.c1.Appendix D

Detailed summary of aliphatic (f1) hydrocarbon determinations for Year
01

(Values are [not]{.underline} corrected for percent recovery)

\[NOTE: THE FONT SIZE USED IN THIS SECTION OF THE DOCUMENT WAS
APPROXIMATELY 5. ERRORS IN TRANSCRIPTION MAY HAVE OCCURRED DUE TO FONT
SIZE AND ILLEGIBILITY OF THE COPY OF THE DOCUMENT USED FOR RESCUE.
QUESTIONABLE TRANSCRIPTIONS ARE NOTED WITH A QUESTION MARK. THE COPY OF
DOCUMENT USED TO GENERATE THIS DOCUMENT IS ARCHIVED AT THE
NOAA/NMFS/SEFSC LIBRARY IN MIAMI.\]

BISCAYNE BAY HYDROCARBON STUDY

ALIPHATIC HYDROCARBONS

SAMPLE: 1 DATE ANALYZED: 11/09/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 14.30

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 3498 .0017 5.9466 .2189

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .2189

SAMPLE: 2 DATE ANALYZED: 10/13/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 19.08

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .2256

C15 2119 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 164 .0008 .0000 .0000

PRISTANE 727 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 438 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 11061 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 1292 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 2621 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 19530 .0017 1.8836 .6815

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .6815

SAMPLE: 5 DATE ANALYZED: 09/09/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 29.82

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT 2.9733

C14 0 .0008 .0000 .0000 C17/PRIST .0691

C15 873 .0008 .0000 .0000 C18/PHYT .5688

C16 0 .0008 .0000 .0000

C17 100 .0011 .0000 .0000

PRISTANE 1448 .0022 .0000 .0000

C18 277 .0009 .0000 .0000

PHYTANE 487 .0019 .0000 .0000

C19 1237 .0008 .0000 .0000

C20 314 .0009 .0000 .0000 CPI 2.3326

ANDROSTANE 0 .0016 .0000 .0000

C21 996 .0010 .0000 .0000

C22 555 .0012 .0000 .0000 RECOVERY %

C23 858 .0008 .0000 .0000 ANDROSTANE .0000

C24 1244 .0021 .0000 .0000

C25 1511 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 16993 .0016 11.3488 .4735

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .4735

SAMPLE: 6 DATE ANALYZED: 08/20/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 40.90

SAMPLE SIZE INJECTED (µL): 1.5

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0012 .0000 .0000 RESOL/UNRESOL .3799

C13 0 .0014 .0000 .0000 PRIST/PHYT .5127

C14 0 .0011 .0000 .0000 C17/PRIST 2.3368

C15 975 .0015 1.4625 .0238 C18/PHYT 2.4303

C16 1688 .0013 2.1944 .358

C17 2269 .0016 3.6304 .0592

PRISTANE 971 .0040 3.8840 .0633

C18 4603 .0014 6.4442 .1050

PHYTANE 1894 .0039 7.3866 .1204

C19 7231 .0016 11.5696 .1886

C20 6025 .0014 8.4350 .1375 CPI 1.5853

ANDROSTANE 0 .0016 .0000 .0000

C21 12606 .0017 21.4302 .3493

C22 4794 .0015 7.1910 .1172 RECOVERY %

C23 4182 .0015 6.2730 .1022 ANDROSTANE .0000

C24 1446 .0017 2.4582 .0401

C25 2153 .0030 6.4590 .1053

C26 0 .0000 .0000 .0000

C27 0 .0000 .0000 .0000

C28 0 .0000 .0000 .0000

C29 0 .0000 .0000 .0000

C30 0 .0000 .0000 .0000

RESOLVED 65983 .0016 26.2336 1.8427

UNRESOLVED 173666 .0016 277.8656 4.5292

TOTAL 6.3719

SAMPLE: 7 DATE ANALYZED: 09/17/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 24.84

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 3179 .0008 2.5432 .0902 RESOL/UNRESOL .4578

C13 1357 .0008 1.0856 .0385 PRIST/PHYT .6725

C14 2352 .0008 1.8816 .0667 C17/PRIST .2167

C15 3440 .0008 2.7520 .0976 C18/PHYT .5106

C16 268 .0008 .2144 .0076

C17 117 .0011 .1287 .0046

PRISTANE 540 .0022 1.1880 .0421

C18 410 .0069 .3690 .0131

PHYTANE 803 .0019 1.5257 .0541

C19 2458 .0001 1.9664 .0697

C20 539 .0009 .4851 .0172 CPI 1.7465

ANDROSTANE 0 .0016 .0000 .0000

C21 1064 .0010 1.0640 .0377

C22 2065 .0012 2.4780 .0879 RECOVERY %

C23 2684 .0008 2.1472 .0782 ANDROSTANE .0000

C24 2615 .0021 5.4915 .1948

C25 3287 .0027 8.8749 .3148

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 53823 .0016 42.6320 2.7248

UNRESOLVED 117575 .0016 188.1200 6.6719

TOTAL 9.3966

SAMPLE: 8 DATE ANALYZED: 09/17/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 25.13

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 100 .0008 .0000 .0000 PRIST/PHYT .9431

C14 0 .0008 .0000 .0000 C17/PRIST .3359

C15 0 .0008 .0000 .0000 C18/PHYT .5796

C16 0 .0008 .0000 .0000

C17 217 .0008 .1736 .0036

PRISTANE 646 .0022 1.4212 .0298

C18 397 .0016 .6352 .0133

PHYTANE 685 .0020 1.3700 .0287

C19 1641 .0010 1.6410 .0344

C20 396 .0013 .5148 .0108 CPI 8.9808

ANDROSTANE 0 .0017 .0000 .0000

C21 11631 .0011 12.7941 .2680

C22 927 .0013 1.2051 .0252 RECOVERY %

C23 1182 .0012 1.4184 .0297 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 776 .0020 1.5520 .0325

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 19220 .0017 1.2274 .5017

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .5017

SAMPLE: 9 DATE ANALYZED: 11/12/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 24.47

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 622 .0011 .6842 .0147

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 622 .0017 .0000 .0147

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .0147

SAMPLE: 10 DATE ANALYZED: 09/30/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 36.96

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 896 .0016 1.4336 .0204

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 320 .0013 .4160 .0059 CPI 1.5728

ANDROSTANE 0 .0017 .0000 .0000

C21 2025 .0011 2.2275 .0317

C22 379 .0013 .4927 .0070 RECOVERY %

C23 1092 .0012 1.3104 .0187 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 1639 .0020 3.2780 .0467

C26 1429 .0029 4.1441 .0590

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 20516 .0017 21.6512 .4977

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .4977

SAMPLE: 11 DATE ANALYZED: 10/19/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 8.66

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT 73.3930

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .9472

C16 604 .0008 .4832 .0294

C17 0 .0008 .0000 .0000

PRISTANE 54164 .0022 119.1608 7.2421

C18 699 .0016 1.1184 .0680

PHYTANE 738 .0020 1.4760 .0897

C19 3238 .0010 3.2380 .1968

C20 2026 .0013 2.6338 .1601 CPI 2.5755

ANDROSTANE 0 .0017 .0000 .0000

C21 16520 .0011 17.8750 1.0864

C22 4191 .0013 5.4483 .3311 RECOVERY %

C23 9544 .0012 11.4528 .6960 ANDROSTANE .0000

C24 8251 .0017 14.0267 .8525

C25 11586 .0020 23.1720 1.4083

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 119800 .0017 5.9466 13.0394

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 13.0394

SAMPLE: 12 DATE ANALYZED: 09/23/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 17.22

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .3648

C13 0 .0008 .0000 .0000 PRIST/PHYT 6.2874

C14 0 .0008 .0000 .0000 C17/PRIST 1.0603

C15 0 .0008 .0000 .0000 C18/PHYT 3.4253

C16 0 .0008 .0000 .0000

C17 580 .0008 .4640 .0142

PRISTANE 547 .0022 1.2034 .0368

C18 298 .0016 .4768 .0146

PHYTANE 87 .0020 .1740 .0053

C19 234 .0010 .2340 .0072

C20 326 .0013 .4238 .0130 CPI 18.3363

ANDROSTANE 0 .0017 .0000 .0000

C21 10260 .0011 11.2860 .3449

C22 902 .0013 1.1726 .0358 RECOVERY %

C23 2378 .0012 2.8536 .0872 ANDROSTANE .0000

C24 376 .0017 .9792 .0299

C25 1171 .0020 2.3420 .0716

C26 0 .0029 .0000 .0000

C27 20953 .0095 199.0535 6.0839

C28 0 .0076 .0000 .0000

C29 2967 .0124 36.7908 1.1245

C30 0 .0050 .0000 .0000

RESOLVED 75286 .0017 57.8119 9.6358

UNRESOLVED 206358 .0017 350.8086 10.7222

TOTAL 20.3580

SAMPLE: 13 DATE ANALYZED: 11/01/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 25.60

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0422

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 1834 .0008 1.4672 .0302 C17/PRIST .0000

C15 1494 .0008 1.1952 .0246 C18/PHYT .7018

C16 1592 .0008 1.2736 .0262

C17 6889 .0008 5.5112 .1133

PRISTANE 0 .0022 .0000 .0000

C18 579 .0016 .9264 .0190

PHYTANE 825 .0020 1.6500 .0339

C19 112 .0010 .1120 .0023

C20 1838 .0013 2.3894 .0491 CPI 2.0928

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 3733 .0012 4.4796 .0921 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 24848 .0017 10.1184 .5987

UNRESOLVED 588415 .0017 1000.3055 20.5655

TOTAL 21.1642

SAMPLE: 14 DATE ANALYZED: 09/28/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 16.03

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 1382 .0022 3.0404 .0998

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 870 .0010 .8700 .0286

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 1174 .0011 1.2914 .0424

C22 0 .0013 .0000 .0000 RECOVERY %

C23 619 .0012 .7428 .0244 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 7305 .0017 5.5420 .3771

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .3771

SAMPLE: 15 DATE ANALYZED: 09/10/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 13.80

SAMPLE SIZE INJECTED (µL): 1.5

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .5598

C15 1422 .0008 1.1376 .9434 ? C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 309 .0021 .3399 .0230

PRISTANE 552 .0022 1.2144 .0463

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 1179 .0008 .9432 .0360

C20 0 .0009 .0000 .0000 CPI 3.6167

ANDROSTANE 0 .0016 .0000 .0000

C21 166 .0010 .1660 .0063

C22 785 .0012 .9420 .0359 RECOVERY %

C23 1653 ? .0008 1.0824 .0413 ANDROSTANE .0000

C24 684 .0021 1.4364 .0548

C25 884 .0027 2.3868 .0910

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 9827 .0016 3.9888 .5201

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .5201

SAMPLE: 16 DATE ANALYZED: 09/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 9.93

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 1755 .0008 1.4040 .0744

PRISTANE 0 .0022 .0000 .0000

C18 342 .0016 .5472 .0290

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI 5.1316

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 2808 .0017 1.2087 .1675

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .1675

SAMPLE: 17 DATE ANALYZED: 09/14/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 0.5

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 14.86

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 654 .0008 .5232 .0095

C20 124 .0009 .1116 .0020 CPI 1.6899

ANDROSTANE 0 .0016 .0000 .0000

C21 370 .0010 .3700 .0066

C22 148 .0012 .1776 .0031 RECOVERY %

C23 3779 .0008 3.0232 .0535 ANDROSTANE .0000

C24 3359 .0021 7.0539 .1249

C25 1333 .0027 3.5991 .0637

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 12522 .0016 4.4080 .3412

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .3412

SAMPLE: 18 DATE ANALYZED: 09/10/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 23.94

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 0 .0008 .0000 .0000

C20 0 .0009 .0000 .0000 CPI .0000

ANDROSTANE 0 .0016 .0000 .0000

C21 0 .0010 .0000 .0000

C22 927 .0012 1.1124 .0245 RECOVERY %

C23 0 .0008 .0000 .0000 ANDROSTANE .0000

C24 0 .0021 .0000 .0000

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 927 .0016 5.9466 .0245

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .0245

SAMPLE: 19 DATE ANALYZED: 09/24/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 16.83

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 706 .0008 .5648 .0177 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT 3.0282

C14 730 .0008 .5840 .0183 C17/PRIST .0000

C15 1589 .0008 1.2712 .0398 C18/PHYT 3.9061

C16 2930 .0008 2.3440 .0733

C17 100 .0008 .0800 .0025

PRISTANE 4839 .0022 10.6458 .3329

C18 6242 .0016 9.9872 .3123

PHYTANE 1598 .0020 3.1960 .0999

C19 8788 .0010 8.7880 .2748

C20 7401 .0013 9.6213 .3009 CPI .9986

ANDROSTANE 0 .0017 .0000 .0000

C21 9837 .0011 10.8207 .3364

C22 4586 .0013 5.9618 .1864 RECOVERY %

C23 5349 .0012 6.4188 .2007 ANDROSTANE .0000

C24 1653 .0017 2.8101 .0879

C25 1532 .0020 3.0640 .0958

C26 3690 .0029 10.7010 .3346

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 78588 .0017 28.9306 3.2610

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 3.2610

SAMPLE: 20 DATE ANALYZED: 09/07/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 27.61

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 8281 .0022 18.2182 .3473

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 0 .0008 .0000 .0000

C20 1 .0009 .0009 .0000 CPI 12.0559

ANDROSTANE 370000 .0016 592.0000 11.2850

C21 8266 .0010 8.2660 .1576

C22 856 .0012 1.0272 .0196 RECOVERY %

C23 6829 .0008 5.4632 .1041 ANDROSTANE 12.0559

C24 0 .0021 .0000 .0000

C25 15322 .0027 41.3694 .7886

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 1666 .0051 8.4966 .1620

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 48350 .0016 21.4064 1.7966

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 1.7966

SAMPLE: 21 DATE ANALYZED: 11/01/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 36.29

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .1453

C13 0 .0008 .0000 .0000 PRIST/PHYT 30.3806

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 1530 .0008 .0000 .0000 C18/PHYT .8161

C16 1114 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 67107 .0022 .0000 .0000

C18 1087 .0016 .0000 .0000

PHYTANE 1332 .0020 .0000 .0000

C19 3835 .0010 .0000 .0000

C20 1292 .0013 .0000 .0000 CPI 3.3332

ANDROSTANE 0 .0017 .0000 .0000

C21 7632 .0011 .0000 .0000

C22 1081 .0013 .0000 .0000 RECOVERY %

C23 2249 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 95859 .0017 12.9200 2.6843

UNRESOLVED 659607 .0017 1121.3319 16.2627

TOTAL 18.9472

SAMPLE: 22 DATE ANALYZED: 08/18/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 40.50

SAMPLE SIZE INJECTED (µL): 1.5

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0012 .0000 .0000 RESOL/UNRESOL .0190

C13 0 .0014 .0000 .0000 PRIST/PHYT .0000

C14 0 .0011 .0000 .0000 C17/PRIST .0000

C15 0 .0015 .0000 .0000 C18/PHYT .0000

C16 0 .0013 .0000 .0000

C17 0 .0016 .0000 .0000

PRISTANE 0 .0040 .0000 .0000

C18 0 .0014 .0000 .0000

PHYTANE 0 .0039 .0000 .0000

C19 0 .0016 .0000 .0000

C20 0 .0014 .0000 .0000 CPI .0000

ANDROSTANE 0 .0016 .0000 .0000

C21 0 .0017 .0000 .0000

C22 1011 .0015 .0000 .0250 RECOVERY %

C23 0 .0015 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0030 .0000 .0000

C26 0 .0000 .0000 .0000

C27 0 .0000 .0000 .0000

C28 0 .0000 .0000 .0000

C29 0 .0000 .0000 .0000

C30 0 .0000 .0000 .0000

RESOLVED 1755 .0016 1.1904 .0446

UNRESOLVED 92236 .0016 147.5776 2.4293

TOTAL 2.4738

SAMPLE: 23 DATE ANALYZED: 10/14/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 3564

