Patent ID: 11958866
Assignee: KING FAISAL UNIVERSITY
Field: Organic fine chemistry (Chemistry)
Classification: CPC C | IPC C

Claim 7:
8. A process for synthesizing a thiadiazole, the process comprising:
preparing a first solution of a thiourea compound in acetonitrile;
preparing a second solution of auric chloride (HAuCl4) in acetonitrile;
adding the first solution to the second solution to obtain a reaction mixture;
stirring the reaction mixture for at least six hours;
filtering the reaction mixture to obtain a solid product;
dissolving the solid product in chloroform to obtain a third solution; and
recrystallizing the thiadiazole from the third solution;
wherein the thiourea compound is 1-phenyl-3-(thiazole-2-yl)thiourea, the thiadiazole is 5-Methyl-N-phenyl-4λ4-[1,2,4]thiadiazolo[2,3-a]pyridine-2-aminegold(III) chloride, and the process comprises the following reaction:,