FrancophonIA/DGT-Translation_Memory huggingface dataset:
English: Dry and spray with 2,6-dichloro-4-(caloroimino)cyclohexa-2,5-dienone solution (4.18). The quinolin-8-ol becomes visible as a blue spot.
Polish: Wysuszyć i spryskać roztworem 2,6-dichloro-4-(chloroimino)-cykloheksa-2,5-dienonu (4.18). Chinolin-8-ol staje się widoczny w postaci niebieskiej plamy.
English: The first 10 ml of eluate is further treated as described in 6.2.2.4. 6.2.2.4.
Polish: Pierwsze l0 ml eluatu jest następnie poddane postępowaniu opisanemu w ppkt. 6.2.2.4.
English: a = milligrams of quinolin-8-ol on the standard curve
Polish: a = ilość miligramów chinolin-8-olu odczytana z krzywej standardowej
English: Apparatus for sampling of aerosols (transfer bottle, microsyringe connectors, etc.) as described in Chapter II of the Annex to Commission Directive 80/1335/EEC of 22 December 1980
Polish: Aparatura do pobierania próbek aerozoli (butelka do przenoszenia, łączniki do mikrostrzykawek itp.) jak opisano w rozdziale II załącznika do dyrektywy Komisji 80/1335/EWG z dnia 22 grudnia 1980 r.
English: Ethyl acetate (4.2.1.9),
Polish: Octan etylu (4.2.1.9),
English: chloroform (4.2.1.10),
Polish: chloroform (4.2.1.10),
English: diisopropyl ether (4.2.1.11),
Polish: eter diizopropylowy (4.2.1.11),
English: acetic acid (4.2.1.13) (20 : 20 : 10 : 10, by volume).
Polish: kwas octowy (4.2.1.13) (20:20:10:10 objętościowo).
English: Chloroform (4.2.1.10),
Polish: Chloroform (4.2.1.10),
English: acetic acid (4.2.1.13) (90 : 20, by volume).
Polish: kwas octowy (4.2.1.13) (90:20 objętościowo).
English: (see NB)
Polish: (patrz Notabene)
English: Hexachlorophene spots on the thin-layer plate are visualized as indicated under 6.5.1 or 6.5.2. 6.5.1. Spray the visualizing agent I (3.5) evenly on the plate. After 30 minutes examine the plate under UV light at 254 nm.
Polish: Plamy heksachlorofenu na płytce cienkowarstwowej wywołuje się według opisu w ppkt. 6.5.l lub 6.5.2. 6.5.1. Spryskać płytkę równomiernie roztworem wywołującym I (3.5). Po 30 minutach oceniać płytkę w świetle UV przy 254 nm.
English: Visualizing agent I
Polish: Środek wywołujący I
English: Visualizing agent II
Polish: Środek wywołujący II
English: If the yellow colour does not persist, repeat the methylation with a further 200 mg of diazald (4.2)
Polish: Jeśli żółty kolor nie jest trwały, należy powtórzyć metylowanie dodając następną porcję 200 mg diazaldu (4.2)
English: Stock solution. 0,250 mg F-/ml.
French: Solution étalon 0,250 mg fluorure/ml.
Portuguese: Solução padrão de 0,250 mg de fluoreto/ml.
Polish: Roztwór bazowy, 0,250 mg F-/ml
English: Select a dental-cream tube not previously opened, cut open the tube and remove the whole contents. Transfer to a plastics container, mix thoroughly and store under conditions avoiding deterioration.
Polish: Wybrać tubę pasty do zębów uprzednio nieotwieraną, obciąć dolną część tuby i usunąć całą zawartość do plastikowego pojemnika, wymieszać starannie i przechowywać w warunkach zapobiegających pogorszeniu jakości.
Lithuanian: Parenkama anksčiau neatidaryta dantų pastos tūbelė, perpjaunama, išimamas visas jos turinys, kuris įdedamas į plastikinį indą, gerai išmaišomas ir laikomas tokiomis sąlygomis, kad nesugestų.