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0296

C13 0 .0008 .0000 .0000 PRIST/PHYT 2.6680

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 2761 .0008 2.2088 .0326 C18/PHYT .0413

C16 1406 .0008 1.1248 .0166

C17 0 .0008 .0000 .0000

PRISTANE 3446 .0022 7.5812 .1120

C18 53 .0016 .0848 .0013

PHYTANE 1282 .0020 2.5640 .0379

C19 4710 .0010 4.7100 .0696

C20 1031 .0013 1.3403 .0198 CPI 2.8271

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 1390 .0013 1.8070 .0267 RECOVERY %

C23 3498 .0012 4.1976 .0620 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 22908 .0017 5.6627 .4619

UNRESOLVED 772631 .0017 1313.4727 19.3968

TOTAL 19.8587

SAMPLE: 25 DATE ANALYZED: 09/17/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 36.24

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .1675

C13 0 .0008 .0000 .0000 PRIST/PHYT 1.2998

C14 439 .0008 .3512 .0051 C17/PRIST 18.5584

C15 806 .0008 .6448 .0094 C18/PHYT 1.4280

C16 387 .0008 .3096 .0045

C17 12230 .0011 13.4530 .1954

PRISTANE 659 .0022 1.4498 .0211

C18 724 .0009 .6516 .0095

PHYTANE 507 .0019 .9633 .0140

C19 2499 .0008 1.9992 .0290

C20 265 .0009 .2385 .0035 CPI 8.5087

ANDROSTANE 0 .0016 .0000 .0000

C21 3007 .0010 3.0070 .0437

C22 198 .0012 .2376 .0035 RECOVERY %

C23 1584 .0008 1.2672 .0184 ANDROSTANE .0000

C24 812 .0021 1.7052 .0248

C25 3913 .0027 10.5597 .1534

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 84459 .0016 90.2896 1.8463

UNRESOLVED 504278 .0016 806.8464 11.7179

TOTAL 13.5642

SAMPLE: 26 DATE ANALYZED: 09/23/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 40.65

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 436 .0008 .3488 .0045 RESOL/UNRESOL .0962

C13 0 .0008 .0000 .0000 PRIST/PHYT 5.4893

C14 585 .0008 .4680 .0061 C17/PRIST .0000

C15 1028 .0008 .8224 .0106 C18/PHYT 1.1277

C16 921 .0008 .7368 .0095

C17 0 .0008 .0000 .0000

PRISTANE 5632 .0022 12.3904 .1604

C18 1157 .0016 1.8512 .0240

PHYTANE 1026 .0020 2.0520 .0266

C19 2541 .0010 2.5410 .0329

C20 857 .0013 1.1141 .0144 CPI 2.2789

ANDROSTANE 0 .0017 .0000 .0000

C21 6390 .0011 7.0290 .0910

C22 1622 .0013 2.1086 .0273 RECOVERY %

C23 1759 .0012 2.1108 .0273 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 37988 .0017 23.8578 .7436

UNRESOLVED 394936 .0017 671.3912 8.6298

TOTAL 9.4364

SAMPLE: 27 DATE ANALYZED: 09/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 30.20

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT 5.5496

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT 1.3014

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 1565 .0022 3.4430 .0600

C18 367 .0016 .5872 .0102

PHYTANE 282 .0020 .5640 .0098

C19 939 .0010 .9390 .0164

C20 551 .0013 .7163 .0125 CPI 2.1683

ANDROSTANE 0 .0017 .0000 .0000

C21 2101 .0011 2.3111 .0403

C22 484 .0013 .6292 .0110 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 3498 .0017 8.0597 .3006

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .3006

SAMPLE: 28 DATE ANALYZED: 09/09/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 26.03

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 0 .0008 .0000 .0000

C20 0 .0009 .0000 .0000 CPI 1.8426

ANDROSTANE 0 .0016 .0000 .0000

C21 276 .0010 .2760 .0056

C22 324 .0012 .3888 .0079 RECOVERY %

C23 321 .0008 .2568 .0052 ANDROSTANE .0000

C24 0 .0021 .0000 .0000

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 1426 .0016 .0800 .0350

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .0350

SAMPLE: 29 DATE ANALYZED: 09/03/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 23.99

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .2176

C14 0 .0008 .0000 .0000 C17/PRIST 3.2252

C15 0 .0008 .0000 .0000 C18/PHYT 2.3617

C16 0 .0008 .0000 .0000

C17 487 .0011 .5357 .0118

PRISTANE 151 .0022 .3322 .0073

C18 1639 .0009 1.4751 .0324

PHYTANE 694 .0019 1.3186 .0289

C19 2787 .0008 2.2296 .0489

C20 2755 .0009 2.4795 .0544 CPI 1.2551

ANDROSTANE 0 .0016 .0000 .0000

C21 3927 .0010 3.9270 .0862

C22 2486 .0012 2.9832 .0654 RECOVERY %

C23 3265 .0008 2.6120 .0573 ANDROSTANE .0000

C24 2316 .0021 4.8636 .1067

C25 5475 .0027 14.7825 .3243

C26 3505 .0034 11.9170 .2614

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 47868 .0016 29.4096 1.7302

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 1.7302

SAMPLE: 30 DATE ANALYZED: 09/27/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 43.64

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 902 .0008 .7216 .0087

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 902 .0017 5.9466 .0087

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .0087

SAMPLE: 31 DATE ANALYZED: 09/24/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 24.76

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1093 .0008 .8744 .0186 RESOL/UNRESOL .0000

C13 739 .0008 .5912 .0126 PRIST/PHYT .0000

C14 722 .0008 .5776 .0123 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 505 .0008 .4040 .0086

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .7626

ANDROSTANE 0 .0017 .0000 .0000

C21 732 .0011 .8052 .0171

C22 0 .0013 .0000 .0000 RECOVERY %

C23 1633 .0012 1.9596 .0417 ANDROSTANE .0000

C24 8337 .0017 14.1729 .3013

C25 3299 .0020 6.5980 .1403

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 121787 .0017 178.0359 4.3368

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 4.3368

SAMPLE: 32 DATE ANALYZED: 09/24/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 40.28

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 648 .0008 .5184 .0068 RESOL/UNRESOL .5024

C13 648 .0008 .5184 .0068 PRIST/PHYT 2.7322

C14 575 .0008 .4600 .0060 C17/PRIST .3202

C15 2151 .0008 1.7208 .0225 C18/PHYT 1.3526

C16 1487 .0008 1.1896 .0155

C17 908 .0008 .7264 .0095

PRISTANE 2836 .0022 6.2392 .0815

C18 1404 .0016 2.2464 .0294

PHYTANE 1038 .0020 2.0760 .0271

C19 669 .0010 .6690 .0087

C20 3394 .0013 4.4122 .0577 CPI 4.8078

ANDROSTANE 0 .0017 .0000 .0000

C21 5030 .0011 5.5330 .0723

C22 4447 .0013 5.7811 .0755 RECOVERY %

C23 8364 .0012 10.0368 .1311 ANDROSTANE .0000

C24 2740 .0017 4.6580 .0609

C25 7299 .0020 14.5980 .1907

C26 10211 .0029 29.6119 .3869

C27 72627 .0095 689.9565 9.0153

C28 498 .0076 1.7848 .0495

C29 21325 .0124 264.4300 3.4552

C30 0 .0050 .0000 .0000

RESOLVED 280449 .0017 224.6550 16.6443

UNRESOLVED 554958 .0017 946.4286 12.3272

TOTAL 28.9715

SAMPLE: 33 DATE ANALYZED: 09/09/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 10.51

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .1976

C16 268 .0008 .2144 .1070

C17 4592 .0011 5.0512 .2530

PRISTANE 0 .0022 .0000 .0000

C18 375 .0009 .3375 30169.0000

PHYTANE 1898 .0019 3.6062 .1806

C19 2027 .0008 1.6216 .0812

C20 931 .0009 .8379 .0420 CPI 4.9639

ANDROSTANE 223340 .0016 357.3440 17.8945

C21 13026 .0010 13.0260 .6523

C22 675 .0012 .8100 .0406 RECOVERY %

C23 1589 .0008 1.2712 .0637 ANDROSTANE 37.6152

C24 1309 .0021 2.7489 .1377

C25 3764 .0027 10.1628 .5089

C26 1478 .0034 5.0252 .2517

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 42390 .0016 .0000 3.0771

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 3.0771

SAMPLE: 34 DATE ANALYZED: 09/13/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 33.71

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0288

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT 1.8420

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 641 .0008 .5769 .0090

C20 348 .0009 .6612 .0103 CPI 2.4652

ANDROSTANE 910 .0016 .7280 .0114

C21 531 .0010 .4779 .0075

C22 0 .0012 .0000 .0000 RECOVERY %

C23 3244 .0008 3.2440 .0506 ANDROSTANE .0000

C24 1081 .0021 1.2972 .0203

C25 1400 .0027 1.1200 .0175

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 10101 .0016 3.1136 .1752

UNRESOLVED 350755 .0016 561.2080 8.7622

TOTAL 8.9373

SAMPLE: 35 DATE ANALYZED: 10/12/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 35.05

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT 7.2197

C14 1131 .0008 .9048 .0136 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 1084 .0008 .8672 .0130

C17 0 .0008 .0000 .0000

PRISTANE 1906 .0022 4.1932 .0630

C18 0 .0016 .0000 .0000

PHYTANE 264 .0020 .5280 .0079

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 5300 .0017 1.5555 .1209

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .1209

SAMPLE: 36 DATE ANALYZED: 08/20/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 41.28

SAMPLE SIZE INJECTED (µL): 1.5

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0012 .0000 .0000 RESOL/UNRESOL .0311

C13 0 .0014 .0000 .0000 PRIST/PHYT .0000

C14 0 .0011 .0000 .0000 C17/PRIST .0000

C15 0 .0015 .0000 .0000 C18/PHYT .0000

C16 0 .0013 .0000 .0000

C17 0 .0016 .0000 .0000

PRISTANE 826 .0040 3.3040 .0534

C18 0 .0014 .0000 .0000

PHYTANE 0 .0039 .0000 .0000

C19 1549 .0016 2.4784 .0400

C20 0 .0014 .0000 .0000 CPI .0000

ANDROSTANE 0 .0016 .0000 .0000

C21 845 .0017 1.4365 .0232

C22 0 .0015 .0000 .0000 RECOVERY %

C23 0 .0015 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0030 .0000 .0000

C26 0 .0000 .0000 .0000

C27 0 .0000 .0000 .0000

C28 0 .0000 .0000 .0000

C29 0 .0000 .0000 .0000

C30 0 .0000 .0000 .0000

RESOLVED 3676 .0016 .7296 .1284

UNRESOLVED 118114 .0016 188.9824 3.0520

TOTAL 3.1804

SAMPLE: 38 DATE ANALYZED: 11/09/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 40.89

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 2896 .0008 2.3168 .0298 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 975 .0008 .7800 .0100 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 38710 .0017 59.2263 .8022

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .8022

SAMPLE: 40 DATE ANALYZED: 09/24/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 16.74

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1093 .0008 .8744 .0275 RESOL/UNRESOL .0000

C13 987 .0008 .7896 .0248 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 2643 .0017 .9571 .0824

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .0824

SAMPLE: 41 DATE ANALYZED: 09/13/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 33.15

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1536 .0008 1.2288 .0195 RESOL/UNRESOL .0455

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 2.4080 .0382 C17/PRIST .0000

C15 3010 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 0 .0008 .0000 .0000

C20 0 .0009 .0000 .0000 CPI .0000

ANDROSTANE 0 .0016 .0000 .0000

C21 0 .0010 .0000 .0000

C22 0 .0012 .0000 .0000 RECOVERY %

C23 0 .0008 .0000 .0000 ANDROSTANE .0000

C24 0 .0021 .0000 .0000

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 8342 .0016 6.0736 .1542

UNRESOLVED 183374 .0016 293.3984 4.6582

TOTAL 4.8124

SAMPLE: 42 DATE ANALYZED: 11/10/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 19.77

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 961 .0008 .7688 .0389 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 853 .0008 .6824 .0345 C17/PRIST .0000

C15 1394 .0008 1.1520 .0564 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 3447 .0008 2.7576 .1395

PRISTANE 0 .0022 .0000 .0000

C18 297 .0016 .4752 .0240

PHYTANE 0 .0020 .0000 .0000

C19 1847 .0010 1.8470 .0934

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 3804 .0011 4.1844 2117.0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 4814 .0020 9.6280 .4870

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 19572 .0017 3.6635 1.2707

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 1.2707

SAMPLE: 43 DATE ANALYZED: 09/03/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 17.10

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT 8.2500

C14 344 .0008 .2752 .0085 C17/PRIST .4169

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 743 .0011 .8173 .2520

PRISTANE 1782 .0022 3.9204 .1207

C18 0 .0009 .0000 .0000

PHYTANE 216 .0019 .4104 .0126

C19 751 .0008 .6008 .1850

C20 0 .0009 .0000 .0000 CPI .1341

ANDROSTANE 0 .0016 .0000 .0000

C21 697 .0010 .6970 .0215

C22 4242 .0012 5.0904 .1567 RECOVERY %

C23 1217 .0008 .9736 .0300 ANDROSTANE .0000

C24 4856 .0021 10.1976 .3139

C25 1749 .0027 4.7223 .1453

C26 29026 .0034 98.6884 3.0375

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 556962 .0016 16.5424 4.3994

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 4.3994

SAMPLE: 44 DATE ANALYZED:10/20/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 41.58

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI 15.3658

ANDROSTANE 0 .0017 .0000 .0000

C21 1009 .0011 1.1099 .0140

C22 298 .0013 .3874 .0049 RECOVERY %

C23 3570 .0012 4.2840 .0542 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 27889 .0017 39.1204 .2189

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .2189

SAMPLE: 45 DATE ANALYZED: 09/02/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 37.63

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 2107 .0008 1.6856 .0236 RESOL/UNRESOL .1102

C13 421 .0008 .3368 .0047 PRIST/PHYT .3493

C14 1581 .0008 1.2648 .0177 C17/PRIST 5.4702

C15 332 .0008 .2656 .0037 C18/PHYT .2635

C16 549 .0008 .4392 .0061

C17 1559 .0011 1.7149 .0240

PRISTANE 285 .0022 .6270 .0088

C18 215 .0009 .1935 .0027

PHYTANE 816 .0019 1.5504 .0217

C19 1094 .0008 .8752 .0122

C20 609 .0009 .5481 .0077 CPI 1.8722

ANDROSTANE 0 .0016 .0000 .0000

C21 3243 .0010 3.2430 .0454

C22 2664 .0012 3.1968 .0447 RECOVERY %

C23 4877 .0008 3.9060 .0546 ANDROSTANE .0000

C24 4393 .0021 9.2253 .1290

C25 7217 .0027 19.4859 .2725

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 41739 .0016 15.6432 .8979

UNRESOLVED 378614 .0016 605.7824 8.4728

TOTAL 9.3707

SAMPLE: 46 DATE ANALYZED:10/13/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 18.49

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .6088

C14 1065 .0008 .8520 .0243 C17/PRIST .1622

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 773 .0008 .6184 .0176

C17 344 .0008 .2752 .0078

PRISTANE 2121 .0022 4.6662 .1328

C18 0 .0016 .0000 .0000

PHYTANE 3484 .0020 6.9680 .1983

C19 2403 .0010 2.4030 .0684

C20 2826 .0013 3.6738 .1046 CPI .7712

ANDROSTANE 0 .0017 .0000 .0000

C21 850 .0011 .9350 .0266

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 28280 .0017 24.5038 1.2779

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 1.2779

SAMPLE: 47 DATE ANALYZED: 09/13/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 28.43

