From: mtymp15@staff.tc.umn.edu (David Hutton)
Newsgroups: alt.drugs
Subject: New posting: DMT FAQ
Summary: from LearyBot@irc
Date: 15 Nov 92 19:55:19 GMT
Organization: University of Minnesota



 
 
                         How To Make DMT
 
DMT stands for N,N-dimethyltryptamine. It is a semisynthetic 
compound similar to psilocin(the hallucinogenic substance in 
psilocybin) ins structure. The most common method of ingestion is 
smoking. Soaked parsley leaves are the usual method of ingestion 
although persons have dipped marijuana in it and said the 
experience was fantastic. The following recipe can be performed in 
the kitchen.
 
Recipe for DMT:

Mix thoroughly and dissolve 25 grams of indole with a pound of 
dry ethyl ether in a 2000 ml flask(2 quart jar.)
 
2. Take an ice tray and fill with chipped or shaved ice. Cool 
solution for about 35 minutes until it reaches 0 degrees C. At the 
same time cool 50 ml dry oxalychloride to about 5 degrees below 0 
C. in the same ice tray.
 
3. VERY slowly add the oxalychloride solution to the indole 
solution. These two chemicals are highly reactive. Avoid boiling 
over, contact with skin, and fumes.
 
4. Wait until all the bubbling has died down, then add a few 
handfuls of table salt to the ice tray, to cool the solution 
further. Label the solution "solution 1" and put it in the 
freezer.
 
5. Cool 100 ml. of dry ethyl ether in a 500 ml. flask to 0 degrees 
C. in a salted ice tray. At the same time cool an unopened bottle 
of dimethylamine to 0 degrees C. in the same ice bath.
 
6. Open the seal of the dimethylamine bottle and slowly pour a 
steady stream into the ether. Label "solution 2."
 
7. Very slowly and carefully add solution "1" and "2" together.
 
8. Now take the mixed solutions from the ice tray and bring up to 
room temperature stirring the solution all the time. You should be 
left with a solution that is almost clear. If it is still murky, 
continue stirring until it becomes as clear as possible.
 
9. Now filter the solution to seperate the precipitate by suction.
 
                       <---Solution and Precipitate
        ------------
        \          /<---Funnel  /    / <-- Rubber hose to
         \        /     and    /    /      Vacuum source
          \      /      Filter/____/
     \*****\    /*************{   }*****/ <--- Two hole
      \****{    }*************{   }****/       rubber stopper
       \   {    }             {   } <-/--- Glass Tube
        \  {    }             {   }  /
         | {    }             {   } |
         |                          |
         |                          |
         |                          |
         |                          |
         |__________________________|
                  Figure A.
            
10. Refilter with suction after pouring technical ether over the 
precipitate.
 
11. Repeat filtering once more with ether, then twice with water.
 
12. Let this substance dry on a plastic or china plate.(do not use 
metal) After drying, a solid material will be formed. Take 
particles and place them in an 800 ml beaker.
 
13. Mix 100 ml. benzene with 100 ml. methyl alcohol. After this 
mixture has been stirred, cover solid particles from step 12 with 
about 1/2 inch of the solution and heat the beaker in water until 
all solid material had dissolved. Add more solvent if 
necessary.(Note: Do not place beaker in water bath directly over 
the flame.)
 
14. After all solid material has dissolved, remove beaker from the 
heat, and allow to cool. As it cools, small needle-shaped crystals 
will appear. When this happens, try to pour off as much solvent as 
possible without disturbing the crystals.
 
15. Place crystals in a 1000 ml flask and dissolve in 
tetrahydrofurane.(Use only as much as absolutely necessary.) Label 
this solution "A".
 
16. Slowly mix 200 ml. tetrahydrofurane and 20 grams lithium 
aluminum hydride in a 500 ml flask, and label it solution "B".
(By the way, lithuim aluminum hydride ignites on contact with 
moisture. Protect eyes and hands.)
 
17. Mix solutions "A" and "B" slowly, stirring constantly.
 
18. Prepare a water bath and heat solution for three hours, 
stirring for four minutes every half hour. When not stirring, make 
sure to use aspirator tube.
                             /  / <--- Rubber Tubing
                             ---
                         \**{   }**/<---- One hole rubber stopper      
                         /**{   }**\      and glass tubing 
                        /   {   }   \
                       /    {   }    \
                       :             : 
                       :             :        
                       :             :
      \ ~~~~~~~~~~~~~~~:_____________:~/
       \______________________________/
 
           Heat source
 
           Figure B.
 
Place Figure B. flask at a higher level than Figure A. flask. Run 
tube from Figure B. flask down to left side of figure A. flask, 
replacing funnel with glass tubing. Disconnect right side tube 
from vacuum source. This will be used as the aspirator tube.
 
19. When this is completed, allow the flask to remain at room 
temperature for about 20 minutes. Then place in salted ice bath, 
and cool to 0 degrees C. Add a small amount of chilled methanol, 
stirring gently until solution appears murky.
 
20. Filter this murky solution through a paper filter in a funnel, 
and collect the filtered liquid in a flask.
 
21. Add 100 ml. of tetrahydrofuran through the filter and collect 
in the same flask. Now heat the solution in a water bath until 
most of the tetrahydrofuran is evaporated and a gooey substance 
remains.
 
22. Place little piles of this substance on a cookie tray and dry 
with a heat lamp for three or four hours.
 
Well, after all that you now have DMT. Was it worth it? To ingest, 
crumble a small quantity with parsley or mint, and smoke. Do not 
inject. Do not mix with tobacco.
 
 
                     Keep your thoughts free
                      and your reality...err
                            different.
 
                          - Black Adder
 

-- 
send flames, comments, questions, pap smear results, $10,000 in small bills, and
a large packet of neurotransmitter precursors to :  mtymp15@staff.tc.umn.edu
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