LMucko/crystallography-open-database huggingface dataset:
Alkyl(amino)- and Alkyl(chloro)phosphanyl-Substituted Cyclopentadienyl Complexes of Titanium and Zirconium
Kotov, V. V.; Avtomonov, E. V.; Sundermeyer, J.; Harms, K.; Lemenovskii, D. A.; European Journal of Inorganic Chemistry 2002 (2002) 678–691; doi:10.1002/1099-0682(200203)2002:3<678::AID-EJIC678>3.0.CO;2-3

data_1100267
_publ_section_title
;
 Alkyl(amino)- and Alkyl(chloro)phosphanyl-Substituted Cyclopentadienyl
 Complexes of Titanium and Zirconium
;
_journal_coden_ASTM              EJICFO
_journal_issue                   3
_journal_name_full               'European Journal of Inorganic Chemistry'
_journal_page_first              678
_journal_page_last               691
_journal_paper_doi
10.1002/1099-0682(200203)2002:3<678::AID-EJIC678>3.0.CO;2-3
_journal_volume                  2002
_journal_year                    2002
_chemical_formula_moiety         'C23 H38 N1 P1'
_chemical_formula_sum            'C23 H38 N P'
_chemical_name_systematic
;
t-Butyl(N-t-butylamino)(2,3,4,5,6,7-hexamethyl-1H-inden-1-yl)phosphane
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 91.138(10)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   7.7683(10)
_cell_length_b                   22.196(1)
_cell_length_c                   12.8267(10)
_cell_volume                     2211.210
_diffrn_ambient_temperature      223
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.08
_exptl_crystal_description       plate
_refine_ls_R_factor_gt           7.54
_refine_ls_wR_factor_gt          7.54
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C23 H38 N1 P1'
_cod_database_code               1100267
Alkyl(amino)- and Alkyl(chloro)phosphanyl-Substituted Cyclopentadienyl Complexes of Titanium and Zirconium
Kotov, V. V.; Avtomonov, E. V.; Sundermeyer, J.; Harms, K.; Lemenovskii, D. A.; European Journal of Inorganic Chemistry 2002 (2002) 678–691; doi:10.1002/1099-0682(200203)2002:3<678::AID-EJIC678>3.0.CO;2-3

data_1100268
_publ_section_title
;
 Alkyl(amino)- and Alkyl(chloro)phosphanyl-Substituted Cyclopentadienyl
 Complexes of Titanium and Zirconium
;
_journal_coden_ASTM              EJICFO
_journal_issue                   3
_journal_name_full               'European Journal of Inorganic Chemistry'
_journal_page_first              678
_journal_page_last               691
_journal_paper_doi
10.1002/1099-0682(200203)2002:3<678::AID-EJIC678>3.0.CO;2-3
_journal_volume                  2002
_journal_year                    2002
_chemical_formula_moiety         'C17 H31 Cl3 N1 P1 Ti1'
_chemical_formula_sum            'C17 H31 Cl3 N P Ti'
_chemical_name_systematic
(\h^5^-1-(t-Butyl(N,N-diethylamino)phosphanyl)-2,3,4,5-tetramethyl-cyclopentadienyl)-trichloro-titanium
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 91.387(11)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.3510(15)
_cell_length_b                   15.6371(19)
_cell_length_c                   14.7317(13)
_cell_volume                     2153.475
_diffrn_ambient_temperature      203
_exptl_crystal_colour            'dark red.'
_exptl_crystal_density_diffrn    1.341
_exptl_crystal_description       prism
_refine_ls_R_factor_gt           5.5
_refine_ls_wR_factor_gt          5.5
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C17 H31 Cl3 N1 P1 Ti1'
_cod_database_code               1100268
Crystal structure of (2PMDETA)-dilithium-1-(cyclononatetraenyl)-enolate, C~29~H~56~Li~2~N~6~O
Demyanov, P.; Marsch, M.; Harms, K.; Boche, G.; Zeitschrift für Kristallographie - New Crystal Structures 216 (2001) 423–424; doi:10.1524/ncrs.2001.216.14.445

