Patent ID: 9662353
Date: 2017-05-30
CPC Classifications: A61K,A61P

Claim:
1. A method for preparing an iron-based montmorillonite medicine comprises: (1) adding pharmaceutical montmorillonite into deionized water to yield a mixture, the pH value being adjusted to 2.0-3.5 with hydrochloric acid; treating the mixture by ultrasonication under stirring for 10-30 minutes; static standing, layering the mixture and separating the upper water of the mixture; adding the deionized water into the water-removed mixture with the equal volume of the separated water for washing; separating the upper water from the mixture; repeating the washing for several times until the pH value of the washing buffer reaches 6.5-7.5; filtering the water-removed mixture by plate and frame pressing, collecting a solid material, drying the solid material until water content is no more than 10 wt %; then powdering the solid material by pulverizer until particle diameter is no more than 45 μm, then screening the solid material under 325 mesh and obtaining a medicinal montmorillonite; (2) soaking or eluting the medicinal montmorillonite in step (1) by a water soluble iron salt solution to yield a mixture two, washing the mixture two by the deionized water until the pH value reaches 6.5-7.5, filtering the mixture two and obtaining a solid material two, vacuum drying the solid material two, powdering the solid material two by pulverizer until the particle diameter is no more than 45 μm, then screening the solid material two under 325 mesh, obtaining the iron-based montmorillonite (Fe-montmorillonite).