Patent ID: 9730907
Date: 2017-08-15
CPC Classifications: A23D,A23L,A23V,A61K

Claim:
1. A method for preparing a microencapsulated omega-3 (Ω3) polyunsaturated fatty acid (PUFA) powder for Ω3-enriching animal feeds for meat, egg, and milk production, comprising the steps of: (a) heating to 30-35° C. a starch paste that has been formed by mixing starch and water with continuous stirring and adding sodium hydroxide until the starch paste has a pH value of 8.5-9; (b) following step (a) with continuous stirring gradually over 1-2 hours adding to the starch paste a composition comprising sodium octenylsuccinate diluted in ethanol while maintaining a pH value of 8.2-8.8 by adding sodium hydroxide until addition of sodium octenylsuccinate is complete and the pH value is stabilized at 8.5; (c) following step (b) with continuous stirring adding dilute nitric acid to the starch paste until the pH value is 6.5 and then heating the starch paste to 90° C. to obtain a neutralized starch paste; (d) combining, while stirring and heating to a temperature of 70-80° C. in an aqueous phase tank, water, disodium hydrogen phosphate, sodium citrate, and at least one material selected from the group consisting of dextran, water-soluble syrup, whey powder and chitosan, and then adding to the aqueous phase tank the neutralized starch paste of step (c) until the starch paste is dissolved, to obtain an aqueous solution; (e) combining, while stirring and heating to a temperature of 70-80° C. in an oil phase tank, an Ω3 oil, stearic acyl lactylate and a composite emulsifier, to obtain an oil phase solution that is maintained at 70-80° C. and in which the stearic acyl lactylate and the composite emulsifier are dissolved; (f) mixing the aqueous solution of (d) with the oil phase solution of (e) to form a feed solution; (g) homogenizing the feed solution by a high pressure controlled at 20˜45 MPa after milling the feed solution with a colloid mill or shearing the feed solution with a shear pump and pressuring to 2˜12 MPa, to obtain a homogenized feed solution; and (h) pressure spray drying the homogenized feed solution by controlling an inlet air temperature of a drying tower at 135˜190° C. and an outlet air temperature of the drying tower at 55˜95° C., thereby to obtain the microencapsulated omega-3 (Ω3) polyunsaturated fatty acid (PUFA) powder.