development of single crystal σ shaped quartz porphyroclasts by dissolution precipitation creep in a calcite marble shear zone abstract within a greenschist facies calcite marble shear zone isolated quartz grains change shape across the shear zone profile whereas quartz grains have a spherical to elongated shape in the coarse grained marble protolith and protomylonite they are asymmetric shaped porphyroclasts with wedge shaped appendages wings in ultramylonites in all cases quartz grains are single crystals they are sometimes twinned but never recrystallized stress induced dissolution precipitation creep is the favourable shape controlling process during deformation providing a relatively undeformed core truncation of pre existing cathodoluminescence cl patterns and syntaxial precipitation of wings the necessary fluids may have been released from fluid inclusions during dynamic recrystallization of the calcite matrix the development of shape is not related to the crystallographic orientation of the quartz porphyroclasts crystallographic orientation analysis by electron backscatter diffraction ebsd and cl analyses exclude crystal plasticity as a shape controlling mechanism of quartz grains during mylonitisation however in ultramylonites quartz clasts have a strong crystallographic preferred orientation cpo with c axes sub parallel to the shear direction this fabric is uncommon for quartz under greenschist facies conditions it might be explained by a strengthening of a pre existing weak cpo during mylonitisation by rigid particle rotation of elongated quartz grains

a flow law for dislocation creep of quartz aggregates determined with the molten salt cell we have used the molten salt cell to conduct an experimental study on the rheology of a natural quartzite containing 0 15 wt water co axial deformation experiments were conducted at constant piston displacement rates approximating constant strain rates at low strain the strengths of our natural quartzite measured in the molten salt cell are approximately half those measured at the same conditions in solid media because unlike solid confining media molten salt does not contribute to the strength of the sample it reduces the friction on the moving piston and it allows clear identification of the hit point we have limited the experimental conditions to those required for dislocation creep and have used only steady state flow stresses measured during climb accommodated dislocation creep to calculate the flow law parameters two flow laws were determined one for samples containing minor amounts of melt 1 2 and one for melt free samples in both cases the power law stress exponent n is 4 0 0 9 which is greater than that previously reported in flow laws for dislocation creep of quartz aggregates determined in solid media the activation energy q is 137 34 kj mol 1 for samples with melt and 223 56 kj mol 1 for those without within the range of previously determined values for quartz aggregates containing 0 1 wt water the pre exponential term a is 1 1 10 4 2 mpa ns 1 for samples without melt and 1 8 10 8 2 mpa ns 1 for those with melt the lower strengths measured in the molten salt cell indicate that previous piezometer relations for quartz experimentally determined in solid media are not correct extrapolation of the flow law for melt free aggregates to natural strain rates predicts higher strengths than most previous quartz flow laws however accurate extrapolation requires determining the dependence of flow stress on fh2o and or ah

simple shear experiments on calcite rocks rheology and microfabric ideal simple shearing of carrara marble and solnhofen limestone was achieved by inserting calcite rock slices into sandstone cylinders precut at 35 the experiments covered a wide range in temperatures 25 900 c at confining pressures of 200 and 250 mpa and at strain rates between 10 3 and 10 5 s 1 shear strains of up 2 7 were achieved the stress strain data for simple shear favourably compare with predictions on the basis of existing flow laws established in coaxial testing this comparison demonstrates that the simple shear experiments covered most of the previously established flow regimes for calcite rocks at the highest temperatures carrara marble exhibited substantial work softening after high shear strains a complete texture analysis was carried out with the u stage and a texture goniometer the following four distinct microfabric regimes were found 1 twinning regime an oblique c axis maximum deflected from the pole to the flattening plane towards 1 and against the imposed sense of shear results directly from e twinning extensive twinning some grains are completely twinned rapidly rotates the c axes into near parallelism with 1 this regime was observed for carrara marble deformed at temperatures below 700 c and for solnhofen limestone at room temperature 2 intracrystalline slip regime three c axis maxima were observed in both rock types at more elevated temperatures and in the absence of twinning these c axis orientations result from an alignment of slip planes and slip directions into parallelism with the shear zone boundary and the shear direction respectively this finding supports the idea of an orientation for easy slip resulting from simple shearing in addition to r and f glide basal glide is inferred to have been operative 3 grain boundary sliding regime a great circle distribution of c axes approximately perpendicular to the direction of finite shortening is observed this texture is weaker compared to the other regimes it is interpreted to result from minor contributions of f slip towards total strain this regime is restricted to fine grained solnhofen limestone deformed at the highest temperatures 4 grain boundary migration regime only in carrara marble deformed at the highest temperatures is there substantial grain boundary migration recrystallization the texture consists of a dominant c axis maximum oriented perpendicular to the shear zone boundary this single maximum corresponds to an orientation for easy slip for basal slip grain boundary migration assists rapid lattice reorientation and leads to geometrical work softening quantitative analysis of grain boundary surface orientations gave the following results within the twinning and the intracrystalline slip regimes the characteristic grain shape is elliptical for both rock types the strain ellipses derived from this analysis closely correspond to the known finite strain at the lowest temperatures at intermediate temperatures and especially in carrara marble there is a consistent trend for the aspect ratios to indicate too little flattening and for the angles between the long axis of the strain ellipse and the shear zone boundary to be too small in the absence of grain boundary migration recrystallization this finding indicates minor translations of grains with respect to one another grain boundary sliding or translations accommodated in the mantle regions of grains at the highest temperatures where extensive grain boundary migration occurs in carrara marble grain boundary migration regime two preferred orientations of grain boundaries are observed 1 parallel to the shear zone boundary and 2 parallel to an oblique direction deflected 20 away from the normal to the shear zone boundary in the sense of the imposed shear the same pattern of grain boundary alignment is observed in solnhofen limestone deformed in the grain boundary sliding regime the geological applications of this experimental work are discussed in terms of calcite tectonites in particular and sheared rocks in general

