Patent ID: 11864561
Assignee: THANH DUC LE
Field: Basic materials chemistry (Chemistry)
Classification: CPC A  C | IPC A  C

Claim 10:
11. A multipurpose fertilizer composition having anti-insect properties, water-retaining, and capable of improving to absorb micronutrients for plants obtained from the process of forming a homogeneous mixture by mixing a fertilizer mixture with at least three other ingredients including a chelation of trace elements solution, a water-retaining ingredient, and a plant extracts ingredients having anti-insect properties;
(A) wherein the plant extracts ingredients having anti-insect properties is obtained by mixing homogenizing a tobacco waste extracts solution with at least one ingredients is a plant mixture extracts solution; wherein the plant extracts ingredients having anti-insect properties (A) containing at least 0.009% % by weight of a nicotine compound;
the tobacco waste extracts solution extracted from fresh, or dried, crushed/chopped/cut tobacco waste, soaked in ethanol 98% at 30° C.-45° C. for 7 days, with the combination of stirring once/day for 10 minutes, then filtered and separated an extracted waste tobacco residues; wherein a ratio of soaking the tobacco waste and ethanol 98% having 3:10; wherein the tobacco waste including leaf veins, stems, roots, and leaves have been removed;
the plant mixture extracts solution created by performed in a specific order from (a) to (f) comprising:
(a) preparing plant mixture consisting of green tomatoes, sprouted potatoes, eggplants, chilli/peppers/bell pepper, and pond apple seeds (Annona glabra seeds); all are chopped and mixed in the respective ratio of 1:1:1:1:1;
(b) soaking said chopped plant mixture with ethanol 70% in a ratio of 1:5 at room temperature, with the combination of stirring at 100 rpm for 3 days;
(c) filtering said soaked plant mixture to obtained a first solution, and a first residue;
(d) soaking the first residue with ethanol 70% in a ratio of 1:5 at room temperature, with the combination of stirring at 100 rpm for 3 days;
(e) filtering said soaked first residue to obtained a second solution, and an extracted plant mixture residue; wherein the filter hole diameter at step (e) is 25% smaller than the filter hole diameter at step (c); and
(f) mixing homogenizing the first solution with the second solution to obtained the plant mixture extracts solution;

(B) wherein the water-retaining ingredient created by performed in a specific order from (a′) to (b′) comprising:
(a′) preparing a pectin extracts by steps comprising:
creating a raw pectin extracts mixture by mixing 1 part a pectin extract from coffee husks and cocoa shells, with 2 parts a pectin extract from yam (Dioscorea alata L.), and 3 parts a pectin extract from okra (Abelmoschus esculentus (L.) Moench);
precipitation with isopropanol in the ratio of 1 part the raw pectin with 2 parts isopropanol at the temperature of 90° C.-95° C. for 90-100 minutes; then centrifuging at 400-500 rpm for 20-30 minutes; to create a precipitate solution;
filtering and washing the precipitate solution with ethanol 70% until the precipitate solution having white; then dyring at 50° C.-60° C. for 20-24 hours to create the pectin extracts having moisture content of 7%-9%; and

(b′) creating the water-retaining ingredient by steps comprising:
gelatinizing the pectin extracts for 5-7 minutes at 70° C.-75° C.;
adding acetyl peroxide with the combination of stirring at 85° C. for 40 minutes; wherein Acetyl peroxide having concentration of 0.1%-0.3%;
adding acrylic acid with the combination of stirring at 40° C. for 20 minutes;
adding 1,4-butanediol diacrylate with the combination of stirring at 55° C.-60° C. for 5 minutes, then drying at 65° C. to constant weight to obtain the water-retaining ingredient;

(C) wherein the chelation of trace elements solution by steps comprising:
creating a extract from katuk/star gooseberry/sweet leaves (Sauropus androgynous) and kale leaves by extracted from katuk/star gooseberry/sweet leaves (Sauropus androgynous) and kale leaves fresh are crushed/chopped/cut, then soaking in a in solvent, or saturated brine solution for 2 hours; wherein a ratio of mixing the katuk/star gooseberry/sweet leaves (Sauropus androgynous) with kale leaves is 1:3;
creating a trace solution by mixing the extract from katuk/star gooseberry/sweet leaves (Sauropus androgynous) and kale leaves with a micronutrient extracts from rare earth in the ratio 1:1; wherein the micronutrient extracts from rare earth having pH of 6.2, and obtained by combining treatment with dilute HNO3 55% and aqua regia solution;
grinding peat to obtain a peat powder; wherein said peat has been treated bituminous, and having moisture content of 30%-35%;
treating the peat powder with NaOH 10% in the ratio 1:3 for 60 minutes; then filtering to obtain a first temporary solution, and a first temporary residue;
treating the first temporary residue with NaOH 50% in the ratio 1:2 for 30 minutes; then filtering to obtain a second temporary solution, and a second temporary residue;
treating the second temporary residue with acid solution having 50% concentration in a ratio of 1:1.5 for 30 minutes; then filtering to obtain a third solution, and a treated peat residue; wherein acid solution used is selected from one of the following acids: acetic acid, HCl acid, and HNO3 acid;
admixing the first solution with the second solution, and the third solution to create a base solution; and
admixing the trace solution and the base solution in the ratio 1:(1-3), with the combination of stirring to create the chelation of trace elements solution;