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0681

C13 0 .0008 .0000 .0000 PRIST/PHYT .9712

C14 0 .0008 .0000 .0000 C17/PRIST .1874

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 202 .0011 .2222 .0041

PRISTANE 1078 .0022 2.3716 .0439

C18 0 .0009 .0000 .0000

PHYTANE 1110 .0019 2.1090 .0390

C19 0 .0008 .0000 .0000

C20 2903 .0009 2.6127 .0484 CPI .0092

ANDROSTANE 0 .0016 .0000 .0000

C21 0 .0010 .0000 .0000

C22 19003 .0012 22.8036 .4222 RECOVERY %

C23 0 .0008 .0000 .0000 ANDROSTANE .0000

C24 0 .0021 .0000 .0000

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 36234 .0016 19.1008 .9112

UNRESOLVED 531785 .0016 850.8560 25.7516

TOTAL 16.6628

SAMPLE: 48 DATE ANALYZED: 09/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 35.87

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0440

C13 0 .0008 .0000 .0000 PRIST/PHYT .5510

C14 0 .0008 .0000 .0000 C17/PRIST .8884

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 398 .0008 .3184 .0047

PRISTANE 448 .0022 .9856 .0145

C18 0 .0016 .0000 .0000

PHYTANE 813 .0020 1.6260 .0239

C19 315 .0010 .3150 .0046

C20 723 .0013 .9399 .0138 CPI 1.4802

ANDROSTANE 0 .0017 .0000 .0000

C21 1494 .0011 1.6434 .0241

C22 768 .0013 .9984 .0146 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 14116 .0017 15.5669 .3286

UNRESOLVED 320582 .0017 544.9894 7.9966

TOTAL 8.3251

SAMPLE: 49 DATE ANALYZED: 09/03/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 11.12

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .6079

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 842 .0022 1.8524 .0877

C18 0 .0009 .0000 .0000

PHYTANE 1385 .0019 2.6315 .1246

C19 578 .0008 .4624 .0219

C20 235 .0009 .2115 .0100 CPI 1.9245

ANDROSTANE 0 .0016 .0000 .0000

C21 355 .0010 .3550 .0168

C22 3318 .0012 3.9816 .1885 RECOVERY %

C23 7764 .0008 6.2122 .2940 ANDROSTANE .0000

C24 6837 .0021 14.3577 .6796

C25 16922 .0027 45.6894 2.1625

C26 2922 .0034 9.9348 .4702

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 77731 .0016 58.5168 6.8253

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 6.8253

SAMPLE: 51 DATE ANALYZED: 10/12/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 21.10

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1758 .0008 1.4064 .0351 RESOL/UNRESOL .0842

C13 1213 .0008 .9704 .0242 PRIST/PHYT 16.6061

C14 1487 .0008 1.1896 .0297 C17/PRIST .0000

C15 1722 .0008 1.3776 .0344 C18/PHYT .0000

C16 508 .0008 .4064 .0101

C17 0 .0008 .0000 .0000

PRISTANE 3836 .0022 8.4392 .0215

C18 0 .0016 .0000 .0000

PHYTANE 231 .0020 .4620 .0115

C19 8348 ? .0010 3.3480 .0835

C20 864 ? .0013 .7852 .0196 CPI 2.2197

ANDROSTANE 0 .0017 .0000 .0000

C21 2181 .0011 2.3991 .0598

C22 688 .0013 .0000 .0000 RECOVERY %

C23 1524 .0012 .8256 .0206 ANDROSTANE .0000

C24 0 .0017 2.5908 .0646

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 28060 .0017 15.2320 .9836

UNRESOLVED 383343 ? .0017 566.6831 14.1353

TOTAL 15.1189

SAMPLE: 52 DATE ANALYZED: 09/14/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 31.23

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0826

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 0 .0008 .0000 .0000

C20 0 .0009 .0000 .0000 CPI 3.6466 ?

ANDROSTANE 0 .0016 .0000 .0000

C21 1389 .0010 1.3890 .0234

C22 614 .0012 .7368 .0124 RECOVERY %

C23 850 .0008 .6800 .0115 ANDROSTANE .0000

C24 0 .0021 .0000 .0000

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 11884 .0016 14.4496 .2908

UNRESOLVED 143858 .0016 230.1728 3.8791

TOTAL 4.1699

SAMPLE: 53 DATE ANALYZED: 09/20/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 36.62

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL 1.2407

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST 6.5346

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 1418 .0011 1.5598 .0224

PRISTANE 217 .0022 .4774 .0069

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 986 .0008 .7888 .0113

C20 215 .0009 .1935 .0028 CPI 12.7788

ANDROSTANE 0 .0016 .0000 .0000

C21 8095 .0010 8.0950 .1163

C22 680 .0012 .8160 .0117 RECOVERY %

C23 938 .0008 .7504 .0108 ANDROSTANE .0000

C24 0 .0021 .0000 .0000

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 52862 .0016 64.5008 1.1093

UNRESOLVED 42808 .0016 68.1728 .9798

TOTAL 2.0891

SAMPLE: 54 DATE ANALYZED: 09/27/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 40.77

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT 2.7474

C14 0 .0008 .0000 .0000 C17/PRIST 1.2739

C15 0 .0008 .0000 .0000 C18/PHYT 2.7526

C16 0 .0008 .0000 .0000

C17 665 .0008 .5320 .0130

PRISTANE 522 .0022 1.1484 .0282

C18 523 .0016 .8368 .0205

PHYTANE 190 .0020 .3800 .0093

C19 774 .0010 .7740 .0190

C20 620 .0013 .8060 .0198 CPI 1.8226

ANDROSTANE 0 .0017 .0000 .0000

C21 934 .0011 1.0274 .0252

C22 430 .0013 .5590 .0137 RECOVERY %

C23 494 .0012 .5928 .0145 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 10378 .0017 8.8842 .3812

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .3812

SAMPLE: 55 DATE ANALYZED: 11/10/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 36.19

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 1259 .0011 1.3849 .0383

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 1970 .0017 1.2087 .0717

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .0717

SAMPLE: 56 DATE ANALYZED: 09/21/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 38.36

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0469

C13 1927 .0008 1.5416 .0442 PRIST/PHYT .0151

C14 382 .0008 .3056 .0088 C17/PRIST 153.9881

C15 1296 .0008 1.0368 .0297 C18/PHYT .4328

C16 1107 .0008 .8856 .0254

C17 12935 .0011 14.2285 .4079

PRISTANE 84 .0022 .1848 .0053

C18 2411 .0009 2.1399 .0622

PHYTANE 5571 .0019 10.5849 .3034

C19 2142 .0008 1.7136 .0491

C20 1900 .0009 1.7100 .0490 CPI 2.6827

ANDROSTANE 0 .0016 .0000 .0000

C21 512 .0010 .5130 .0147

C22 0 .0012 .0000 .0000 RECOVERY %

C23 603 .0008 .4824 .0138 ANDROSTANE .0000

C24 1437 .0021 3.0177 .0865

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 77952 .0016 73.0320 3.1936

UNRESOLVED 1661693 .0016 2658.7088 76.2157

TOTAL 79.4093

SAMPLE: 57 DATE ANALYZED: 08/28/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 21.13

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1620 .0008 1.2960 .6130 RESOL/UNRESOL .0375

C13 1213 .0008 .9704 .0459 PRIST/PHYT .0674

C14 207 .0008 .1656 .0078 C17/PRIST 5.9368

C15 169 .0008 .1352 .0064 C18/PHYT .5436

C16 916 .0008 .7328 .0347

C17 1502 .0011 1.6522 .0782

PRISTANE 253 .0022 .5566 .0263

C18 2040 .0009 1.8360 .0869

PHYTANE 3753 .0019 7.1307 .3375

C19 2641 .0008 2.1128 .0000

C20 959 .0009 .8631 .0408 CPI 1.0714

ANDROSTANE 0 .0016 .0000 .0000

C21 1108 .0010 1.1080 .0524

C22 403 .0012 .4836 .0229 RECOVERY %

C23 526 .0008 .4208 .0139 ANDROSTANE .0000

C24 2157 .0021 4.5297 .2144

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 90706 .0016 113.9824 6.5299

UNRESOLVED 5415684 .0016 3865.0944 182.9198

TOTAL 189.4496

SAMPLE: 58 DATE ANALYZED: 09/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 22.99

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0360

C13 0 .0008 .0000 .0000 PRIST/PHYT 6.3298

C14 791 .0008 .6328 .0145 C17/PRIST .1391

C15 999 .0008 .7992 .0183 C18/PHYT .5069

C16 794 .0008 .6352 .0145

C17 1660 .0011 1.8260 .0418

PRISTANE 11938 .0022 26.2636 .6013

C18 956 .0009 .8604 .0197

PHYTANE 1886 .0019 3.5834 .0820

C19 779 .0008 .6232 .0143

C20 216 .0009 .1944 .0045 CPI 1.5803

ANDROSTANE 0 .0016 .0000 .0000

C21 919 .0010 .9190 .0210

C22 0 .0012 .0000 .0000 RECOVERY %

C23 0 .0008 .0000 .0000 ANDROSTANE .0000

C24 0 .0021 .0000 .0000

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 50271 .0016 46.9328 1.9063

UNRESOLVED 1394938 .0016 2231.9008 51.0955

TOTAL 53.0018

SAMPLE: 59 DATE ANALYZED: 09/2782

INTERNAL STANDARD SAMPLE VOLUME (ML): 3.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 33.70

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0401

C13 0 .0008 .0000 .0000 PRIST/PHYT 1.4713

C14 0 .0008 .0000 .0000 C17/PRIST .1326

C15 1089 .0008 .8712 .0776 C18/PHYT .6613

C16 1110 .0008 .8880 .7910

C17 681 .0008 .5548 .0485

PRISTANE 5135 .0022 11.2970 1.0057

C18 2308 .0016 3.6928 .3287

PHYTANE 349 .0020 6.9800 .6214

C19 459 .0010 4.5900 .4086

C20 4607 .0013 5.9891 .5332 CPI 1.7717

ANDROSTANE 0 .0017 .0000 .0000

C21 8163 .0011 8.9859 .7999

C22 0 .0013 .0000 .0000 RECOVERY %

C23 2407 .0012 2.8884 .2371 ANDROSTANE .0000

C24 1534 .0017 2.6078 .2321

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 66012 .0017 52.5134 9.0669

UNRESOLVED 1647093 .0017 2800.0581 249.2633

TOTAL 258.3302

SAMPLE: 60 DATE ANALYZED: 10/12/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 3.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 27.02

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1427 .0008 1.1416 .0667 RESOL/UNRESOL .0356

C13 1301 .0008 1.0408 .0608 PRIST/PHYT 1.9261

C14 4246 .0008 3.3968 .1985 C17/PRIST .0803

C15 6761 .0008 5.4088 .3161 C18/PHYT .8307

C16 3918 .0008 3.1344 .1832

C17 653 .0008 .5224 .0305

PRISTANE 8136 .0022 17.8992 1.0460

C18 3509 .0016 5.6144 .3281

PHYTANE 4224 .0020 8.4480 .4937

C19 10414 .0010 10.4140 .6086

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 2070 .0011 2.2770 .1331

C22 495 .0013 .6435 .0376 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 100999 .0017 91.5365 8.8518

UNRESOLVED 2839348 .0017 4826.8915 282.0645

TOTAL 290.9172

SAMPLE: 61 DATE ANALYZED: 11/12/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 5.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 20.36

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0276

C13 0 .0008 .0000 .0000 PRIST/PHYT 9.9393

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 323 .0008 .2584 .0635 C18/PHYT .0000

C16 1480 .0008 1.1840 .2908

C17 0 .0008 .0000 .0000

PRISTANE 11957 .0022 26.3054 6.4601

C18 0 .0016 .0000 .0000

PHYTANE 1203 .0020 3.4060 .5909

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .2182

ANDROSTANE 30703 .0017 52.1951 12.8180

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 52.1951

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 44439 .0017 50.1092 19.7110

UNRESOLVED 1611967 .0017 2740.3439 672.9725

TOTAL 692.6884

SAMPLE: 62 DATE ANALYZED: 11/12/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 5.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 29.48

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0172

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 414 .0008 .3312 .0112 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 5138 .0022 11.3036 .3834

C18 175 .0016 .2800 .0095

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI 2.3657

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 15402 .0017 16.4475 .9621

UNRESOLVED 893141 .0017 1518.3397 51.5041

TOTAL 52.4661

SAMPLE: 63 DATE ANALYZED: 09/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 5.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 28.21

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 1165 .0011 1.2815 .0239

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 3943 .0017 4.7226 .1120

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .1120

SAMPLE: 64 DATE ANALYZED: 10/20/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 30.34

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .1887

C14 0 .0008 .0000 .0000 C17/PRIST 1.4610

C15 1849 .0008 1.4792 .0257 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 225 .0008 .1800 .0031

PRISTANE 154 .0022 .3388 .0059

C18 0 .0016 .0000 .0000

PHYTANE 816 .0020 1.6320 .0283

C19 1507 .0010 1.5070 .0261

C20 0 .0013 .0000 .0000 CPI 7.1264

ANDROSTANE 0 .0017 .0000 .0000

C21 1572 .0011 1.7292 .0300

C22 2617 .0013 3.4021 .0590 RECOVERY %

C23 3476 .0012 4.1712 .0724 ANDROSTANE .0000

C24 2035 .0017 3.4595 .0600

C25 16686 .0020 33.3720 .5789

C26 15212 .0029 44.4309 .7708

C27 117020 .0095 1111.6900 19.2848

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 191270 .0017 47.5864 21.7704

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 21.7704

SAMPLE: 65 DATE ANALYZED: 09/28/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 31.13

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .2214

C14 0 .0008 .0000 .0000 C17/PRIST .9396

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 249 .0008 .1192 .0034

PRISTANE 265 .0022 .5830 .0099

C18 0 .0016 .0000 .0000

PHYTANE 1197 .0020 2.3940 .0405

C19 1231 .0010 1.2310 .0208

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 1010 .0011 1.1110 .0188

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 5879 .0017 3.2759 .1487

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .1487

SAMPLE: 66 DATE ANALYZED: 10/20/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 15.54

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .1351

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 2708 .0008 2.1664 .0734 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 2907 .0022 6.3954 .2166

C18 574 .0016 .9184 .0311

PHYTANE 0 .0020 .0000 .0000

C19 1714 .0010 1.7140 .0581

C20 3964 .0013 5.1532 .1745 CPI 2.6061

ANDROSTANE 0 .0017 .0000 .0000

C21 5718 .0011 6.2898 .2130

C22 2264 .0013 2.9432 .0997 RECOVERY %

C23 5086 .0012 6.1032 .2067 ANDROSTANE .0000

C24 5259 .0017 8.9403 .3028

C25 16206 .0020 32.4120 1.0977

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 52557 .0017 10.4669 2.8281

UNRESOLVED 388900 .0017 661.1300 22.3915

TOTAL 25.2196

SAMPLE: 67 DATE ANALYZED: 09/28/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 43.19

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT 1.0457

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 1746 .0008 1.3968 .0170 C18/PHYT .5734

C16 310 .0008 .2480 .0030

C17 0 .0008 .0000 .0000

PRISTANE 755 .0022 1.6610 .0202

C18 414 .0016 .6624 .0081

PHYTANE 722 .0020 1.4440 .0176

C19 490 .0010 .4900 .0060

C20 874 .0013 1.1362 .0138 CPI 1.3992

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 10174 .0017 8.2671 .1865

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .1865

SAMPLE: 68 DATE ANALYZED: 09/09/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 11.18

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .5243

C13 0 .0008 .0000 .0000 PRIST/PHYT 2.0991

C14 0 .0008 .0000 .0000 C17/PRIST .9764

C15 1605 .0008 1.2840 .0604 C18/PHYT 3.4180

C16 0 .0008 .0000 .0000

C17 662 .0011 .7282 .0343

PRISTANE 678 .0022 1.4916 .0702

C18 1104 .0009 .9936 .0468

PHYTANE 323 .0019 .6137 .0289

C19 2165 .0008 1.7320 .0815

C20 2757 .0009 2.4813 .1168 CPI 1.7947

ANDROSTANE 0 .0016 .0000 .0000

C21 3314 .0010 3.3140 .1560

C22 2046 .0012 2.4552 .1156 RECOVERY %

C23 2810 .0008 2.2480 .1058 ANDROSTANE .0000

C24 1682 .0021 4.1622 .1959

C25 3602 .0027 9.7524 .4578

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 26581 .0016 5.6528 1.7363

UNRESOLVED 50698 .0016 81.1168 3.8187

TOTAL 5.5550

SAMPLE: 69 DATE ANALYZED: 10/21/82

INTERNAL STANDARD SAMPLE VOLUME (ML): .5

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 39.75

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0466

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 849 .0008 .6792 .0045 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 442 .0013 .5746 .0038 CPI 2.9317

