Cobaltaelectro-catalyzed oxidative allene annulation by electro-removable hydrazides.
Mei, Ruhuai; Fang, Xinyue; He, Liang; Sun, Junmei; Zou, Liang; Ma, Wenbo; Ackermann, Lutz; Chemical communications (Cambridge, England) 56 (2020) 1393–1396; doi:10.1039/c9cc09076b

data_7125690
_publ_section_title
;
 Cobaltaelectro-catalyzed oxidative allene annulation by electro-removable
 hydrazides.
;
_journal_issue                   9
_journal_name_full               'Chemical communications (Cambridge, England)'
_journal_page_first              1393
_journal_page_last               1396
_journal_paper_doi               10.1039/c9cc09076b
_journal_volume                  56
_journal_year                    2020
_chemical_formula_sum            'C28 H24 N3 O2 P'
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_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2019-11-06 deposited with the CCDC.	2019-12-23 downloaded from the CCDC.
;
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_cell_measurement_temperature    293(2)
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_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      293(2)
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_diffrn_radiation_type           CuK\a
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_diffrn_reflns_theta_max         71.900
_diffrn_reflns_theta_min         3.927
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_refine_ls_restrained_S_all      1.016
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.1220P)^2^+0.3630P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
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_reflns_number_total             4561
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            c9cc09076b2.cif
_cod_data_source_block           cd-meh-hl-rmc87b
_cod_depositor_comments
'Adding full bibliography for 7125690--7125691.cif.'
_cod_original_cell_volume        2379.00(11)
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               7125690
_shelx_shelxl_version_number     2014/7
_shelx_res_checksum              51696