.c1.Appendix G

Detailed summary of aromatic (f2) hydrocarbon determinations for Year 02

(Values are [not]{.underline} corrected for percent recovery)

\[NOTE: ALL VALUES OTHER THAN RESPONSE FACTORS WERE ROUNDED OFF TO TWO
DECIMAL FIGURES. THE USE OF A SLASH TO DISTINGUISH BETWEEN A ZERO AND A
LETTER \"O\" RESULTED IN DIFFICULTIES IN DISTINGUISHING BETWEEN ZERO AND
A NUMBER EIGHT. THE FONT SIZE USED IN THIS SECTION OF THE DOCUMENT WAS
APPROXIMATELY 5. ERRORS IN TRANSCRIPTION MAY HAVE OCCURRED DUE TO FONT
SIZE AND ILLEGIBILITY OF THE COPY OF THE DOCUMENT USED FOR RESCUE.
QUESTIONABLE TRANSCRIPTIONS ARE NOTED WITH A QUESTION MARK. CAUTION
SHOULD BE TAKEN WHEN USING THIS DATA SET. THE COPY OF DOCUMENT USED TO
GENERATE THIS DOCUMENT IS ARCHIVED AT THE NOAA/NMFS/SEFSC LIBRARY IN
MIAMI.\]

Sample: 2016-1 ?

Data analyzed: Nov 10, 1983

Int. Std. (µg): 101

Dry weight (g): 27.93

Inject. volume (µL): 0.5

Sample volume (mL): 0.3

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00126 1233 1.55 0.06 Resol./Unres.

Phenanthrene 3R .00105 0 0 0

*o*-Terphenyl 4R .00128 78414 ? 90.13 Int. std.

1-Methylphenanthrene 5R .00163 0 0 0

Pyrene 6R .00532 0 0 0

\% Recovery 52.54

TOTALS

Resolved for all peaks 76473

Resolved - known peaks 1233 0.06

Resolved - unknown peaks 4826 6.18 0.25

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.31

Sample: 201B-2 ?

Data analyzed: Nov 20, 1983

Int. Std. (µg): 101

Dry weight (g): 18.31

Inject. volume (µL): 2

Sample volume (mL): 0.25

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00076 0 0 0

Dibenzothiophene 2R .00115 0 0 0 Resol./Unres.

Phenanthrene 3R .00890 0 0 0

*o*-Terphenyl 4R .00100 189180 189.10 Int. std.

1-Methylphenanthrene 5R .00136 0 0 0

Pyrene 6R .00433 286 1.24 0.04

\% Recovery 23.40

TOTALS

Resolved for all peaks 195478

Resolved - known peaks 286 0.04

Resolved - unknown peaks 6884 6.08 0.18

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.21

Sample: 201B-3 ?

Data analyzed: Nov 15, 1983

Int. Std. (µg): 101

Dry weight (g): 17.39

Inject. volume (µL): 1.5

Sample volume (mL): 1.9

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00069 0 0 0

Dibenzothiophene 2R .00112 0 0 0 Resol./Unres.

Phenanthrene 3R .00095 0 0 0

*o*-Terphenyl 4R .00113 43882 49.59 Int. std.

1-Methylphenanthrene 5R .00163 0 0 0

Pyrene 6R .00654 0 0 0

\% Recovery 62.19

TOTALS

Resolved for all peaks 49221

Resolved - known peaks 0 0

Resolved - unknown peaks 5339 6.03 0.71 ?

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.71 ?

Sample: 202B-1 ?

Data analyzed: Nov 30, 1983

Int. Std. (µg): 101

Dry weight (g): 30.68

Inject. volume (µL): 2

Sample volume (mL): 0.8

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00076 0 0 0

Dibenzothiophene 2R .00115 0 0 0 Resol./Unres.

Phenanthrene 3R .00890 1191 1.07 0.04 ?

*o*-Terphenyl 4R .00100 85426 85.43 Int. std.

1-Methylphenanthrene 5R .00136 2246 3.05 0.12

Pyrene 6R .00433 0 0 0

\% Recovery 33.83

TOTALS

Resolved for all peaks 103370

Resolved - known peaks 3437 0.16

Resolved - unknown peaks 14587 ? 14.59 0.56

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.72

Sample: 203B-2 ?

Data analyzed: Nov 14 1983

Int. Std. (µg): 101

Dry weight (g): 43.83 ?

Inject. volume (µL): 1.5

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00087 ? 0 0 0 Resol./Unres.

Phenanthrene 3R .00709 0 0 0

*o*-Terphenyl 4R .00084 14665 12.32 Int. std.

1-Methylphenanthrene 5R .00100 0 0 0

Pyrene 6R .00267 0 0 0

\% Recovery 12.28

TOTALS

Resolved for all peaks 14665

Resolved - known peaks 0 0 0

Resolved - unknown peaks 0 0 0

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0

Sample: 203B-1 ?

Data analyzed: Nov 30, 1983

Int. Std. (µg): 101

Dry weight (g): 56.89 ?

Inject. volume (µL): 2

Sample volume (mL): 0.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00076 0 0 0

Dibenzothiophene 2R .00115 0 0 0 Resol./Unres.

Phenanthrene 3R .00890 0 0 0

*o*-Terphenyl 4R .00100 37845 ? 37.85 Int. std.

1-Methylphenanthrene 5R .00136 0 0 0

Pyrene 6R .00433 1160 5.02 0.27

\% Recovery 9.37

TOTALS

Resolved for all peaks 52748 ?

Resolved - known peaks 1160 0.24

Resolved - unknown peaks 13743 13.74 0.64

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.88

Sample: 202B-3

Data analyzed: Nov 10, 1983

Int. Std. (µg): 101

Dry weight (g): 21.04 ?

Inject. volume (µL): 1

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00126 0 0 0 Resol./Unres.

Phenanthrene 3R .00105 0 0 0

*o*-Terphenyl 4R .00128 14475 18.53 Int. std.

1-Methylphenanthrene 5R .00163 0 0 0

Pyrene 6R .00532 0 0 0

\% Recovery 27.52

TOTALS

Resolved for all peaks 15286

Resolved - known peaks 0 0

Resolved - unknown peaks 731 0.94 0.24

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.24

Sample: 203B-3 ?

Data analyzed: Nov 10, 1983

Int. Std. (µg): 101

Dry weight (g): 33.91

Inject. volume (µL): 1

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00126 1101 1.49 0.22 Resol./Unres.

Phenanthrene 3R .00105 0 0 0

*o*-Terphenyl 4R .00128 15591 19.96 Int. std.

1-Methylphenanthrene 5R .00163 0 0 0

Pyrene 6R .00532 0 0 0

\% Recovery 29.64

TOTALS

Resolved for all peaks 19598

Resolved - known peaks 1181 0.22

Resolved - unknown peaks 2826 3.62 0.54

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.76

Sample: D-18-1

Data analyzed: Nov 30, 1983

Int. Std. (µg): 101

Dry weight (g): 43.43 ?

Inject. volume (µL): 2

Sample volume (mL): 1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00076 0 0 0

Dibenzothiophene 2R .00115 1374 ? 2.04 0.03 Resol./Unres.

Phenanthrene 3R .00890 6944 ? 6.25 0.08

*o*-Terphenyl 4R .00100 156420 ? 156.32 Int. std.

1-Methylphenanthrene 5R .00136 3460 ? 4.71 0.06

Pyrene 6R .00433 1582 ? 4.65 0.09

\% Recovery 77.39

TOTALS

Resolved for all peaks 336650 ?

Resolved - known peaks 13760 0.26

Resolved - unknown peaks 166570 ? 166.57 2.17

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 2.43

Sample: D-18-2

Data analyzed: Nov 23, 1983

Int. Std. (µg): 101

Dry weight (g): 26.95

Inject. volume (µL): 2

Sample volume (mL): 1.4

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00067 0 0 0

Dibenzothiophene 2R .00054 2354 2.22 0.05 Resol./Unres.

Phenanthrene 3R .00080 0 0 0

*o*-Terphenyl 4R .00121 13410 162.52 Int. std.

1-Methylphenanthrene 5R .00136 0 0 0

Pyrene 6R .00500 0 0 0

\% Recovery 112.60

TOTALS

Resolved for all peaks 149880

Resolved - known peaks 2354 0.05

Resolved - unknown peaks 13216 15.99 0.37

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.42

Sample: D-20-1 ?

Data analyzed: Nov 30, 1983 ?

Int. Std. (µg): 101

Dry weight (g): 24.3 ?

Inject. volume (µL): 2

Sample volume (mL): 0.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00076 0 0 0

Dibenzothiophene 2R .00115 3295 3.79 0.81 Resol./Unres.

