###############################################################################
 ### ARP/wARP Program Suite: ARP Ver. 6.1  08 Jul 2004 V.Lamzin & A.Perrakis ###
 ############ Copyright 1998 European Molecular Biology Laboratory #############
 ###############################################################################

 User: phzwart  Run date and time: Thu Nov 23 20:42:24 2006

    0.00 CPU        0 Elapsed  
 Data line --  MODE WILSON NRES 40

 Required keywords:
 FILES        CCP4 file_names
 RESOLUTION   resmin resmax
 LABELS       input labels for FP SIGFP FUSE [FOMUSE]
 END (must be the last keyword)

 Data line --  FILES CCP4 HKLIN arp_46.mtz
 Data line --  RESOLUTION   20.0 2.3
 Data line --  LABELS     FP=FP SIGFP=SIGFP FUSE=2FOFCWT
 Data line --  END

 Comments:  Wilson plot will be examined using FP and SIGFP
 Comments:    within resolution range  20.00  2.30
 Comments:  Map scale will be derived using FUSE

 Comments:  Number of residues in the asymmetric unit                40
 Comments:  Number of protein atoms in the asymmetric unit          312
 Comments:  Total number of atoms expected in the asymmetric unit   355

  (Q)QOPEN: file opened on unit  1      Status: READONLY
<B><FONT COLOR="#FF0000"><!--SUMMARY_BEGIN-->
 Logical Name: arp_46.mtz      Filename: arp_46.mtz
<!--SUMMARY_END--></FONT></B>


 Header information in the file arp_46.mtz                                                                                                                                                                                                                                                                                                                                                                                                      
 Number of columns         12
 Number of reflections   1891
 Cell parameters       76.748  76.748  76.748  90.000  90.000  90.000
 Resolution range       19.19    2.30
 Label in the file                    H
 Label in the file                    K
 Label in the file                    L
 Label in the file                   FP
 Label in the file                SIGFP
 Label in the file                   FC
 Label in the file                 PHIC
 Label in the file              2FOFCWT
 Label in the file            PH2FOFCWT
 Label in the file               FOFCWT
 Label in the file             PHFOFCWT
 Label in the file                  FOM
 Cell parameters       76.748  76.748  76.748  90.000  90.000  90.000
 Cell parameters       76.748  76.748  76.748  90.000  90.000  90.000


   Space group number        211     I432      
   No of symmetry operators   48

   1 symmetry matrix (identity matrix) and translation vector:
   1.000   0.000   0.000       0.000
   0.000   1.000   0.000       0.000
   0.000   0.000   1.000       0.000

   2 symmetry matrix (2-fold rotation) and translation vector:
  -1.000   0.000   0.000       0.000
   0.000  -1.000   0.000       0.000
   0.000   0.000   1.000       0.000

   3 symmetry matrix (2-fold rotation) and translation vector:
  -1.000   0.000   0.000       0.000
   0.000   1.000   0.000       0.000
   0.000   0.000  -1.000       0.000

   4 symmetry matrix (2-fold rotation) and translation vector:
   1.000   0.000   0.000       0.000
   0.000  -1.000   0.000       0.000
   0.000   0.000  -1.000       0.000

   5 symmetry matrix (3-fold rotation) and translation vector:
   0.000   0.000   1.000       0.000
   1.000   0.000   0.000       0.000
   0.000   1.000   0.000       0.000

   6 symmetry matrix (3-fold rotation) and translation vector:
   0.000   0.000   1.000       0.000
  -1.000   0.000   0.000       0.000
   0.000  -1.000   0.000       0.000

   7 symmetry matrix (3-fold rotation) and translation vector:
   0.000   0.000  -1.000       0.000
  -1.000   0.000   0.000       0.000
   0.000   1.000   0.000       0.000

   8 symmetry matrix (3-fold rotation) and translation vector:
   0.000   0.000  -1.000       0.000
   1.000   0.000   0.000       0.000
   0.000  -1.000   0.000       0.000