ANDROSTANE 0 .0017 .0000 .0000

C21 3170 .0011 3.4870 .0231

C22 2400 .0013 3.1200 .0207 RECOVERY %

C23 4313 .0012 5.1756 .0343 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 15228 .0017 6.8918 .1319

UNRESOLVED 326870 .0017 555.8790 3.6788

TOTAL 3.8107

SAMPLE: 70 DATE ANALYZED: 10/11/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 32.68

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 4686 .0008 3.4788 .0604 RESOL/UNRESOL .0000

C13 2951 .0008 2.3608 .0380 PRIST/PHYT .9776

C14 4344 .0008 3.4752 .0560 C17/PRIST .1881

C15 3135 .0008 2.5080 .0404 C18/PHYT .1819

C16 967 .0008 .7736 .0125

C17 566 .0008 .4528 .0073

PRISTANE 3009 .0022 6.6198 .1066

C18 560 .0016 .8960 .0144

PHYTANE 3078 .0020 6.1560 .0991

C19 1578 .0010 1.5780 .0254

C20 574 .0013 .7462 .0120 CPI 1.3964

ANDROSTANE 0 .0017 .0000 .0000

C21 793 .0011 .8723 .0140

C22 629 .0013 .8177 .0132 RECOVERY %

C23 855 .0012 1.0260 .0165 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 30866 .0017 5.3397 .6019

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .6019

SAMPLE: 71 DATE ANALYZED: 10/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 20.00

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1787 .0008 1.4296 .0376 RESOL/UNRESOL .0000

C13 687 .0008 .5496 .0145 PRIST/PHYT .0000

C14 239 .0008 .1912 .0050 C17/PRIST .0000

C15 3323 .0008 1.6584 .0700 C18/PHYT .0000

C16 1261 .0008 1.0088 .0265

C17 465 .0008 .3720 .0098

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 2021 .0020 4.0420 .1064

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI 1.7618

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 1040 .0013 1.3520 .0356 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 37192 .0017 44.8273 1.4850

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 1.4850

SAMPLE: 72 DATE ANALYZED: 08/30/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 11.98

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .2726

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 265 .0011 .2915 .0128

PRISTANE 972 .0022 2.1384 .0939

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 0 .0008 .0000 .0000

C20 0 .0009 .0000 .0000 CPI 5.4907

ANDROSTANE 0 .0016 .0000 .0000

C21 692 .0010 .6920 .0304

C22 1512 .0012 1.8144 .0797 RECOVERY %

C23 22073 .0008 17.6584 .7758 ANDROSTANE .0000

C24 11359 .0021 23.8539 1.0480

C25 71061 .0027 191.8647 8.4292

C26 7529 .0034 25.5986 1.1246

C27 52945 .0065 344.1425 15.1192

C28 6379 .0051 32.5329 1.4293

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 180652 .0016 9.3840 28.5551

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 28.5551

SAMPLE: 73 DATE ANALYZED: 09/14/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 39.47

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST 2.4381

C15 910 .0008 .7280 .0097 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 1497 .0011 1.6467 .0220

PRISTANE 814 .0022 1.3508 .0180

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 0 .0008 .0000 .0000

C20 0 .0009 .0000 .0000 CPI 5.2380

ANDROSTANE 0 .0016 .0000 .0000

C21 540 .0010 .5400 .0072

C22 0 .0012 .0000 .0000 RECOVERY %

C23 552 .0008 .4416 .0059 ANDROSTANE .0000

C24 668 .0021 1.4028 .0187

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 5460 .0016 1.0864 .0960

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .0960

SAMPLE: 74 DATE ANALYZED: 10/12/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 26.20

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 2794 .0022 6.1498 .1235

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 1048 .0011 1.1528 .0232

C22 0 .0013 .0000 .0000 RECOVERY %

C23 1944 .0012 2.3328 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0496

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 9140 .0017 5.7018 .3080

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .3080

SAMPLE: 75 DATE ANALYZED: 10/21/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 3.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 31.38

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0175

C13 0 .0008 .0000 .0000 PRIST/PHYT 38.4000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 2148 .0008 1.7184 .0865 C18/PHYT .0000

C16 316 .0008 .2528 .0127

C17 0 .0008 .0000 .0000

PRISTANE 2688 .0022 5.9136 .2976

C18 0 .0016 .0000 .0000

PHYTANE 70 .0020 .1400 .0070

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI 6.7975

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 18940 .0017 23.3206 1.5772

UNRESOLVED 1085252 .0017 1844.9284 92.8313

TOTAL 94.4085

SAMPLE: 76 DATE ANALYZED: 11/10/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 38.27

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 2564 .0008 2.0512 .0536 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 7632 .0022 16.7904 .4387

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 2681 .0011 2.9491 .0771

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 2927 .0095 27.8065 .7266

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 16540 .0017 1.2512 1.3287

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 1.3287

SAMPLE: 77 DATE ANALYZED: 09/23/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 25.19

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 757 .0008 .6056 .0127 RESOL/UNRESOL .0976

C13 0 .0008 .0000 .0149 PRIST/PHYT .5725

C14 893 .0008 .7144 .0304 C17/PRIST 1.2224

C15 1821 .0008 1.4568 .0213 C18/PHYT .8530

C16 1276 .0008 1.0208 .0113

C17 676 .0008 .5408 .0254

PRISTANE 553 .0022 1.2166 .0275

C18 824 .0016 1.3184 .0404

PHYTANE 966 .0020 1.9320 .0247

C19 1183 .0010 1.1830 .0176

C20 647 .0013 .8411 .0000 CPI 4.8468

ANDROSTANE 0 .0017 .0000 .0307

C21 1334 .0011 1.4674 .0000

C22 0 .0013 .0000 .0267 RECOVERY %

C23 1064 .0012 1.2768 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0188

C25 450 .0020 .9000 .0950

C26 1568 .0029 4.5472 2.8696

C27 14457 .0095 137.3415 .0000

C28 0 .0076 .0000 1.1029

C29 4257 .0124 52.7868 .0000

C30 0 .0050 .0000 .0000

RESOLVED 44847 .0017 20.6057 4.8005

UNRESOLVED 459591 .0017 781.3047 16.3245

TOTAL 21.1249

SAMPLE: 78 DATE ANALYZED: 10/12/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 23.94

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 0 .0017 .0000 .0000

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .0000

SAMPLE: 79 DATE ANALYZED: 09/28/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 25.02

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .5311

C15 752 .0008 .6016 .0127 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 802 .0008 .6416 .0135

PRISTANE 1510 .0022 3.3220 .0699

C18 1607 .0016 2.5712 .0541

PHYTANE 0 .0020 .0000 .0000

C19 674 .0010 .6740 .0142

C20 319 .0013 .4147 .0087 CPI 1.7285

ANDROSTANE 0 .0017 .0000 .0000

C21 1101 .0011 1.2111 .0255

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 19228 .0017 21.1871 .6442

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .6442

SAMPLE: 80 DATE ANALYZED: 08/31/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 27.50

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .2532

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .8347

C16 0 .0008 .0000 .0000

C17 3001 .0011 3.3011 .0632

PRISTANE 0 .0022 .0000 .0000

C18 692 .0009 .6228 .0119

PHYTANE 829 .0019 1.5751 .0301

C19 6493 .0008 5.1944 .0994

C20 565 .0009 .5085 .0097 CPI 3.5754

ANDROSTANE 0 .0016 .0000 .0000

C21 7908 .0010 7.9080 .1513

C22 495 .0012 .5940 .0114 RECOVERY %

C23 20329 .0008 16.2632 .3113 ANDROSTANE .0000

C24 4634 .0021 9.7314 .1862

C25 17193 .0027 46.4211 .8884

C26 8692 .0034 29.5528 .5656

C27 63603 .0065 413.4195 7.9123

C28 18073 .0051 92.1723 1.7641

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 0 .0016 125.7440 14.4116

UNRESOLVED 231097 .0016 1458.3632 27.9113

TOTAL 911477 42.3229

SAMPLE: 81 DATE ANALYZED: 08/24/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 16.41

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 852 .0022 1.8744 .0601

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 269 .0008 .2152 .0069

C20 0 .0009 .0000 .0000 CPI 3.1869

ANDROSTANE 0 .0016 .0000 .0000

C21 1118 .0010 1.1180 .0359

C22 4622 .0012 5.5464 .1779 RECOVERY %

C23 3049 .0008 2.4392 .0782 ANDROSTANE .0000

C24 21 .0021 .0441 .0014

C25 10361 .0027 27.9747 .8972

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 34440 .0016 22.6368 1.9837

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 1.9837

SAMPLE: 82 DATE ANALYZED: 10/14/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 19.23

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 2539 .0008 2.0312 .0556 C18/PHYT .0000

C16 773 .0008 .6184 .0169

C17 0 .0008 .0000 .0000

PRISTANE 1106 .0022 2.4332 .0666

C18 618 .0016 .9888 .0271

PHYTANE 0 .0020 .0000 .0000

C19 1570 .0010 1.5700 .0430

C20 0 .0013 .0000 .0000 CPI 7.1216

ANDROSTANE 238200 .0017 404.9400 11.0830

C21 5284 .0011 5.8124 .1591

C22 3039 .0013 3.9507 .1081 RECOVERY %

C23 16355 .0012 19.6236 .5371 ANDROSTANE 42.6253

C24 10493 .0017 17.8381 .4882

C25 44660 .0020 89.3200 2.4446

C26 0 .0029 .0000 .0000

C27 26544 .0095 252.1680 6.9017

C28 0 .0076 .0000 .0000

C29 9325 .0124 115.6300 3.1647

C30 0 .0050 .0000 .0000

RESOLVED 138220 .0017 27.0572 14.7533

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 14.7533

SAMPLE: 83 DATE ANALYZED: 08/25/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 28.13

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 2957 .0008 2.3656 .0625 RESOL/UNRESOL .2022

C13 2038 .0008 1.6304 .0431 PRIST/PHYT 2.6464

C14 3338 .0008 2.6704 .0706 C17/PRIST .0000

C15 8030 .0008 6.4240 .1698 C18/PHYT .0000

C16 5869 .0008 4.6952 .1241

C17 0 .0011 .0000 .0000

PRISTANE 12377 .0022 27.2294 .7198

C18 0 .0009 .0000 .0000

PHYTANE 4677 .0019 9.3540 .2473

C19 15832 .0008 15.8320 .4185

C20 0 .0009 .0000 .0000 CPI 1.9308

ANDROSTANE 131680 .0016 233.8560 5.9176

C21 11841 .0010 13.0251 .3443

C22 9743 .0012 12.6659 .3348 RECOVERY %

C23 7192 .0008 8.6304 .2281 ANDROSTANE 23.5638

C24 4322 .0021 7.3474 .1942

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 113115 .0016 42.3283 4.0782

UNRESOLVED 559347 .0016 950.8899 25.1365

TOTAL 29.2127

SAMPLE: 86 DATE ANALYZED: 10/19/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 34.34

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 3804 .0008 3.0432 .0466 RESOL/UNRESOL .0000

C13 1402 .0008 1.1216 .0172 PRIST/PHYT .3574

C14 2701 .0008 2.1608 .0331 C17/PRIST 1.4074

C15 5178 .0008 4.1424 .0635 C18/PHYT 1.8640

C16 3621 .0008 2.8968 .0444

C17 418 .0008 .3344 .0051

PRISTANE 297 .0022 .6534 .0100

C18 1549 .0016 2.4784 .0380

PHYTANE 831 .0020 1.6620 .0255

C19 6739 .0010 6.7390 .1033

C20 1150 .0013 1.4950 .0229 CPI 1.6185

ANDROSTANE 203330 .0017 345.6610 5.2978

C21 6330 .0011 6.9630 .1067

C22 4943 .0013 6.4259 .0985 RECOVERY %

C23 5089 .0012 6.1068 .9360 ANDROSTANE 36.3854

C24 2819 .0017 4.7923 .0734

C25 2008 .0020 4.0160 .0616

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 64810 .0017 27.0827 1.2585

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 1.2585

SAMPLE: 87 DATE ANALYZED: 10/21/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 34.22

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0745

C13 0 .0008 .0000 .0000 PRIST/PHYT 3.8113

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .6167

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 1959 .0022 4.3098 .0663

C18 317 .0016 .5072 .0078

PHYTANE 514 .0020 1.0280 .0158

C19 3023 .0010 3.0230 .0465

C20 0 .0013 .0000 .0000 CPI 2.1650

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 6091 .0013 7.9183 .1218 RECOVERY %

C23 18561 .0012 22.2732 .3426 ANDROSTANE .0000

C24 12827 .0017 21.8059 .3354

C25 29830 .0020 59.6600 .9176

C26 4513 .0029 13.0877 .2013

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 131210 .0017 91.0775 3.4558

UNRESOLVED 1762186 .0017 2995.7162 46.0752

TOTAL 49.5310

SAMPLE: 88 DATE ANALYZED: 09/17/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 0.0

DRY WEIGHT EXTRACTED (G): 35.06

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 4764 .0022 10.4808 .1573

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 279 .0008 .2232 .0034

C20 0 .0009 .0000 .0000 CPI .6293

ANDROSTANE 0 .0016 .0000 .0000

C21 894 .0010 .8940 .0134

C22 1864 .0012 2.2368 .0336 RECOVERY %

C23 0 .0008 .0000 .0000 ANDROSTANE .0000

C24 0 .0021 .0000 .0000

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 8190 .0016 .6224 .2170

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .2170

SAMPLE: 89 DATE ANALYZED: 09/09/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 52.02

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 400 .0008 .3200 .0032 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 652 .0008 .5216 .0053 C17/PRIST .0000

C15 2087 .0008 1.6696 .0169 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 81 .0011 .0891 .0009

PRISTANE 0 .0022 .0000 .0000

C18 341 .0009 .3069 .0031

PHYTANE 0 .0019 .0000 .0000

C19 420 .0008 .3360 .0034

C20 367 .0009 .3303 .0033 CPI 1.6443

ANDROSTANE 107680 .0016 172.2880 1.7431

C21 403 .0010 .4030 .0041

C22 459 .0012 .5508 .0056 RECOVERY %

C23 0 .0008 .0000 .0000 ANDROSTANE 18.1356

C24 0 .0021 .0000 .0000

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 6350 .0016 1.8240 .0643

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .0643

SAMPLE: 90 DATE ANALYZED: 09/15/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 30.59

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 439 .0008 .3512 .0060 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT 34.1230

C14 476 .0008 .3808 .0066 C17/PRIST .0000

C15 2276 .0008 1.8208 .0313 C18/PHYT 1.6623

C16 551 .0008 .4408 .0076

C17 0 .0011 .0000 .0000

PRISTANE 13035 .0022 28.6770 .4934

C18 635 .0009 .5715 .0098

PHYTANE 382 .0019 .7258 .0125

C19 1275 .0008 1.0200 .0175

C20 709 .0009 .6381 .0110 CPI 4.0347

ANDROSTANE 168570 .0016 265.7120 4.6405

C21 8050 .0010 8.0500 .1385

C22 890 .0012 1.0680 .0184 RECOVERY %

C23 818 .0008 .6544 .0113 ANDROSTANE 58.3907

C24 0 .0021 .0000 .0000

C25 738 .0027 1.9926 .0543

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 37535 .0016 11.6176 .9981

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .9981

SAMPLE: 92 DATE ANALYZED: 10/15/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 27.59

