Inter- and intra-molecular pathways in polyamine synthesis from diamines †
Choi, Min-Ho; Kim, Bok Jo; Kim, Il-Chool; Kim, Seo-Hyang; Kim, Yang; Harrowfield, Jack M.; Lee, Man-Kil; Mocerino, Mauro; Rukmini, Elisabeth; Skelton, Brian W.; White, Allan H.; Journal of the Chemical Society, Dalton Transactions  (2001) 707–; doi:10.1039/b008452m

data_7010403
_publ_section_title
;
 Inter- and intra-molecular pathways in polyamine synthesis from
 diamines&#x200A;&#x2020;
;
_journal_issue                   5
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              707
_journal_paper_doi               10.1039/b008452m
_journal_year                    2001
_chemical_formula_sum            'C23 H57 Cl5 Co N6 O4.5'
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_symmetry_space_group_name_H-M   'P 21 21 21'
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_cell_angle_beta                 90.00000
_cell_angle_gamma                90.00000
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_cell_measurement_theta_max      23.2
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_computing_cell_refinement       'Enraf Nonius software'
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  CAD4 diffractometer
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_diffrn_measurement_method       '2\q-\w scans'
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_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'sealed tube'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     .71073
_diffrn_reflns_limit_h_max       24
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       0
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_diffrn_reflns_limit_l_min       0
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_diffrn_standards_interval_time  60
_diffrn_standards_number         10
_exptl_absorpt_coefficient_mu    .937
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_exptl_absorpt_correction_T_min  .68
_exptl_absorpt_correction_type   gaussian
_exptl_absorpt_process_details
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 XTAL absorb                
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_exptl_crystal_colour            green
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_exptl_crystal_description       prism
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_exptl_crystal_size_mid          .42
_exptl_crystal_size_min          .32
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      calc
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_reflns_limit_k_min              0
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_reflns_limit_l_min              0
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_cod_depositor_comments
;
The following automatic conversions were performed:
'_refine_ls_matrix_type' value 'Full' changed to 'full' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_Hall     p_2ac_2ab
_cod_original_sg_symbol_H-M      P_21_21_21
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