Phenanthrene 3R .00890 25530 22.98 0.88

*o*-Terphenyl 4R .00100 486570 406.57 ? Int. std.

1-Methylphenanthrene 5R .00136 11181 15.21 0.86 ?

Pyrene 6R .00433 4120 17.84 0.07 ?

\% Recovery 108.6 ?

TOTALS

Resolved for all peaks 947880

Resolved - known peaks 44137 0.23

Resolved - unknown peaks 497173 497.17 1.93

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 2.15

Sample: D-20-2 ?

Data analyzed: Nov 20, 1983 ?

Int. Std. (µg): 101

Dry weight (g): 47.12

Inject. volume (µL): 2 ?

Sample volume (mL): 2.2 ?

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00076 0 0 0

Dibenzothiophene 2R .00115 1032 1.32 0.05 Resol./Unres.

Phenanthrene 3R .00890 0 0 0

*o*-Terphenyl 4R .00100 50264 62.33 Int. std.

1-Methylphenanthrene 5R .00136 1036 1.33 0.05

Pyrene 6R .00433 0 0 0

\% Recovery 67.86

TOTALS

Resolved for all peaks 78565

Resolved - known peaks 2868 0.09

Resolved - unknown peaks 26233 32.53 1.11

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 1.21

Sample: D-20-3 ?

Data analyzed: Nov 14, 1983 ?

Int. Std. (µg): 101

Dry weight (g): 32.xx ?

Inject. volume (µL): 2 ?

Sample volume (mL): 1?

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00072 0 0 0

Dibenzothiophene 2R .00087 1291 1.12 0.04 Resol./Unres.

Phenanthrene 3R .00709 0 0 0

*o*-Terphenyl 4R .00054 89014 75.44 Int. std.

1-Methylphenanthrene 5R .00100 1037 1.04 0.04

Pyrene 6R .00207 0 0 0

\% Recovery 37.35

TOTALS

Resolved for all peaks 106568 ?

Resolved - known peaks 2328 0.09

Resolved - unknown peaks 14418 12.11 0.48

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.56

Sample: D-30-1 ?

Data analyzed: Nov 30, 1983 ?

Int. Std. (µg): 101

Dry weight (g): 71.06

Inject. volume (µL): 2

Sample volume (mL): 1.4 ?

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00076 0 0 0

Dibenzothiophene 2R .00115 1106 1.27 0.01 Resol./Unres.

Phenanthrene 3R .00890 10116 9.10 0.11

*o*-Terphenyl 4R .00100 120130 120.13 Int. std.

1-Methylphenanthrene 5R .00136 4153 5.65 0.06

Pyrene 6R .00433 ? 1754 7.59 0.09

\% Recovery 83.26

TOTALS

Resolved for all peaks 348430

Resolved - known peaks 17129 0.28

Resolved - unknown peaks 211171 211.17 2.50

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 2.78

Sample: D-30-2 ?

Data analyzed: Nov 28, 1983

Int. Std. (µg): 101

Dry weight (g): 42.67

Inject. volume (µL): 2

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00019 0 0 0

Dibenzothiophene 2R .00238 1491 3.50 0.04 Resol./Unres.

Phenanthrene 3R .00193 725 1.40 0.02

*o*-Terphenyl 4R .00221 82350 181.99 Int. std.

1-Methylphenanthrene 5R .00226 857 1.94 0.03

Pyrene 6R .00535 0 0 0

\% Recovery 135.1

TOTALS

Resolved for all peaks 99815

Resolved - known peaks 3053 0.09

Resolved - unknown peaks 14412 31.86 0.41

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.50

Sample: D-30-3 ?

Data analyzed: Nov 15, 1983

Int. Std. (µg): 101

Dry weight (g): 41.83

Inject. volume (µL): 2

Sample volume (mL): 2.4

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00069 0 0 0

Dibenzothiophene 2R .00112 0 0 0 Resol./Unres.

Phenanthrene 3R .00095 0 0 0

*o*-Terphenyl 4R .00113 95522 187.94 Int. std.

1-Methylphenanthrene 5R .00163 1372 2.24 0.05

Pyrene 6R .00654 607 3.97 0.10

\% Recovery 128.2

TOTALS

Resolved for all peaks 106640 ?

Resolved - known peaks 1979 0.14

Resolved - unknown peaks 9139 10.33 0.24

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.38

Sample: JU JETTIES B-1 ?

Data analyzed: Nov 18, 1983 ?

Int. Std. (µg): 101

Dry weight (g): 42.33 ?

Inject. volume (µL): 1

Sample volume (mL): 1.8

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00126 1994 2.51 0.12 Resol./Unres.

Phenanthrene 3R .00105 0 0 0

*o*-Terphenyl 4R .00128 37946 48.58 Int. std.

1-Methylphenanthrene 5R .00163 636 1.04 0.06

Pyrene 6R .00532 1065 5.67 0.28

\% Recovery 86.56

TOTALS

Resolved for all peaks 76988

Resolved - known peaks 3695 0.46

Resolved - unknown peaks 35347 45.24 2.21

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 2.66

Sample: JU JETTIES B-2 ?

Data analyzed: Nov 18, 1983 ?

Int. Std. (µg): 101

Dry weight (g): 37.82

Inject. volume (µL): 2

Sample volume (mL): 1.75

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00126 1059 1.33 0.05 Resol./Unres.

Phenanthrene 3R .00105 1163 1.22 0.05

*o*-Terphenyl 4R .00128 53637 68.66 Int. std.

1-Methylphenanthrene 5R .00163 0 0 0

Pyrene 6R .00532 0 0 0

\% Recovery 59.48

TOTALS

Resolved for all peaks 63598

Resolved - known peaks 2222 0.10

Resolved - unknown peaks 7739 9.91 0.39

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.49

Sample: JU JETTIES B-3 ?

Data analyzed: Nov 18, 1983 ?

Int. Std. (µg): 101

Dry weight (g): 40.56

Inject. volume (µL): 1

Sample volume (mL): 0.9

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00126 3806 4.80 0.11 Resol./Unres.

Phenanthrene 3R .00105 0 0 0

*o*-Terphenyl 4R .00128 85324 109.21 Int. std.

1-Methylphenanthrene 5R .00163 5847 8.23 0.19

Pyrene 6R .00532 1978 10.52 0.24

\% Recovery 97.32

TOTALS

Resolved for all peaks 139370

Resolved - known peaks 10831 ? 0.54

Resolved - unknown peaks 43215 55.32 1.26

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 1.80

Sample: JU ALT. B B-2 ?

Data analyzed: Nov 18, 1983 ?

Int. Std. (µg): 101

Dry weight (g): 10.93 ?

Inject. volume (µL): 2

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00126 0 0 0 Resol./Unres.

Phenanthrene 3R .00105 0 0 0

*o*-Terphenyl 4R .00128 69734 89.26 Int. std.

1-Methylphenanthrene 5R .00163 0 0 0

Pyrene 6R .00532 0 0 0

\% Recovery 66.28

TOTALS

Resolved for all peaks 75435

Resolved - known peaks 0 0

Resolved - unknown peaks 5701 7.30 0.76

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.76

Sample: JU N6A-B-1 ?

Data analyzed: Nov 122, 1983 ?

Int. Std. (µg): 101

Dry weight (g): 52.64?

Inject. volume (µL): 2

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00067 0 0 0

Dibenzothiophene 2R .00108 ? 0 0 0 Resol./Unres.

Phenanthrene 3R .00096 2376 2.29 0.04

*o*-Terphenyl 4R .00121 93658 113.32 Int. std.

1-Methylphenanthrene 5R .00200 0 0 0

Pyrene 6R .00980 0 0 0

\% Recovery 84.15

TOTALS

Resolved for all peaks 110138 ?

Resolved - known peaks 2376 0.04

Resolved - unknown peaks 14184 ? 17.07 0.28

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0..32

Sample: JU N6A-B-2 ?

Data analyzed: Nov 22, 1983 ?

Int. Std. (µg): 101

Dry weight (g): 67.52

Inject. volume (µL): 1.5

Sample volume (mL): 1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00067 0 0 0

Dibenzothiophene 2R .00108 ? 0 0 0 Resol./Unres.

Phenanthrene 3R .00096 5336 5.12 0.06

*o*-Terphenyl 4R .00121 99424 120.30 Int. std.

1-Methylphenanthrene 5R .00200 5027 10.05 0.13

Pyrene 6R .00980 1582 15.50 0.19

\% Recovery 79.41

TOTALS

Resolved for all peaks 260010 ?

Resolved - known peaks 11945 0.38

Resolved - unknown peaks 148641 ? 179.86 2.24

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 2.62

Sample: JU N6A-B-3 ?