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI 2.9131

ANDROSTANE 0 .0017 .0000 .0000

C21 5118 .0011 5.6298 .1074

C22 2647 .0013 3.4411 .0656 RECOVERY %

C23 2593 .0012 3.1116 .0594 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 16068 .0017 9.7070 .4176

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .4176

SAMPLE: 93 DATE ANALYZED: 10/13/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 30.64

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 2470 .0008 1.9760 .0339 RESOL/UNRESOL .0000

C13 1928 .0008 1.5424 .0265 PRIST/PHYT .0000

C14 452 .0008 .3616 .0062 C17/PRIST 1.5698

C15 11873 .0008 9.4984 .1632 C18/PHYT .0000

C16 1393 .0008 1.1144 .0191

C17 8397 .0008 6.7176 .1154

PRISTANE 5349 .0022 11.7678 .2021

C18 2876 .0016 4.6016 .0790

PHYTANE 0 .0020 .0000 .0000

C19 4540 .0010 4.5400 .0780

C20 8726 .0013 11.3438 .1949 CPI 1.3312

ANDROSTANE 0 .0017 .0000 .0780

C21 494 .0011 .5434 .0093

C22 11319 .0013 14.7147 .2528 RECOVERY %

C23 19088 .0012 22.9056 .3935 ANDROSTANE .0000

C24 11498 .0017 19.5466 .3358

C25 8487 .0020 16.9740 .2916

C26 4906 .0029 14.2274 .2444

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 162245 .0017 99.3633 4.1524

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 4.1524

SAMPLE: 94 DATE ANALYZED: 08/23/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 21.16

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1208 .0012 1.4496 .0361 RESOL/UNRESOL .0000

C13 795 .0014 1.1130 .0277 PRIST/PHYT .0000

C14 779 .0011 .8569 .0213 C17/PRIST .0000

C15 0 .0015 .0000 .0000 C18/PHYT .0000

C16 614 .0013 .7982 .0199

C17 106 .0016 .1696 .0042

PRISTANE 0 .0040 .0000 .0000

C18 409 .0014 .5726 .0142

PHYTANE 0 .0039 .0000 .0000

C19 1230 .0016 1.9680 .0490

C20 225 .0014 .3150 .0078 CPI 1.0513

ANDROSTANE 129380 .0016 207.0080 5.1489

C21 0 .0017 .0000 .0000

C22 0 .0015 .0000 .0000 RECOVERY %

C23 0 .0015 .0000 .0000 ANDROSTANE 31.7903

C24 0 .0017 .0000 .0000

C25 0 .0030 .0000 .0000

C26 0 .0000 .0000 .0000

C27 0 .0000 .0000 .0000

C28 0 .0000 .0000 .0000

C29 0 .0000 .0000 .0000

C30 0 .0000 .0000 .0000

RESOLVED 11887 .0016 10.4336 .4397

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .4397

SAMPLE: 95 DATE ANALYZED: 08/23/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 10.86

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 733 .0012 .8796 .0426 RESOL/UNRESOL .0000

C13 0 .0014 .0000 .0000 PRIST/PHYT .0000

C14 0 .0011 .0000 .0000 C17/PRIST 1.2849

C15 699 .0015 1.0485 .0508 C18/PHYT .0000

C16 0 .0013 .0000 .0000

C17 478 .0016 .7648 .0371

PRISTANE 372 .0040 1.4880 .0721

C18 0 .0014 .0000 .0000

PHYTANE 0 .0039 .0000 .0000

C19 0 .0016 .0000 .0000

C20 1202 .0014 1.6828 .0816 CPI 1.5033

ANDROSTANE 155750 .0016 249.2000 12.0772

C21 630 .0017 1.0810 .0519

C22 0 .0015 .0000 .0000 RECOVERY %

C23 0 .0015 .0000 .0000 ANDROSTANE 26.2316

C24 0 .0017 .0000 .0000

C25 0 .0030 .0000 .0000

C26 0 .0000 .0000 .0000

C27 0 .0000 .0000 .0000

C28 0 .0000 .0000 .0000

C29 0 .0000 .0000 .0000

C30 0 .0000 .0000 .0000

RESOLVED 21018 .0016 27.0464 1.6468

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 1.6468

SAMPLE: 96 DATE ANALYZED: 10/25/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 22.71

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 3424 .0008 2.7392 .0635 RESOL/UNRESOL .1566

C13 1586 .0008 1.2688 .0294 PRIST/PHYT .5404

C14 1647 .0008 1.3176 .0305 C17/PRIST .0000

C15 5306 .0008 4.2448 .0994 C18/PHYT 1.6119

C16 4278 .0008 3.4224 .0793

C17 0 .0008 .0000 .0000

PRISTANE 408 .0022 .8976 .0208

C18 1217 .0016 1.9472 .0451

PHYTANE 755 .0020 1.5100 .0350

C19 5705 .0010 5.7050 .1322

C20 720 .0013 .9360 .0217 CPI 1.5461

ANDROSTANE 175660 .0017 298.6220 6.9207

C21 5283 .0011 5.8113 .1347

C22 4075 .0013 5.2975 .1228 RECOVERY %

C23 2510 .0012 5.0120 .0698 ANDROSTANE 31.4339

C24 2117 .0017 3.5989 .0834

C25 1339 .0020 2.6780 .6210

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 55481 .0017 25.6887 1.6240

UNRESOLVED 354379 .0017 602.4443 13.9620

TOTAL 15.5860

SAMPLE: 97 DATE ANALYZED: 10/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 27.65

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1954 .0008 1.5632 .0298 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 1770 .0008 1.4160 .0270 C17/PRIST .0000

C15 3001 .0008 2.4008 .0457 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 23282 .0022 51.2204 .9750

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 1625 .0010 1.6250 .0309

C20 0 .0013 .0000 .0000 CPI 4.2395

ANDROSTANE 0 .0017 .0000 .0000

C21 2878 .0011 3.1658 .0603

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 43737 .0017 15.6859 1.4672

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 1.4672

SAMPLE: 99 DATE ANALYZED: 10/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 27.65

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 392 .0008 .3136 .0057 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 2200 .0008 1.7600 .0320 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 10587 .0022 23.2914 .4229

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 636 .0010 .6360 .0115

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 2625 .0011 2.8875 .0524

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 118863 .0017 174.1191 3.6856

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 3.6856

SAMPLE: 100 DATE ANALYZED: 09/16/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 13.18

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 211 .0008 .1688 .0067 C17/PRIST 11.8295

C15 650 .0008 .5200 .0208 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 8624 .0011 9.4864 .3788

PRISTANE 729 .0022 1.6038 .0640

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 2767 .0008 2.2136 .0884

C20 0 .0009 .0000 .0000 CPI 7.3951

ANDROSTANE 163880 .0016 262.2080 10.4707

C21 5186 .0010 5.1860 .2071

C22 441 .0012 .5292 .0211 RECOVERY %

C23 2166 .0008 1.7328 .6920 ANDROSTANE 27.6008

C24 2130 .0021 4.5990 .1837

C25 1624 .0027 4.3848 .1751

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 31332 .0016 10.7904 1.6458

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 1.6458

SAMPLE: 101 DATE ANALYZED: 09/16/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 14.89

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1228 .0008 .9824 .0347 RESOL/UNRESOL .1214

C13 1787 .0008 1.4296 .0505 PRIST/PHYT .1406

C14 968 .0008 .7744 .0274 C17/PRIST 88.4088

C15 483 .0008 .3864 .0137 C18/PHYT 1.0703

C16 678 .0008 .5424 .0192

C17 26169 .0011 28.7859 1.0175

PRISTANE 296 .0022 .6512 .0230

C18 2253 .0009 2.0277 .0717

PHYTANE 2105 .0019 3.9995 .1424

C19 3968 .0008 3.1744 .1122

C20 4292 .0009 3.8628 .1365 CPI 3.2840

ANDROSTANE 153080 .0016 244.9280 8.6575 25.7819

C21 3260 .0010 3.2600 .1152

C22 2508 .0012 3.0096 .1064 RECOVERY %

C23 5545 .0008 4.4360 .1568 ANDROSTANE .0000

C24 5662 .0021 11.8902 .4203

C25 11230 .0027 30.3210 1.0718

C26 0 .0034 .0000 .0000

C27 1287 .0065 8.3655 .2957

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 111392 .0016 60.2768 5.9445

UNRESOLVED 917566 .0016 1468.1056 51.8930

TOTAL 57.8375

SAMPLE: 102 DATE ANALYZED: 09/14/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 10.21

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 2086 .0008 1.6688 .0860 RESOL/UNRESOL .2229

C13 771 .0008 .6168 .0318 PRIST/PHYT 54.4304

C14 463 .0008 .3704 .0191 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .5392

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 34019 .0022 74.8418 3.8580

C18 337 .0009 .3033 .0156

PHYTANE 625 .0019 1.1875 .0612

C19 131 .0008 .1048 .0054

C20 509 .0009 .4581 .0236 CPI 2.9030

ANDROSTANE 116650 .0016 186.6400 9.6211

C21 1807 .0010 1.8070 .0931

C22 0 .0012 .0000 .0000 RECOVERY %

C23 523 .0008 .4184 .0216 ANDROSTANE 19.6463

C24 0 .0021 .0000 .0000

C25 568 .0027 1.5336 .0791

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 59560 .0016 28.3536 5.7562

UNRESOLVED 267242 .0016 427.5872 22.0417

TOTAL 27.7979

SAMPLE: 103 DATE ANALYZED: 09/29/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 7.75

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .1004

C13 0 .0008 .0000 .0000 PRIST/PHYT 3.3879

C14 0 .0008 .0000 .0000 C17/PRIST 2.5776

C15 1818 .0008 1.4544 .0988 C18/PHYT .1291

C16 1092 .0008 .8736 .5930

C17 33341 .0008 26.6728 1.8114

PRISTANE 12935 .0022 28.4570 1.9326

C18 493 .0016 .7888 .0536

PHYTANE 3818 .0020 7.6360 .5186

C19 4606 .0010 4.6060 .3128

C20 2167 .0013 2.8171 .1913 CPI 8.7938

ANDROSTANE 129300 .0017 219.8100 14.9277

C21 5353 .0011 5.8883 .3999

C22 374 .0013 .4862 .0330 RECOVERY %

C23 1751 .0012 2.1012 .1427 ANDROSTANE 23.1379

C24 1247 .0017 2.1199 .1440

C25 5753 .0020 11.5060 .7814

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 175289 .0017 170.9197 18.0867

UNRESOLVED 1746770 .0017 2969.5090 201.6644

TOTAL 219.7512

SAMPLE: 104 DATE ANALYZED: 08/18/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 24.2

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0012 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0014 .0000 .0000 PRIST/PHYT .0000

C14 0 .0011 .0000 .0000 C17/PRIST .0000

C15 0 .0015 .0000 .0000 C18/PHYT .0000

C16 0 .0013 .0000 .0000

C17 0 .0016 .0000 .0000

PRISTANE 0 .0040 .0000 .0000

C18 0 .0014 .0000 .0000

PHYTANE 0 .0039 .0000 .0000

C19 0 .0016 .0000 .0000

C20 0 .0014 .0000 .0000 CPI .0000

ANDROSTANE 0 .0016 .0000 .0000

C21 0 .0017 .0000 .0000

C22 0 .0015 .0000 .0000 RECOVERY %

C23 0 .0015 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0030 .0000 .0000

C26 0 .0000 .0000 .0000

C27 0 .0000 .0000 .0000

C28 0 .0000 .0000 .0000

C29 0 .0000 .0000 .0000

C30 0 .0000 .0000 .0000

RESOLVED 0 .0016 .0000 .0000

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .0000

SAMPLE: 105 DATE ANALYZED: 09/16/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 13.57

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1920 .0008 1.5360 .0596 RESOL/UNRESOL .0000

C13 1456 .0008 1.1648 .0452 PRIST/PHYT 75.6971

C14 1439 .0008 1.1512 .0446 C17/PRIST .0000

C15 655 .0008 .5240 .0203 C18/PHYT .6050

C16 1135 .0008 .9080 .0352

C17 0 .0011 .0000 .0000

PRISTANE 91215 .0022 200.6730 7.7832

C18 729 .0009 .6561 .0254

PHYTANE 1205 .0019 2.2895 .0888

C19 1201 .0008 .9608 .0373

C20 499 .0009 .4491 .0174 CPI 1.6404

ANDROSTANE 17427 .0016 278.8320 10.8146

C21 1828 .0010 1.8280 .0709

C22 921 .0012 1.1052 .0429 RECOVERY %

C23 4266 .0008 3.4128 .1324 ANDROSTANE 29.3507

C24 5429 .0021 11.4009 .4422

C25 11082 .0027 29.9214 1.1605

C26 0 .0034 .0000 .0000

C27 5921 .0065 38.4865 1.4927

C28 5947 .0051 30.3267 1.1763

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 162741 .0016 41.4268 14.2817

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 14.2817

SAMPLE: 106 DATE ANALYZED: 09/10/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 26.57

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 935 .0008 .7480 .0148 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 712 .0008 .5696 .0113 C17/PRIST .1576

C15 1468 .0008 1.1744 .0233 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 157 .0011 .1727 .0034

PRISTANE 996 .0022 2.1912 .0434

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 0 .0008 .0000 .0000

C20 0 .0009 .0000 .0000 CPI .9337

ANDROSTANE 152280 .0016 243.6480 4.8263

C21 246 .0010 .2460 .0049

C22 446 .0012 .5352 .0106 RECOVERY %

C23 539 .0008 .4312 .0085 ANDROSTANE 25.6472

C24 1423 .0021 2.9883 .0592

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 10893 .0016 6.3536 .3053

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .3053

SAMPLE: 107 DATE ANALYZED: 08/24/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 8.02

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 573 .0022 1.2606 .0000

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 0 .0008 .0000 .0000

C20 0 .0009 .0000 .0000 CPI .0000

ANDROSTANE 0 .0016 .0000 .0000

C21 0 .0010 .0000 .0000

C22 0 .0012 .0000 .0000 RECOVERY %

C23 0 .0008 .0000 .0000 ANDROSTANE .0000

C24 0 .0021 .0000 .0000

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 16991 .0016 28.2688 1.8066

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 1.8066

SAMPLE: 108 DATE ANALYZED: 08/24/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 8.02

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 458 .0010 .4580 .0044

C20 0 .0013 .0000 .0000 CPI 1.4708

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 14835 .0012 17.8020 .1722 ANDROSTANE .0000

C24 10398 .0017 17.6766 .1710

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 55583 .0017 .0000 .0000

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .0000

SAMPLE: 109 DATE ANALYZED: 09/13/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 24.33

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 836 .0008 .6688 .0145 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT 13.6067

C14 0 .0008 .0000 .0000 C17/PRIST .1289

C15 998 .0008 .7984 .0173 C18/PHYT 5.6494

C16 1564 .0008 1.2672 .0274

C17 1561 .0011 1.7171 .0371

PRISTANE 12110 .0022 26.6420 .5763

C18 5028 .0009 4.5252 .0979

PHYTANE 890 .0019 1.6910 .0366

C19 4970 .0008 3.9760 .0860

C20 6877 .0009 6.1893 .1339 CPI .8645

ANDROSTANE 0 .0016 .0000 .0000

C21 1537 .0010 1.5370 .0332

C22 2672 .0012 3.2064 .0694 RECOVERY %

C23 2533 .0008 2.0264 .0438 ANDROSTANE .0000

C24 0 .0021 .0000 .0000

C25 2372 .0027 6.4044 .1385

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 71733 .0016 44.4240 2.2730

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 2.2730

SAMPLE: 110 DATE ANALYZED: 11/09/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 11.02

SAMPLE SIZE INJECTED (µL): 1.0

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 9296 .0008 7.4368 .6748

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 145100 .0017 347.1800 22.4301

C21 1647 .0011 1.8117 .1644

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 48.4380

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 14700 .0017 6.3869 1.4188

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 1.4188

SAMPLE: 111 DATE ANALYZED: 09/25/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 2.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 21.93

