Structural investigations of 1,2,3,4-tetrahydrocarbazole derivatives. I. 2,3-Dihydro-9-(phenylsulfonyl)carbazole-4(1<i>H</i>)-one and 1,2,3,4-tetrahydrocarbazole-1-spiro-2'-[1,3]dithiolane
Hökelek, T.; Patir, S.; Gülce, A.; Okay, G.; Acta Crystallographica Section C 50 (1994) 450–453; doi:10.1107/S0108270193007516

data_2009505
_publ_section_title
;
 Structural investigations of 1,2,3,4-tetrahydrocarbazole derivatives.
 I. 2,3-Dihydro-9-(phenylsulfonyl)carbazole-4(1<i>H</i>)-one and
 1,2,3,4-tetrahydrocarbazole-1-spiro-2'-[1,3]dithiolane
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              450
_journal_page_last               453
_journal_paper_doi               10.1107/S0108270193007516
_journal_volume                  50
_journal_year                    1994
_chemical_formula_sum            'C18 H15 N O3 S'
_chemical_formula_weight         325.38
_space_group_crystal_system      orthorhombic
_space_group_IT_number           61
_space_group_name_Hall           '-P 2bc 2ac'
_space_group_name_H-M_alt        'P c a b'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.
_cell_angle_beta                 90.
_cell_angle_gamma                90.
_cell_formula_units_Z            8
_cell_length_a                   8.952(5)
_cell_length_b                   21.979(4)
_cell_length_c                   15.709(3)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293
_cell_measurement_theta_max      12
_cell_measurement_theta_min      5
_cell_volume                     3090.8(19)
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \w/2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  'not calculated'
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            6408
_diffrn_reflns_theta_max         37.5
_diffrn_standards_decay_%        1
_diffrn_standards_interval_time  180
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.21
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.398
_exptl_crystal_description       prismatic
_exptl_crystal_size_max          1.1
_exptl_crystal_size_mid          0.45
_exptl_crystal_size_min          0.35
_refine_diff_density_max         0.44
_refine_diff_density_min         -0.24
_refine_ls_goodness_of_fit_obs   'not calculated'
_refine_ls_hydrogen_treatment    refall
_refine_ls_number_parameters     268
_refine_ls_number_reflns         1210
_refine_ls_R_factor_obs          0.033
_refine_ls_shift/esd_max         0.01
_refine_ls_structure_factor_coef F
_refine_ls_wR_factor_obs         0.032
_reflns_number_observed          1389
_reflns_number_total             2417
_reflns_observed_criterion       F>=3\s(F)
_cod_data_source_file            ab1076.cif
_cod_data_source_block           ab1076_structure_1_of_2
_cod_original_cell_volume        3090.8(1.9)
_cod_original_formula_sum        'C18 H15 N1 O3 S1'
_cod_database_code               2009505