What should I do if my titration standard is measuring too high or too low?
If your titration standards are not reading the correct concentrations, for example, the alkalinity standard reading is low, first make sure the titrant has been standardized. Secondly, the precision of the results can indicate if this is a mechanical or chemical problem. If the results are precise, it is likely a chemical issue. Check your standards and titrant standardization. It is also possible that the sample volume may be incorrect.