N,1,4-Tri(4-alkoxy-2-hydroxybenzyl)-DAZA: efficient one-pot synthesis and labelling with <sup>68</sup>Ga for PET liver imaging in ovo.
Greiser, Julia; Kühnel, Christian; Görls, Helmar; Weigand, Wolfgang; Freesmeyer, Martin; Dalton transactions (Cambridge, England : 2003) 47 (2018) 9000–9007; doi:10.1039/c8dt01038b

data_7046638
_publ_section_title
;
 N,1,4-Tri(4-alkoxy-2-hydroxybenzyl)-DAZA: efficient one-pot synthesis and
 labelling with <sup>68</sup>Ga for PET liver imaging in ovo.
;
_journal_issue                   27
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              9000
_journal_page_last               9007
_journal_paper_doi               10.1039/c8dt01038b
_journal_volume                  47
_journal_year                    2018
_chemical_formula_moiety         'C32 H43 N3 O6'
_chemical_formula_sum            'C32 H43 N3 O6'
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_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
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_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   difmap
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_atom_sites_solution_secondary   difmap
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_audit_update_record
;
2018-01-29 deposited with the CCDC.
2018-06-12 downloaded from the CCDC.
;
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_cell_angle_gamma                79.603(1)
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_computing_publication_material  SHELXL-97
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      133(2)
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_diffrn_measured_fraction_theta_max 0.970
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_diffrn_measurement_method       'phi- + omega-scan'
_diffrn_radiation_monochromator  graphite
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_exptl_crystal_colour            colourless
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_refine_ls_R_factor_gt           0.0660
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0000P)^2^+2.0804P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_cod_depositor_comments
'Adding full bibliography for 7046637--7046639.cif.'
_cod_original_cell_volume        1481.73(6)
_cod_database_code               7046638