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0995

C15 1912 .0008 1.2960 .0734 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 298 .0008 .2384 .0114

PRISTANE 2995 .0022 6.5890 .3163

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 684 .0010 .6840 .0328

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 3130 .0011 3.4430 .1653

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 17104 .0017 13.7445 1.2590

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 1.2590

SAMPLE: 112 DATE ANALYZED: 08/15/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 2.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 17.87

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1709 .0012 2.0508 .0611 RESOL/UNRESOL .0000

C13 1036 .0014 1.4504 .0432 PRIST/PHYT .0000

C14 846 .0011 .9306 .0277 C17/PRIST 1.1629

C15 0 .0015 .0000 .0000 C18/PHYT .0000

C16 436 .0013 .5668 .0169

C17 4534 .0016 7.2544 .2161

PRISTANE 3899 .0040 15.5960 .4645

C18 0 .0014 .0000 .0000

PHYTANE 0 .0039 .0000 .0000

C19 0 .0016 .0000 .0000

C20 0 .0014 .0000 .0000 CPI 5.7348

ANDROSTANE 102640 .0016 164.2240 4.8915

C21 1263 .0017 2.1471 .0640

C22 0 .0015 .0000 .0000 RECOVERY %

C23 519 .0015 .7785 .0232 ANDROSTANE 17.2867

C24 0 .0017 .0000 .0000

C25 0 .0030 .0000 .0000

C26 0 .0000 .0000 .0000

C27 0 .0000 .0000 .0000

C28 0 .0000 .0000 .0000

C29 0 .0000 .0000 .0000

C30 0 .0000 .0000 .0000

RESOLVED 22131 .0016 12.6224 1.2926

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 1.2926

SAMPLE: 113 DATE ANALYZED: 09/15/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 2.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 20.69

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 1156 .0011 1.2716 .0323

PRISTANE 0 .0022 .0000 .0000

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 524 .0008 .4192 .0107

C20 0 .0009 .0000 .0000 CPI 12.1085

ANDROSTANE 0 .0016 .0000 .0000

C21 2013 .0010 2.0130 .0512

C22 516 .0012 .6192 .0158 RECOVERY %

C23 851 .0008 .6808 .0173 ANDROSTANE .0000

C24 0 .0021 .0000 .0000

C25 1704 .0027 4.6008 .1170

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 12656 .0016 9.4272 .4841

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .4841

SAMPLE: 114 DATE ANALYZED: 11/13/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 20.00

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST 1.7266

C15 1030 .0008 .8240 .0217 C18/PHYT .0000

C16 1328 .0008 1.0624 .0280

C17 1105 .0008 .8840 .0233

PRISTANE 640 .0022 1.4080 .0371

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 465 .0010 .4650 .0132

C20 0 .0013 .0000 .0000 CPI 1.9578

ANDROSTANE 145490 .0017 347.3330 6.5088

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 6579 .0017 3.4187 .2122

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .2122

SAMPLE: 115 DATE ANALYZED: 09/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 17.03

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 5587 .0022 12.2914 .3799

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .4191

ANDROSTANE 0 .0017 .0000 .0000

C21 1798 .0011 1.9778 .0611

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 4290 .0017 7.2930 .2254

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 13175 .0017 2.5500 .7452

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .7452

SAMPLE: 116 DATE ANALYZED: 09/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 17.03

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 2124 .0008 1.6992 .0386 RESOL/UNRESOL .0000

C13 945 .0008 .7560 .0172 PRIST/PHYT .0000

C14 5571 .0008 4.4568 .1012 C17/PRIST .0000

C15 3144 .0008 2.5152 .0571 C18/PHYT .0000

C16 301 .0008 .2408 .0055

C17 0 .0008 .0000 .0000

PRISTANE 16341 .0022 35.9502 .8159

C18 341 .0016 .5456 .0124

PHYTANE 0 .0020 .0000 .0000

C19 1389 .0010 1.3890 .0315

C20 0 .0013 .0000 .0000 CPI .6266

ANDROSTANE 182110 .0017 309.5870 7.0263

C21 0 .0011 .0000 .0000

C22 2529 .0013 3.2877 .0746 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 32.5881

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 34627 .0017 3.3014 1.2288

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 1.2288

SAMPLE: 117 DATE ANALYZED: 10/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 25.25

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 3155 .0022 8.9410 .2749

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 3540 .0013 4.6020 .1823 CPI .4226

ANDROSTANE 0 .0017 .0000 .0000

C21 2088 .0011 2.2968 .0910

C22 1401 .0013 1.8213 .0721 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 11847 .0017 1.8277 .7322

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .7322

SAMPLE: 118 DATE ANALYZED: 10/11/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 12.68

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT 5.3177

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 3281 .0022 7.2182 .2996

C18 0 .0016 .0000 .0000

PHYTANE 617 .0020 1.2340 .0512

C19 2754 .0010 2.7540 .1143

C20 1368 .0013 1.7784 .0738 CPI 2.4736

ANDROSTANE 139490 .0017 237.1330 9.8428

C21 2522 .0011 2.7742 .1152

C22 961 .0013 1.2493 .0519 RECOVERY %

C23 485 .0012 .5820 .0242 ANDROSTANE 24.9614

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 153400 .0017 240.4004 10.7086

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 10.7086

SAMPLE: 119 DATE ANALYZED: 09/29/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 32.14

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT 1.1569

C14 0 .0008 .0000 .0000 C17/PRIST 23.0924

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 15241 .0008 12.1928 .1997

PRISTANE 660 .0022 1.4520 .0238

C18 0 .0016 .0000 .0000

PHYTANE 306 .0020 .6120 .0100

C19 1803 .0010 1.8030 .0295

C20 670 .0013 .8710 .0143 CPI 29.3229

ANDROSTANE 0 .0017 .0000 .0000

C21 23343 .0011 25.6773 .4205

C22 739 .0013 .9607 .0157 RECOVERY %

C23 929 .0012 1.1148 .0183 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 61778 .0017 30.7479 1.2352

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 1.2352

SAMPLE: 120 DATE ANALYZED: 09/29/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 5.50

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 640 .0008 .5120 .0490 PRIST/PHYT .0000

C14 309 .0008 .2472 .0237 C17/PRIST .0000

C15 161 .0008 .1288 .0123 C18/PHYT 1.7608

C16 517 .0008 .4136 .0396

C17 26782 .0008 21.4256 2.0503

PRISTANE 0 .0022 .0000 .0000

C18 611 .0016 .9776 .0936

PHYTANE 347 .0020 .6940 .0664

C19 930 .0010 .9300 .0890

C20 453 .0013 .5889 .0564 CPI 8.4400

ANDROSTANE 0 .0017 .0000 .0000

C21 2329 .0011 2.5619 .2452

C22 362 .0013 .4706 .0450 RECOVERY %

C23 2127 .0012 2.5524 .2442 ANDROSTANE .0000

C24 2046 .0017 3.4782 .3328

C25 3306 .0020 6.6120 .6327

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 50000 .0017 15.4360 5.4573

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 5.4573

SAMPLE: 121 DATE ANALYZED: 09/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 10.69

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 2190 .0008 1.7520 .0863 RESOL/UNRESOL .0000

C13 1069 .0008 .8552 .0421 PRIST/PHYT 274.0333

C14 1463 .0008 1.1704 .0576 C17/PRIST .0000

C15 3943 .0008 3.1544 .1553 C18/PHYT .0000

C16 947 .0008 .7576 .0373

C17 0 .0008 .0000 .0000

PRISTANE 65768 .0022 144.6896 7.1237

C18 790 .0016 1.2640 .0622

PHYTANE 240 .0020 .4800 .0236

C19 9801 .0010 9.8010 .4825

C20 639 .0013 .8307 .0409 CPI 2.4271

ANDROSTANE 7851 .0017 13.3487 .6571

C21 803 .0011 .8833 .0435

C22 2886 .0013 3.7518 .1847 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 2203 .0029 6.3887 .3145

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 6053 .0124 75.0572 3.6954

C30 0 .0050 .0000 .0000

RESOLVED 126939 .0017 47.8448 14.7054

UNRESOLVED 0 .0017 .0000 14.7054

TOTAL .0000

SAMPLE: 122 DATE ANALYZED: 09/07/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 20.00

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 3277 .0008 2.6216 .0690 RESOL/UNRESOL .0000

C13 1309 .0008 1.0472 .0276 PRIST/PHYT 12.8532

C14 2115 .0008 1.6920 .0445 C17/PRIST .0000

C15 291 .0008 .2328 .0061 C18/PHYT .0205

C16 226 .0008 .1808 .0048

C17 274 .0008 .2192 .0058

PRISTANE 13393 .0022 29.4646 .7754

C18 0 .0016 .0000 .0000

PHYTANE 1042 .0020 2.0840 .0548

C19 2355 .0010 2.3550 .0620

C20 0 .0013 .0000 .0000 CPI 3.9260

ANDROSTANE 201140 .0017 341.9380 8.9984

C21 3662 .0011 4.0282 .1060

C22 2254 .0013 2.9302 .0771 RECOVERY %

C23 3667 .0012 4.4004 .1158 ANDROSTANE 35.9935

C24 3890 .0017 6.6130 .1740

C25 2523 .0020 5.0460 .1328

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 19231 .0124 238.4644 6.2754

C30 0 .0050 .0000 .0000

RESOLVED 280086 .0017 374.9809 17.7990

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 17.7990

SAMPLE: 123 DATE ANALYZED: 09/10/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 21.90

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 893 .0008 .7144 .0172 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 634 .0011 .6974 .0168

PRISTANE 0 .0022 .0000 .0000

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 393 .0008 .3144 .0076

C20 0 .0009 .0000 .0000 CPI 1.8186

ANDROSTANE 0 .0016 .0000 .0000

C21 335 .0010 .3350 .0081

C22 709 .0012 .8508 .0204 RECOVERY %

C23 893 .0008 .7144 .0172 ANDROSTANE .0000

C24 1022 .0021 2.1462 .0516

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 6656 .0016 2.8432 .2071

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .2071

SAMPLE: 124 DATE ANALYZED: 09/09/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 9.45

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST 3.9584

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 3234 .0011 3.5574 .1981

PRISTANE 817 .0022 1.7974 .1001

C18 317 .0009 .2853 .0159

PHYTANE 0 .0019 .0000 .0000

C19 0 .0008 .0000 .0000

C20 331 .0009 .2979 .0166 CPI .7668

ANDROSTANE 159670 .0016 255.4720 14.2285

C21 165 .0010 .1650 .0092

C22 1189 .0012 1.4268 .0795 RECOVERY %

C23 1212 .0008 .9696 .0540 ANDROSTANE 26.8918

C24 8222 .0021 17.2662 .9616

C25 1096 .0027 2.9592 .1648

C26 0 .0034 .0000 .0000

C27 2006 .0065 13.0390 .7262

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 32503 .0016 22.2624 3.5659

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 3.5659

SAMPLE: 125 DATE ANALYZED: 09/13/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 26.34

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1711 .0008 1.3688 .0274 RESOL/UNRESOL .2281

C13 832 .0008 .6656 .0133 PRIST/PHYT .1793

C14 964 .0008 .7712 .0154 C17/PRIST 15.4922

C15 1838 .0008 1.4704 .0294 C18/PHYT 1.7173

C16 819 .0008 .6552 .0131

C17 4973 .0011 5.4703 .1093

PRISTANE 321 .0022 .7062 .0141

C18 3074 .0009 2.7666 .0555

PHYTANE 1790 .0019 3.4010 .0680

C19 0 .0008 .0000 .0000

C20 2070 .0009 1.8630 .0372 CPI .9010

ANDROSTANE 0 .0016 .0000 .0000

C21 267 .0010 .2670 .0053

C22 1115 .0012 1.3380 .0267 RECOVERY %

C23 1786 .0008 1.4288 .2850 ANDROSTANE .0000

C24 4103 .0021 8.6163 .1722

C25 1950 .0027 5.2850 .1052

C26 780 .0034 3.6520 .0530

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 82219 .0016 86.1216 2.4942

UNRESOLVED 360453 .0016 576.7248 44.5239

TOTAL 14.0181

SAMPLE: 126 DATE ANALYZED: 09/17/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 16.77

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 879 .0008 .7032 .0221 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 901 .0022 1.9822 .0622

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 0 .0008 .0000 .0000

C20 0 .0009 .0000 .0000 CPI .0000

ANDROSTANE 103670 .0016 165.8720 5.2058

C21 3559 .0010 3.5590 .1117

C22 0 .0012 .0000 .0000 RECOVERY %

C23 0 .0008 .0000 .0000 ANDROSTANE 17.4602

C24 0 .0021 .0000 .0000

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 6642 .0016 2.0848 .2614

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .2614

SAMPLE: 127 DATE ANALYZED: 09/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 29.66

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT 11.7350

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 1730 .0008 1.3840 .0246 C18/PHYT 2.2686

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 3321 .0022 7.3062 .1296

C18 642 .0016 1.0272 .0182

PHYTANE 283 .0020 .5660 .0100

C19 1396 .0010 1.3960 .0248

C20 824 .0013 1.0712 .0190 CPI 2.4601

ANDROSTANE 151050 .0017 256.7850 4.5566

C21 1461 .0011 1.6071 .0285

C22 690 .0013 .8970 .0159 RECOVERY %

C23 717 .0012 .8604 .0153 ANDROSTANE 27.0300

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 12460 .0017 2.3732 .3281

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .3281

SAMPLE: 127 DATE ANALYZED: 11/01/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 0.5

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 29.66

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST 1.3633

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 1047 .0008 .8376 .0074

PRISTANE 768 .0022 1.6896 .0150

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 1184 .0013 1.5392 .0137 CPI .8843

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 13894 .0017 18.5215 .2004

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .2004

SAMPLE: 128 DATE ANALYZED: 08/31/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 35.75

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .3441

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 847 .0008 .6776 .0100 C18/PHYT 2.1518

C16 311 .0008 .2488 .0037

C17 46652 .0011 51.3172 .7555

PRISTANE 0 .0022 .0000 .0000

C18 964 .0009 .8676 .0128

PHYTANE 448 .0019 .8512 .0125

C19 1479 .0008 1.1832 .0174

C20 787 .0009 .7083 .0104 CPI 13.0223

ANDROSTANE 0 .0016 .0000 .0000

C21 25418 .0010 25.4180 .3742

C22 2471 .0012 2.9652 .0437 RECOVERY %

C23 2236 .0008 1.7888 .0263 ANDROSTANE .0000

C24 1739 .0021 3.6519 .0538

C25 5044 .0027 13.6188 .2005

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 113383 .0016 .0000 2.1093

UNRESOLVED 329534 .0016 .0000 7.7623

TOTAL 9.8716

SAMPLE: 129 DATE ANALYZED: 10/21/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 36.65

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 240 .0011 .2640 .0038

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 240 .0017 .0000 .0038

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .0038

SAMPLE: 130 DATE ANALYZED: 10/25/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 35.30

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .2640 .0038

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 2574 .0017 4.3758 .0652

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .0652

SAMPLE: 132 DATE ANALYZED: 09/16/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 23.54

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1938 .0008 1.5504 .0347 RESOL/UNRESOL .0000

C13 1038 .0008 .8304 .0186 PRIST/PHYT .9743

C14 674 .0008 .5392 .0121 C17/PRIST 9.4376

C15 0 .0008 .0000 .0000 C18/PHYT .5716

C16 831 .0008 .6648 .0149

C17 8928 .0011 9.8208 .2196

PRISTANE 946 .0022 2.0812 .0465

C18 555 .0009 .4995 .0112

PHYTANE 971 .0019 1.8449 .0142

C19 1154 .0008 .9232 0.0206 ?

