Patent ID: 9249264
Filing Date: 2016-02-02
CPC Classification: B01J,C01G,C08G,C08K,C09D

Claim Text:
1. A method of preparing a composition, the method comprising: (a) forming an aqueous mixture comprising: to produce a siloxy compound; (b) boiling the aqueous mixture; (c) adding a base to the aqueous mixture to substantially neutralize the mixture and to form a hydroxide of the metal; (d) forming a colloidal suspension comprising the metal hydroxide and the siloxy compound; (e) adding a peroxide-based solution to form a suspension comprising a peroxide of the metal; (f) allowing the suspension to equilibrate at room temperature; and (g) boiling the suspension at a pressure greater than atmospheric pressure to form a hybrid film-forming composition comprising a condensation product of the siloxy compound and the metal peroxide, wherein the composition has a tighter particle size distribution and provides a more transparent coating than when the suspension is boiled at atmospheric pressure.