English: Stationary phase :
Slovak: Stacionárna fáza:
Polish: Faza stacjonarna:
Slovenian: Stacionarna faza:
Romanian: Fază staționară:
Bulgarian: Неподвижна фаза:
English: silicon oil DC 200 or equivalent, 20 %. Condition the column overnight at 100 °C (carrier gas flow at 25 ml nitrogen per minute) and repeat every night.
Polish: olej silikonowy DC 200 lub równoważny, 20 %, kondycjonowanie kolumny przez noc w 100 °C (gaz nośny azot, przepływ 25 ml na minutę) i powtarzane każdej nocy.
English: Separation and identification 4.2.1.
French: Séparation et identification 4.2.1.
Polish: Rozdzielanie i identyfikowanie 4.2.1.
Slovenian: Separacija in kvalitativna določitev 4.2.1
Romanian: Separare și identificare
English: Repeat 5.2.1 and record the reading. If the reading is not zero mineralization was incomplete and analysis must be repeated.
Polish: Powtórzyć postępowanie według ppkt. 5.2.l i zarejestrować odczyt. Jeśli różni się on od zera oznacza to, że mineralizacja nie zaszła całkowicie i analizę należy powtórzyć.
English: This method describes the determination of sulphides present in cosmetic products. The presence of thiols or other reducing agents (including sulphites) does not interfere.
Polish: Metoda opisuje oznaczanie siarczków obecnych w produktach kosmetycznych. Obecność tioli lub innych środków redukujących (łącznie z siarczynami) (IV) nie przeszkadza w oznaczeniu.
English: The entraining apparatus must pass the following leak-tightness test :
Slovak: Aparatúra na uvoľnenie sulfidov musí prejsť nasledujúcim testom tesnosti:
Polish: Aparatura wprowadzająca powinna przejść następujący test szczelności.
Slovenian: Opomba: priprava za pretvorbo mora prestati preskus tesnjenja:
Romanian: Aparatul de antrenare trebuie să treacă de următorul test de etanșeitate:
Bulgarian: Апаратът за засмукване на газа трябва да бъде подложен на следното изпитване за херметичност:
English: simulating the test conditions, replace the product to be determined by 10 ml of a sulphide solution (prepared from 4.4) containing "X mg" of sulphide (iodometrically determined).
Slovak: za rovnakých skúšobných podmienok sa vzorka, ktorá sa má skúšať, sa nahradí 10 ml roztoku sulfidu sodného (pripraveného podľa 4.4) obsahujúceho "X mg" sulfidu (stanoveného jodometricky).
Polish: Symulując warunki testu, zastąpić próbkę wyrobu przeznaczoną do wykonania oznaczenia przez l0 ml roztworu siarczku (przygotowanego jak w 4.4) zawierającego "X mg" siarczku (oznaczonego jodometrycznie).
Slovenian: v simuliranih pogojih reakcije nadomesti vzorec z 10-mililitrsko raztopino sulfida (pripravljeno po 4.4), ki vsebuje X mg' sulfida (določeno z jodometrijo).
Romanian: simulând condițiile de testare, se înlocuiește produsul care urmează să fie determinat în 10 ml soluție de sufură (preparată la 4.4) conținând „x mg" de sulfură (determinată iodometric).
Bulgarian: симулирайки условията на изпитването, предназначеният за анализ продукт се подменя с 10 мл сулфиден разтвор (приготвен от 4.4), съдържащ ”Х мг” сулфид (йодометрично определяне).
English: A2 = the area of the 1,1,1-trichloroethane peak, then:
Estonian: A2 = 1,1,1-trikloroetaani piigi pindala, siis:
English: I : Butan-1-ol (4.11) / acetic acid (4.12) / water (80 : 20 : 20; v/v/v).
Slovenian: I: butan-1-ol (4.11)/ocetna kislina (4.12)/voda (80: 20: 20; v/v/v).
Estonian: I: 1-butanool (4.11)/äädikhape (4.12)/vesi (mahuvahekorras 80:20:20).
Latvian: I: Butān-1-ols (4.11.)/etiķskābe (4.12.)/ūdens (80: 20: 20 v/v/v).
English: m = the mass (in milligrams) of the test portion (6.1) taken, then:
Estonian: m = võetud katsekoguse (6.1) mass milligrammides, siis:
Latvian: m = noteikšanai ņemtā parauga (6.1.) masa (miligramos), tad:
English: Length : 1,5 m. Diameter : 3 mm.