   9 symmetry matrix (3-fold rotation) and translation vector:
   0.000   1.000   0.000       0.000
   0.000   0.000   1.000       0.000
   1.000   0.000   0.000       0.000

  10 symmetry matrix (3-fold rotation) and translation vector:
   0.000  -1.000   0.000       0.000
   0.000   0.000   1.000       0.000
  -1.000   0.000   0.000       0.000

  11 symmetry matrix (3-fold rotation) and translation vector:
   0.000   1.000   0.000       0.000
   0.000   0.000  -1.000       0.000
  -1.000   0.000   0.000       0.000

  12 symmetry matrix (3-fold rotation) and translation vector:
   0.000  -1.000   0.000       0.000
   0.000   0.000  -1.000       0.000
   1.000   0.000   0.000       0.000

  13 symmetry matrix (2-fold rotation) and translation vector:
   0.000   1.000   0.000       0.000
   1.000   0.000   0.000       0.000
   0.000   0.000  -1.000       0.000

  14 symmetry matrix (2-fold rotation) and translation vector:
   0.000  -1.000   0.000       0.000
  -1.000   0.000   0.000       0.000
   0.000   0.000  -1.000       0.000

  15 symmetry matrix (4-fold rotation) and translation vector:
   0.000   1.000   0.000       0.000
  -1.000   0.000   0.000       0.000
   0.000   0.000   1.000       0.000

  16 symmetry matrix (4-fold rotation) and translation vector:
   0.000  -1.000   0.000       0.000
   1.000   0.000   0.000       0.000
   0.000   0.000   1.000       0.000

  17 symmetry matrix (4-fold rotation) and translation vector:
   1.000   0.000   0.000       0.000
   0.000   0.000   1.000       0.000
   0.000  -1.000   0.000       0.000

  18 symmetry matrix (2-fold rotation) and translation vector:
  -1.000   0.000   0.000       0.000
   0.000   0.000   1.000       0.000
   0.000   1.000   0.000       0.000

  19 symmetry matrix (2-fold rotation) and translation vector:
  -1.000   0.000   0.000       0.000
   0.000   0.000  -1.000       0.000
   0.000  -1.000   0.000       0.000

  20 symmetry matrix (4-fold rotation) and translation vector:
   1.000   0.000   0.000       0.000
   0.000   0.000  -1.000       0.000
   0.000   1.000   0.000       0.000

  21 symmetry matrix (4-fold rotation) and translation vector:
   0.000   0.000   1.000       0.000
   0.000   1.000   0.000       0.000
  -1.000   0.000   0.000       0.000

  22 symmetry matrix (2-fold rotation) and translation vector:
   0.000   0.000   1.000       0.000
   0.000  -1.000   0.000       0.000
   1.000   0.000   0.000       0.000

  23 symmetry matrix (4-fold rotation) and translation vector:
   0.000   0.000  -1.000       0.000
   0.000   1.000   0.000       0.000
   1.000   0.000   0.000       0.000

  24 symmetry matrix (2-fold rotation) and translation vector:
   0.000   0.000  -1.000       0.000
   0.000  -1.000   0.000       0.000
  -1.000   0.000   0.000       0.000

  25 symmetry matrix (identity matrix) and translation vector:
   1.000   0.000   0.000       0.500
   0.000   1.000   0.000       0.500
   0.000   0.000   1.000       0.500

  26 symmetry matrix (2-fold rotation) and translation vector:
  -1.000   0.000   0.000       0.500
   0.000  -1.000   0.000       0.500
   0.000   0.000   1.000       0.500

  27 symmetry matrix (2-fold rotation) and translation vector:
  -1.000   0.000   0.000       0.500
   0.000   1.000   0.000       0.500
   0.000   0.000  -1.000       0.500

  28 symmetry matrix (2-fold rotation) and translation vector:
   1.000   0.000   0.000       0.500
   0.000  -1.000   0.000       0.500
   0.000   0.000  -1.000       0.500

  29 symmetry matrix (3-fold rotation) and translation vector:
   0.000   0.000   1.000       0.500
   1.000   0.000   0.000       0.500
   0.000   1.000   0.000       0.500

