Crystal structures of nitridotechnetium(V) complexes of amine oximes differing in carbon chain lengths
Kani, Yuko; TakayamaTsutomuSekine, Tsutomu; Kudo, Hiroshi; Journal of the Chemical Society, Dalton Transactions  (1999) 209–; doi:10.1039/a806245e

data_7027050
_publ_section_title
;
 Crystal structures of nitridotechnetium(V) complexes of amine oximes
 differing in carbon chain lengths
;
_journal_issue                   2
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              209
_journal_paper_doi               10.1039/a806245e
_journal_year                    1999
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_cell_length_b                   30.636(2)
_cell_length_c                   13.967(3)
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_cell_measurement_temperature    286.2
_cell_measurement_theta_max      24.7
_cell_measurement_theta_min      23.3
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_computing_publication_material  teXsan
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_diffrn_radiation_detector       'scintillation counter'
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_cod_data_source_file            806245Esup1.cif
_cod_data_source_block           TcN-PentAO(3)
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_original_cell_volume        4254(2)
_cod_original_sg_symbol_H-M      'P 21/n     '
_cod_original_formula_sum        'C42 H59 B N5 O4 Tc '
_cod_database_code               7027050