Estonian: Pikkus: 1,5 m. Läbimõõt: 3 mm.
Lithuanian: Ilgis: 1,5 m. Skersmuo: 3 mm.
English: pressure : 2,2 bar, flow : 35 ml/min.
Estonian: rõhk: 2,2 baari, voolukiirus: 35 ml/min.
Lithuanian: slėgis: 2,2 baro, srautas: 35 ml/min.
English: pressure : 1,8 bar, flow : 15 ml/min.
Estonian: rõhk: 1,8 baari, voolukiirus: 15 ml/min.
Lithuanian: slėgis: 1,8 baro, srautas: 15 ml/min.
English: This method relates to the quantitative thin-layer chromatographic determination of tosylchloramide sodium (chloramine-T) in cosmetic products. (1) Norm ISO 5725.
Hungarian: Ez a módszer a tozil-kóramid-nátrium (klóramin-T) vékonyréteg kromatográfiás mennyiségi meghatározását írja le kozmetikai termékekben.
Romanian: Prezenta metodă se referă la determinarea cantitativă prin cromatografie în strat subțire a tosilcloramidei de sodiu (cloramină-T) în produsele cosmetice.
Estonian: Käesolev meetod käsitleb tosüülklooramiidnaatriumi (kloramiin-T) kvantitatiivset määramist kosmeetikatoodetes õhekihikromatograafia (ÕKK) abil.
English: If necessary purify by distillation (5.8). (1) Norm ISO 5725.
Slovak: Ak je to potrebné, prečistí sa destiláciou (5.8).
Slovenian: Če je treba, se očisti z destilacijo (5.8).
Romanian: Dacă este necesar, se purifică prin distilare.
Bulgarian: При необходимост, се пречиства чрез дестилация (5.8).
Estonian: Vajaduse korral puhastatakse destilleerimise teel (5.8).
English: Determination 5.2.1.
Romanian: Determinare
Estonian: Määramine
English: Transfer bottle, 50 to 100 ml (see sampling method 5.3).
Latvian: Pudele šķīduma pārnešanai, 50 līdz 100 ml (skat. paraugu ņemšanas metodi 5.3.).
English: Ma = its mass in the mixture, Aa = its peak area,
Latvian: Ma = tās masa maisījumā, Aa = tās pīķa laukums,
English: For a dichloromethane and/or 1,1,1-trichloroethane content of 25 % (m/m), the difference between the results of two determinations carried out in parallel on the same sample should not exceed an absolute value of 2,5 % (m/m).
Latvian: No viena parauga ar dihlormetāna un/vai 1,1,1-trihloretāna saturu 25 % (m/m) divās paralēlās noteikšanās iegūto rezultātu starpībai nevajadzētu pārsniegt 2,5 % (m/m).
English: The pH of part of the test sample is adjusted to 7.5 and 10l are spotted on the starting line of a pretreated silica gel thin-layer plate (4.23).
Latvian: Analizējamā parauga daļas pH noregulē uz 7,5 un 10 l uznes uz iepriekš apstrādātas silikagēla plānslāņa plates (4.23.) starta līnijas.
English: 10 and 30l of the standard solution (4.15.2) is spotted on two more points of the starting line after which the plate is developed in one of the two eluents (4.17).
Latvian: Standartšķīduma (4.15.2.) 10 un 30 l uznes vēl divos starta līnijas punktos, pēc tam plati attīsta vienā no diviem eluentiem (4.17.).
English: Dissolve the residue in 2 ml of chloroform (4.3) and spot 10 and 30l of the solution obtained on a silica gel, thin-layer plate (4.23) in accordance with the method described in 6.1.1.1 onward.
Latvian: Izšķīdina atlikumu 2 ml hloroforma (4.3.) un 10 un 30 l iegutā šķīduma uznes uz silikagēla plānslāņa plates (4.23.) saskaņā ar metodi, kas aprakstīta 6.1.1.1. un turpmākajos apakšpunktos.
English: Apply 10 and 30l of the standard solution (4.15.2) to the plate and continue as described in 6.1.1.2 to 6.1.1.4.