data_1100270
_publ_section_title
;
 Crystal structure of (2PMDETA)-dilithium-1-(cyclononatetraenyl)-enolate,
 C~29~H~56~Li~2~N~6~O
;
_journal_issue                   1-4
_journal_name_full
;
 Zeitschrift f\"ur Kristallographie - New Crystal Structures
;
_journal_page_first              423
_journal_page_last               424
_journal_paper_doi               10.1524/ncrs.2001.216.14.445
_journal_volume                  216
_journal_year                    2001
_chemical_formula_moiety         'C29 H56 Li2 N6 O1'
_chemical_formula_sum            'C29 H56 Li2 N6 O'
_chemical_name_systematic
(\m~2~-\h^3^,\h^2^-1-(Cyclononatetraenyl)ethenolato)-bis(bis(2-(dimethylamino)ethyl)methylamine)-di-lithium
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 98.707(5)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.9363(4)
_cell_length_b                   22.9584(15)
_cell_length_c                   15.9613(8)
_cell_volume                     3236.931
_diffrn_ambient_temperature      193
_exptl_crystal_colour            'light yellow.'
_exptl_crystal_density_diffrn    1.064
_exptl_crystal_description       prism
_refine_ls_R_factor_gt           0.038
_refine_ls_wR_factor_gt          0.092
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_original_formula_sum        'C29 H56 Li2 N6 O1'
_cod_database_code               1100270
_cod_duplicate_entry             8101025
Crystal structure of 2-(1,3-dimethylbenzotriazolium) nickeltetrabromide, (C~8~H~10~N~3~)~2~NiBr~4~
Hassani, K.; Marsch, M.; Harms, K.; Boche, G.; Zeitschrift für Kristallographie - New Crystal Structures 216 (2001) 425–426; doi:10.1524/ncrs.2001.216.14.447

data_1100271
_publ_section_title
;
 Crystal structure of 2-(1,3-dimethylbenzotriazolium) nickeltetrabromide,
 (C~8~H~10~N~3~)~2~NiBr~4~
;
_journal_issue                   1-4
_journal_name_full
;
 Zeitschrift f\"ur Kristallographie - New Crystal Structures
;
_journal_page_first              425
_journal_page_last               426
_journal_paper_doi               10.1524/ncrs.2001.216.14.447
_journal_volume                  216
_journal_year                    2001
_chemical_formula_moiety         '2(C8 H10 N3 1+),Br4 Ni1 2-'
_chemical_formula_sum            'C16 H20 Br4 N6 Ni'
_chemical_name_systematic
;
bis(1,3-Dimethylbenzotriazolium) tetrabromo-nickel
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 103.989(5)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   13.3352(6)
_cell_length_b                   10.2840(7)
_cell_length_c                   16.6530(7)
_cell_volume                     2216.047
_diffrn_ambient_temperature      193
_exptl_crystal_colour            blue.
_exptl_crystal_density_diffrn    2.022
_exptl_crystal_description       prism
_refine_ls_R_factor_gt           2.99
_refine_ls_wR_factor_gt          2.99
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_original_formula_sum        'C16 H20 Br4 N6 Ni1'
_cod_database_code               1100271
_cod_duplicate_entry             8101026
Crystal structure of (3THF)-N-lithiium-N-(2',4',6'-tris-t-butyl-phenyl)-E'pentene(1)-amide, C~35~H~62~LiNO~3~
Bosold, F.; Marsch, M.; Harms, K.; Boche, G.; Zeitschrift für Kristallographie - New Crystal Structures 216 (2001) 427–428; doi:10.1524/ncrs.2001.216.14.449

data_1100272
_publ_section_title
;
 Crystal structure of
 (3THF)-N-lithiium-N-(2',4',6'-tris-t-butyl-phenyl)-E'pentene(1)-amide,
 C~35~H~62~LiNO~3~
;
_journal_issue                   1-4
_journal_name_full
;
 Zeitschrift f\"ur Kristallographie - New Crystal Structures
;
_journal_page_first              427
_journal_page_last               428
_journal_paper_doi               10.1524/ncrs.2001.216.14.449
_journal_volume                  216
_journal_year                    2001
_chemical_formula_moiety         'C35 H62 Li1 N1 O3'
_chemical_formula_sum            'C35 H62 Li N O3'
_chemical_name_systematic
;
(N-(2',4',6'-tris-t-butylphenyl)-E-pent-1-enamide)-tris(tetrahydrofuran)-lithium
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 95.112(8)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   9.1764(6)
_cell_length_b                   13.1644(10)
_cell_length_c                   30.036(3)
_cell_volume                     3613.971
_diffrn_ambient_temperature      213
_exptl_crystal_colour            colorless.
_exptl_crystal_density_diffrn    1.014
_exptl_crystal_description       prism
_refine_ls_R_factor_gt           7.85
_refine_ls_wR_factor_gt          7.85
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C35 H62 Li1 N1 O3'
_cod_database_code               1100272
Gallium-Gallium Single Bonds Terminally Coordinated by Tropolonato Ligands
Uhl, W.; Prott, M.; Geiseler, G.; Harms, K.; Zeitschrift für Naturforschung B 57 (2002) 141–144; doi:10.1515/znb-2002-0202