Data analyzed: Nov 22, 1983 ?

Int. Std. (µg): 101

Dry weight (g): 67.90

Inject. volume (µL): 2

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00067 0 0 0

Dibenzothiophene 2R .00108 ? 0 0 0 Resol./Unres.

Phenanthrene 3R .00096 0 0 0

*o*-Terphenyl 4R .00121 5168 6.24 Int. std.

1-Methylphenanthrene 5R .00200 0 0 0

Pyrene 6R .00980 0 0 0

\% Recovery 4.64

TOTALS

Resolved for all peaks 20673 ?

Resolved - known peaks 0 0

Resolved - unknown peaks 15513 10.78 4.47

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 4.47

Sample: 205B

Data analyzed: Sep 9, 1983 ?

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00085 0 0 0

Dibenzothiophene 2R .00118 0 0 0 Resol./Unres.

Phenanthrene 3R .00095 0 0 0

*o*-Terphenyl 4R .00098 538850 528.07 Int. std.

1-Methylphenanthrene 5R .00096 0 0 0

Pyrene 6R .00102 0 0 0

\% Recovery 25.89

TOTALS

Resolved for all peaks 582310?

Resolved - known peaks 0 0

Resolved - unknown peaks 43460 42.59 4.58

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 4.58

Sample: 206B

Data analyzed: Sep 8, 1983 ?

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 0.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00085 0 0 0

Dibenzothiophene 2R .00118 0 0 0 Resol./Unres.

Phenanthrene 3R .00095 0 0 0

*o*-Terphenyl 4R .00098 321510 315.08 Int. std.

1-Methylphenanthrene 5R .00096 0 0 0

Pyrene 6R .00102 0 0 0

\% Recovery 77.23

TOTALS

Resolved for all peaks 923580 ?

Resolved - known peaks 0 0

Resolved - unknown peaks 602070 598.03 10.61

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 10.61

Sample: 207B

Data analyzed: Sep 14, 1983 ?

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 1

Sample volume (mL): 0.1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00090 0 0 0 Resol./Unres.

Phenanthrene 3R .00072 0 0 0

*o*-Terphenyl 4R .00073 725450 529.58 Int. std.

1-Methylphenanthrene 5R .00077 0 0 0

Pyrene 6R .00095 1357 1.29 0.01

\% Recovery 51.92

TOTALS

Resolved for all peaks 703380

Resolved - known peaks 1357 0.01

Resolved - unknown peaks 56573 41.30 0.44

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.46

Sample: 208B

Data analyzed: Sep 14, 1983 ?

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 1

Sample volume (mL): 0.1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00090 0 0 0 Resol./Unres.

Phenanthrene 3R .00072 0 0 0

*o*-Terphenyl 4R .00073 627300 457.93 Int. std.

1-Methylphenanthrene 5R .00077 0 0 0

Pyrene 6R .00095 0 0 0

\% Recovery 44.90

TOTALS

Resolved for all peaks 656240

Resolved - known peaks 0 0

Resolved - unknown peaks 28940 21.13 0.26

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.26

Sample: 209B

Data analyzed: Sep 14, 1983 ?

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 1

Sample volume (mL): 0.1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00090 1937 1.74 0.01 Resol./Unres.

Phenanthrene 3R .00072 0 0 0

*o*-Terphenyl 4R .00073 955160 697.27 Int. std.

1-Methylphenanthrene 5R .00077 0 0 0

Pyrene 6R .00095 1296 1.23 0.01

\% Recovery 68.36

TOTALS

Resolved for all peaks 988660

Resolved - known peaks 3233 0.02

Resolved - unknown peaks 30267 22.09 0.18

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.20

Sample: 210B

Data analyzed: Sep 14, 1983 ?

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 1

Sample volume (mL): 0.1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00089 0 0 0

Dibenzothiophene 2R .00126 1926 2.42 0.05 Resol./Unres. 10.11

Phenanthrene 3R .00102 1316 1.34 0.03

*o*-Terphenyl 4R .00108 239900 259.09 Int. std.

1-Methylphenanthrene 5R .00123 5359 6.59 0.14

Pyrene 6R .00229 8435 19.32 0.42

\% Recovery 25.40

TOTALS

Resolved for all peaks 2543000

Resolved - known peaks 17036 0.65

Resolved - unknown peaks 226064 2468.95 54.00

Unresolved (UCM) 226910 247.11 5.40

Total aliphatic hydrocarbons 60.05

Sample: 211B

Data analyzed: Sep 15, 1983 ?

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 1

Sample volume (mL): 0.1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00089 0 0 0

Dibenzothiophene 2R .00126 977 1.23 0.02 Resol./Unres.

Phenanthrene 3R .00102 0 0 0

*o*-Terphenyl 4R .00108 251240 271.34 Int. std.

1-Methylphenanthrene 5R .00123 0 0 0

Pyrene 6R .00229 0 0 0

\% Recovery 26.60

TOTALS

Resolved for all peaks 1119600

Resolved - known peaks 977 0.03

Resolved - unknown peaks 867383 936.77 19.56

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 19.59

Sample: 212B

Data analyzed: Sep 8, 1983 ?

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00085 0 0 0

Dibenzothiophene 2R .00118 7110 8.39 0.69 Resol./Unres.

Phenanthrene 3R .00095 0 0 0

*o*-Terphenyl 4R .00098 79563 77.97 Int. std.

1-Methylphenanthrene 5R .00096 0 0 0

Pyrene 6R .00102 0 0 0

\% Recovery 38.22

TOTALS

Resolved for all peaks 790680

Resolved - known peaks 7110 0.61

Resolved - unknown peaks 704087 689.93 50.14

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 50.76

Sample: 221B

Data analyzed: Sep 9, 1983 ?

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 0.8

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00071 0 0 0

Dibenzothiophene 2R .00105 0 0 0 Resol./Unres.

Phenanthrene 3R .00083 0 0 0

*o*-Terphenyl 4R .00088 267030 234.99 Int. std.

1-Methylphenanthrene 5R .00094 0 0 0

Pyrene 6R .00113 953 1.08 0.03

\% Recovery 92.15

TOTALS

Resolved for all peaks 57120

Resolved - known peaks 953 0.03

Resolved - unknown peaks 304137 267.65 6.45

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 6.48

Sample: 222B

Data analyzed: Sep 9, 1983 ?

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 0.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00071 0 0 0

Dibenzothiophene 2R .00105 0 0 0 Resol./Unres.

Phenanthrene 3R .00083 0 0 0

*o*-Terphenyl 4R .00088 141450 124.48 Int. std.

1-Methylphenanthrene 5R .00094 0 0 0

Pyrene 6R .00113 1636 1.85 0.08

\% Recovery 92.15

TOTALS

Resolved for all peaks 357580

Resolved - known peaks 1636 0.08

Resolved - unknown peaks 214494 188.75 8.59

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 8.68

Sample: 224B

Data analyzed: Sep 9, 1983

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 0.35

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00071 0 0 0

Dibenzothiophene 2R .00105 0 0 0 Resol./Unres.

Phenanthrene 3R .00083 0 0 0

*o*-Terphenyl 4R .00088 620100 545.69 Int. std.

1-Methylphenanthrene 5R .00094 0 0 0

Pyrene 6R .00113 0 0 0

\% Recovery 93.62

TOTALS

Resolved for all peaks 835830

Resolved - known peaks 0 0

Resolved - unknown peaks 215730 189.84 1.97

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 1.97

Sample: 224B

Data analyzed: Sep 9, 1983

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 0.2

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00071 0 0 0

Dibenzothiophene 2R .00105 0 0 0 Resol./Unres.

Phenanthrene 3R .00083 0 0 0

*o*-Terphenyl 4R .00088 958110 843.14 Int. std.

1-Methylphenanthrene 5R .00094 0 0 0

Pyrene 6R .00113 1749 1.98 0.01

\% Recovery 82.66

TOTALS

Resolved for all peaks 1331504

Resolved - known peaks 17490 0.01

Resolved - unknown peaks 371641 327.04 2.20

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 2.21

Sample: 227B

Data analyzed: Sep 14, 1983

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 0.1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00090 29993 26.99 0.08 Resol./Unres. 1.67

Phenanthrene 3R .00072 17632 12.70 0.04 ?

*o*-Terphenyl 4R .00073 2557800 1867.19 Int. std.

1-Methylphenanthrene 5R .00077 0 0 0

Pyrene 6R .00095 0 0 0

\% Recovery 91.53

TOTALS

Resolved for all peaks 3154700

Resolved - known peaks 47625 0.12

Resolved - unknown peaks 549275 400.98 ? 1.22

Unresolved (UCM) 361667 264.02 ? 0.70

Total aliphatic hydrocarbons 2.14

Sample: 230B

Data analyzed: Sep 9, 1983

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 0.2

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00090 0 0 0 Resol./Unres.

