Electron crystallography with the EIGER detector
Tinti, Gemma; Fröjdh, Erik; van Genderen, Eric; Gruene, Tim; Schmitt, Bernd; de Winter, D. A. Matthijs; Weckhuysen, Bert M.; Abrahams, Jan Pieter; IUCrJ 5 (2018) 190–199; doi:10.1107/S2052252518000945

data_1548908
_publ_section_title
;
 Electron crystallography with the EIGER detector
;
_journal_coeditor_code           SP5002
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_journal_name_full               IUCrJ
_journal_page_first              190
_journal_page_last               199
_journal_paper_doi               10.1107/S2052252518000945
_journal_volume                  5
_journal_year                    2018
_chemical_formula_sum            'Al O4 P'
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_space_group_name_Hall           '-P 3*'
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_symmetry_space_group_name_H-M   'R -3 :R'
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_cell_length_c                   9.6090(17)
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_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.950
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_diffrn_reflns_av_R_equivalents  0.1787
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_diffrn_reflns_limit_h_min       -11
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_diffrn_reflns_limit_l_min       -11
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_diffrn_reflns_theta_max         1.103
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_refine_ls_extinction_method     none
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_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
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_refine_ls_number_reflns         1673
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_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.2000P)^2^] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            sp5002.cif
_cod_data_source_block           I
_cod_depositor_comments          'Adding full bibliography for 1548908.cif.'
_cod_original_cell_volume        878.7(5)
_cod_database_code               1548908
_shelx_shelxl_version_number     2016/6
_shelx_estimated_absorpt_t_min   1.000
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_shelx_res_checksum              47922
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