  30 symmetry matrix (3-fold rotation) and translation vector:
   0.000   0.000   1.000       0.500
  -1.000   0.000   0.000       0.500
   0.000  -1.000   0.000       0.500

  31 symmetry matrix (3-fold rotation) and translation vector:
   0.000   0.000  -1.000       0.500
  -1.000   0.000   0.000       0.500
   0.000   1.000   0.000       0.500

  32 symmetry matrix (3-fold rotation) and translation vector:
   0.000   0.000  -1.000       0.500
   1.000   0.000   0.000       0.500
   0.000  -1.000   0.000       0.500

  33 symmetry matrix (3-fold rotation) and translation vector:
   0.000   1.000   0.000       0.500
   0.000   0.000   1.000       0.500
   1.000   0.000   0.000       0.500

  34 symmetry matrix (3-fold rotation) and translation vector:
   0.000  -1.000   0.000       0.500
   0.000   0.000   1.000       0.500
  -1.000   0.000   0.000       0.500

  35 symmetry matrix (3-fold rotation) and translation vector:
   0.000   1.000   0.000       0.500
   0.000   0.000  -1.000       0.500
  -1.000   0.000   0.000       0.500

  36 symmetry matrix (3-fold rotation) and translation vector:
   0.000  -1.000   0.000       0.500
   0.000   0.000  -1.000       0.500
   1.000   0.000   0.000       0.500

  37 symmetry matrix (2-fold rotation) and translation vector:
   0.000   1.000   0.000       0.500
   1.000   0.000   0.000       0.500
   0.000   0.000  -1.000       0.500

  38 symmetry matrix (2-fold rotation) and translation vector:
   0.000  -1.000   0.000       0.500
  -1.000   0.000   0.000       0.500
   0.000   0.000  -1.000       0.500

  39 symmetry matrix (4-fold rotation) and translation vector:
   0.000   1.000   0.000       0.500
  -1.000   0.000   0.000       0.500
   0.000   0.000   1.000       0.500

  40 symmetry matrix (4-fold rotation) and translation vector:
   0.000  -1.000   0.000       0.500
   1.000   0.000   0.000       0.500
   0.000   0.000   1.000       0.500

  41 symmetry matrix (4-fold rotation) and translation vector:
   1.000   0.000   0.000       0.500
   0.000   0.000   1.000       0.500
   0.000  -1.000   0.000       0.500

  42 symmetry matrix (2-fold rotation) and translation vector:
  -1.000   0.000   0.000       0.500
   0.000   0.000   1.000       0.500
   0.000   1.000   0.000       0.500

  43 symmetry matrix (2-fold rotation) and translation vector:
  -1.000   0.000   0.000       0.500
   0.000   0.000  -1.000       0.500
   0.000  -1.000   0.000       0.500

  44 symmetry matrix (4-fold rotation) and translation vector:
   1.000   0.000   0.000       0.500
   0.000   0.000  -1.000       0.500
   0.000   1.000   0.000       0.500

  45 symmetry matrix (4-fold rotation) and translation vector:
   0.000   0.000   1.000       0.500
   0.000   1.000   0.000       0.500
  -1.000   0.000   0.000       0.500

  46 symmetry matrix (2-fold rotation) and translation vector:
   0.000   0.000   1.000       0.500
   0.000  -1.000   0.000       0.500
   1.000   0.000   0.000       0.500

  47 symmetry matrix (4-fold rotation) and translation vector:
   0.000   0.000  -1.000       0.500
   0.000   1.000   0.000       0.500
   1.000   0.000   0.000       0.500

  48 symmetry matrix (2-fold rotation) and translation vector:
   0.000   0.000  -1.000       0.500
   0.000  -1.000   0.000       0.500
  -1.000   0.000   0.000       0.500

 Inverse symmetry   1.000   0.000   0.000   0.000
 Inverse symmetry   0.000   1.000   0.000   0.000
 Inverse symmetry   0.000   0.000   1.000   0.000