problems in the extrapolation of laboratory rheological data abstract the many types of variables and deformation regimes that need to be taken into account in extrapolating rheological behaviour from the laboratory to the earth are reviewed the problems of extrapolation are then illustrated with two particular cases in the case of divine rich rocks recent experimental work indicates that within present uncertainties of extrapolation the flow in the upper mantle could be either grain size dependent and near newtonian or grain size independent and distinctly non newtonian both types of behaviour would be influenced by the present of trace amounts of water in the case of quartz rich rocks the uncertainties are even greater and it is still premature to attempt any extrapolation to geological conditions except as an upper bound the fugacity and the scale of dispersion of the water are probably two important variables but the quantitative laws governing their influence are not yet clear

the effect of dissolved magnesium on creep of calcite ii transition from diffusion creep to dislocation creep we extended a previous study on the influence of mg solute impurity on diffusion creep in calcite to include deformation under a broader range of stress conditions and over a wider range of mg contents synthetic marbles were produced by hot isostatic pressing hip mixtures of calcite and dolomite powders for different intervals 2 30 h at 850 c and 300 mpa confining pressure the hip treatment resulted in high magnesian calcite aggregates with mg content ranging from 0 5 to 17 mol both back scattered electron images and chemical analysis suggested that the dolomite phase was completely dissolved and that mg distribution was homogeneous throughout the samples at the scale of about two micrometers the grain size after hip varied from 8 to 31 m increased with time at temperature and decreased with increasing mg content 3 0 mol grain size and time were consistent with a normal grain growth equation with exponents from 2 4 to 4 7 for samples containing 0 5 17 0 mol mg respectively we deformed samples after hip at the same confining pressure with differential stresses between 20 and 200 mpa using either constant strain rate or stepping intervals of loading at constant stresses in a paterson gas medium deformation apparatus the deformation tests took place at between 700 and 800 c and at strain rates between 10 6 and 10 3 s 1 after deformation to strains of about 25 a bimodal distribution of large protoblasts and small recrystallized neoblasts coexisted in some samples loaded at higher stresses the deformation data indicated a transition in mechanism from diffusion creep to dislocation creep at stresses below 40 mpa the strength was directly proportional to grain size and decreased with increasing mg content due to the reductions in grain size at about 40 mpa the sensitivity of log strain rate to log stress n became greater than 1 and eventually exceeded 3 for stresses above 80 mpa at a given strain rate and temperature the stress at which that transition occurred was larger for samples with higher mg content and smaller grain size at given strain rates constant temperature and fixed grain size the strength of calcite in the dislocation creep regime increased with solute content while the strength in the diffusion creep regime was independent of mg content the results suggest that chemical composition will be an important element to consider when solid substitution can occur during natural deformation