Latvian: Uz plates uznes 10 un 30 l standartskīduma (4.15.2.) un turpina, kā aprakstīts no 6.1.1.2. līdz 6.1.1.4.
English: Inject about 10 l using the specified microsyringe (5.2.2). Make five injections.
Latvian: Ar minēto mikrošļirci (5.2.2.) ievada apmēram 10 l. Ievada piecas reizes.
English: The (1) OJ No L 383, 31.12.1980, p. 27. prepared combined column must yield a resolution "R" equal to, or better than, 1,5, where:
Romanian: Coloana combinată astfel pregătită trebuie să producă o rezoluție "R" egală cu 1,5 sau superioară, unde:
Latvian: Sagatavotajai kombinētajai kolonnai jānodrošina izšķirtspēja R, kas ir vienāda ar 1,5 vai labāka:
English: Hydrogensulphide, recognizable by its smell, is evolved and a black lead sulphide precipitate forms on the lead di(acetate) paper (4.1.1.1).
Latvian: Rodas hidrogēnsulfīds, ko konstatē pēc smaržas, un uz svina acetāta papīra (4.1.1.1.) veidojas melnas svina sulfīda nogulsnes.
English: Place on the plate 1l of sample solution (4.2.3.1) and one litre of each of the five reference solutions (4.2.1.18).
Latvian: Uznes uz plates 1 l parauga skīduma (4.2.3.1.) un vienu litru katra no pieciem standartšķīdumiem (4.2.1.18.).
English: Then add 5 ml of cadmium di(acetate) solu tion (5.2.2.4).
Latvian: Pēc tam pievieno 5 ml kadmija diacetāta šķīduma (5.2.2.4).
Lithuanian: Tada įpilama 5 ml kadmio diacetato tirpalo (5.2.2.4).
English: Into the methylation apparatus (5.2.3.2) containing 1 ml of ether (5.2.2.11) introduce 50l of solution "S" and methylate by the method (5.2.3.2) with about 300 mg of 1-methyl-3-nitro-1-nitrosoguanidine (5.2.2.8).
Latvian: Metilēšanas iekārtā (5.2.3.2.), kur ir 1 ml ētera (5.2.2.11.), ievada 50 l S šķīduma un metilē pēc metodes (5.2.3.2.) ar 300 mg 1-metil-3-nitro-1-nitrozoguanidīna (5.2.2.8.).
English: Introduce, into a 5 ml stoppered flask, 1 ml of diazomethane solution (5.2.2.12) then 50 l of solution "S".
Latvian: Ievada 5 ml kolbā ar aizbāzni 1 ml diazometāna šķīduma (5.2.2.12.), pēc tam 50 l S šķīduma.
English: 3 l Carry out five injections.
Latvian: 3 l. Ievada piecas reizes.
English: let: kt = its response factor,
French: kt = son coefficient de proportionnalité,
Hungarian: kt = az arányossági tényezője,
Latvian: kt = tās signāla attiecība pret masas vienību,
Lithuanian: kt - jos reaktingumo koeficientas,
English: Eluting solvent :
Slovak: Elučné rozpúšťadlo:
Slovenian: Elucijsko topilo (topilo za elucijo):
Romanian: Solvent de eluție:
Bulgarian: Елюиращ разтворител:
Latvian: Eluents:
English: Benzene containing 1 % (v/v) of glacial acetic acid.
Slovak: benzén obsahujúci 1 % (obj.) ľadovej kyseliny octovej.
Slovenian: benzen, ki vsebuje 1 % (v/v) ocetne kisline.
Romanian: Benzen conținând 1% (v/v) acid acetic glacial.
Bulgarian: Бензол, съдържащ 1% (v/v) ледена оцетна киселина.
Latvian: benzols, kas satur 1 % (v/v) ledus etiķskābes.
English: PREPARA TION OF THE TEST SAMPLE
Latvian: ANALIZĒJAMĀ PARAUGA SAGATAVOŠANA
English: At the same time and in the same manner, apply 8, 12, 16 and 20l of the standard solution of 4-toluenesulphonamide (4.2).