Phenanthrene 3R .00072 0 0 0

*o*-Terphenyl 4R .00073 1054700? 928.14 Int. std.

1-Methylphenanthrene 5R .00077 0 0 0

Pyrene 6R .00095 0 0 0

\% Recovery 98.99 ?

TOTALS

Resolved for all peaks 1313780

Resolved - known peaks 0 0

Resolved - unknown peaks 259000 ? 227.92 1.39

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 1.39

Sample: 231B

Data analyzed: Sep 14, 1983

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 1

Sample volume (mL): 0.1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00090 0 0 0 Resol./Unres.

Phenanthrene 3R .00072 0 0 0

*o*-Terphenyl 4R .00073 1011000? 738.03 Int. std.

1-Methylphenanthrene 5R .00077 0 0 0

Pyrene 6R .00095 0 0 0

\% Recovery 72.36

TOTALS

Resolved for all peaks 1173100 ?

Resolved - known peaks 0 0

Resolved - unknown peaks 162100 ? 118.33 0.91

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.91

Sample: 232B

Data analyzed: Sep 14, 1983

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 1

Sample volume (mL): 0.1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00090 709 0.64 0.01 Resol./Unres. 0.38

Phenanthrene 3R .00072 978 0.70 0.01

*o*-Terphenyl 4R .00073 487790 356.09 Int. std.

1-Methylphenanthrene 5R .00077 1555 1.20 0.02

Pyrene 6R .00095 0 0 0

\% Recovery 34.91

TOTALS

Resolved for all peaks 550850 ?

Resolved - known peaks 3242 0.04

Resolved - unknown peaks 59710 ? 43.59 0.69

Unresolved (UCM) 164762 120.28 1.91

Total aliphatic hydrocarbons 2.65

Sample: 233B

Data analyzed: Sep 12, 1983

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00074 0 0 0

Dibenzothiophene 2R .00104 0 0 0 Resol./Unres.

Phenanthrene 3R .00085 0 0 0

*o*-Terphenyl 4R .00090 162140 145.93 Int. std.

1-Methylphenanthrene 5R .00095 0 0 0

Pyrene 6R .00114 0 0 0

\% Recovery 71.4 ?

TOTALS

Resolved for all peaks 178510 ?

Resolved - known peaks 15634 0.69

Resolved - unknown peaks 736 0.66 0.03

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.71

Sample: 234B

Data analyzed: Sep 12, 1983

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00074 0 0 0

Dibenzothiophene 2R .00104 0 0 0 Resol./Unres.

Phenanthrene 3R .00085 0 0 0

*o*-Terphenyl 4R .00090 51752 46.58 Int. std.

1-Methylphenanthrene 5R .00095 0 0 0

Pyrene 6R .00114 0 0 0

\% Recovery 22.83

TOTALS

Resolved for all peaks 52258

Resolved - known peaks 0 0

Resolved - unknown peaks 506 0.46 0.06

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.06

Sample: 235B

Data analyzed: Sep 12, 1983

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00074 0 0 0

Dibenzothiophene 2R .00104 0 0 0 Resol./Unres.

Phenanthrene 3R .00085 0 0 0

*o*-Terphenyl 4R .00090 74913 67.42 Int. std.

1-Methylphenanthrene 5R .00095 0 0 0

Pyrene 6R .00114 0 0 0

\% Recovery 33.05

TOTALS

Resolved for all peaks 78145

Resolved - known peaks 0 0

Resolved - unknown peaks 3232 2.91 0.24

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.24

Sample: 237B

Data analyzed: Sep 12, 1983

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00074 0 0 0

Dibenzothiophene 2R .00104 0 0 0 Resol./Unres.

Phenanthrene 3R .00085 0 0 0

*o*-Terphenyl 4R .00090 55859 50.27 Int. std.

1-Methylphenanthrene 5R .00095 0 0 0

Pyrene 6R .00114 0 0 0

\% Recovery 24.64

TOTALS

Resolved for all peaks 63031

Resolved - known peaks 0 0

Resolved - unknown peaks 717 6.45 0.73

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.73

Sample: 238B

Data analyzed: Sep 12, 1983

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00074 0 0 0

Dibenzothiophene 2R .00104 0 0 0 Resol./Unres.

Phenanthrene 3R .00085 0 0 0

*o*-Terphenyl 4R .00090 81091 72.98 Int. std.

1-Methylphenanthrene 5R .00095 0 0 0

Pyrene 6R .00114 0 0 0

\% Recovery 53.66

TOTALS

Resolved for all peaks 89614

Resolved - known peaks 0 0

Resolved - unknown peaks 8523 7.68 0.60

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.60

Sample: 240B-1

Data analyzed: Sep 12, 1983

Int. Std. (µg): 102

Dry weight (g): 9

Inject. volume (µL): 2

Sample volume (mL): 1.25

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00074 0 0 0

Dibenzothiophene 2R .00104 0 0 0 Resol./Unres.

Phenanthrene 3R .00085 0 0 0

*o*-Terphenyl 4R .00090 145350 130.82 Int. std.

1-Methylphenanthrene 5R .00095 0 0 0

Pyrene 6R .00114 0 0 0

\% Recovery 80.16

TOTALS

Resolved for all peaks 148670

Resolved - known peaks 0 0

Resolved - unknown peaks 3320 2.99 0.26

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.26

Sample: 241B-1

Data analyzed: Sep 14, 1983

Int. Std. (µg): 102

Dry weight (g): 9

Inject. volume (µL): 1

Sample volume (mL): 0.1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00090 811 0.73 0.01 Resol./Unres.

Phenanthrene 3R .00072 0 0 0

*o*-Terphenyl 4R .00073 891040 650.46 Int. std.

1-Methylphenanthrene 5R .00077 0 0 0

Pyrene 6R .00095 0 0 0

\% Recovery 63.77

TOTALS

Resolved for all peaks 980450

Resolved - known peaks 811 0.01

Resolved - unknown peaks 8599 6.28 0.11

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.12

Sample: 242B

Data analyzed: Sep 12, 1983

Int. Std. (µg): 102

Dry weight (g): 18

Inject. volume (µL): 2

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00074 0 0 0

Dibenzothiophene 2R .00104 0 0 0 Resol./Unres.

Phenanthrene 3R .00085 0 0 0

*o*-Terphenyl 4R .00090 84395 75.96 Int. std.

1-Methylphenanthrene 5R .00095 0 0 0

Pyrene 6R .00114 0 0 0

\% Recovery 55.85

TOTALS

Resolved for all peaks 86040

Resolved - known peaks 0 0

Resolved - unknown peaks 1645 1.48 0.11

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.11

Sample: 246B-1

Data analyzed: Sep 14, 1983

Int. Std. (µg): 102

Dry weight (g): 9

Inject. volume (µL): 1

Sample volume (mL): 0.1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00090 3265 2.94 0.04 Resol./Unres.

Phenanthrene 3R .00072 2974 2.14 0.03

*o*-Terphenyl 4R .00073 1168308? 847.02 ? Int. std.

1-Methylphenanthrene 5R .00077 0 0 0

Pyrene 6R .00095 0 0 0

\% Recovery 83.04 ?

TOTALS

Resolved for all peaks 1197200?

Resolved - known peaks 6239 0.07

Resolved - unknown peaks 38661 22.38 0.30

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.37

Sample: 247B-1

Data analyzed: Sep 14, 1983

Int. Std. (µg): 102

Dry weight (g): 9

Inject. volume (µL): 1

Sample volume (mL): 0.1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00090 0 0 0 Resol./Unres.

Phenanthrene 3R .00072 0 0 0

*o*-Terphenyl 4R .00073 328340 239.69 Int. std.

1-Methylphenanthrene 5R .00077 0 0 0

Pyrene 6R .00095 0 0 0

\% Recovery 23.50

TOTALS

Resolved for all peaks 332590

Resolved - known peaks 0 0

Resolved - unknown peaks 4250 3.10 0.15

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.15

Sample: 213B ? (0 - 5)

Data analyzed: Nov 14, 1983

Int. Std. (µg): 101

Dry weight (g): 21.84

Inject. volume (µL): 1.5

Sample volume (mL): 2

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00067 1595 1.39 0.11 Resol./Unres.

Phenanthrene 3R .00709 50476 35.78 2.85

*o*-Terphenyl 4R .00084 69242 58.16 Int. std.

1-Methylphenanthrene 5R .00100 1064 1.06 0.08

Pyrene 6R .00207 17656 50.67 4.83

\% Recovery 76.78

TOTALS

Resolved for all peaks 204593 ?