 Inverse symmetry  -1.000   0.000   0.000   0.000
 Inverse symmetry   0.000  -1.000   0.000   0.000
 Inverse symmetry   0.000   0.000   1.000   0.000

 Inverse symmetry  -1.000   0.000   0.000   0.000
 Inverse symmetry   0.000   1.000   0.000   0.000
 Inverse symmetry   0.000   0.000  -1.000   0.000

 Inverse symmetry   1.000   0.000   0.000   0.000
 Inverse symmetry   0.000  -1.000   0.000   0.000
 Inverse symmetry   0.000   0.000  -1.000   0.000

 Inverse symmetry   0.000   1.000   0.000   0.000
 Inverse symmetry   0.000   0.000   1.000   0.000
 Inverse symmetry   1.000   0.000   0.000   0.000

 Inverse symmetry   0.000  -1.000   0.000   0.000
 Inverse symmetry   0.000   0.000  -1.000   0.000
 Inverse symmetry   1.000   0.000   0.000   0.000

 Inverse symmetry   0.000  -1.000   0.000   0.000
 Inverse symmetry   0.000   0.000   1.000   0.000
 Inverse symmetry  -1.000   0.000   0.000   0.000

 Inverse symmetry   0.000   1.000   0.000   0.000
 Inverse symmetry   0.000   0.000  -1.000   0.000
 Inverse symmetry  -1.000   0.000   0.000   0.000

 Inverse symmetry   0.000   0.000   1.000   0.000
 Inverse symmetry   1.000   0.000   0.000   0.000
 Inverse symmetry   0.000   1.000   0.000   0.000

 Inverse symmetry   0.000   0.000  -1.000   0.000
 Inverse symmetry  -1.000   0.000   0.000   0.000
 Inverse symmetry   0.000   1.000   0.000   0.000

 Inverse symmetry   0.000   0.000  -1.000   0.000
 Inverse symmetry   1.000   0.000   0.000   0.000
 Inverse symmetry   0.000  -1.000   0.000   0.000

 Inverse symmetry   0.000   0.000   1.000   0.000
 Inverse symmetry  -1.000   0.000   0.000   0.000
 Inverse symmetry   0.000  -1.000   0.000   0.000

 Inverse symmetry   0.000   1.000   0.000   0.000
 Inverse symmetry   1.000   0.000   0.000   0.000
 Inverse symmetry   0.000   0.000  -1.000   0.000

 Inverse symmetry   0.000  -1.000   0.000   0.000
 Inverse symmetry  -1.000   0.000   0.000   0.000
 Inverse symmetry   0.000   0.000  -1.000   0.000

 Inverse symmetry   0.000  -1.000   0.000   0.000
 Inverse symmetry   1.000   0.000   0.000   0.000
 Inverse symmetry   0.000   0.000   1.000   0.000

 Inverse symmetry   0.000   1.000   0.000   0.000
 Inverse symmetry  -1.000   0.000   0.000   0.000
 Inverse symmetry   0.000   0.000   1.000   0.000

 Inverse symmetry   1.000   0.000   0.000   0.000
 Inverse symmetry   0.000   0.000  -1.000   0.000
 Inverse symmetry   0.000   1.000   0.000   0.000

 Inverse symmetry  -1.000   0.000   0.000   0.000
 Inverse symmetry   0.000   0.000   1.000   0.000
 Inverse symmetry   0.000   1.000   0.000   0.000

 Inverse symmetry  -1.000   0.000   0.000   0.000
 Inverse symmetry   0.000   0.000  -1.000   0.000
 Inverse symmetry   0.000  -1.000   0.000   0.000

 Inverse symmetry   1.000   0.000   0.000   0.000
 Inverse symmetry   0.000   0.000   1.000   0.000
 Inverse symmetry   0.000  -1.000   0.000   0.000

 Inverse symmetry   0.000   0.000  -1.000   0.000
 Inverse symmetry   0.000   1.000   0.000   0.000
 Inverse symmetry   1.000   0.000   0.000   0.000

