Neutral and Cationic Bis-Chelate Monoorganosilicon(IV) Complexes of 1-Hydroxy-2-pyridinone
Koch, James G.; Brennessel, William W.; Kraft, Bradley M.; Organometallics 36 (2017) 594–; doi:10.1021/acs.organomet.6b00796

data_4086924
_publ_section_title
;
 Neutral and Cationic Bis-Chelate Monoorganosilicon(IV) Complexes of
 1-Hydroxy-2-pyridinone
;
_journal_issue                   3
_journal_name_full               Organometallics
_journal_page_first              594
_journal_paper_doi               10.1021/acs.organomet.6b00796
_journal_volume                  36
_journal_year                    2017
_chemical_formula_moiety         'C17 H15 Cl N2 O4 Si'
_chemical_formula_sum            'C17 H15 Cl N2 O4 Si'
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_chemical_name_common            sjfbk33
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_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
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_cell_measurement_temperature    100.0(5)
_cell_measurement_theta_max      38.21
_cell_measurement_theta_min      3.01
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_diffrn_ambient_temperature      100.0(5)
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.974
_diffrn_measurement_device_type  'Bruker SMART APEX II CCD platform'
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_type           MoK\a
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_refine_ls_extinction_method     none
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_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.032
_refine_ls_R_factor_all          0.0659
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_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0447P)^2^+0.5558P] where P=(Fo^2^+2Fc^2^)/3'
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_reflns_number_total             9188
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            20161212_Combined.cif
_cod_data_source_block           03
_cod_depositor_comments
'Adding full bibliography for 4086922--4086931.cif.'
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_shelx_hkl_checksum              77735