Resolved - known peaks 78791 ? 7.87

Resolved - unknown peaks 64557 54.23 4.31

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 11.39

Sample: 214B ? (0 - 5)

Data analyzed: Nov 14, 1983

Int. Std. (µg): 101

Dry weight (g): 14.18 ?

Inject. volume (µL): 1.5

Sample volume (mL): 1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00067 1593 1.39 0.12 Resol./Unres. 0.49

Phenanthrene 3R .00709 19596 13.89 1.22

*o*-Terphenyl 4R .00084 96424 81.00 Int. std.

1-Methylphenanthrene 5R .00100 2987 2.99 0.26

Pyrene 6R .00207 12297 35.29 3.10

\% Recovery 53.46

TOTALS

Resolved for all peaks 244940?

Resolved - known peaks 36473 4.79

Resolved - unknown peaks 112043 94.12 8.28

Unresolved (UCM) 357478 300.28 26.41 ?

Total aliphatic hydrocarbons 39.39

Sample: 214B ? (20 - 25)

Data analyzed: Nov 14, 1983

Int. Std. (µg): 101

Dry weight (g): 21.84

Inject. volume (µL): 1.5

Sample volume (mL): 1.8

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00067 4509 3.92 0.31 Resol./Unres. 0.31

Phenanthrene 3R .00709 2289 1.62 0.13

*o*-Terphenyl 4R .00084 69125 58.87 Int. std.

1-Methylphenanthrene 5R .00100 1446 1.45 0.11

Pyrene 6R .00207 2426 6.96 0.55

\% Recovery 68.99

TOTALS

Resolved for all peaks 138150

Resolved - known peaks 10678 ? 1.11

Resolved - unknown peaks 58655 49.81 3.90

Unresolved (UCM) 238416 208.27 ? 15.96

Total aliphatic hydrocarbons 20.97

Sample: 215B ? (0 - 5)

Data analyzed: Nov 9, 1983

Int. Std. (µg): 101

Dry weight (g): 26.84

Inject. volume (µL): 1

Sample volume (mL): 2

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00071 0 0 0

Dibenzothiophene 2R .00105 2624 2.76 0.33 Resol./Unres. 0.28

Phenanthrene 3R .00083 0 0 0

*o*-Terphenyl 4R .00088 34931 30.74 Int. std.

1-Methylphenanthrene 5R .00094 2081 1.96 0.24

Pyrene 6R .00113 0 0 0

\% Recovery 60.87

TOTALS

Resolved for all peaks 99070

Resolved - known peaks 4705 0.58

Resolved - unknown peaks 59434 52.30 6.40 ?

Unresolved (UCM) 227888 200.54 ? 24.55

Total aliphatic hydrocarbons 31.53

Sample: 216B ? (0 - 5)

Data analyzed: Nov 23, 1983

Int. Std. (µg): 101

Dry weight (g): 14.92

Inject. volume (µL): 1.5

Sample volume (mL): 2.25

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00097 6228 6.84 1.74

Dibenzothiophene 2R .00128 10011 12.81 3.70 Resol./Unres. 1.71

Phenanthrene 3R .00104 3082 3.12 0.90

*o*-Terphenyl 4R .00124 18954 23.58 Int. std.

1-Methylphenanthrene 5R .00128 1349 1.73 0.50

Pyrene 6R .00242 3536 8.56 2.46

\% Recovery 34.91

TOTALS

Resolved for all peaks 319478

Resolved - known peaks 24126 9.29

Resolved - unknown peaks 276390 342.72 98.71

Unresolved (UCM) 176540 218.91 ? 63.05 ?

Total aliphatic hydrocarbons 171.06

Sample: 217B ? (0 - 5)

Data analyzed: Nov 14, 1983

Int. Std. (µg): 101

Dry weight (g): 33.57

Inject. volume (µL): 1.5

Sample volume (mL): 1.3

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073 0 0 0

Dibenzothiophene 2R .00067 2331 2.03 0.07 Resol./Unres. 0.59

Phenanthrene 3R .00709 12162 8.62 0.29

*o*-Terphenyl 4R .00084 107540 90.33 Int. std.

1-Methylphenanthrene 5R .00100 8676 8.68 0.29

Pyrene 6R .00207 1502 4.31 0.14

\% Recovery 77.51

TOTALS

Resolved for all peaks 288130

Resolved - known peaks 24671 0.79

Resolved - unknown peaks 155919 130.97 4.36

Unresolved (UCM) 311437 261.61 8.71

Total aliphatic hydrocarbons 13.86

Sample: 218B-1 ? (0 - 5)

Data analyzed: Nov 15, 1983

Int. Std. (µg): 101

Dry weight (g): 39.29

Inject. volume (µL): 1.5

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00069 0 0 0

Dibenzothiophene 2R .00112 1987 2.23 0.06 Resol./Unres. 1.04

Phenanthrene 3R .00095 14864 14.13 0.42 ?

*o*-Terphenyl 4R .00113 78296 88.47 Int. std.

1-Methylphenanthrene 5R .00163 1054 1.72 0.05 ?

Pyrene 6R .00654 3176 20.77 0.60 ?

\% Recovery 87.60

TOTALS

Resolved for all peaks 135220

Resolved - known peaks 21081 1.13

Resolved - unknown peaks 35843 40.50 ? 1.18

Unresolved (UCM) 67449 76.22 2.21

Total aliphatic hydrocarbons 4.52

Sample: 218B (20 - 25)

Data analyzed: Nov 15, 1983

Int. Std. (µg): 101

Dry weight (g): 33.91

Inject. volume (µL): 1

Sample volume (mL): 1.2

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00069 0 0 0

Dibenzothiophene 2R .00112 7049 7.89 0.15 Resol./Unres. 1.63

Phenanthrene 3R .00095 34338 32.62 0.62 ?

*o*-Terphenyl 4R .00113 138630 ? 156.65 Int. std.

1-Methylphenanthrene 5R .00163 3183 5.19 0.10

Pyrene 6R .00654 18090 65.99 1.25

\% Recovery 186.1 ?

TOTALS

Resolved for all peaks 331070 ?

Resolved - known peaks 54660 2.12

Resolved - unknown peaks 137780 155.69 ? 2.97

Unresolved (UCM) 145455 164.36 3.13

Total aliphatic hydrocarbons 8.29

Sample: 218B ? (60 - 65)

Data analyzed: Nov 15, 1983

Int. Std. (µg): 101

Dry weight (g): 17.17

Inject. volume (µL): 1.5

Sample volume (mL): 2

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00069 0 0 0

Dibenzothiophene 2R .00112 9732 10.90 1.05 Resol./Unres. 1.04

Phenanthrene 3R .00095 12653 12.02 1.16

*o*-Terphenyl 4R .00113 53789 60.78 ? Int. std.

1-Methylphenanthrene 5R .00163 3234 5.27 0.51 ?

Pyrene 6R .00654 2605 17.04? 1.65

\% Recovery 80.24

TOTALS

Resolved for all peaks 297180

Resolved - known peaks 28224 4.38

Resolved - unknown peaks 215167 243.14 23.54

Unresolved (UCM) 244281 276.04 26.71

Total aliphatic hydrocarbons 54.62

Sample: 219B (0 - 5)

Data analyzed: Nov 30, 1983

Int. Std. (µg): 101

Dry weight (g): 17.15

Inject. volume (µL): 2

Sample volume (mL): 1.1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00076 472 0.36 0.18

Dibenzothiophene 2R .00115 960 1.18 0.55 Resol./Unres. 0.27

Phenanthrene 3R .00090 640 0.58 0.29

*o*-Terphenyl 4R .00100 11897 11.90 Int. std.

1-Methylphenanthrene 5R .00136 893 1.21 0.60

Pyrene 6R .00433 962 4.17 2.06

\% Recovery 6.48

TOTALS

Resolved for all peaks 32951

Resolved - known peaks 3927 3.67

Resolved - unknown peaks 17127 17.13 8.48

Unresolved (UCM) 91202 91.20 45.15

Total aliphatic hydrocarbons 57.30

Sample: 222B ? (0 - 5)

Data analyzed: Nov 15, 1983

Int. Std. (µg): 101

Dry weight (g): 28.04 ?

Inject. volume (µL): 1.5

Sample volume (mL): 1.2

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00069 0 0 0

Dibenzothiophene 2R .00112 4472 5.01 0.16 Resol./Unres. 1.26

Phenanthrene 3R .00095 36055 ? 36.15 1.16

*o*-Terphenyl 4R .00113 98051 111.78 ? Int. std.