 Inverse symmetry   0.000   0.000   1.000   0.000
 Inverse symmetry   0.000  -1.000   0.000   0.000
 Inverse symmetry   1.000   0.000   0.000   0.000

 Inverse symmetry   0.000   0.000   1.000   0.000
 Inverse symmetry   0.000   1.000   0.000   0.000
 Inverse symmetry  -1.000   0.000   0.000   0.000

 Inverse symmetry   0.000   0.000  -1.000   0.000
 Inverse symmetry   0.000  -1.000   0.000   0.000
 Inverse symmetry  -1.000   0.000   0.000   0.000

 Inverse symmetry   1.000   0.000   0.000  -0.500
 Inverse symmetry   0.000   1.000   0.000  -0.500
 Inverse symmetry   0.000   0.000   1.000  -0.500

 Inverse symmetry  -1.000   0.000   0.000   0.500
 Inverse symmetry   0.000  -1.000   0.000   0.500
 Inverse symmetry   0.000   0.000   1.000  -0.500

 Inverse symmetry  -1.000   0.000   0.000   0.500
 Inverse symmetry   0.000   1.000   0.000  -0.500
 Inverse symmetry   0.000   0.000  -1.000   0.500

 Inverse symmetry   1.000   0.000   0.000  -0.500
 Inverse symmetry   0.000  -1.000   0.000   0.500
 Inverse symmetry   0.000   0.000  -1.000   0.500

 Inverse symmetry   0.000   1.000   0.000  -0.500
 Inverse symmetry   0.000   0.000   1.000  -0.500
 Inverse symmetry   1.000   0.000   0.000  -0.500

 Inverse symmetry   0.000  -1.000   0.000   0.500
 Inverse symmetry   0.000   0.000  -1.000   0.500
 Inverse symmetry   1.000   0.000   0.000  -0.500

 Inverse symmetry   0.000  -1.000   0.000   0.500
 Inverse symmetry   0.000   0.000   1.000  -0.500
 Inverse symmetry  -1.000   0.000   0.000   0.500

 Inverse symmetry   0.000   1.000   0.000  -0.500
 Inverse symmetry   0.000   0.000  -1.000   0.500
 Inverse symmetry  -1.000   0.000   0.000   0.500

 Inverse symmetry   0.000   0.000   1.000  -0.500
 Inverse symmetry   1.000   0.000   0.000  -0.500
 Inverse symmetry   0.000   1.000   0.000  -0.500

 Inverse symmetry   0.000   0.000  -1.000   0.500
 Inverse symmetry  -1.000   0.000   0.000   0.500
 Inverse symmetry   0.000   1.000   0.000  -0.500

 Inverse symmetry   0.000   0.000  -1.000   0.500
 Inverse symmetry   1.000   0.000   0.000  -0.500
 Inverse symmetry   0.000  -1.000   0.000   0.500

 Inverse symmetry   0.000   0.000   1.000  -0.500
 Inverse symmetry  -1.000   0.000   0.000   0.500
 Inverse symmetry   0.000  -1.000   0.000   0.500

 Inverse symmetry   0.000   1.000   0.000  -0.500
 Inverse symmetry   1.000   0.000   0.000  -0.500
 Inverse symmetry   0.000   0.000  -1.000   0.500

 Inverse symmetry   0.000  -1.000   0.000   0.500
 Inverse symmetry  -1.000   0.000   0.000   0.500
 Inverse symmetry   0.000   0.000  -1.000   0.500

 Inverse symmetry   0.000  -1.000   0.000   0.500
 Inverse symmetry   1.000   0.000   0.000  -0.500
 Inverse symmetry   0.000   0.000   1.000  -0.500

 Inverse symmetry   0.000   1.000   0.000  -0.500
 Inverse symmetry  -1.000   0.000   0.000   0.500
 Inverse symmetry   0.000   0.000   1.000  -0.500