silicon diffusion in a natural quartz aggregate constraints on solution transfer diffusion creep abstract silicon bulk diffusion rates were determined in a fine grained 1 2 m diameter natural quartz aggregate novaculite from hot springs ar the diffusion experiments were done at 600 800 c and 150 mpa confining pressure hydrothermal and at 800 1100 c and 1 atm in a stream of dry n2 the technique employed an isotopic tracer 30si and standard step scan analysis using an ion microprobe sims the temperature dependence of silicon bulk diffusion in the novaculite is described by the arrhenius parameters d0 bulk 3 7 10 10 m2 s and q 137 18 kj mol and d0 bulk 6 2 10 9 m2 s and q 178 38 kj mol for the hydrothermal and dry experiments respectively at 800 c the silicon bulk diffusion rate at 150 mpa hydrothermal is about a factor of 10 greater than at 1 atm dry for an assumed effective grain boundary width of 2 nm the silicon grain boundary diffusion rates in novaculite are a factor of two to three less than oxygen diffusion rates for similar hydrothermal conditions and more than 12 orders of magnitude greater than anhydrous silicon volume diffusion rates extrapolated to the temperature of these experiments the results of this study provide valuable constraints on the role of diffusion accommodated deformation in quartz rich rocks

vertical air motion and raindrop size distributions in convective systems using a 94 ghz radar this paper presents a method for the observation of air vertical velocity and raindrop size distribution in convective storms based on the interpretation of mie backscattering oscillations seen in the doppler spectrum observed at vertical incidence with a 94 ghz doppler radar the location of the first minimum allows an accurate determination of vertical air motion which is used to shift the spectrum so that it relates to the raindrops terminal velocity alone the drop size distribution is then retrieved from the shifted doppler spectrum an example of the structure of two dimensional updrafts and downdrafts observed in the low levels of a convective storm is presented drop size distributions can also be estimated and evidence of small drop removal by the updraft is presented

determination of deviatoric stress tensors based on inversion of calcite twin data from experimentally deformed monophase samples preliminary results abstract following previous successful paleo stress determinations from numerically generated aggregates and naturally deformed samples preliminary results about stress reconstructions based on inversion of calcite twin data from experimentally deformed monophase samples are reported this new study carried out on samples of carrara marble and crinoidic limestone from eastern france provides a test of the validity of stress reconstructions using inverse methods which had not been properly calibrated before the percentages of correlated twins are discussed for each stress tesnor and the range of uncertainties on the determination of stress orientations and differential stress magnitudes is evaluated

experimental study of the influence of stress temperature and strain on the dynamic recrystallization of carrara marble carrara marble has been deformed experimentally at temperatures ranging between 500 and 1000 c at confining pressures of 200 and 300 mpa and up to very large strains in extension and compression in order to study the microstructural and mechanical property changes associated with dynamic recrystallization microstructural studies were made by optical microscopy on ultrathin sections and automatic grain size measurement techniques were used when the temperature is sufficiently high 600 c and the stresses are high enough for deformation twinning to occur twin boundary migration is a powerful recrystallization mechanism that does not modify the grain size at stress levels too low to activate twinning recrystallization occurs in two stages the formation of nuclei by grain boundary bulging and subgrain rotation recrystallization in the grain boundary regions followed by a second stage of grain boundary migration recrystallization to a larger grain size that eventually overprints the entire rock volume the recrystallization process requires larger prestrains at the lower temperatures the size to which migration recrystallized grains grow seems to be limited by the stress and grain size dependent twinning field boundary or by the boundary between the dislocation creep and grain size sensitive flow mechanisms within the range of experimental observations dynamically recrystallized grain size does not depend on strain rate or temperature separate empirical stress versus grain size relations are presented for rotation and migration recrystallization that may be used for palaeopiezometry no unequivocal experimental evidence of weakening resulting from recrystallization to finer grain sizes at laboratory strain rates was found however extrapolation of the experimental data to low natural strain rates suggests that weakening following recrystallization may occur in nature

