; Dalton transactions (Cambridge, England : 2003) 48 (2019) 2953–2958; doi:10.1039/c8dt05113e

data_7048827
_publ_section_title
;
 A study of di(amino)stibines with terminal Sb(iii) hydrogen-ligands by
 X-ray- and neutron-diffraction.
;
_journal_issue                   9
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2953
_journal_page_last               2958
_journal_paper_doi               10.1039/c8dt05113e
_journal_volume                  48
_journal_year                    2019
_chemical_formula_moiety         '2(C28 H47 N2 O Sb Si2), C6 H14'
_chemical_formula_sum            'C62 H108 N4 O2 Sb2 Si4'
_chemical_formula_weight         1297.40
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
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2019-01-30 deposited with the CCDC.
2019-01-31 downloaded from the CCDC.
;
_cell_angle_alpha                73.916(2)
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_cell_measurement_temperature    120.01(10)
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        CrysAlisPro, Agilent Technologies,
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Numerical absorption correction based on gaussian integration over
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        Empirical absorption correction using spherical harmonics,
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_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.27
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0244P)^2^+1.5501P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_depositor_comments
'Adding full bibliography for 7048824--7048828.cif.'
_cod_database_code               7048827