Latvian: Vienlaicīgi tāpat klāj 8, 12, 16 un 20 l 4-toluolsulfonamīda standartšķīduma (4.2.).
English: a = the quantity (in g) of 4-toluenesulphonamide in the sample as read from the calibration curves,
Latvian: a = 4-toluolsulfonamīda daudzums (g) paraugā saskaņā ar kalibrēšanas līknēm,
English: Pipettes, adjustable to deliver volumes of 50 to 200 l, with disposable plastics tips.
Latvian: Pipetes, ko var noregulēt 50 - 200 l tilpuma pārnešanai, ar vienreizējas lietošanas plastmasas uzgaļiem.
English: Centrifuge 10 minutes as such a speed as to produce a clear separation of the phases, uncap the tube, withdraw the organic layer and inject 3l of the organic phase on to the column of the gas chromatograph (5.2).
Latvian: Centrifugē 10 minūtes tādā ātrumā, lai fāzes skaidri atdalās, atskrūvē mēģeni, izņem organisko slāni un ievada 3 l organiskās fāzes gāzu hromatogrāfa (5.2.) kolonnā.
English: Sodium hloride.
Latvian: Nātrija hlorīds.
English: Place some palladium dichloride impregnated glass wool (3.9) between the mercury reduction vessel and the flow cell of the instrument (4.2). Repeat 5.2.1 and record the reading.
Latvian: Ieliek ar palādija dihlorīdu piesūcinātu stikla vati (3.9.) starp dzīvsudraba reducēšanas trauku un kiveti (4.2.).Atkārto 5.2.1. un reģistrē mērījumu.
English: n = the quantity of mercury (in g) read on the instrument.
Latvian: n = izmērītais dzīvsudraba daudzums (g).
English: The entraining apparatus must pass the following leak-tightness test : simulating the test conditions, replace the product to be determined by 10 ml of a sulphide solution (prepared from 4.4) containing "X mg" of sulphide (iodometrically determined).
Latvian: Atdalīšanas iekārtas hermētiskums jāpārbauda šādi: imitējot testa apstākļus, aizstāj nosakāmo kosmētikas līdzekli ar 10 ml sulfīda šķīduma (gatavots no 4.4.), kas satur "X mg" sulfīda (nosaka jodometriski).
English: As examples the following response factors have been obtained (for chloroform : k = 1)
Lithuanian: Pavyzdžiui, buvo gauti tokie reaktingumo koeficientai (chloroformo k = 1):
English: Standard solutions 4.15.1.
Romanian: Soluții standard.
Lithuanian: Etaloniniai tirpalai
English: Proceed as described in
Lithuanian: Toliau laikomasi
English: If "n" represents nitromethane: let:
French: Si n représente le nitrométhane: kn = le facteur de réponse,
Lithuanian: Jeigu nitrometanas pažymimas "n" ir jeigu:
English: If "c" represents the internal standard, chloroform or 2,4-dimathylheptane: let:
French: et si c représente l'étalon interne, chloroforme ou 2,4-diméthylheptane:
Lithuanian: Jeigu vidinė etaloninė medžiaga, chloroformas arba 2,4-dimetilheptanas, pažymima "c" ir jeigu:
English: If "c" represents the internal standard, chloroform or 2,4-dimethylheptane: let:
French: et si c représente l'étalon interne, chloroforme ou 2,4-diméthylheptane:
Lithuanian: Jeigu vidinė etaloninė medžiaga, chloroformas arba 2,4-dimetilheptanas, pažymima "c" ir jeigu:
English: If "c" represents methyl octanoate: let:
French: c = le caprylate de méthyle,
Lithuanian: Jeigu "c" - metiloktanoatas:
English: If "t" represents mercaptoacetic acid: let:
Lithuanian: Jeigu "t" - merkaptoacto rūgštis:
English: Place about 200 mg of diazald (4.2) in the central reservoir, add 1 ml of carbitol (4.5 1c00 ) and 1 ml of diethyl ether (4.3) and dissolve.
Lithuanian: Į centrinę kamerą įdedama apie 200 mg diazaldo (4.2), įpilama 1 ml karbitolio (4.5), 1 ml dietileterio (4.3) ir ištirpinama.