palaeostress estimation using calcite twinning experimental calibration and application to nature abstract by means of high temperature deformation experiments on calcite rocks of different grain sizes we have established the relationships between differential stress and twinning incidence twin density and volume fraction and the way that these relationships depend on grain size both twinning incidence and volume fraction increase with grain size at a constant level of differential stress log twin density is proportional to stress but is independent of grain size at a given grain size volume fraction of twinning increases non linearly with differential stress twinning activity measured by twinning incidence increases linearly with stress the behaviour of each of these parameters is independent of temperature strain and strain rate these relationships can be used as a basis for the estimation of palaeostress values in naturally deformed calcite rocks this is illustrated by a study of twinning activity in limestones close to thrust faults in the cantabrian zone of the variscan orogenic belt in northwestern spain high peak differential stresses were measured ranging from 150 to 250 mpa using the turner dynamic analysis technique however it is clear that shear stresses resolved parallel to the fault planes were very low the attainment of high stress differences when the resistance to faulting was low is attributed either to bending forces induced during the motion of the non planar surfaces relative to each other or to the stress peak being attained prior to the localization of deformation onto the fault surfaces

the influence of grain boundary fluids on the microstructure of quartz feldspar mylonites quartz rich domains in pre alpine water deficient amphibolite facies 510 580 c 250 450 mpa pegmatite mylonites from mont mary mm western alps preserve a fine dynamically recrystallized grain size without significant annealing despite the high synkinematic temperatures and subsequent static greenschist facies alpine overprint the microstructure is dramatically different from more typical water rich amphibolite facies mylonites such as from the simplon fault zone in the central alps where the recrystallized grain size is on the millimetre scale the difference reflects the dominant strain induced recrystallization mechanism 1 progressive subgrain rotation and grain boundary bulging for the dry mm examples and 2 fast grain boundary migration for the wet simplon examples the grain boundary microstructure imaged with sem is also very different with most grain boundaries in the dry mm samples lacking porosity whereas grain boundaries in the wet samples are decorated by a multitude of pores quartz grain boundaries from both wet and dry samples are locally coated by thin 100 s of nanometres possibly amorphous silica films despite the differences in microstructure the crystallographic preferred orientations cpos of quartz rich domains from both areas are very similar water deficient conditions hinder grain boundary mobility and thereby modify the dominant recrystallization mechanism s but apparently have little influence on the intracrystalline slip systems as reflected in the cpos strong c axis y maxima in mm mylonites both k feldspar and plagioclase an33 38 dynamically recrystallize consistent with the inferred metamorphic conditions under water deficient conditions mid to lower crustal rocks can deform heterogeneously under transitional ductile brittle conditions at high differential stress for mm ca 300 500 mpa as estimated for dry mohr coulomb failure and preserve this high stress microstructure because of the low mobility of dry grain boundaries

deformation mechanisms and rheology why marble is weaker than quartzite when deformed together in nature calcite rocks invariably appear weaker and more ductile than quartz rocks this can be reconciled with experimental flow data only by taking into account grain size sensitive gss flow in calcite rocks which is predicted to dominate even at grain sizes on the order of 1mm at middle metamorphic grades using new experimental data that demonstrate the transition between intracrystalline plastic and gss flow of quartz rocks we predict that unnaturally small grain sizes at temperatures of 700 c or higher are required for gss flow of quartz in nature thus natural flow of quartzite is expected to occur by intracrystalline plastic processes even after recrystallization to a fine grain size

experimental observations on the effect of interface slip on rotation and stabilisation of rigid particles in simple shear and a comparison with natural mylonites for axial ratios r not vert similar3 porphyroclasts from three mylonites all show a very strong spo with the long axis of the best fit ellipse at an antithetic angle of 5 10 to the shear direction this is more consistent with a stable end orientation than with the transient fabrics predicted by theory for elliptical rigid particles in simple shear the cause of this divergence is investigated in a series of high simple shear strain 15 analogue experiments performed in a ring shear machine couette flow using a linear viscous matrix pdms the rotational behaviour of elongate r not vert similar5 rigid particles with elliptical and rhomboidal shapes comparable with the natural examples is modelled for both coherent and slipping particle matrix interfaces interface slip causes a dramatic reduction in the rotation rate of the elliptical particle compared with theory when the long axis is close to the shear direction but not stabilisation interface slip does result in stabilisation of the rhomboidal particle with the long diagonal oriented at a small antithetic angle to the shear direction for monoclinic particles mirror image shapes referred to here as types 1 and 2 show different rotational behaviour for the type 1 particle with a shape comparable to porphyroclast systems and mica fish the long side rotates asymptotically into parallelism with the shear direction natural examples of type 1 particles such as hornblende and olivine porphyroclasts measured from the finero mylonites southern alps show a very strong preferred orientation for r not vert similar3 with the long side parallel or at a small 5 antithetic angle to the mylonitic foliation for type 2 particles the short side stabilises close to the shear direction or at a small synthetic angle as also observed for sillimanite porphyroclasts from the mont mary mylonites western alps in this natural case stabilisation of the short sides is against an extensional crenulation cleavage rather than the mylonitic foliation the analogue experiments establish that interface slip is one mechanism for stabilisation of elongate rhomboidal particles in natural examples decoupling from the matrix may be affected by extensional crenulation cleavage or c planes in s c fabrics

