Patent ID: 9682987
Date: 2017-06-20
CPC Classifications: A61K,A61P,C07B,C07D

Claim:
1. Crystalline (1-{3-[6-(9,9-difluoro-7-{2-[5-(2-methoxycarbonylamino-3-methyl-butyryl)-5-aza-spiro[2.4]hept-6-yl]-3H-imidazol-4-yl}-9H-fluoren-2-yl)-1H-benzoimidazol-2-yl]-2-aza-bicyclo[2.2.1]heptane-2-carbonyl}-2-methyl-propyl)-carbamic acid methyl ester ethyl acetate solvate (Compound I Form IV), characterized by an X-ray powder diffractogram comprising the following peaks: 15.1, 17.2, and 21.5° 2θ+0.2 °2θ, as determined on a diffractometer using Cu-Kα radiation at a wavelength of 1.54178 Å.