High Performance n-Type Organic Field-Effect Transistors Based on π-Electronic Systems with Trifluoromethylphenyl Groups
Shinji Ando; Jun-ichi Nishida; Hirokazu Tada; Youji Inoue; Shizuo Tokito; Yoshiro Yamashita; Journal of the American Chemical Society 127 (2005) 5336–5337; doi:10.1021/ja042219+

data_4111637
_publ_contact_author_email       ' yoshiro@echem.titech.ac.jp'
_publ_contact_author_fax         ' +81-45-924-5489'
_publ_contact_author_name        ' Yoshiro Yamashita'
_publ_contact_author_phone       ' +81-45-924-5571'
_publ_section_title
;
 High Performance n-Type Organic Field-Effect Transistors Based on
 \p-Electronic Systems with Trifluoromethylphenyl Groups
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              5336
_journal_page_last               5337
_journal_paper_doi               10.1021/ja042219+
_journal_volume                  127
_journal_year                    2005
_chemical_formula_moiety         'C26 H12 F6 N2 S4 '
_chemical_formula_sum            'C26 H12 F6 N2 S4'
_chemical_formula_weight         594.62
_chemical_melting_point          571
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_audit_creation_date             2005-1-12
_audit_creation_method           'by teXsan'
_cell_angle_alpha                98
_cell_angle_beta                 93
_cell_angle_gamma                97
_cell_formula_units_Z            2
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_cell_length_b                   8.1828
_cell_length_c                   23.2685
_cell_measurement_reflns_used    7879
_cell_measurement_temperature    296.2
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      3.3
_cell_volume                     1129.529
_computing_cell_refinement       PROCESS-AUTO
_computing_data_collection       PROCESS-AUTO
_computing_data_reduction        'teXsan Ver. 1.11'
_computing_publication_material  'teXsan Ver. 1.11'
_computing_structure_refinement  'teXsan Ver. 1.10'
_computing_structure_solution    SIR97
_diffrn_detector_area_resol_mean 10.00
_diffrn_measured_fraction_theta_full 0.9893
_diffrn_measured_fraction_theta_max 0.9893
_diffrn_measurement_device_type  'Rigaku RAXIS-RAPID Imaging Plate'
_diffrn_measurement_method       \w
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.081
_diffrn_reflns_limit_h_max       7
_diffrn_reflns_limit_h_min       -6
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -30
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_diffrn_reflns_theta_full        27.49
_diffrn_reflns_theta_max         27.49
_exptl_absorpt_coefficient_mu    0.495
_exptl_absorpt_correction_T_max  0.952
_exptl_absorpt_correction_T_min  0.217
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(Higashi, 1995)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.756
_exptl_crystal_description       platelet
_exptl_crystal_size_max          0.200
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.100
_refine_diff_density_max         1.24
_refine_diff_density_min         -1.07
_refine_ls_extinction_method     none
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_refine_ls_hydrogen_treatment    noref
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_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^) + (0.05000(Max(Fo^2^,0) + 2Fc^2^)/3)^2^]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1971
_reflns_number_gt                2122
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_reflns_threshold_expression     F^2^>2.0\s(F^2^)
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_cod_data_source_block           General
_cod_original_cell_volume        1124.4100
_cod_original_sg_symbol_H-M      'P -1 '
_cod_original_formula_sum        'C26 H12 F6 N2 S4 '
_cod_database_code               4111637