the recrystallized grain size piezometer for quartz d 1 0 3 56 0 27 s 1 26 0 13 with no change in slope at the regime 2 3 transition and no effect of temperature or a b stability field another experimental piezometer relation for regime 1 of hirth and tullis 1992 differs in slope suggesting that different recrystallization mechanisms require different piezometer calibrations index terms 3902 mineral physics creep and deformation 5120 physical properties of rocks plasticity diffusion and creep 8030 structural geology microstructures 8159 tectonophysics rheology crust and lithosphere 8164 tectonophysics stresses crust and lithosphere citation stipp m and j tullis the recrystallized grain size piezometer for quartz geophys res lett 30 21 2088 doi 10 1029 2003gl018444 2003

why calcite can be stronger than quartz 1 in the neves area eastern alps calcite forms asymmetric centimeter scale single crystal porphyroclasts in quartz mylonites developed during hydrous amphibolite facies metamorphism at 550 c under these conditions coarse calcite was clearly stronger than the surrounding polycrystalline dynamically recrystallized quartz matrix experimental results indicate that coarse calcite is less strain rate sensitive than wet quartzite consistent with an inversion in strength on extrapolation to natural strain rates for this to occur wet quartzite must be weak flowing at differential stress of 10 mpa the lack of high temperature twins showing bulging or recrystallization in calcite clasts is consistent with such low stresses during shear zone development under near peak metamorphic conditions the maximum effective viscosity ratio of coarse calcite to quartzite for these conditions is probably not large 10 however numerical modeling shows that ratios of around 2 are sufficient to maintain near rigid calcite clast behavior for power law rheology with stress exponents appropriate to quartz n 3 4 and coarse calcite n 6 the inversion in relative strength reflects the difference in influence of water on the crystal plastic flow of calcite and quartz water has a dramatic effect for quartz but little or no effect for calcite quartz rich rocks under hydrous amphibolite facies conditions in the middle to lower crust are therefore relatively weak in fact weaker than coarse calcite and flow at much lower stresses than dry quartz rich rocks at similar crustal levels

critical re evaluation of differential stress estimates from calcite twins in coarse grained limestone abstract comparison of two techniques to estimate differential stress magnitude based on calcite twinning reveals significantly different calculated values of differential stress for limestone experimentally and naturally deformed at low temperature this inequality may be due to fundamental differences between the rock type marble versus limestone and deformation temperatures above and below 200 c for samples used in technique calibration versus samples used in testing and application a technique that was empirically derived from marble experimentally deformed at 200 800 c yields values of differential stress that are factors of 2 to 9 times larger than maximum differential stress measured during experimental deformation of limestone at low temperature

alpine metamorphism and veining in the zentralgneis complex of the sw tauern window a model of fluid rock interactions based on fluid inclusions abstract the granitic to tonalitic gneisses of the zentralgneis complex in the sw tauern window contain numerous discordant quartz biotite plagioclase veins occurring either as isolated or in parallel sets with a preferential orientation perpendicular to the main foliation of host rocks veins show a zonal distribution of minerals with plagioclase and biotite at the walls and quartz in the centre quartz contains abundant fluid inclusions fi mostly occurring along secondary planes all primary and most secondary inclusions three phase h2o co2 inclusions formed from a dominant fluid type of aqueous carbonic composition fi have been characterized by microthermometry laser raman and laser ablation optical emission spectroscopies which have confirmed their similarity also with respect to composition and density fluids display a somewhat unusual composition especially a wide range of rather high salinities 3 7 mol deduced from the final melting temperature of clathrate which covers a wide range from 4 2 to 4 0 c the volatile phase is dominated by co2 3 12 mol with small amounts of n2 the final homogenization temperature of these inclusions is generally 300 c but independently constrained trapping temperatures of 550 600 c yield to pressure estimates of 3 5 7 5 kbar highest pressures are in agreement with the p t conditions reached during the tauern metamorphism peak veining was triggered by hydrofracturing induced by pl bt producing devolatilization and probably decarbonation reactions in the adjacent gneisses and quartz precipitated in response to the significant pressure and or salinity fluctuations shown by fi during each microfracturing healing stage

