Patent ID: 11858885
Assignee: COUNCIL OF SCIENTIFIC & INDUSTRIAL RESEARCH
Field: Macromolecular chemistry, polymers (Chemistry)
Classification: CPC C | IPC C

Claim 5:
6. A process for obtaining a fluorinated compound using the non-hygroscopic, recyclable, and thermally stable complex according to claim 1, the process comprising:
(i) charging a substrate compound and the complex in a w/w ratio from 1:1 to 2:1 into a solvent to obtain a reaction mixture;
(ii) stirring the reaction mixture obtained in (i) at a temperature from 50° C. to 100° C. for 3 hours;
(iii) cooling the reaction mixture obtained in (ii) to a temperature from 25° C. to 35° C., filtering, and washing with ethyl acetate solvent;
(iv) removing the solvent from the reaction mixture as obtained in (iii) under reduced pressure to obtain a fluorinated compound;
(v) purifying the fluorinated compound obtained in (iv) using flash chromatography by using 20% ethyl acetate in hexane eluent to obtain a pure fluorinated compound.