Fine-tuning of boron complexes with cage-shaped ligand geometry: rational design of triphenolic ligand as a template for structure control.
Yasuda, Makoto; Yoshioka, Sachiko; Nakajima, Hideto; Chiba, Kouji; Baba, Akio; Organic letters 10 (2008) 929–932; doi:10.1021/ol7030944

data_1504554
_publ_section_title
;
 Fine-tuning of boron complexes with cage-shaped ligand geometry: rational
 design of triphenolic ligand as a template for structure control.
;
_journal_issue                   5
_journal_name_full               'Organic letters'
_journal_page_first              929
_journal_page_last               932
_journal_paper_doi               10.1021/ol7030944
_journal_volume                  10
_journal_year                    2008
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_chemical_formula_sum            'C27 H22 B Cl3 O5'
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_symmetry_cell_setting           triclinic
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_symmetry_space_group_name_Hall  '-P 1'
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_cell_length_b                   9.3224(13)
_cell_length_c                   16.548(2)
_cell_measurement_reflns_used    4397
_cell_measurement_temperature    273.1
_cell_measurement_theta_max      30.3
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_cell_volume                     1275.0(3)
_computing_cell_refinement       PROCESS-AUTO
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_computing_publication_material  'CrystalStructure 3.8'
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_diffrn_measurement_method       \w
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_exptl_crystal_colour            colorless
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_refine_ls_R_factor_gt           0.0846
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_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[0.0194Fo^2^ + 1.0000\s(Fo^2^)]'
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