English: At the same time and in th e same manner, apply 8, 12, 16 and 20 ¶l of the standard solution of 4-toluenesulphonamide (4.2).
Lithuanian: Tuo pačiu metu ir tokiu pačiu būdu užlašinama 8, 12, 16 ir 20 l etaloninio 4-toluensulfonamido tirpalo (4.2).
English: Condition the column overnight at 100 °C (carrier gas flow at 25 ml nitrogen per minute)
Lithuanian: Kolonėlė per naktį kondicionuojama 100 °C temperatūroje (stumiančiųjų dujų srautas - 25 ml azoto per minutę);
English: and repeat every night.
Lithuanian: taip kartojama kiekvieną naktį.
English: Place, by pipette, into a series of six centrifuge tubes (5.6), 0, 1, 2, 3, 4 and 5 ml of the diluted fluoride standard s 1c00 olution (4.7.2).
Lithuanian: Į šešis centrifugos mėgintuvėlius (5.6) pipete įpilama 0, 1, 2, 3, 4 ir 5 ml atskiesto etaloninio fluoro tirpalo (4.7.2).
English: DETERMINATIO
Lithuanian: KIEKIO NUSTATYMAS
English: Turn the nitrogen (4.8) stream on again when nearly all the acid has been transferred, leaving a minimum liqu id seal to prevent leakage of hydrogen sulphide.
Lithuanian: Sulašinus beveik visą vandenilio chloridą, vėl paleidžiama azoto (4.8) srovė, paliekant labai mažą izoliuojantį skysčio sluoksnį, kad nenutekėtų vandenilio sulfidas.
English: Whereas Directive 76/768/EEC provides for the official testing of cosmetic products with the aim of ensuring that the conditions laid down by Community provisions concerning the composition of cosmetic products are satisfied; Whereas all the necessary methods of analysis should be laid down as quickly as possible;
French: considérant que la directive 76/768/CEE prévoit des contrôles officiels des produits cosmétiques visant à constater que les conditions prévues par les dispositions communautaires concernant la composition des produits cosmétiques sont respectées;
English: identification and determination of organomercury compounds, (1) OJ No L 262, 27.9.1976, p. 169.
French: l'identification et le dosage des composés organomercuriels, (1) JO no L 262 du 27.9.1976, p. 169.
English: OJ No L 188, 13.7.1983, p. 15.
French: JO no L 188 du 13.7.1983, p. 15.
English: OJ No L 383, 31.12.1980, p. 27.
French: JO no L 383 du 31.12.1980, p. 27.
English: OJ No L 185, 30.6.1982, p. 1.
French: JO no L 185 du 30.6.1982, p. 1.
English: Aa = its peak area, then:
French: Aa = l'aire de son pic,
English: Benzene. In view of its toxicity great care must be taken when working with benzene.
French: Benzène (vu la toxicité du produit, prendre les précautions adéquates).
English: Weigh 100 mg of quinolin-8-ol into a 100 ml standard flask. Dissolve in ethanol (4.10).
French: Placer 100 mg d'hydroxy-8-quinoléine (4.1) dans une fiole jaugée de 100 ml.
Romanian: într-un balon cotat de 100 ml se cântăresc 100 mg 8-chinolinol (4.1).Se dizolvă în etanol (4.10).
English: When the solvent front has advanced 150 mm, the plate is dried at 110 °C (for 15 minutes). Under a UV lamp (366 nm) the quinolin-8-ol spots fluoresce yellow.
French: Lorsque le front du solvant a atteint 15 cm, la plaque est séchée à 110 °C pendant 15 min. Sous lumière UV (366 nm), les taches d'hydroxy-8-quinoléine se caractérisent par une fluorescence jaune.
English: Add 10 ml of Fehling's solution (4.16). Extract the quinolin-8-ol copper complex [oxine copper (ISO)] obtained with three times 8 ml of chloroform (4.3).
French: Après addition de 10 ml de liqueur de Fehling (4.16), extraire le complexe de cuivre formé par trois fois 8 ml de chloroforme (4.3).
English: Use a 10 or 20 ml glass syringe, without needle, adapted to the transfer piece following the technique described in paragraph 5 of Chapter II of the abovementioned Commission Directive. Reweigh to determine the quantity introduced.