data_1100273
_publ_section_title
;
 Gallium-Gallium Single Bonds Terminally Coordinated by Tropolonato Ligands
;
_journal_issue                   2
_journal_name_full               'Zeitschrift f\"ur Naturforschung B'
_journal_page_first              141
_journal_page_last               144
_journal_paper_doi               10.1515/znb-2002-0202
_journal_volume                  57
_journal_year                    2002
_chemical_formula_moiety         'C21 H29 Ga1 O4 Si2'
_chemical_formula_sum            'C21 H29 Ga O4 Si2'
_chemical_name_systematic
;
bis(Tropolonato-O,O')-(bis(trimethylsilyl)methyl)-gallium(iii)
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                88.11(1)
_cell_angle_beta                 73.33(1)
_cell_angle_gamma                66.56(1)
_cell_formula_units_Z            2
_cell_length_a                   9.610(2)
_cell_length_b                   10.605(2)
_cell_length_c                   13.459(3)
_cell_volume                     1200.431
_diffrn_ambient_temperature      193
_exptl_crystal_density_diffrn    1.304
_refine_ls_R_factor_gt           8.37
_refine_ls_wR_factor_gt          8.37
_cod_original_formula_sum        'C21 H29 Ga1 O4 Si2'
_cod_database_code               1100273
Gallium-Gallium Single Bonds Terminally Coordinated by Tropolonato Ligands
Uhl, W.; Prott, M.; Geiseler, G.; Harms, K.; Zeitschrift für Naturforschung B 57 (2002) 141–144; doi:10.1515/znb-2002-0202

data_1100274
_publ_section_title
;
 Gallium-Gallium Single Bonds Terminally Coordinated by Tropolonato Ligands
;
_journal_issue                   2
_journal_name_full               'Zeitschrift f\"ur Naturforschung B'
_journal_page_first              141
_journal_page_last               144
_journal_paper_doi               10.1515/znb-2002-0202
_journal_volume                  57
_journal_year                    2002
_chemical_formula_moiety         'C28 H48 Ga2 O4 Si4'
_chemical_formula_sum            'C28 H48 Ga2 O4 Si4'
_chemical_melting_point          396.15
_chemical_name_systematic
;
1,2-bis(bis(Trimethylsilyl)methyl)-1,2-bis(tropolonato)-di-gallium
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 111.47(2)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   10.242(4)
_cell_length_b                   13.280(1)
_cell_length_c                   13.844(4)
_cell_volume                     1752.314
_diffrn_ambient_temperature      293
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.328
_exptl_crystal_preparation       pentane
_refine_ls_R_factor_gt           5.74
_refine_ls_wR_factor_gt          5.74
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               1100274
Diels-alder reactions of malondialdehyde derivatives with reversed electron demand; an easy approach to structurally unique carbohydrates and compounds of the thromboxane type
Tietze, Lutz-F.; Glüsenkamp, Karl-Heinz; Harms, Klaus; Remberg, Gert; Sheldrick, George M.; Tetrahedron Letters 23 (1982) 1147–1150; doi:10.1016/S0040-4039(00)87045-8

