<i>catena</i>-Poly[[diphenylpropyltin(IV)]-μ-chloroacetato-κ^2^<i>O</i>:<i>O</i>']
Amini, Mostafa M.; Hajiashrafi, Taraneh; Khavasi, Hamid Reza; Nematin Kharat, Ali; Acta Crystallographica Section E 64 (2008) m1007–; doi:10.1107/S160053680802028X

data_2219185
_publ_section_title
<i>catena</i>-Poly[[diphenylpropyltin(IV)]-\m-chloroacetato-\k^2^<i>O</i>:<i>O</i>']
_journal_coeditor_code           WM2181
_journal_issue                   8
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1007
_journal_paper_doi               10.1107/S160053680802028X
_journal_volume                  64
_journal_year                    2008
_chemical_formula_iupac          '[Sn (C3 H7) (C6 H5)2 (C2 H2 Cl O2)]'
_chemical_formula_moiety         'C17 H19 Cl O2 Sn'
_chemical_formula_sum            'C17 H19 Cl O2 Sn'
_chemical_formula_weight         409.48
_chemical_name_systematic
;
catena-Poly[[diphenylpropyltin(IV)]-\m-chloroacetato-\k^2^O:O']
;
_space_group_IT_number           29
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  'P 2c -2ac'
_symmetry_space_group_name_H-M   'P c a 21'
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   19.330(4)
_cell_length_b                   11.440(2)
_cell_length_c                   16.390(3)
_cell_measurement_reflns_used    7531
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      29.25
_cell_measurement_theta_min      2.07
_cell_volume                     3624.4(12)
_computing_cell_refinement       'X-AREA (Stoe & Cie, 2005)'
_computing_data_collection       'X-AREA (Stoe & Cie, 2005)'
_computing_data_reduction        'X-AREA (Stoe & Cie, 2005)'
_computing_molecular_graphics    'ORTEP-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS97 (Sheldrick, 2008)'
_diffrn_measured_fraction_theta_full 0.985
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measurement_device_type  'Stoe IPDSII'
_diffrn_measurement_method       \w
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0341
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -26
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            13588
_diffrn_reflns_theta_full        29.25
_diffrn_reflns_theta_max         29.25
_diffrn_reflns_theta_min         2.07
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    1.558
_exptl_absorpt_correction_T_max  0.8256
_exptl_absorpt_correction_T_min  0.6786
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   '[X-RED and X-SHAPE (Stoe & Cie, 2005)]'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.501
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             1632
_exptl_crystal_size_max          0.49
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.19
_refine_diff_density_max         0.787
_refine_diff_density_min         -0.552
_refine_ls_abs_structure_details 'Flack (1983), with 3643 Friedel pairs'
_refine_ls_abs_structure_Flack   -0.04(4)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.115
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     380
_refine_ls_number_reflns         8672
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.115
_refine_ls_R_factor_gt           0.0446
_refine_ls_shift/su_max          0.026
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w = 1/[\s^2^(Fo^2^)+(0.0589P)^2^+2.5701P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.1233
_reflns_number_gt                7285
_reflns_number_total             8672
_reflns_threshold_expression     I>2\s(I)
_cod_data_source_file            wm2181.cif
_cod_data_source_block           I
_cod_original_cell_volume        3624.4(13)
_cod_database_code               2219185
_cod_database_fobs_code          2219185