Ferrocene-Decorated (Phthalocyaninato)(Porphyrinato) Double- and Triple-Decker Rare Earth Complexes: Synthesis, Structure, and Electrochemical Properties
Peihua Zhu; Xiuwen Zhang; Hailong Wang; Yuexing Zhang; Yongzhong Bian; Jianzhuang Jiang; Inorganic Chemistry 51 (2012) 5651–5659; doi:10.1021/ic202613r

data_4329175
_publ_contact_author_address
; 
Department of Chemistry, University of
 Science and Technology Beijing, Beijing 
100083, China 
;
_publ_contact_author_name        'Jianzhuang Jiang'
_publ_section_title
;
 Ferrocene-Decorated (Phthalocyaninato)(Porphyrinato) Double- and
 Triple-Decker Rare Earth Complexes: Synthesis, Structure, and
 Electrochemical Properties
;
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              5651
_journal_page_last               5659
_journal_paper_doi               10.1021/ic202613r
_journal_volume                  51
_journal_year                    2012
_chemical_formula_sum            'C73 H45 Cl3 Eu Fe2 N12 O0'
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_chemical_name_systematic
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 ?
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;
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CrysAlisPro, Oxford Diffraction Ltd.,
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(compiled Aug 27 2010,11:50:40)
;
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CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.34.40 (release 27-08-2010 CrysAlis171 .NET)
(compiled Aug 27 2010,11:50:40)
;
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
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_diffrn_ambient_temperature      120(2)
_diffrn_detector_area_resol_mean 16.2141
_diffrn_measured_fraction_theta_full 0.992
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CrysAlisPro, Oxford Diffraction Ltd.,
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empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    1.706
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_refine_ls_extinction_method     none
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_refine_ls_number_reflns         8374
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_refine_ls_R_factor_all          0.0643
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0655P)^2^+3.9757P] where P=(Fo^2^+2Fc^2^)/3'
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_cod_data_source_file            ic202613r_si_002_2.cif
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_cod_original_cell_volume        2842.5(3)
_cod_original_sg_symbol_Hall     -P1
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