French: Utiliser une seringue en verre de 10 ou 20 ml sans aiguille, adaptée à la pièce de transfert selon la technique décrite au paragraphe 5 chapitre II de ladite directive.
English: Inject about 10 ¶l using the specified microsyringe
French: Injecter 10 ¶l environ en utilisant la microseringue
English: Make up to volume with 95 % ethanol
French: Porter au volume au moyen d'éthanol à 95 %
English: The (1) OJ No L 383, 31.12.1980, p. 27. prepared combined column must yield a resolution "R" equal to, or better than, 1,5, where: let:
French: JO no L 383 du 31.12.1980, p. 27. La colonne double ainsi préparée doit donner une résolution R égale ou supérieure à 1,5, étant entendu que:
English: As examples the following two parts yield the required resolution: Column A:
French: À titre d'exemple, les 2 parties suivantes donnent la résolution voulue.
English: Temperature conditions The following have been found suitable:
French: Températures
English: let: kn = its response factor,
French: kn = le facteur de réponse,
English: kn = its response factor, Sn = its peak area.
French: Sn = la surface de son pic,
English: Place a drop of the sample to be analyzed on lead di(acetate) paper
French: Déposer une goutte de l'échantillon à analyser sur du papier au di(acétate) de plomb
English: Characterization of inorganic sulphides by the formulation of hydrogen sulphide on acidification Introduce, into a test tube, a few milligrams of the sample to be studied.
French: Caractérisation des sulfures par formation d'H2S après passage en milieu acide Dans un tube à essais, introduire quelques mg de l'échantillon à étudier.
English: Add 2 ml of distilled water and 1 ml of hydrochloric acid (4.1.1.2). Hydrogen (1) Norm ISO 5725.
French: Ajouter (1) Selon la norme ISO 5725. 2 ml d'eau distillée et 1 ml d'HCl 1 : 1 (4.1.1.2).
English: sulphide, recognizable by its smell, is evolved and a black lead sulphide precipitate forms on the lead di(acetate) paper
French: Il se forme un dégagement d'H2S reconnaissable à son odeur et à la formation du précipité noir de PbS sur un papier au di(acétate) de plomb
English: Apparatus for the preparation of diazomethane for in situ methylation (see Fales, H.M., Jaouni, T.M. and Babashak, J.F., Analyt. Chem.1973, 45, 2302).
French: Appareil pour préparation extemporanée du diazométhane (An. Chem.1973 45, 2302).
English: Introduce, into a 5 ml stoppered flask, 1 ml of diazomethane solution (5.2.2.12) then 50 ¶l of solution "S". Leave in the refrigerator overnight.
French: Dans un flacon bouché de 5 ml, introduire 1 ml de diazométhane (5.2.2.12), puis 50 ¶l de la solution S. Laisser dans un réfrigérateur pendant une nuit.
English: let: kt its response factor,
French: kt = son coefficient de proportionnalité,
Hungarian: kt = az arányossági tényezője,
English: Cool, finely powder the residue and transfer to a glass column. (1) Because of the wide range of product types in which hexachlorophene could be present, it is important to first check recovery of hexachlorophene from the sample by this procedure before recording results.
French: Refroidir, réduire en poudre fine (1) Du fait de la grande variété de produits dans lesquels l'hexachlorophène peut être présent, il est important de vérifier d'abord la récupération de l'hexachlorophène de l'échantillon par ce procédé avant d'enregistrer les résultats.
English: Cool all reagents and apparatus to between 0 and 4 °C for two hours. Into the external compartment of the diazomethane apparatus place 1,2 ml of the solution obtained in 6.2 and 0,1 ml of methanol (4.4).
French: Faire refroidir tous les réactifs et l'appareillage entre 0 °C et 4 °C pendant 2 h. Placer 1,2 ml de la solution obtenue en 6.2 et 0,1 ml de méthanol (4.4) dans le compartiment externe de l'appareil à diazométhane.
English: Support: chromosorb : WAW sieve analysis : 80 to 100 mesh. Stationary phase : 10 % OV 17.
French: Remplissage : 10 % OV 17 sur chromosorb WAW 80 à 100 mesh.