1-Methylphenanthrene 5R .00163 2424 3.95 0.13

Pyrene 6R .00654 7101 46.44 1.50

\% Recovery 58.48 ?

TOTALS

Resolved for all peaks 355108

Resolved - known peaks 52853 2.95

Resolved - unknown peaks 204196 238.74 7.45

Unresolved (UCM) 225806 255.16 8.23

Total aliphatic hydrocarbons 18.63

Sample: 223B ? (0 - 5)

Data analyzed: Nov 22, 1983

Int. Std. (µg): 101

Dry weight (g): 17.57

Inject. volume (µL): 2

Sample volume (mL): 1.4

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00067 0 0 0

Dibenzothiophene 2R .00108 1457 1.57 0.88 Resol./Unres.

Phenanthrene 3R .00096 16821 18.87 0.88

*o*-Terphenyl 4R .00121 98002 ? 118.58 Int. std.

1-Methylphenanthrene 5R .00200 1766 3.53 0.17

Pyrene 6R .00980 5269 51.64 2.50

\% Recovery 82.18

TOTALS

Resolved for all peaks 339728

Resolved - known peaks 27313 3.63

Resolved - unknown peaks 214407 259.42 12.58

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 16.21

Sample: 225B (0 - 5)

Data analyzed: Nov 30, 1983

Int. Std. (µg): 101

Dry weight (g): 25.25

Inject. volume (µL): 2

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00076 0 0 0

Dibenzothiophene 2R .00115 669 0.76 0.03 Resol./Unres.

Phenanthrene 3R .00090 3794 3.41 0.15

*o*-Terphenyl 4R .00100 91696 91.70 Int. std.

1-Methylphenanthrene 5R .00136 1116 1.52 0.07

Pyrene 6R .00433 2532 18.96 0.48

\% Recovery 68.09

TOTALS

Resolved for all peaks 172840

Resolved - known peaks 8111 0.73

Resolved - unknown peaks 73833 73.83 3.19

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 3.91

Sample: 225B (25 - 30)

Data analyzed: Nov 16, 1983

Int. Std. (µg): 101

Dry weight (g): 27.14

Inject. volume (µL): 2

Sample volume (mL): 1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00067 0 0 0

Dibenzothiophene 2R .00108 2551 3.34 0.12 Resol./Unres.

Phenanthrene 3R .00096 0 0 0

*o*-Terphenyl 4R .00121 75285 103.78 Int. std.

1-Methylphenanthrene 5R .00200 10 0 0

Pyrene 6R .00980 0 0 0

\% Recovery 51.38

TOTALS

Resolved for all peaks 81181

Resolved - known peaks 2551 0.12

Resolved - unknown peaks 3425 4.73 0.17

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0.29

Sample: 225B (55 - 60)

Data analyzed: Nov 16, 1983

Int. Std. (µg): 101

Dry weight (g): 9.89

Inject. volume (µL): 2

Sample volume (mL): 1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00067 0 0 0

Dibenzothiophene 2R .00101 ? 2748 3.60 ? 0.18 Resol./Unres.

Phenanthrene 3R .00114 ? 0 0 0

*o*-Terphenyl 4R .00126 ? 151050 ? 206.50 ? Int. std.

1-Methylphenanthrene 5R .00216 488 1.05 0.05

Pyrene 6R .00957 0 0 0

\% Recovery 103.2

TOTALS

Resolved for all peaks 213620 ?

Resolved - known peaks 3206 ? 0.23

Resolved - unknown peaks 59304 ? 91.84 4.01

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 4.24

Sample: 228B (0 - 5)

Data analyzed: Nov 22, 1983

Int. Std. (µg): 101

Dry weight (g): 39.81

Inject. volume (µL): 2

Sample volume (mL): 2.2

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00097 0 0 0

Dibenzothiophene 2R .00128 588 0.75 0.05 Resol./Unres.

Phenanthrene 3R .00104 1050 1.10 0 .08

*o*-Terphenyl 4R .00124 28448 35.27 Int. std.

1-Methylphenanthrene 5R .00128 0 0 0

Pyrene 6R .00242 2006 ? 4.85 0.35

\% Recovery 28.41 ?

TOTALS

Resolved for all peaks 50552 ?

Resolved - known peaks 3644 ? 0.48

Resolved - unknown peaks 18468 ? 22.91 ? 1.64 ?

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 2.72 ?

Sample: 229B (0 - 5)

Data analyzed: Nov 16, 1983

Int. Std. (µg): 101

Dry weight (g): 14.54

Inject. volume (µL): ?

Sample volume (mL): ?

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00067 0 0 0

Dibenzothiophene 2R .00101 ? 5800 7.70 0.48 Resol./Unres.

Phenanthrene 3R .00114 ? 2444 2.78 ? 0.18

*o*-Terphenyl 4R .00126 ? 79852 110.20 ? Int. std.

1-Methylphenanthrene 5R .00216 2672 5.77 0.36

Pyrene 6R .00957 0 0 0

\% Recovery 109.1

TOTALS

Resolved for all peaks 176120

Resolved - known peaks 10996 ? 1.02

Resolved - unknown peaks 85282 ? 117.69 7.42

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 8.44

Sample: 232B-1 (0 - 5)

Data analyzed: Nov 30, 1983

Int. Std. (µg): 101

Dry weight (g): 78.72 ?

Inject. volume (µL): 2

Sample volume (mL): 1.8 ?

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00076 0 0 0

Dibenzothiophene 2R .00115 14972 17.22 0.50 Resol./Unres. 0.52

Phenanthrene 3R .00090 108 0.90 ? 0.00 ?

*o*-Terphenyl 4R .00100 91185 91.11 ? Int. std.

1-Methylphenanthrene 5R .00136 2251 3.06 0.08 ?

Pyrene 6R .00432 633 2.75 0.08

\% Recovery 81.18

TOTALS

Resolved for all peaks 256680 ?

Resolved - known peaks 17964 0.57

Resolved - unknown peaks 147531 147.53 4.27

Unresolved (UCM) 327273 327.27 9.47

Total aliphatic hydrocarbons 14.49

Sample: 233B (0 - 5)

Data analyzed: Nov 16, 1983

Int. Std. (µg): 101

Dry weight (g): 15.86

Inject. volume (µL): 2

Sample volume (mL): 2

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00155 0 0 0

Dibenzothiophene 2R .00201 ? 21752 28.50 4.05 Resol./Unres. 1.34

Phenanthrene 3R .00168 ? 0 0 0

*o*-Terphenyl 4R .00175 32455 44.79 Int. std.

1-Methylphenanthrene 5R .00203 3875 8.37 1.19

Pyrene 6R .00118 ? 1262 12.08 1.72

\% Recovery 44.34

TOTALS

Resolved for all peaks 272220 ?

Resolved - known peaks 26989 ? 6.96

Resolved - unknown peaks 212876 ? 293.77? 41.77

Unresolved (UCM) 184751 254.96 36.25

Total aliphatic hydrocarbons 84.98

Sample: 238B? (0 - 5)

Data analyzed: Nov 28, 1983

Int. Std. (µg): 101

Dry weight (g): 32.56

Inject. volume (µL): 2

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00062 0 0 0

Dibenzothiophene 2R .00093 2603 2.42 0.14 Resol./Unres.

Phenanthrene 3R .00080 0 0 0

*o*-Terphenyl 4R .00117 42894 50.10 ? Int. std.

1-Methylphenanthrene 5R .00161 1672 2.69 0.16

Pyrene 6R .00727 0 0 0

\% Recovery 37.27

TOTALS

Resolved for all peaks 153500 ?

Resolved - known peaks 4275 0.31

Resolved - unknown peaks 106331 ? 124.41 7.44

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 7.74

Sample: 234B? (0 - 5)

Data analyzed: Nov 28, 1983

Int. Std. (µg): 101

Dry weight (g): 24.6

Inject. volume (µL): 2

Sample volume (mL): 2

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00062 0 0 0

Dibenzothiophene 2R .00093 6494 6.03 ? 0.42 Resol./Unres.

Phenanthrene 3R .00080 0 0 0

*o*-Terphenyl 4R .00117 49000 ? 58.36 ? Int. std.

1-Methylphenanthrene 5R .00161 5473 8.81 ? 0.62

Pyrene 6R .00727 0 0 0

\% Recovery 57.78

TOTALS

Resolved for all peaks 109950 ?

Resolved - known peaks 11967 1.04 ?

Resolved - unknown peaks 148103 ? 173.21 12.20 ?

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 13.24

Sample: 2xxB? (55 - 60) ?

Data analyzed: Nov 14, 1983

Int. Std. (µg): 101

Dry weight (g): 15.73

Inject. volume (µL): 2

Sample volume (mL): 1.9 ?