 Inverse symmetry   1.000   0.000   0.000  -0.500
 Inverse symmetry   0.000   0.000  -1.000   0.500
 Inverse symmetry   0.000   1.000   0.000  -0.500

 Inverse symmetry  -1.000   0.000   0.000   0.500
 Inverse symmetry   0.000   0.000   1.000  -0.500
 Inverse symmetry   0.000   1.000   0.000  -0.500

 Inverse symmetry  -1.000   0.000   0.000   0.500
 Inverse symmetry   0.000   0.000  -1.000   0.500
 Inverse symmetry   0.000  -1.000   0.000   0.500

 Inverse symmetry   1.000   0.000   0.000  -0.500
 Inverse symmetry   0.000   0.000   1.000  -0.500
 Inverse symmetry   0.000  -1.000   0.000   0.500

 Inverse symmetry   0.000   0.000  -1.000   0.500
 Inverse symmetry   0.000   1.000   0.000  -0.500
 Inverse symmetry   1.000   0.000   0.000  -0.500

 Inverse symmetry   0.000   0.000   1.000  -0.500
 Inverse symmetry   0.000  -1.000   0.000   0.500
 Inverse symmetry   1.000   0.000   0.000  -0.500

 Inverse symmetry   0.000   0.000   1.000  -0.500
 Inverse symmetry   0.000   1.000   0.000  -0.500
 Inverse symmetry  -1.000   0.000   0.000   0.500

 Inverse symmetry   0.000   0.000  -1.000   0.500
 Inverse symmetry   0.000  -1.000   0.000   0.500
 Inverse symmetry  -1.000   0.000   0.000   0.500

 Label                     FP          Column number    4
 Label                  SIGFP          Column number    5
 Label                2FOFCWT          Column number    8


     1891 reflections in the file
        9 reflections flagged as missing
        0 reflections with too low sigma
        0 reflections outside resolution limits
        0 reflections are systematic absences
        0 reflections skipped for other reasons
     1882 reflections to work

 For FP/SIGFP:
 Resol_high  2.30  Bfactor  28.8  ChiSquare    4.56  Two_omega  1.46

 For FUSE/FOMUSE/SIGFP:
 Resol_huse  2.30  Bfacuse  26.5  ChiSquuse    7.64  Two_omuse  1.45