data_1100275
_publ_section_title
;
 Diels-alder reactions of malondialdehyde derivatives with reversed
 electron demand; an easy approach to structurally unique carbohydrates
 and compounds of the thromboxane type
;
_journal_coden_ASTM              TELEAY
_journal_issue                   11
_journal_name_full               'Tetrahedron Letters'
_journal_page_first              1147
_journal_page_last               1150
_journal_paper_doi               10.1016/S0040-4039(00)87045-8
_journal_volume                  23
_journal_year                    1982
_chemical_formula_sum            'C10 H14 O4'
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90
_cell_angle_beta                 104.36(5)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   12.799(5)
_cell_length_b                   5.977(5)
_cell_length_c                   13.083(6)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               1100275
(6aRS,9RS,10aRS)-4-Bromo-1-methoxy-6,6,9-trimethyl-6a,7,8,9,10,10a-hexahydro-6H-dibenzo[b,d]pyran
Harms, K.; Jones, P. G.; Sheldrick, G. M.; Acta Crystallographica, Section B: Structural Crystallography and Crystal Chemistry 36 (1980) 3157–3159; doi:10.1107/S0567740880011132

data_1100276
_publ_section_title
;
 (6aRS,9RS,10aRS)-4-Bromo-1-methoxy-6,6,9-trimethyl-6a,7,8,9,10,10a-hexahydro-6H-dibenzo[b,d]pyran
;
_journal_coden_ASTM              ACBCAR
_journal_issue                   12
_journal_name_full
;
 Acta Crystallographica, Section B: Structural Crystallography
 and Crystal Chemistry
;
_journal_page_first              3157
_journal_page_last               3159
_journal_paper_doi               10.1107/S0567740880011132
_journal_volume                  36
_journal_year                    1980
_chemical_formula_sum            'C17 H23 Br O2'
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                80.83(4)
_cell_angle_beta                 81.26(4)
_cell_angle_gamma                81.88(4)
_cell_formula_units_Z            2
_cell_length_a                   7.378(4)
_cell_length_b                   9.740(5)
_cell_length_c                   11.406(6)
_cod_original_formula_sum        'C17 H23 Br1 O2'
_cod_database_code               1100276
An enantiospecific hetero Diels-Alder product
Harms, K.; Sheldrick, G. M.; Glüsenkamp, K.-H.; Tietze, L.-F.; Acta Crystallographica, Section C: Crystal Structure Communications 42 (1986) 1268–1269; doi:10.1107/S0108270186092636

data_1100277
_publ_section_title
;
 An enantiospecific hetero Diels-Alder product
;
_journal_coden_ASTM              ACSCEE
_journal_issue                   9
_journal_name_full
;
 Acta Crystallographica, Section C: Crystal Structure Communications
;
_journal_page_first              1268
_journal_page_last               1269
_journal_paper_doi               10.1107/S0108270186092636
_journal_volume                  42
_journal_year                    1986
_chemical_formula_sum            'C19 H24 O8'
_space_group_IT_number           19
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      19
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   6.056(1)
_cell_length_b                   14.434(6)
_cell_length_c                   21.298(4)
_cod_database_code               1100277
Kristallstruktur von 2,4,4-Trifluor-1,3-dithietan-2-ylium-hexafluoroarsenat
Antel, Jochen; Harms, Klaus; Jones, Peter G.; Mews, Rüdiger; Sheldrick, George M.; Waterfeld, Alfred; Chemische Berichte 118 (1985) 5006–5008; doi:10.1002/cber.19851181231

data_1100278
_publ_section_title
;
 Kristallstruktur von 2,4,4-Trifluor-1,3-dithietan-2-ylium-hexafluoroarsenat
;
_journal_coden_ASTM              CHBEAM
_journal_issue                   12
_journal_name_full               'Chemische Berichte'
_journal_page_first              5006
_journal_page_last               5008
_journal_paper_doi               10.1002/cber.19851181231
_journal_volume                  118
_journal_year                    1985
_chemical_formula_sum            'C2 As F9 S2'
_space_group_IT_number           59
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-P 2ab 2a'
_symmetry_space_group_name_H-M   'P m m n :2'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   7.649(1)
_cell_length_b                   8.317(1)
_cell_length_c                   6.903(1)
_cod_original_sg_symbol_H-M      'P m m n'
_cod_original_formula_sum        'C2 As1 F9 S2'
_cod_database_code               1100278
X-Ray Structure Determination of [α-(Phenylsulfonyl)benzyllithium-Tetramethylethylenediamine]~2~: Chirality of an α-Sulfonyl "Carbanion"
Boche, Gernot; Marsch, Michael; Harms, Klaus; Sheldrick, George M.; Angewandte Chemie, International Edition in English 24 (1985) 573–575; doi:10.1002/anie.198505731