C20 987 .0009 .8883 .0199 CPI 4.2486

ANDROSTANE 212490 .0016 339.9840 7.6015

C21 5696 .0010 5.6960 .1274

C22 1242 .0012 1.4904 .0333 RECOVERY %

C23 1407 .0008 1.1256 .0252 ANDROSTANE 35.7878

C24 654 .0021 1.3734 .0307

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 2778 .0065 18.0570 .4037

C30 0 .0064 .0000 .0000

RESOLVED 37082 .0016 11.6258 1.3200

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 1.3200

SAMPLE: 134 DATE ANALYZED: 09/24/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 22.05

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1271 .0008 1.0168 .0243 RESOL/UNRESOL .3079

C13 1096 .0008 .8768 .0209 PRIST/PHYT .0000

C14 947 .0008 .7576 .0181 C17/PRIST .0000

C15 1965 .0008 1.5720 .0375 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 23946 .0022 52.6812 1.2575

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 3929 .0010 3.9290 .0938

C20 4601 .0013 5.9813 .1428 CPI 3.4088

ANDROSTANE 0 .0017 .0000 .0000

C21 10377 .0011 11.4147 .2725

C22 687 .0013 .8931 .0213 RECOVERY %

C23 1319 .0012 1.5828 .0378 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 2568 .0020 5.1360 .1226

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 71338 .0017 31.6744 2.8050

UNRESOLVED 231681 .0017 393.8577 9.4011

TOTAL 12.2061

SAMPLE: 135 DATE ANALYZED: 09/15/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 12.47

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0390

C13 0 .0008 .0000 .0000 PRIST/PHYT .8575

C14 0 .0008 .0000 .0000 C17/PRIST 18.8083

C15 0 .0008 .0000 .0000 C18/PHYT 1.3973

C16 0 .0008 .0000 .0000

C17 5887 .0011 6.4757 .2733

PRISTANE 313 .0022 .6886 .0291

C18 510 .0009 .4590 .0194

PHYTANE 365 .0019 .6935 .0293

C19 0 .0008 .0000 .0000

C20 0 .0009 .0000 .0000 CPI 9.9220

ANDROSTANE 0 .0016 .0000 .0000

C21 4697 .0010 4.6970 .1982

C22 1017 .0012 1.2304 .0515 RECOVERY %

C23 2120 .0008 1.6960 .0716 ANDROSTANE .0000

C24 230 .0021 .4830 .0204

C25 4729 .0027 12.7683 .5389

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 37420 .0016 28.0832 2.4169

UNRESOLVED 958515 .0016 1533.6240 64.7290

TOTAL 67.1459

SAMPLE: 136 DATE ANALYZED: 11/01/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 15.62

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 2424 .0008 1.9392 .0653 RESOL/UNRESOL .0331

C13 1980 .0008 1.5840 .0534 PRIST/PHYT .0000

C14 896 .0008 .7168 .0242 C17/PRIST .0000

C15 4941 .0008 3.9528 .1332 C18/PHYT 1.8531

C16 849 .0008 .6792 .0229

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 856 .0016 1.0496 .0354

PHYTANE 354 .0020 .7080 .0239

C19 1003 .0010 1.0030 338.0000

C20 0 .0013 .0000 .0000 CPI 2.6460

ANDROSTANE 0 .0017 .0000 .0000

C21 5077 .0011 5.5847 .1882

C22 1005 .0013 1.3065 .0440 RECOVERY %

C23 5044 .0012 6.0528 .2039 ANDROSTANE .0000

C24 5677 .0017 9.6509 .3252

C25 5989 .0020 11.9780 .4036

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 76889 .0017 69.6898 3.9051

UNRESOLVED 3323458 .0017 3949.8786 133.0911

TOTAL 136.9962

SAMPLE: 137 DATE ANALYZED: 08/20/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 17.23

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 738 .0012 .8856 .0271 RESOL/UNRESOL .0174

C13 0 .0014 .0000 .0000 PRIST/PHYT .0000

C14 216 .0011 .2376 .0073 C17/PRIST .0000

C15 0 .0015 .0000 .0000 C18/PHYT .0000

C16 0 .0013 .0000 .0000

C17 0 .0016 .0000 .0000

PRISTANE 10 .0040 .0400 .0012

C18 0 .0014 .0000 .0000

PHYTANE 0 .0039 .0000 .0000

C19 0 .0016 .0000 .0000

C20 0 .0014 .0000 .0000 CPI 2.1250

ANDROSTANE 183370 .0016 296.3920 8.9621

C21 459 .0017 .7803 .0238

C22 0 .0015 .0000 .0000 RECOVERY %

C23 0 .0015 .0000 .0000 ANDROSTANE 30.8834

C24 0 .0017 .0000 .0000

C25 0 .0030 .0000 .0000

C26 0 .0000 .0000 .0000

C27 0 .0000 .0000 .0000

C28 0 .0000 .0000 .0000

C29 0 .0000 .0000 .0000

C30 0 .0000 .0000 .0000

RESOLVED 2859 .0016 2.2976 .1296

UNRESOLVED 163958 .0016 262.3328 8.0133

TOTAL 8.1429

SAMPLE: 138 DATE ANALYZED: 09/02/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 40.63

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .1139

C13 0 .0008 .0000 .0000 PRIST/PHYT .4437

C14 0 .0008 .0000 .0000 C17/PRIST 3.7070

C15 3251 .0008 2.6008 .0337 C18/PHYT 3.1629

C16 523 .0008 .4181 .0054

C17 949 .0011 1.0439 .0135

PRISTANE 256 .0022 .5632 0..73

C18 1825 .0009 1.6425 .0213

PHYTANE 577 .0019 1.0963 .0142

C19 2978 .0008 2.3824 .0309

C20 3507 .0009 3.1563 .0409 CPI 1.5938

ANDROSTANE 178490 .0016 285.5840 3.6994

C21 4555 .0010 4.5550 .0590

C22 2701 .0012 3.2412 .0420 RECOVERY %

C23 3253 .0008 2.6024 .0337 ANDROSTANE 30.0615

C24 2637 .0021 5.5377 .0717

C25 2853 .0027 7.7031 .0998

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 34961 .0016 8.1536 .5790

UNRESOLVED 306882 .0016 491.0112 6.3605

TOTAL 6.9395

SAMPLE: 139 DATE ANALYZED: 09/16/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 36.81

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0249

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 925 .0008 .7432 .0106 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 407 .0008 .3256 .0047

C20 0 .0009 .0000 .0000 CPI 2.7930

ANDROSTANE 109170 .0016 174.6720 2.4975

C21 1575 .0010 1.5750 .0225

C22 636 .0012 .7632 .0109 RECOVERY %

C23 1002 .0008 .8026 .0115 ANDROSTANE 18.3865

C24 765 .0021 1.6065 .0230

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 6435 .0016 1.7936 .1088

UNRESOLVED 258082 .0016 412.9312 5.9042

TOTAL 6.0130

SAMPLE: 140 DATE ANALYZED: 09/13/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 26.55

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0478

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 640 .0022 1.4080 .0279

C18 269 .0009 .2421 .0048

PHYTANE 0 .0019 .0000 .0000

C19 715 .0008 .5720 .0113

C20 403 .0009 .3627 .0072 CPI 5.0142

ANDROSTANE 0 .0016 .0000 .0000

C21 4493 .0010 4.4930 .0891

C22 455 .0012 .5460 .0108 RECOVERY %

C23 443 .0008 .3544 .0070 ANDROSTANE .0000

C24 0 .0021 .0000 .0000

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 11466 .0016 6.4768 .2865

UNRESOLVED 239763 .0016 383.6208 7.6047

TOTAL 7.8913

SAMPLE: 142 DATE ANALYZED: 10/23/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.5

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 16.91

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0422

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 1622 .0008 1.2976 .1150 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 1774 .0008 1.4208 .1260

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 3105 .0010 3.1050 .2753

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 7343 .0011 8.0773 .7161

C22 0 .0013 .0000 .0000 RECOVERY %

C23 786 .0012 .9432 .0836 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 23688 .0017 15.3952 2.6808

UNRESOLVED 561505 .0017 954.5585 84.6240

TOTAL 87.3048

SAMPLE: 143 DATE ANALYZED: 09/14/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 29.57

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 2029 .0008 1.6232 .0289 RESOL/UNRESOL .0000

C13 694 .0008 .5552 .0099 PRIST/PHYT .0000

C14 974 .0008 .7792 .0139 C17/PRIST 3.0108

C15 110 .0008 .0880 .0016 C18/PHYT .0000

C16 548 .0008 .4384 .0078

C17 280 .0011 .3080 .0055

PRISTANE 93 .0022 .2046 .0036

C18 308 .0009 .2772 .0049

PHYTANE 0 .0019 .0000 .0000

C19 0 .0008 .0000 .0000

C20 0 .0009 .0000 .0000 CPI .9701

ANDROSTANE 0 .0016 .0000 .0000

C21 558 .0010 .5580 .0099

C22 477 .0012 .5724 .0102 RECOVERY %

C23 596 .0008 .4768 .0085 ANDROSTANE .0000

C24 0 .0021 .0000 .0000

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 13768 .0016 11.3616 .3069

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .3069

SAMPLE: 144 DATE ANALYZED: 09/23/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 34.88

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0357

C13 0 .0008 .0000 .0000 PRIST/PHYT 1.0302

C14 0 .0008 .0000 .0000 C17/PRIST .3115

C15 0 .0008 .0000 .0000 C18/PHYT .7977

C16 0 .0008 .0000 .0000

C17 138 .0008 .1104 .0017

PRISTANE 443 .0022 .9746 .0147

C18 343 .0016 .5488 .0083

PHYTANE 430 .0020 .8600 .0130

C19 686 .0010 .6860 .0104

C20 840 .0013 1.0920 .0165 CPI 10.7358

ANDROSTANE 0 .0017 .0000 .0000

C21 14569 .0011 16.0259 .2418

C22 331 .0013 .4303 .0065 RECOVERY %

C23 861 .0012 1.0332 .0156 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 28004 .0017 15.9171 .5685

UNRESOLVED 783407 .0017 1331.7919 20.0958

TOTAL 20.6644

SAMPLE: 145 DATE ANALYZED: 09/10/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 22.97

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1799 .0008 1.4392 .0330 RESOL/UNRESOL .0000

C13 744 .0008 .5952 .0136 PRIST/PHYT .0000

C14 916 .0008 .7328 .0168 C17/PRIST 5.4249

C15 2490 .0008 1.9920 .0456 C18/PHYT .0000

C16 236 .0008 .1888 .0043

C17 1698 .0011 1.8678 .0428

PRISTANE 313 .0022 .6886 .0158

C18 361 .0009 .3249 .0074

PHYTANE 0 .0019 .0000 .0000

C19 859 .0008 .6872 .0157

C20 1010 .0009 .9090 .0208 CPI 4.4271

ANDROSTANE 124450 .0016 199.1200 4.5625

C21 7822 .0010 7.8220 .1792

C22 722 .0012 .8664 .0199 RECOVERY %

C23 753 .0008 .6024 .0138 ANDROSTANE 20.9600

C24 0 .0021 .0000 .0000

C25 0 .0027 .0000 .0000

C26 0 .0034 .0000 .0000

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 23593 .0016 6.1920 .5707

UNRESOLVED 0 .0016 .0000 .0000

TOTAL .5707

SAMPLE: 146 DATE ANALYZED: 09/07/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 6.50

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0011 .0000 .0000

PRISTANE 435 .0022 .9570 .0775

C18 0 .0009 .0000 .0000

PHYTANE 0 .0019 .0000 .0000

C19 0 .0008 .0000 .0000

C20 0 .0009 .0000 .0000 CPI .5694

ANDROSTANE 0 .0016 .0000 .0000

C21 1163 .0010 1.1630 .0942

C22 1477 .0012 1.7724 .1435 RECOVERY %

C23 0 .0008 .0000 .0000 ANDROSTANE .0000

C24 403 .0021 .8463 .0685

C25 1765 .0027 4.7655 .3859

C26 3262 .0034 11.0908 .8980

C27 0 .0065 .0000 .0000

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 9073 .0016 .9088 1.7412

UNRESOLVED 0 .0016 .0000 .0000

TOTAL 1.7412

SAMPLE: 147 DATE ANALYZED: 10/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 17.25

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0835

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 328 .0022 .7216 .0220

C18 210 .0016 .3360 .0103

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI 8.2382

ANDROSTANE 0 .0017 .0000 .0000

C21 56520 .0011 62.1720 1.8969

C22 1374 .0013 1.7862 .0545 RECOVERY %

C23 7395 .0012 8.8740 .2708 ANDROSTANE .0000

C24 7225 .0017 12.2825 .3748

C25 8655 .0020 17.3100 .5281

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 92660 .0017 18.6201 3.7255

UNRESOLVED 1109525 .0017 1886.1925 57.5497

TOTAL 61.2752

SAMPLE: 148 DATE ANALYZED: 09/15/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 25.42

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0589

C13 0 .0008 .0000 .0000 PRIST/PHYT 8.2854

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 468 .0008 .3744 .0078 C18/PHYT .3817

C16 1306 .0008 1.0448 .0216

C17 0 .0011 .0000 .0000

PRISTANE 6968 .0022 15.3296 .3174

C18 321 .0009 .2889 .0060

PHYTANE 841 .0019 1.5979 .0331

C19 1165 .0008 .9320 .0193

C20 320 .0009 .2880 .0060 CPI 1.7974

ANDROSTANE 0 .0016 .0000 .0000

C21 4030 .0010 4.0300 .0834

C22 738 .0012 .8856 .0183 RECOVERY %

C23 1960 .0008 1.5680 .0325 ANDROSTANE .0000

C24 3664 .0021 7.6944 .1593

C25 2175 .0027 5.8725 .1216

C26 0 .0034 .0000 .0000

C27 1614 .0065 10.4910 .2172

C28 0 .0051 .0000 .0000

C29 0 .0065 .0000 .0000

C30 0 .0064 .0000 .0000

RESOLVED 40813 .0016 24.3888 1.5484

UNRESOLVED 692350 .0016 1107.7600 22.9359

TOTAL 24.4844

SAMPLE: 149 DATE ANALYZED: 09/25/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 19.74

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1181 .0008 .9448 .0252 RESOL/UNRESOL .1435

C13 160 .0008 .1280 .0034 PRIST/PHYT 6.5051

C14 1343 .0008 1.0744 .0286 C17/PRIST .0000

C15 3561 .0008 2.8488 .0760 C18/PHYT 1.1637

C16 1754 .0008 1.4032 .0374

C17 0 .0008 .0000 .0000

PRISTANE 10135 .0022 22.2970 .5945

C18 1813 .0016 2.9008 .0773

PHYTANE 1558 .0020 3.1160 .0831

C19 3265 .0010 3.2650 .0871

C20 606 .0013 .7878 .0210 CPI 9.0794

ANDROSTANE 0 .0017 .0000 .0000

C21 68474 .0011 75.3214 2.0082

C22 0 .0013 .0000 .0000 RECOVERY %

C23 786 .0012 .9432 .0251 ANDROSTANE .0000

C24 2003 .0017 3.4051 .0908

C25 1374 .0020 2.7480 .0733

C26 1030 .0029 2.9870 .0796

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 150819 .0017 88.0192 5.6575

UNRESOLVED 1050648 .0017 1786.1016 47.6218

TOTAL 53.2792

SAMPLE: 150 DATE ANALYZED: 09/25/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 17.10

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 1288 .0022 2.8336 .0872

C18 374 .0016 .5984 .0184

PHYTANE 0 .0020 .0000 .0000

C19 626 .0010 .6260 .0193

C20 500 .0013 .6500 .0200 CPI 5.5333

ANDROSTANE 0 .0017 .0000 .0000

C21 5776 .0011 6.3536 .1956

C22 283 .0013 .3679 .0113 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 11944 .0017 5.2649 .5138

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .5138

SAMPLE: 151 DATE ANALYZED: 09/29/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 500.0

DRY WEIGHT EXTRACTED (G): 20.00

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1902 .0008 1.5216 .0400 RESOL/UNRESOL .0000

