Conformational preferences of a polar biaryl: a phase- and enantiomeric purity-dependent molecular hinge.
Clayden, Jonathan; Fletcher, Stephen P.; Rowbottom, S. J. M.; Helliwell, Madeleine; Organic letters 11 (2009) 2313–2316; doi:10.1021/ol9006635

data_1503921
_publ_contact_author
; 
    Madeleine Helliwell 
;
_publ_section_title
;
 Conformational preferences of a polar biaryl: a phase- and enantiomeric
 purity-dependent molecular hinge.
;
_journal_issue                   11
_journal_name_full               'Organic letters'
_journal_page_first              2313
_journal_page_last               2316
_journal_paper_doi               10.1021/ol9006635
_journal_volume                  11
_journal_year                    2009
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_diffrn_reflns_theta_min         1.25
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_exptl_crystal_colour            colourless
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_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0174P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Trigonal' changed to 'trigonal'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        2676.9(5)
_cod_original_sg_symbol_H-M      P3(1)
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