 $TABLE: Wilson plot statistics - credits to Sasha Popov, EMBL Hamburg :
 $GRAPHS: Log<Intensity> vrs Resolution :A:3,4,5:
 : ChiSquare vrs Resolution :N:3,6:
 : Iobs/Iexp ratio vrs Resolution :N:3,7:
 $$
   Dmin  Dmax  1/resol^2  Log<Istd>  Log<Icalc> ChiSq  Iobs/Iexp  Comment
 $$
    (A)   (A)   (A^(-2)   (expected (calculated
                          intensity) intensity)
 $$
  14.27 10.54    0.0070     11.69      11.31     4.66     0.68 .
  10.54  8.74    0.0110     11.53      10.94    12.44     0.55 <===Problems
   8.74  7.63    0.0151     11.31      10.71     9.41     0.55 <===Problems
   7.63  6.86    0.0192     11.06      11.43     2.62     1.45 .
   6.86  6.28    0.0233     10.97      10.47    21.84     0.61 <===Problems
   6.28  5.83    0.0274     11.03      10.61     7.44     0.66 <===Problems
   5.83  5.46    0.0315     11.19      11.08     0.52     0.90 .
   5.46  5.15    0.0356     11.41      11.44     0.02     1.03 .
   5.15  4.89    0.0397     11.61      11.87     1.93     1.31 .
   4.89  4.67    0.0438     11.75      11.33    10.47     0.66 <===Problems
   4.67  4.48    0.0479     11.83      11.76     0.21     0.93 .
   4.48  4.30    0.0520     11.85      12.04     1.02     1.21 .
   4.30  4.15    0.0561     11.83      12.05     0.73     1.24 .
   4.15  4.01    0.0601     11.80      12.09     2.34     1.33 .
   4.01  3.88    0.0642     11.77      11.48     5.22     0.74 .
   3.88  3.77    0.0683     11.74      12.04     1.81     1.35 .
   3.77  3.66    0.0724     11.70      12.08     4.12     1.46 .
   3.66  3.57    0.0765     11.66      11.62     0.06     0.96 .
   3.57  3.48    0.0806     11.62      12.16     4.34     1.72 .
   3.48  3.40    0.0847     11.56      12.05     7.55     1.64 <===Problems
   3.40  3.32    0.0888     11.49      11.57     0.19     1.09 .
   3.32  3.25    0.0929     11.41      12.11     6.97     2.02 <===Problems
   3.25  3.18    0.0970     11.33      12.52    21.52     3.28 <===Problems
   3.18  3.11    0.1011     11.27      12.15    13.69     2.43 <===Problems
   3.11  3.05    0.1052     11.20      11.80    10.42     1.82 <===Problems
   3.05  3.00    0.1093     11.15      11.87     8.30     2.05 <===Problems
   3.00  2.94    0.1133     11.09      11.44     3.49     1.43 .
   2.94  2.89    0.1174     11.03      11.43     4.19     1.49 .
   2.89  2.84    0.1215     10.98      11.28     1.63     1.35 .
   2.84  2.80    0.1256     10.93      11.17     2.05     1.27 .
   2.80  2.75    0.1297     10.89      10.82     0.12     0.94 .
   2.75  2.71    0.1338     10.86      10.78     0.35     0.93 .
   2.71  2.67    0.1379     10.84      10.68     1.51     0.85 .
   2.67  2.63    0.1420     10.82      10.74     0.42     0.92 .
   2.63  2.60    0.1461     10.81      10.58     2.34     0.80 .
   2.60  2.56    0.1502     10.78      10.84     0.17     1.06 .
   2.56  2.53    0.1543     10.76      10.47     4.56     0.75 .
   2.53  2.50    0.1584     10.75      10.38     9.17     0.69 <===Problems
   2.50  2.47    0.1625     10.75      10.74     0.01     0.99 .
   2.47  2.44    0.1665     10.73      10.65     0.64     0.92 .
   2.44  2.41    0.1706     10.74      10.70     0.04     0.97 .
   2.41  2.38    0.1747     10.73      10.61     0.67     0.88 .
   2.38  2.35    0.1788     10.74      10.86     0.68     1.13 .
   2.35  2.33    0.1829     10.73      10.41     6.65     0.72 <===Problems
   2.33  2.30    0.1870     10.74      10.47     6.50     0.77 <===Problems
 $$

 Comments:  Overall fit of the data to the Wilson curve:

 Comments:  Problems           Resolution range   3.48  to   3.40
 Comments:  Problems           Resolution range   3.32  to   3.25
 Comments:  Problems           Resolution range   3.25  to   3.18
 Comments:  Problems           Resolution range   3.18  to   3.11
 Comments:  Problems           Resolution range   3.11  to   3.05
 Comments:  Problems           Resolution range   3.05  to   3.00
 Comments:  Possible reasons - salt/ice satellites, pseudosymmetry

 Comments:  Problems           Resolution range  10.54  to   8.74
 Comments:  Problems           Resolution range   8.74  to   7.63
 Comments:  Problems           Resolution range   6.86  to   6.28
 Comments:  Problems           Resolution range   6.28  to   5.83
 Comments:  Problems           Resolution range   4.89  to   4.67
 Comments:  Problems           Resolution range   2.53  to   2.50
 Comments:  Problems           Resolution range   2.35  to   2.33
 Comments:  Problems           Resolution range   2.33  to   2.30
 Comments:  Possible reasons - missing overloads


 PoorAllData
 WARNING ! The data are poor. Discard ALL data !

 Solvent content    0.43

 R.m.s.d. for a map computed with FUSE(FOMUSE)        0.054
 R.m.s.d. expected for a map in the absolute scale    0.342
 Scaling coefficient to be applied for FUSE(FOMUSE)   6.313
    0.01 CPU        0 Elapsed end