LiGaSi~2~O~6~
Sato, A.; Osawa, T.; Ohashi, H.; Acta Crystallographica Section C 50 (1994) 487–488; doi:10.1107/S0108270193009606

data_2009646
_publ_section_title
;
 LiGaSi~2~O~6~
;
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              487
_journal_page_last               488
_journal_paper_doi               10.1107/S0108270193009606
_journal_volume                  50
_journal_year                    1994
_chemical_formula_moiety         'Ga Li O6 Si2'
_chemical_formula_sum            'Ga Li O6 Si2'
_chemical_formula_weight         228.83
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_type_scat_source           IntTabIV
_cell_angle_alpha                90.
_cell_angle_beta                 110.244(3)
_cell_angle_gamma                90.
_cell_formula_units_Z            4
_cell_length_a                   9.5610(10)
_cell_length_b                   8.5690(10)
_cell_length_c                   5.2680(10)
_cell_measurement_reflns_used    22
_cell_measurement_temperature    298
_cell_measurement_theta_max      37
_cell_measurement_theta_min      33
_cell_volume                     404.94(10)
_database_code_amcsd             0010289
_diffrn_measurement_device       'Enraf-Nonius CAD-4'
_diffrn_measurement_method       \w-2\q
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       9
_diffrn_reflns_limit_l_min       -9
_diffrn_reflns_number            1309
_diffrn_reflns_theta_max         40
_diffrn_standards_decay_%        -0.8
_diffrn_standards_interval_count 100
_diffrn_standards_interval_time  240
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    7.29
_exptl_absorpt_correction_T_max  0.501
_exptl_absorpt_correction_T_min  0.371
_exptl_absorpt_correction_type   integration
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    3.75
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.11
_refine_diff_density_max         0.6
_refine_diff_density_min         -1.0
_refine_ls_extinction_coef       12.6E-6
_refine_ls_extinction_method     'isotropic secondary'
_refine_ls_goodness_of_fit_obs   1.7
_refine_ls_number_parameters     48
_refine_ls_number_reflns         1268
_refine_ls_R_factor_obs          0.017
_refine_ls_shift/esd_max         <0.005
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/\s(F)^2^'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_obs         0.038
_reflns_number_observed          1268
_reflns_number_total             1309
_reflns_observed_criterion       I>1.5\s(I)
_cod_data_source_file            oh1040.cif
_cod_data_source_block           oh1040_structure_1_of_1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value '1/\s(F)^2^' was changed to
'calc'. New tag '_refine_ls_weighting_details' was created. The value
of the new tag was set to 'w = 1/\s(F)^2^'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        404.90(5)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               2009646
_amcsd_formula_title             LiGaSi2O6