(D) wherein the fertilizer mixture is obtained by mixing at least two ingredients from three ingredients comprising a base fertilizer, a NPK fertilizer, and a foundation fertilizer;
the base fertilizer comprising chemical components: organic matter having 70.4% by weight, an elemental nitrogen (N) having at least 0.25% by weight, an elemental phosphorus (P) having at least 0.69% by weight, and an elemental potassium (K) having at least 5.4% by weight, an elemental sulfur (S) having at least 0.000005% by weight, an elemental bo (B) having at least 0.003% by weight, an elemental calcium (Ca) having at least 0.025% by weight, and an elemental magnesium (Mg) having at least 0.0113% by weight;
the foundation fertilizer (D3) in solid form obtained from the process of forming a second after incubated mixture, and shaping the second after incubated mixture after adjusting the pH at 6.2-7, and moisture content of less than 13%;
the second after incubated mixture created by performed in a specific order from (i) to (iii) comprising:
(i) creating a base mixture by mixing a manure, a poultry manure, and the tobacco waste in a ratio of 2:1:4; then crushing to size less than 0.05 mm;
wherein the manure, and the poultry manure having moisture content of 42%-45%;
the manure is selected from the group consisting of cow manure, pig manure, horse manure, goat manure, sheep manure, and combinations thereof; wherein cow manure having at least 28% of the weight of the manure;
the poultry manure is selected from the group consisting of chicken manure, duck manure, geese manure, pigeon manure, quail droppings, and combinations thereof; wherein chicken manure having at least 28% of the weight of the poultry manure;
wherein the tobacco waste including leaf veins, stems, roots, and leaves have been removed;

(ii) admixing a microorganism ingredient into a extracted residue mixture, then incubating at 45° C.-60° C. for 5 hours to create a first after incubated mixture; wherein microorganism ingredient having 0.05% of the weight of the extracted residue mixture;
wherein the extracted residue mixture comprising: the extracted waste tobacco residues, the extracted plant mixture residue, the treated peat residue, a coffee husks and cocoa shells mixture residue, a pectin-reduced yams residue, and a pectin-reduced okra residue;

(iii) admixing the base mixture, the first after incubated mixture, and the microorganism ingredient in the ratio of 90:10:1, then incubating at 45° C.-60° C. for 25-28 days with humidity of 60%-65%, with the combination of mixing frequency every one day for 20 minutes; that to create a second after incubated mixture having a chemical components comprising: an elemental nitrogen (N) having 1.77% by weight; an elemental phosphorus (P) having 0.69% by weight; an elemental potassium (K) having 5.4% by weight; an elemental sulfur (S) having 0.39% by weight; an elemental bo (B) having 0.0409% by weight; an elemental calcium (Ca) having 2.82% by weight; an elemental magnesium (Mg) having 0.49% by weight; an elemental copper (Cu) having 0.0024% by weight; an elemental zinc (Zn) having 0.0047% by weight; an elemental manganese (Mn) having 0.0149% by weight; an elemental iron (Fe) having 0.119% by weight; nitrogen-fixing microorganisms having 1.1×106 CFU/g; phosphate solubilizing microorganisms (PSMs) having 2.1×105 CFU/g; cellulose-degrading microorganisms having 7.1×105 CFU/g; humic acid having 2.09% by weight; and organic matter having 86.5% by weight;
wherein the chelation of trace elements solution having 5%-7% of the weight of the fertilizer mixture;
wherein the water-retaining ingredient having 7%-10% of the total weight of the fertilizer mixture, and the chelation of trace elements solution;
wherein the plant extracts ingredients having anti-insect properties having 0.08%-3% of the total weight of the fertilizer mixture, with the chelation of trace elements solution, and the water-retaining ingredient.