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00073? 0 0 0

Dibenzothiophene 2R .00087? 3370 2.93 ? 0.32 Resol./Unres. 0.46

Phenanthrene 3R .00709? 798 0.57 0.06

*o*-Terphenyl 4R .00064? 69360 50.26 ? Int. std.

1-Methylphenanthrene 5R .00100? 2945 2.95 ? 0.32

Pyrene 6R .00207? 2096 6.31 0.92

\% Recovery 54.60

TOTALS

Resolved for all peaks 204850 ?

Resolved - known peaks 10009 1.63

Resolved - unknown peaks 124681? 104.73 11.54

Unresolved (UCM) 311144 261.36 28.80 ?

Total aliphatic hydrocarbons 41.97

Sample: 239B (0 - 5)

Data analyzed: Nov 25, 1983

Int. Std. (µg): 101

Dry weight (g): 24.01 ?

Inject. volume (µL): 2

Sample volume (mL): 1.25 ?

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00155 0 0 0

Dibenzothiophene 2R .00201 ? 0 0 0 Resol./Unres.

Phenanthrene 3R .00168 ? 1560 ? 2.68 ? 0.09

*o*-Terphenyl 4R .00175 68958 120.68 ? Int. std.

1-Methylphenanthrene 5R .00203 271 0.57 0.02 ?

Pyrene 6R .00118 ? 1659 ? 9.52 0.34

\% Recovery 74.68

TOTALS

Resolved for all peaks 1704 ?

Resolved - known peaks 3696 ? 0.45

Resolved - unknown peaks 97766 ? 171.26 ? 5.96

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 6.42

Sample: 242B-1 (0 - 5)

Data analyzed: Nov 20, 1983 ?

Int. Std. (µg): 101

Dry weight (g): 11.01

Inject. volume (µL): 2

Sample volume (mL): 1.4

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00076 0 0 0

Dibenzothiophene 2R .00115 2399 2.64 0.21 Resol./Unres.

Phenanthrene 3R .00090 16199 14.58 1.14

*o*-Terphenyl 4R .00100 116618 116.63 ? Int. std.

1-Methylphenanthrene 5R .00136 190 0.26 0.02 ?

Pyrene 6R .00432 2412 10.45 0.02 ?

\% Recovery 80.82 ?

TOTALS

Resolved for all peaks 400320 ?

Resolved - known peaks 21101 2.20

Resolved - unknown peaks 262609 ? 362.61 ? 20.66

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 22.86

Sample: 242B (60 - 65)

Data analyzed: Nov 22, 1983

Int. Std. (µg): 101

Dry weight (g): 5.03 ?

Inject. volume (µL): 2

Sample volume (mL): 2

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00067 0 0 0

Dibenzothiophene 2R .00105 ? 0 0 0 Resol./Unres.

Phenanthrene 3R .00096 0 0 0

*o*-Terphenyl 4R .00121 94051 113.80 ? Int. std.

1-Methylphenanthrene 5R .00200 0 0 0

Pyrene 6R .00980 0 0 0

\% Recovery 112.7

TOTALS

Resolved for all peaks 123980

Resolved - known peaks 0 0

Resolved - unknown peaks 29929 36.21 5.51

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 5.51

Sample: 240B (120 - 125)

Data analyzed: Nov 28, 1983

Int. Std. (µg): 101

Dry weight (g): 17.72 ?

Inject. volume (µL): 2

Sample volume (mL): 1.9

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00155 0 0 0

Dibenzothiophene 2R .00201 ? 571 1.15 0.03 Resol./Unres.

Phenanthrene 3R .00168 ? 805 1.49 ? 0.04

*o*-Terphenyl 4R .00175 115370 201.70 ? Int. std.

1-Methylphenanthrene 5R .00228 0 0 0

Pyrene 6R .00528 ? 699 3.70 0.118

\% Recovery 189.9

TOTALS

Resolved for all peaks 138670 ?

Resolved - known peaks 2159 ? 0.18

Resolved - unknown peaks 97766 ? 37.00 ? 1.04

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 1.22

Sample: 241B (0 - 5)

Data analyzed: Nov 28, 1983

Int. Std. (µg): 101

Dry weight (g): 30. ? ?

Inject. volume (µL): 2

Sample volume (mL): 1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

.03 ?

Naphthalene 1R .00155 1139 1.76 0.04 ?

Dibenzothiophene 2R .00201 ? 1056 ? 2.52 0.05 Resol./Unres.

Phenanthrene 3R .00168 ? 5300 ? 18.96 ? 0.19

*o*-Terphenyl 4R .00175 90433 158.26 ? Int. std.

1-Methylphenanthrene 5R .00205 ? 8343 17.35 0.36

Pyrene 6R .00528 ? 2903 15.33 0.32

\% Recovery 78.35

TOTALS

Resolved for all peaks 346500 ?

Resolved - known peaks 15974 ? 0.95

Resolved - unknown peaks 237093? 414.91? 8.60

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 9.55

Sample: 242B (0 - 5)

Data analyzed: Nov 22, 1983

Int. Std. (µg): 101

Dry weight (g): 32.02 ?

Inject. volume (µL): 2

Sample volume (mL): 2

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00067 0 0 0

Dibenzothiophene 2R .00108 ? 1724 1.86 0.06 Resol./Unres.

Phenanthrene 3R .00096 5162 4.96 0.13

*o*-Terphenyl 4R .00121 94416 114.24 ? Int. std.

1-Methylphenanthrene 5R .00200 1809 3.62 0.90 ?

Pyrene 6R .00980 667 6.54 0.18

\% Recovery 113.1

TOTALS

Resolved for all peaks 178800

Resolved - known peaks 9362 0.45

Resolved - unknown peaks 75822 90.78 2.45

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 2.90

Sample: 247B ? (0 - 5)

Data analyzed: Nov 22, 1983

Int. Std. (µg): 101

Dry weight (g): 26.82 ?

Inject. volume (µL): 2

Sample volume (mL): 2

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00067 0 0 0

Dibenzothiophene 2R .00108 ? 0 0 0 Resol./Unres.

Phenanthrene 3R .00096 2864 2.75 0.12

*o*-Terphenyl 4R .00121 75095 ? 94.49? Int. std.

1-Methylphenanthrene 5R .00200 4171 8.24 0.33

Pyrene 6R .00980 1312 12.87 0.52

\% Recovery 93.56

TOTALS

Resolved for all peaks 205440

Resolved - known peaks 8348 0.96

Resolved - unknown peaks 118997 143.99 5.78

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 6.74

Sample: 247B ? (0 - 5)

Data analyzed: Nov 22, 1983

Int. Std. (µg): 101

Dry weight (g): 26.82 ?

Inject. volume (µL): 2

Sample volume (mL): 2

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00067 0 0 0

Dibenzothiophene 2R .00108 ? 1956 ? 2.14 0.14 Resol./Unres.

Phenanthrene 3R .00096 25608 ? 24.58 1.64

*o*-Terphenyl 4R .00121 57704 ? 69.82 Int. std.

1-Methylphenanthrene 5R .00200 21811 43.62 2.91

Pyrene 6R .00980 4418 43.30 2.90

\% Recovery 86.41

TOTALS

Resolved for all peaks 844420

Resolved - known peaks 53815 7.59

Resolved - unknown peaks 732901 886.81 59.20

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 66.78

Sample: 245B ? (0 - 5)

Data analyzed: Nov 23, 1983

Int. Std. (µg): 101

Dry weight (g): 27 ?

Inject. volume (µL): ?

Sample volume (mL): ?

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00097 0 0 0

Dibenzothiophene 2R .00 ? 6294 ? 8.06 ? 0.15 Resol./Unres.

Phenanthrene 3R .00104 0 0 0

*o*-Terphenyl 4R .00124 ? 155820 ? 193.22 ? Int. std.

1-Methylphenanthrene 5R .00126 3942 5.05 0.10

Pyrene 6R .00242 528 1.30 0.20

\% Recovery 95.65

TOTALS

Resolved for all peaks 312053 ?

Resolved - known peaks 12734 ? 0.27

Resolved - unknown peaks 145456 ? 138.36 ? 3.45

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 3.72

Sample: 246B ? (0 - 5)

Data analyzed: Nov 22, 1983

Int. Std. (µg): 101

Dry weight (g): 35.49

Inject. volume (µL): 2

Sample volume (mL): 1.2 ?

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00067 0 0 0

Dibenzothiophene 2R .00108 0 0 0 Resol./Unres.

Phenanthrene 3R .00096 754 0.72 ? 0.08

*o*-Terphenyl 4R .00121 22278 ? 26.96 ? Int. std.