C13 881 .0008 .7048 .0185 PRIST/PHYT .0000

C14 1508 .0008 1.2064 .0317 C17/PRIST .0000

C15 191 .0008 .1528 .0040 C18/PHYT .0000

C16 1375 .0008 1.1000 .0289

C17 790 .0008 .6320 .0166

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 1059 .0020 2.1180 .0557

C19 1551 .0010 1.5510 .0408

C20 1346 .0013 1.7498 .0460 CPI 2.7525

ANDROSTANE 129830 .0017 220.7110 5.8082

C21 10238 .0011 11.2618 .2964

C22 857 .0013 1.1141 .0293 RECOVERY %

C23 348 .0012 .4176 .0110 ANDROSTANE 23.2327

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 158948 .0017 232.7334 6.7438

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 6.7438

SAMPLE: 152 DATE ANALYZED: 10/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 25.12

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0810

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 1788 .0008 1.4304 .0300 C18/PHYT .0000

C16 1971 .0008 1.5768 .0330

C17 1000 .0008 .8000 .0168

PRISTANE 0 .0022 .0000 .0000

C18 3176 .0016 5.0816 .1065

PHYTANE 0 .0020 .0000 .0000

C19 8290 .0010 8.2900 .1737

C20 6792 .0013 8.8296 .1850 CPI 1.3646

ANDROSTANE 0 .0017 .0000 .0000

C21 6361 .0011 6.9971 .1466

C22 4457 .0013 5.7941 .1214 RECOVERY %

C23 4551 .0012 5.4612 .1144 ANDROSTANE .0000

C24 2110 .0017 3.5870 .0752

C25 3263 .0020 6.5260 .1367

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 49193 .0017 9.2378 1.3328

UNRESOLVED 607353 .0017 1032.5001 21.6330

TOTAL 22.9658

SAMPLE: 153 DATE ANALYZED: 10/12/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 0.5

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 27.44

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .1323

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 2337 .0008 1.8696 .0341 C17/PRIST .0000

C15 2702 .0008 2.1616 .0394 C18/PHYT 10.0116

C16 1772 .0008 1.4176 .0258

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 2593 .0016 4.1488 .0756

PHYTANE 259 .0020 .5180 .0094

C19 9917 .0010 9.9170 .1807

C20 7441 .0013 9.6733 .1763 CPI 1.1583

ANDROSTANE 0 .0017 .0000 .0000

C21 5753 .0011 6.3283 .1153

C22 1718 .0013 2.2334 .0407 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 47086 .0017 21.4098 1.0874

UNRESOLVED 355997 .0017 605.1949 11.0276

TOTAL 12.1150

SAMPLE: 154 DATE ANALYZED: 11/10/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 26.99

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 1898 .0008 1.5184 .0563

PRISTANE 0 .0022 .0000 .0000

C18 295 .0016 .4720 .0175

PHYTANE 0 .0020 .0000 .0000

C19 684 .0010 .8840 .0253

C20 0 .0013 .0000 .0000 CPI 12.9186

ANDROSTANE 0 .0017 .0000 .0000

C21 1229 .0011 1.3519 .0501

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 4690 .0017 .9928 .1860

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .1860

SAMPLE: 155 DATE ANALYZED: 09/27/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 26.14

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 4149 .0008 3.3192 .1270 RESOL/UNRESOL .1901

C13 2456 .0008 1.9648 .0752 PRIST/PHYT .7607

C14 5330 .0008 4.2640 .1631 C17/PRIST 3.3508

C15 1202 .0008 .9616 .0368 C18/PHYT 2.1063

C16 1627 .0008 1.3026 .0498

C17 3525 .0008 2.8200 .1079

PRISTANE 1052 .0022 2.3144 .0885

C18 2913 .0016 4.6608 .1783

PHYTANE 1383 .0020 2.7660 .1058

C19 4064 .0010 4.0640 .1555

C20 3894 .0013 5.0622 .1937 CPI 1.2036

ANDROSTANE 0 .0017 .0000 .0000

C21 5861 .0011 6.4471 .2466

C22 1888 .0013 2.4544 .0939 RECOVERY %

C23 2380 .0012 2.8560 .1093 ANDROSTANE .0000

C24 539 .0017 .9163 .0351

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 62284 .0017 34.0357 3.0684

UNRESOLVED 327587 .0017 556.8979 21.3044

TOTAL 24.3728

SAMPLE: (301) C14-152-P2 DATE ANALYZED: 12/08/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 11.20

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1708 .0008 1.3672 .1221 RESOL/UNRESOL .0478

C13 0 .0008 .0000 .0000 PRIST/PHYT .2302

C14 1589 .0008 1.2712 .1135 C17/PRIST .0000

C15 1019 .0008 .8152 .0728 C18/PHYT 1.3730

C16 1820 .0008 1.4560 .1300

C17 0 .0008 .0000 .0000

PRISTANE 358 .0022 .7876 .0703

C18 2135 .0016 3.4160 .3050

PHYTANE 1555 .0020 3.1100 .2777

C19 6245 .0010 6.2450 .5576

C20 3890 .0013 5.0570 .4515 CPI .8838

ANDROSTANE 0 .0017 .0000 .0000

C21 1675 .0011 1.8425 .1645

C22 1535 .0013 1.9955 .1782 RECOVERY %

C23 755 .0012 .9060 .0809 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 29890 .0017 9.5285 3.3748

UNRESOLVED 382470 .0017 650.1990 58.0535

TOTAL 61.4283

SAMPLE: (302) C14-72 DATE ANALYZED: 11/08/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 11.17

SAMPLE SIZE INJECTED (µL): 1.0

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT 4.7665

C16 0 .0008 .0000 .0000

C17 3483 .0008 2.7864 .2495

PRISTANE 0 .0022 .0000 .0000

C18 1840 .0016 2.9440 .2636

PHYTANE 386 .0020 .7720 .0691

C19 2208 .0010 2.2080 .1977

C20 3374 .0013 4.3862 .3927 CPI 2.2420

ANDROSTANE 0 .0017 .0000 .0000

C21 1626 .0011 1.7886 .1601

C22 1954 .0013 2.5402 .2274 RECOVERY %

C23 6783 .0012 8.1396 .7287 ANDROSTANE .0000

C24 1663 .0017 4.5271 .4053

C25 7941 .0020 15.8820 1.4218

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 43044 .0017 18.3362 5.7574

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 5.7574

SAMPLE: (305) C14-74-P3 DATE ANALYZED: 10/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 2.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 12.45

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 0 .0017 .0000 .0000

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .0000

SAMPLE: (307) C14-80 DATE ANALYZED: 10/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 2.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 23.39

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 0 .0017 .0000 .0000

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .0000

SAMPLE: (306) C14-81 DATE ANALYZED: 10/22/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 2.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 14.92

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 1683 .0017 2.8611 .2019

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 9521 .0017 13.3246 1.1419

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 1.1419

SAMPLE: (308) C14-74-P2 DATE ANALYZED: 10/23/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 2.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 3.88

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 2055 .0008 1.6440 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .4460 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 5461 .0017 5.7902 2.0169

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 2.0169

SAMPLE: (309) C14-152-P1 DATE ANALYZED: 11/12/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 17.70

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 209 .0016 .3344 .0099

PHYTANE 0 .0020 .0000 .0000

C19 2482 .0010 2.4820 .0738

C20 4448 .0013 5.7824 .1719 CPI .6331

ANDROSTANE 0 .0017 .0000 .0000

C21 1676 .0011 1.8436 .0548

C22 1716 .0013 2.2308 .0663 RECOVERY %

C23 1180 .0012 1.4160 .0421 ANDROSTANE .0000

C24 2056 .0017 3.4986 .1040

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 13796 .0017 .0459 .5243

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .5243

SAMPLE: (309) C14-74-P1 DATE ANALYZED: 11/15/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 6.49

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 419 .0016 .6704 .0544

PHYTANE 0 .0020 .0000 .0000

C19 3062 .0010 3.0620 .2483

C20 2706 .0013 5.5178 .2853 CPI .9073

ANDROSTANE 0 .0017 .0000 .0000

C21 2029 .0011 2.2319 .1810

C22 2486 .0013 3.2318 .2621 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 11277 .0017 .9775 1.1103

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 1.1103

SAMPLE: (311) C14-78-P1 DATE ANALYZED: 12/20/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 5.70

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 6952 .0008 5.5616 .5135

C17 0 .0008 .0000 .0000

PRISTANE 2000 .0022 4.4000 .4063

C18 1296 .0016 2.0736 .1915

PHYTANE 0 .0020 .0000 .0000

C19 1174 .0010 1.1740 .1084

C20 466 .0013 .6058 .0559 CPI .1219

ANDROSTANE 940 .0017 1.5980 .1476

C21 0 .0011 .0000 .0000

C22 920 .0013 1.1960 .1104 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 27258 .0017 24.5650 3.6543

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 3.6543

SAMPLE: (312) C14-78-P2 DATE ANALYZED: 12/20/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 8.17

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 245 .0020 .4900 .0316

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI 1.8217

ANDROSTANE 1098 .0017 1.8666 .1202

C21 1002 .0011 1.1022 .0710

C22 1464 .0013 1.9032 .1226 RECOVERY %

C23 1665 .0012 1.9980 .1287 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 9450 .0017 8.6258 .9096

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .9096

SAMPLE: (318) SEA TROUT #1 (WHOLE) DATE ANALYZED: 12/13/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): .0

DRY WEIGHT EXTRACTED (G): 0.60

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 0 .0017 .0000 .0000

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE .0000

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 0 .0017 .0000 .0000

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .0000

SAMPLE: (319) PINFISH (WHOLE) DATE ANALYZED: 12/10/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 50.0

DRY WEIGHT EXTRACTED (G): 1.78

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 2876 .0008 2.3008 .6803 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 3019 .0008 2.4152 .7141 C17/PRIST .0000

C15 1937 .0008 1.5496 .4582 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .6416

ANDROSTANE 35246 .0017 59.9152 17.7168

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 63.0718

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 8740 .0017 1.5436 2.3090

UNRESOLVED 0 .0017 .0000 2.3090

TOTAL .0000

SAMPLE: (320) GREY SNAPPER (WHOLE) DATE ANALYZED: 12/10/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 50.0

DRY WEIGHT EXTRACTED (G): 1.78

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 514 .0008 .4112 .0913 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 4186 .0017 7.1162 1.5803

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 7.4907

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 7513 .0017 11.8983 2.7336

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 2.7336

SAMPLE: (321) SCALLOPS (WHOLE) DATE ANALYZED: 12/10/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 50.0

DRY WEIGHT EXTRACTED (G): 1.05

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 1674 .0008 1.3392 .6713 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 8078 .0022 17.7738 8.9092

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 52769 .0017 89.7073 44.9661

C21 4842 .0011 5.3265 2.6698

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 94.4287

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 653840 .0017 1086.7165 556.9703

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 556.9703

SAMPLE: (322) TOADFISH (WHOLE) DATE ANALYZED: 12/13/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 50.0

DRY WEIGHT EXTRACTED (G): 1.61

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 1237 .0008 .9896 .3235 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 21448 .0010 21.4480 7.0114

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 16831 .0017 28.6127 9.3536

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 30.1186

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 21628 .0017 6.7475 .0000

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 6.7475 .0000

SAMPLE: (323) SHRIMP (WHOLE) DATE ANALYZED: 12/14/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 50.0

DRY WEIGHT EXTRACTED (G): 1.66

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 186 .0008 .1488 .0472 RESOL/UNRESOL .0000

C13 3524 .0008 2.8192 .8938 PRIST/PHYT .0000

C14 5183 .0008 4.1464 1.3146 C17/PRIST .0000

C15 2654 .0008 2.1232 .6732 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI 1.1920

ANDROSTANE 33371 .0017 56.7307 17.9869

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 59.7165

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 19489 .0017 13.4674 7.1988

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 7.1988

SAMPLE: (324) GRUNT (WHOLE) DATE ANALYZED: 12/14/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 50.0

DRY WEIGHT EXTRACTED (G): 1.93

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 1588 .0008 1.2704 .3464 RESOL/UNRESOL .0000

C13 4788 .0008 3.8304 1.0446 PRIST/PHYT .0000

C14 3080 .0008 2.4640 .6719 C17/PRIST .0000

C15 2869 .0008 2.2952 .6259 C18/PHYT .0000

C16 1097 .0008 .8776 .2393

C17 0 .0008 .0000 .0000

PRISTANE 10963 .0022 24.1186 6.5772

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI 1.8331

ANDROSTANE 45712 .0017 77.7104 21.1918

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 81.8004

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 32193 .0017 13.2736 13.1251

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 13.1251

SAMPLE: (328) CRAB (HEPATO-PANCREAS) DATE ANALYZED: 12/16/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 50.0

DRY WEIGHT EXTRACTED (G): 1.04

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 30264 .0017 51.4488 28.0368

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 54.1566

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 0 .0017 .0000 .0000

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .0000

SAMPLE: (327) BLUE CRAB (CLAW MUSCLE) DATE ANALYZED: 12/15/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 100.0

DRY WEIGHT EXTRACTED (G): 0.65

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 78206 .0017 132.9519 107.6534

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 69.9747

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 7433 .0017 12.6361 10.2317

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 10.2317

SAMPLE: (328) SCHOOL MASTER (WHOLE) DATE ANALYZED: 12/16/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 50.0

DRY WEIGHT EXTRACTED (G): 0.87

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 2065 .0008 1.6520 .9994 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 323 .0008 .2584 .1563

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 38274 .0017 65.0658 39.3622

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 68.4903

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 2388 .0017 .0000 1.1557

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 1.1557

SAMPLE: (329) SEA TROUT #2 (WHOLE) DATE ANALYZED: 12/15/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 50.0

DRY WEIGHT EXTRACTED (G): 0.70

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 44880 .0017 76.2960 57.3654

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 80.3116

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 6711 .0017 11.4087 8.5780

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 8.5780

SAMPLE: (330) STONE CRAB (CLAW MUSCLE) DATE ANALYZED: 12/15/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 100.0

DRY WEIGHT EXTRACTED (G): 0.45

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 0 .0008 .0000 .0000

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 81008 .0017 137.7136 161.0685

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 772.4808

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 7254 .0017 12.3318 14.4232

UNRESOLVED 0 .0017 .0000 .0000

TOTAL 14.4232

SAMPLE: (331) BLUE CRAB (HEPATO-PANCREAS) DATE ANALYZED: 12/16/82

INTERNAL STANDARD SAMPLE VOLUME (ML): 1.0

ANDROSTANE (µL): 5.0

DRY WEIGHT EXTRACTED (G): 2.80

SAMPLE SIZE INJECTED (µL): 1.9

RESPONSE

COMPOUND AREA FACTOR NG µG/G RATIOS

C12 0 .0008 .0000 .0000 RESOL/UNRESOL .0000

C13 0 .0008 .0000 .0000 PRIST/PHYT .0000

C14 0 .0008 .0000 .0000 C17/PRIST .0000

C15 0 .0008 .0000 .0000 C18/PHYT .0000

C16 0 .0008 .0000 .0000

C17 1729 .0008 1.3832 .1300

PRISTANE 0 .0022 .0000 .0000

C18 0 .0016 .0000 .0000

PHYTANE 0 .0020 .0000 .0000

C19 0 .0010 .0000 .0000

C20 0 .0013 .0000 .0000 CPI .0000

ANDROSTANE 68797 .0017 116.9549 10.9920

C21 0 .0011 .0000 .0000

C22 0 .0013 .0000 .0000 RECOVERY %

C23 0 .0012 .0000 .0000 ANDROSTANE 761.5552

C24 0 .0017 .0000 .0000

C25 0 .0020 .0000 .0000

C26 0 .0029 .0000 .0000

C27 0 .0095 .0000 .0000

C28 0 .0076 .0000 .0000

C29 0 .0124 .0000 .0000

C30 0 .0050 .0000 .0000

RESOLVED 1729 .0017 12.3318 .1300

UNRESOLVED 0 .0017 .0000 .0000

TOTAL .1300