experimental intracrystalline plastic flow in hot pressed synthetic quartzite prepared from brazilian quartz crystals samples of synthetic ultrafine grained quartzite were prepared by hot pressing aggregates of crushed clear brazilian quartz of mean grain size 0 4 m at 300 mpa and 1373 and 1473 k the samples displayed rapid grain growth to ca 12 20 m with 2 porosity at 1473 k facilitated by the 0 6 wt of water adsorbed onto the grain boundaries during sample preparation this water could be driven off by preheating thereby preventing grain growth sufficient water was incorporated during growth into the coarsened samples to render them weak and ductile these were deformed experimentally in the quartz field using an argon gas medium apparatus at 300 mpa confining pressure at temperatures mainly between t 1273 and 1473 k ductile flow was described by the flow law 10 4 9 3 2 9 7 f h 2 o exp 242000 rt with stress a in mpa and grain size d in microns and strain rate in s 1 r is the gas constant and f h 2 o is water fugacity based on observation of grain flattening optical strain features shapes and densities of dislocation arrays and flow law parameters samples deformed dominantly by dislocation creep with some contribution from grain boundary sliding bearing in mind possible changes in the flow law parameters over the extrapolation interval and possible effects of the phase transition extrapolation to natural strain rates and temperatures predicts plastic flow at higher flow stresses at the same water fugacity at greenschist facies temperatures than previously published flow laws

preboreal oscillation caused by a glacial lake agassiz flood the preboreal oscillation pbo has been attributed to increased meltwater but the source of the meltwater and causative mechanism of the pbo has remained elusive here we attribute the source to a massive meltwater discharge event from an abrupt drainage of glacial lake agassiz canada via the mackenzie river into the arctic ocean a maximum volume of 21 000 km 3 was discharged over a 1 5 3 yr period with a peakdischarge of 0 500 sverdrups sv equivalent to a 6 m rise in the arctic ocean or 0 062 m rise in global sea level the flood occurred at about 11 335 cal yr bp and was followed by a b0 042 sv flow until 10 750 cal yr bp when the southern outlet of lake agassiz reopened and diverted drainage to the mississippi river system we estimate that only 2 4 of the flood water would have frozen into sea ice within the beaufort region but coupled with increased river ice production during winter and thicker pack ice growth throughout the arctic ocean a thicker longer lasting and more extensive packice may have been flushed through fram strait the thicker and more extensive packice and freshened sea surface may have triggered the pbo by increasing albedo and generating a low salinity anomaly upon melting in the north atlantic thus decreasing the formation of north atlantic deep water r 2002 elsevier science ltd all rights reserved

rheological and microstructural evolution of carrara marble with high shear strain results from high temperature torsion experiments abstract this study investigated the rheological and microstructural evolution of carrara marble deformed to large shear strain to understand how dynamic recrystallization and lattice preferred orientation lpo are related to strain softening processes solid cylinders of carrara marble were deformed in torsion up to a shear strain of 11 at constant twist rates which correspond to a shear strain rate of 3 10 4 s 1 at the outer surface and at temperatures of 1000 and 1200 k 727 and 927 c respectively for the initial grain size of 150 m these conditions are within the dislocation creep regime substantial changes in both rheology and microstructure were observed as the marble deformed to high shear strain at 1000 k 1200 k a peak stress was reached at about 1 0 5 followed by moderate strain weakening an apparent steady state flow stress was obtained at high shear strain of 5 2 the stress exponent n decreased slowly with strain from 10 1 to 6 9 at 1000 k but it remained approximately constant at 1200 k n around 10 at the maximum reached shear strain of 11 8 5 the marble had almost completely recrystallized to a fine grain size of about 10 m 20 m a secondary foliation developed in the recrystallized matrix which is at a large oblique angle to the shear zone boundary szb lpo was measured by electron backscatter diffraction ebsd for both temperatures the lpo evolved from an oblique deformation texture to a very sharp and symmetric single orientation component with r 1014 parallel to the shear plane and a 1210 parallel to the shear direction it is concluded that strain weakening was associated with the development of a strong lpo during dynamic recrystallization to a finer grain size mechanical and microstructural steady state is only reached at large shear strain the steady state lattice and grain shape fabrics can hardly be used as shear sense indicators in such recrystallized calcite mylonites