data_1100279
_publ_section_title
;
 X-Ray Structure Determination of
 [\a-(Phenylsulfonyl)benzyllithium-Tetramethylethylenediamine]~2~:
 Chirality of an \a-Sulfonyl "Carbanion"
;
_journal_coden_ASTM              ACIEAY
_journal_issue                   7
_journal_name_full
;
 Angewandte Chemie, International Edition in English
;
_journal_page_first              573
_journal_page_last               575
_journal_paper_doi               10.1002/anie.198505731
_journal_volume                  24
_journal_year                    1985
_chemical_formula_sum            'C38 H56 Li2 N4 O4 S2'
_space_group_IT_number           33
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      33
_symmetry_space_group_name_Hall  'P 2c -2n'
_symmetry_space_group_name_H-M   'P n a 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   17.051(6)
_cell_length_b                   10.017(2)
_cell_length_c                   23.759(30)
_cod_database_code               1100279
Hetero-diels-alder reaction of enaminecarbaldehydes an entry to branched aminosugars
Tietze, Lutz F.; Voß, Edgar; Harms, Klaus; Sheldrick, George M.; Tetrahedron Letters 26 (1985) 5273–5276; doi:10.1016/S0040-4039(00)95013-5

data_1100280
_publ_section_title
;
 Hetero-diels-alder reaction of enaminecarbaldehydes an entry
 to branched aminosugars
;
_journal_coden_ASTM              TELEAY
_journal_issue                   43
_journal_name_full               'Tetrahedron Letters'
_journal_page_first              5273
_journal_page_last               5276
_journal_paper_doi               10.1016/S0040-4039(00)95013-5
_journal_volume                  26
_journal_year                    1985
_chemical_formula_sum            'C13 H9 N O5'
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                77.18(1)
_cell_angle_beta                 87.42(1)
_cell_angle_gamma                83.75(1)
_cell_formula_units_Z            2
_cell_length_a                   7.578(1)
_cell_length_b                   7.829(1)
_cell_length_c                   10.151(1)
_cod_original_formula_sum        'C13 H9 N1 O5'
_cod_database_code               1100280
Structure of an unexpected indole photolysis product
Harms, K.; Sheldrick, G. M.; Brüggemann, K.; Tietze, L. F.; Acta Crystallographica, Section C: Crystal Structure Communications 42 (1986) 1264–1266; doi:10.1107/S010827018609265X

data_1100281
_publ_section_title
;
 Structure of an unexpected indole photolysis product
;
_journal_coden_ASTM              ACSCEE
_journal_issue                   9
_journal_name_full
;
 Acta Crystallographica, Section C: Crystal Structure Communications
;
_journal_page_first              1264
_journal_page_last               1266
_journal_paper_doi               10.1107/S010827018609265X
_journal_volume                  42
_journal_year                    1986
_chemical_formula_sum            'C30 H32 N4 O4'
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                97.53(4)
_cell_angle_beta                 101.65(4)
_cell_angle_gamma                113.84(3)
_cell_formula_units_Z            2
_cell_length_a                   10.340(5)
_cell_length_b                   10.809(5)
_cell_length_c                   13.613(1)
_cod_database_code               1100281
Structure of a photolysis product
Harms, K.; Sheldrick, G. M.; Glüsenkamp, K. H.; Tietze, L. F.; Acta Crystallographica, Section C: Crystal Structure Communications 42 (1986) 1269–1271; doi:10.1107/S0108270186092624

data_1100282
_publ_section_title
;
 Structure of a photolysis product
;
_journal_coden_ASTM              ACSCEE
_journal_issue                   9
_journal_name_full
;
 Acta Crystallographica, Section C: Crystal Structure Communications
;
_journal_page_first              1269
_journal_page_last               1271
_journal_paper_doi               10.1107/S0108270186092624
_journal_volume                  42
_journal_year                    1986
_chemical_formula_sum            'C31 H32 O7'
_space_group_IT_number           19
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      19
_symmetry_space_group_name_Hall  'P 2ac 2ab'
_symmetry_space_group_name_H-M   'P 21 21 21'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   8.424(1)
_cell_length_b                   14.773(2)
_cell_length_c                   22.165(2)
_cod_database_code               1100282