Soluble monometallic salen complexes derived from O-functionalised diamines as metalloligands for the synthesis of heterobimetallic complexes.
Schley, Michael; Fritzsche, Sebastian; Lönnecke, Peter; Hey-Hawkins, Evamarie; Dalton transactions (Cambridge, England : 2003) 39 (2010) 4090–4106; doi:10.1039/b920706f

data_7024727
_publ_section_title
;
 Soluble monometallic salen complexes derived from O-functionalised
 diamines as metalloligands for the synthesis of heterobimetallic
 complexes.
;
_journal_issue                   17
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              4090
_journal_page_last               4106
_journal_paper_doi               10.1039/b920706f
_journal_volume                  39
_journal_year                    2010
_chemical_formula_sum            'C46 H62 Cl Cr N4 O6'
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_chemical_name_systematic
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?
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_cell_length_b                   15.812(3)
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CrysAlis RED, Oxford Diffraction Ltd.,
Version 1.171.30.5 (release 12-06-2006 CrysAlis171 .NET)
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_computing_data_collection
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CrysAlis CCD, Oxford Diffraction Ltd.,
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CrysAlis RED, Oxford Diffraction Ltd.,
Version 1.171.30.5 (release 12-06-2006 CrysAlis171 .NET)
(compiled Jun 12 2006,17:01:16)
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_computing_molecular_graphics
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ORTEP3 for Windows
L. J. Farrugia, J. Appl. Crystallogr. 1997, 30, 565.
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WINGX
L.J. Farrugia,
J. Appl. Cryst., 1999, 32, 837-838.
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SHELXL-97
G. M. Sheldrick, 2008, Acta Cryst., A64, 112-122
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SHELXS-97
Program for Crystal Structure Analysis (Release 97-2)
G. M. Sheldrick, Instit\"ut f\"ur Anorganische Chemie der Universit\"at,
Tammanstrasse 4, D-3400 G\"ottingen, Germany, 1998.
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_diffrn_ambient_temperature      150(2)
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_diffrn_radiation_monochromator  graphite
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CrysAlis RED, Oxford Diffraction Ltd.,
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(compiled Jun 12 2006,17:01:16)
Empirical absorption correction using spherical harmonics,
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_exptl_crystal_colour            'red brown'
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_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             910
_exptl_crystal_size_max          0.3
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_exptl_crystal_size_min          0.1
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_refine_ls_restrained_S_all      1.032
_refine_ls_R_factor_all          0.0811
_refine_ls_R_factor_gt           0.0475
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_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
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'calc w=1/[\s^2^(Fo^2^)+(0.0722P)^2^+0.3478P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_refine_ls_wR_factor_ref         0.1392
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The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_cell_volume        2335.2(7)
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