Patent ID: 11919978
Assignee: GUANGZHOU INSTITUTE OF ENERGY CONVERSION, CHINESE ACADEMY OF SCIENCES
Field: Macromolecular chemistry, polymers (Chemistry)
Classification: CPC C | IPC C

Claim 0:
1. A method for producing a hydrate kinetic inhibitor, wherein the hydrate kinetic inhibitor is hydroxyl terminated poly(N-vinylcaprolactam) having a structure of formula (I), and n=10 to 1000,, the method comprising:
sequentially adding a chain initiator, a N-vinylcaprolactam, a mercaptoethanol, and a isopropanol into the reactor, wherein the molar ratio of the mercaptoethanol to the N-vinylcaprolactam is 1:20, the chain initiator is azobisisobutyronitrile, a molar ratio of the azobisisobutyronitrile to the N-vinylcaprolactam is 0.01:1, and a solid-to-liquid ratio of the N-vinylcaprolactam to the isopropanol is 1:15 g/mL, and stirring until dissolved; sealing the reactor using a rubber plug, and performing three cycles of vacuumizing and introducing nitrogen; reacting under the nitrogen atmosphere at 85° C. for 24 hours to obtain the reaction solution; drying the reaction solution by the rotary evaporation at 50° C., and cooling to the room temperature to obtain the crude product; dissolving the crude product in tetrahydrofuran and precipitating using n-hexane to obtain a precipitate; washing the precipitate with anhydrous ether, and sieving and drying to obtain the hydrate kinetic inhibitor.