Resolvable polymorphism in an intergrowth of two modifications of tris(diethyldithiocarbamato)antimony
Ng, Seik Weng; Acta Crystallographica Section C 77 (2021) 610–614; doi:10.1107/S205322962100886X

data_2022450
_publ_section_title
;
 Resolvable polymorphism in an intergrowth of two modifications of
 tris(diethyldithiocarbamato)antimony
;
_journal_coeditor_code           CU3175
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              610
_journal_page_last               614
_journal_paper_doi               10.1107/S205322962100886X
_journal_volume                  77
_journal_year                    2021
_chemical_formula_iupac          '[Sb (C5 H10 N S2)3]'
_chemical_formula_moiety         'C15 H30 N3 S6 Sb'
_chemical_formula_sum            'C15 H30 N3 S6 Sb'
_chemical_formula_weight         566.53
_chemical_name_systematic
;
Tris(diethyldithiocarbamato-\k<i>S</i>)antimony(III)
;
_space_group_crystal_system      monoclinic
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_space_group_name_Hall           '-P 2ybc'
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_cell_length_c                   14.6614(11)
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_computing_cell_refinement
;
CrysAlis PRO (Rigaku OD, 2020)
;
_computing_data_collection
;
CrysAlis PRO (Rigaku OD, 2020)
;
_computing_data_reduction
;
CrysAlis PRO (Rigaku OD, 2020)
;
_computing_molecular_graphics
;
DIAMOND (Brandenburg & Berndt, 2021)
;
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;
SHELXL2018 (Sheldrick, 2015b)
;
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;
SHELXL2018 (Sheldrick, 2015b)
;
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;
SHELXT (Sheldrick, 2015a)
;
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_exptl_absorpt_correction_T_min  0.62855
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(CrysAlis PRO; Rigaku OD, 2020)
;
_exptl_crystal_colour            orange
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_exptl_crystal_description       prism
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_refine_ls_R_factor_gt           0.0566
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
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'w=1/[\s^2^(Fo^2^)+(0.0185P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
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_cod_data_source_block           monoclinic
_cod_depositor_comments
'Adding full bibliography for 2022449--2022450.cif.'
_cod_original_sg_symbol_H-M      'P 21/c'
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