1-Methylphenanthrene 5R .00200 1081 2.16 0.23

Pyrene 6R .00980 0 0 0

\% Recovery 42.70 ?

TOTALS

Resolved for all peaks 57249 ?

Resolved - known peaks 1835 ? 0.30

Resolved - unknown peaks 33136 ? 14.89 ? 4.23

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 4.54

Sample: 247B ? (0 - 5)

Data analyzed: Nov 22, 1983

Int. Std. (µg): 101

Dry weight (g): ?

Inject. volume (µL): 2

Sample volume (mL): ?

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00067 0 0 0

Dibenzothiophene 2R .00108 3908 4.312 0.07 Resol./Unres.

Phenanthrene 3R .00096 0 0 0

*o*-Terphenyl 4R .00121 130820 ? 156.17? Int. std.

1-Methylphenanthrene 5R .00200 2585 5.17 0.08 ?

Pyrene 6R .00980 0 0 0

\% Recovery 109.6?

TOTALS

Resolved for all peaks 202280 ?

Resolved - known peaks 6485 0.17

Resolved - unknown peaks 65875 ? 78.75 ? 1.35

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 1.51

Sample: 1B Butterfly ray

Data analyzed: Dec 4, 1983

Int. Std. (µg): 101

Dry weight (g): 13.56

Inject. volume (µL): 2

Sample volume (mL): 0.9

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00059 0 0 0

Dibenzothiophene 2R .00093 0 0 0 Resol./Unres.

Phenanthrene 3R .00051 0 0 0

*o*-Terphenyl 4R .00095 152760 ? 145.12 ? Int. std.

1-Methylphenanthrene 5R .00145 445 0.65 0.03 ?

Pyrene 6R .00624 0 0 0

\% Recovery 64.66

TOTALS

Resolved for all peaks 227450 ?

Resolved - known peaks 445 0.03

Resolved - unknown peaks 74245 20.53 ? 3.62

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 3.65

Sample: 3B Catfish

Data analyzed: Dec 4, 1983

Int. Std. (µg): 101

Dry weight (g): 12.12

Inject. volume (µL): 2

Sample volume (mL): 1.1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00059 15383 9.03 0.54

Dibenzothiophene 2R .00093 2758 2.56 0.15 Resol./Unres.

Phenanthrene 3R .00051 2361 1.91 0.12

*o*-Terphenyl 4R .00095 145428 138.15 Int. std.

1-Methylphenanthrene 5R .00145 4685 6.68 0.40

Pyrene 6R .00624 0 0 0

\% Recovery 75.23

TOTALS

Resolved for all peaks 2892230 ?

Resolved - known peaks 25027 1.22

Resolved - unknown peaks 118783 112.84? 6.81

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 8.02

Sample: 5B Grunt

Data analyzed: Dec 4, 1983

Int. Std. (µg): 101

Dry weight (g): 9.67

Inject. volume (µL): 2

Sample volume (mL): 1

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00059 0 0 0

Dibenzothiophene 2R .00093 0 0 0 Resol./Unres.

Phenanthrene 3R .00051 0 0 0

*o*-Terphenyl 4R .00095 37947 ? 36.05 ? Int. std.

1-Methylphenanthrene 5R .00145 0 0 0

Pyrene 6R .00624 0 0 0

\% Recovery 17.85

TOTALS

Resolved for all peaks 46523 ?

Resolved - known peaks 0 0

Resolved - unknown peaks 8576 8.15 ? 2.36

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 2.36

Sample: 5B Pigfish

Data analyzed: Dec 4, 1983

Int. Std. (µg): 101

Dry weight (g): 18.52

Inject. volume (µL): 2

Sample volume (mL): 3

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00059 0 0 0

Dibenzothiophene 2R .00093 0 0 0 Resol./Unres.

Phenanthrene 3R .00051 0 0 0

*o*-Terphenyl 4R .00095 40444 ? 38.42 ? Int. std.

1-Methylphenanthrene 5R .00145 5804 8.42 1.19

Pyrene 6R .00624 0 0 0

\% Recovery 57.06

TOTALS

Resolved for all peaks 234050 ?

Resolved - known peaks 5804 1.19

Resolved - unknown peaks 187582 ? 178.41 ? 25.32

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 26.52

Sample: 6B Shrimp

Data analyzed: Dec 4, 1983

Int. Std. (µg): 101

Dry weight (g): 5.53

Inject. volume (µL): 2

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00059 0 0 0

Dibenzothiophene 2R .00093 0 0 0 Resol./Unres.

Phenanthrene 3R .00051 0 0 0

*o*-Terphenyl 4R .00095 8024 ? 7.62 Int. std.

1-Methylphenanthrene 5R .00145 0 0 0

Pyrene 6R .00624 0 0 0

\% Recovery 5.66

TOTALS

Resolved for all peaks 8024 ?

Resolved - known peaks 0 0

Resolved - unknown peaks 0 0 0

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0

Sample: 8B Crabs

Data analyzed: Dec 4, 1983

Int. Std. (µg): 101

Dry weight (g): 11.42

Inject. volume (µL): 2

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00059 0 0 0

Dibenzothiophene 2R .00093 0 0 0 Resol./Unres.

Phenanthrene 3R .00051 0 0 0

*o*-Terphenyl 4R .00095 7863 ? 7.47 Int. std.

1-Methylphenanthrene 5R .00145 2846 4.13 4.89

Pyrene 6R .00624 1495 9.33 11.05 ?

\% Recovery 5.55

TOTALS

Resolved for all peaks 46042

Resolved - known peaks 4341 15.93

Resolved - unknown peaks 33836 32.15 38.06

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 53.99

Sample: 9B Blue crabs

Data analyzed: Dec 4, 1983

Int. Std. (µg): 101

Dry weight (g): 14.29

Inject. volume (µL): 2

Sample volume (mL): 1.75

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00059 0 0 0

Dibenzothiophene 2R .00093 0 0 0 Resol./Unres.

Phenanthrene 3R .00051 0 0 0

*o*-Terphenyl 4R .00095 97706 92.83 Int. std.

1-Methylphenanthrene 5R .00145 36683 53.19 4.05

Pyrene 6R .00624 64353 401.56 30.58 ?

\% Recovery 80.41

TOTALS

Resolved for all peaks 2375500

Resolved - known peaks 101036 34.63

Resolved - unknown peaks 2176758 2067.93 157.46

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 192.10 ?

Sample: 12B Bivalves

Data analyzed: Dec 4, 1983

Int. Std. (µg): 101

Dry weight (g): 1.17

Inject. volume (µL): 2

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00059 0 0 0

Dibenzothiophene 2R .00093 0 0 0 Resol./Unres.

Phenanthrene 3R .00051 0 0 0

*o*-Terphenyl 4R .00095 11553 10.98 Int. std.

1-Methylphenanthrene 5R .00145 0 0 0

Pyrene 6R .00624 0 0 0

\% Recovery 8.15

TOTALS

Resolved for all peaks 11553

Resolved - known peaks 0 0

Resolved - unknown peaks 0 0 0

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 0

Sample: 11B Oysters

Data analyzed: Dec 4, 1983

Int. Std. (µg): 101

Dry weight (g): 3.61

Inject. volume (µL): 2

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00059 0 0 0

Dibenzothiophene 2R .00093 0 0 0 Resol./Unres.

Phenanthrene 3R .00051 0 0 0

*o*-Terphenyl 4R .00095 12562 11.93 Int. std.

1-Methylphenanthrene 5R .00145 0 0 0

Pyrene 6R .00624 9068 ? 56.50 ? 132.66

\% Recovery 8.86

TOTALS

Resolved for all peaks 24100 ?

Resolved - known peaks 9068 132.66

Resolved - unknown peaks 2470 2.35 5.50

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 138.16

Sample: 12B Oysters, flat tree

Data analyzed: Dec 4, 1983

Int. Std. (µg): 101

Dry weight (g): 9.98

Inject. volume (µL): 2

Sample volume (mL): 1.5

Int. std. *o*-Terphenyl

Compounds Ref. \# Response Area ng µg/g Ratios

factor (corrected)

Naphthalene 1R .00059 0 0 0

Dibenzothiophene 2R .00093 0 0 0 Resol./Unres.

Phenanthrene 3R .00051 0 0 0

*o*-Terphenyl 4R .00095 11298 10.73 Int. std.

1-Methylphenanthrene 5R .00145 4384 6.36 6.00

Pyrene 6R .00624 2463 15.37 14.58

\% Recovery 7.96

TOTALS

Resolved for all peaks 59420 ?

Resolved - known peaks 6847 28.50

Resolved - unknown peaks 412.83 39.22 37.01

Unresolved (UCM) 0 0 0

Total aliphatic hydrocarbons 57.51